#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:01:15 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180943 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/23/2202320.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202320_Fobs loop_ _publ_author_name 'Dale, Sophie H.' 'Elsegood, Mark R. J.' _publ_section_title ; Benzene-1,2,4,5-tetracarboxylic acid dihydrate at 160K ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1087 _journal_page_last o1088 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.941 _cell_angle_beta 88.612 _cell_angle_gamma 72.933 _cell_length_a 5.4651 _cell_length_b 6.4044 _cell_length_c 9.1145 _exptl_crystal_F_000 150.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file bt6288Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mrje37 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 70.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 664.25 566.73 9.54 o 2 0 0 28.98 29.33 1.03 o 3 0 0 142.32 152.68 2.59 o 4 0 0 17.52 17.49 0.91 o 5 0 0 92.42 90.90 1.60 o 6 0 0 0.07 0.72 0.80 o -5 1 0 0.70 1.30 0.68 o -4 1 0 38.44 36.93 0.87 o -3 1 0 31.49 29.50 0.68 o -2 1 0 0.00 0.52 0.43 o -1 1 0 4975.17 4629.57 51.83 o 0 1 0 508.84 480.07 8.02 o 1 1 0 64.18 64.60 1.24 o 2 1 0 232.36 215.08 2.13 o 3 1 0 42.09 46.58 0.66 o 4 1 0 66.00 69.69 0.96 o 5 1 0 11.42 10.42 0.53 o 6 1 0 1.51 3.62 0.89 o -5 2 0 0.36 0.18 0.64 o -4 2 0 9.07 8.88 0.50 o -3 2 0 63.96 62.79 1.73 o -2 2 0 960.68 959.21 26.35 o -1 2 0 212.71 219.80 2.21 o 0 2 0 320.07 321.38 3.08 o 1 2 0 2096.27 2110.92 23.45 o 2 2 0 137.33 159.45 2.50 o 3 2 0 203.03 196.09 2.04 o 4 2 0 82.00 88.56 1.49 o 5 2 0 20.40 23.22 0.73 o 6 2 0 6.02 7.69 0.56 o -4 3 0 4.24 4.05 0.46 o -3 3 0 3.58 4.01 0.55 o -2 3 0 40.67 39.44 0.82 o -1 3 0 4.42 4.29 0.25 o 0 3 0 268.93 267.68 10.12 o 1 3 0 187.45 210.94 7.84 o 2 3 0 180.40 191.09 2.89 o 3 3 0 134.76 129.84 1.62 o 4 3 0 25.46 27.88 0.57 o 5 3 0 4.21 5.30 0.44 o 6 3 0 4.25 4.86 0.51 o -4 4 0 2.15 1.28 0.78 o -3 4 0 0.01 -0.05 0.70 o -2 4 0 112.74 108.49 1.39 o -1 4 0 83.80 89.55 1.15 o 0 4 0 2.31 2.15 0.38 o 1 4 0 41.94 46.36 0.86 o 2 4 0 252.20 235.77 2.97 o 3 4 0 99.77 103.85 1.56 o 4 4 0 51.99 52.73 1.02 o 5 4 0 0.00 0.31 0.86 o 6 4 0 5.24 5.23 0.67 o -3 5 0 12.08 12.88 1.00 o -2 5 0 4.99 4.63 0.45 o -1 5 0 0.50 0.30 0.52 o 0 5 0 84.32 81.69 1.36 o 1 5 0 52.83 50.36 1.00 o 2 5 0 5.65 5.50 0.40 o 3 5 0 3.23 3.23 0.41 o 4 5 0 0.32 0.29 0.60 o 5 5 0 19.77 21.01 0.74 o -1 6 0 0.50 0.51 0.64 o 0 6 0 1.98 2.77 0.65 o 1 6 0 37.84 38.64 1.45 o 2 6 0 0.15 0.55 0.60 o 3 6 0 6.61 6.68 0.71 o 4 6 0 0.91 0.70 1.04 o 5 6 0 6.55 6.74 0.96 o 1 7 0 0.00 0.02 0.84 o 2 7 0 0.34 0.34 0.80 o 3 7 0 0.13 -0.11 0.75 o -4 -6 1 1.16 1.07 0.89 o -3 -6 1 53.59 45.76 1.66 o -2 -6 1 77.21 71.16 2.36 o -1 -6 1 12.90 13.90 0.63 o 0 -6 1 6.73 6.64 0.51 o 1 -6 1 0.03 -0.01 0.73 o -5 -5 1 5.11 5.35 0.76 o -4 -5 1 0.28 0.44 0.63 o -3 -5 1 39.89 34.73 0.83 o -2 -5 1 8.29 7.33 0.67 o -1 -5 1 27.17 28.10 0.87 o 0 -5 1 7.99 8.75 0.51 o 1 -5 1 15.22 13.94 0.59 o 2 -5 1 11.01 11.99 0.89 o -6 -4 1 4.09 4.69 0.64 o -5 -4 1 2.64 4.85 1.06 o -4 -4 1 17.38 20.18 0.63 o -3 -4 1 0.98 0.44 0.54 o -2 -4 1 137.50 133.99 3.85 o -1 -4 1 20.55 23.22 1.05 o 0 -4 1 115.19 127.71 2.24 o 1 -4 1 54.60 54.62 1.05 o 2 -4 1 1.25 2.89 1.00 o 3 -4 1 176.63 188.30 3.90 o -6 -3 1 9.08 9.30 0.85 o -5 -3 1 19.80 22.06 0.69 o -4 -3 1 104.14 98.48 1.23 o -3 -3 1 66.20 67.16 0.88 o -2 -3 1 38.76 47.88 1.36 o -1 -3 1 0.04 1.21 0.38 o 0 -3 1 67.34 78.49 0.94 o 1 -3 1 341.91 344.58 3.46 o 2 -3 1 215.66 205.21 2.73 o 3 -3 1 11.48 11.27 0.54 o 4 -3 1 4.02 3.79 0.41 o -6 -2 1 44.40 49.07 1.17 o -5 -2 1 8.74 8.80 0.51 o -4 -2 1 1.03 1.46 0.47 o -3 -2 1 836.87 909.40 9.72 o -2 -2 1 208.90 243.47 2.42 o -1 -2 1 0.32 0.51 0.31 o 0 -2 1 150.13 140.45 2.89 o 1 -2 1 712.31 731.15 6.94 o 2 -2 1 1.05 1.46 0.57 o 3 -2 1 13.44 13.21 0.96 o 4 -2 1 82.37 73.25 1.36 o 5 -2 1 14.98 14.41 0.65 o -6 -1 1 14.51 15.59 0.72 o -5 -1 1 0.80 1.60 0.70 o -4 -1 1 204.81 208.08 4.09 o -3 -1 1 102.59 120.63 2.19 o -2 -1 1 38.34 37.84 0.83 o -1 -1 1 427.15 376.20 3.55 o 0 -1 1 189.26 196.48 2.37 o 1 -1 1 168.22 195.57 2.38 o 2 -1 1 105.48 109.56 2.22 o 3 -1 1 57.85 58.61 1.05 o 4 -1 1 102.31 100.12 4.06 o 5 -1 1 20.59 18.90 0.70 o -6 0 1 3.69 5.86 0.88 o -5 0 1 131.64 128.02 2.21 o -4 0 1 164.21 169.55 2.65 o -3 0 1 27.93 27.82 0.48 o -2 0 1 798.94 827.93 13.33 o -1 0 1 138.68 139.10 1.68 o 0 0 1 2.54 2.07 0.13 o 1 0 1 166.21 161.78 2.15 o 2 0 1 3.45 4.77 0.30 o 3 0 1 36.49 42.54 0.83 o 4 0 1 10.15 9.99 0.38 o 5 0 1 31.39 31.19 0.85 o 6 0 1 1.46 2.68 0.78 o -5 1 1 43.76 42.21 1.05 o -4 1 1 38.81 38.43 0.89 o -3 1 1 246.53 242.06 7.95 o -2 1 1 141.18 144.71 3.29 o -1 1 1 1549.20 1572.90 17.46 o 0 1 1 2.20 1.85 0.09 o 1 1 1 14.10 12.60 0.21 o 2 1 1 225.23 215.18 2.15 o 3 1 1 219.87 221.38 2.44 o 4 1 1 173.46 166.53 1.86 o 5 1 1 16.08 17.00 0.66 o 6 1 1 37.88 39.73 1.05 o -5 2 1 0.00 -0.19 0.68 o -4 2 1 201.47 190.92 2.72 o -3 2 1 51.30 54.68 1.04 o -2 2 1 280.25 277.26 3.43 o -1 2 1 311.87 319.00 3.11 o 0 2 1 203.58 205.69 2.01 o 1 2 1 2889.24 2726.54 30.19 o 2 2 1 5.66 6.20 0.24 o 3 2 1 65.79 64.05 0.82 o 4 2 1 66.90 63.72 0.90 o 5 2 1 47.52 50.75 1.06 o 6 2 1 105.70 105.46 1.83 o -4 3 1 72.59 62.05 1.27 o -3 3 1 421.33 381.53 11.40 o -2 3 1 7.83 7.78 0.50 o -1 3 1 31.55 27.46 0.88 o 0 3 1 260.53 243.98 2.43 o 1 3 1 16.51 16.33 0.41 o 2 3 1 157.18 152.86 1.95 o 3 3 1 65.57 60.31 1.30 o 4 3 1 25.87 26.08 0.55 o 5 3 1 68.69 71.74 1.07 o 6 3 1 7.82 8.66 0.60 o -4 4 1 60.79 49.95 2.08 o -3 4 1 1.06 1.35 0.58 o -2 4 1 0.53 1.29 0.48 o -1 4 1 54.99 55.47 0.81 o 0 4 1 29.34 28.49 0.50 o 1 4 1 60.79 65.41 0.83 o 2 4 1 323.64 298.64 3.62 o 3 4 1 1.21 3.14 0.58 o 4 4 1 133.24 138.03 1.63 o 5 4 1 95.42 98.27 1.62 o 6 4 1 17.50 19.24 1.03 o -3 5 1 14.09 11.64 0.83 o -2 5 1 32.15 35.19 0.94 o -1 5 1 10.70 10.59 0.54 o 0 5 1 7.68 8.26 0.43 o 1 5 1 25.85 23.62 0.64 o 2 5 1 73.65 71.52 1.18 o 3 5 1 0.74 1.77 0.67 o 4 5 1 127.67 124.65 2.82 o 5 5 1 27.35 28.62 1.28 o -2 6 1 1.39 2.56 0.83 o -1 6 1 62.72 61.34 1.84 o 0 6 1 3.32 3.43 0.71 o 1 6 1 8.73 9.12 0.72 o 2 6 1 11.96 11.48 0.78 o 3 6 1 138.21 125.78 2.89 o 4 6 1 44.41 44.26 1.54 o 5 6 1 14.31 16.02 1.10 o 0 7 1 4.92 5.48 0.88 o 1 7 1 0.29 0.24 0.77 o 2 7 1 55.66 49.33 1.66 o 3 7 1 2.04 2.83 0.93 o -4 -6 2 0.20 0.27 0.61 o -3 -6 2 5.14 5.95 0.51 o -2 -6 2 33.89 32.75 1.03 o -1 -6 2 0.00 -0.12 0.57 o 0 -6 2 41.30 41.34 1.06 o -5 -5 2 16.77 16.34 1.06 o -4 -5 2 6.54 5.69 0.68 o -3 -5 2 74.32 65.88 3.40 o -2 -5 2 18.57 20.55 0.66 o -1 -5 2 67.70 67.99 1.84 o 0 -5 2 19.35 19.18 0.68 o 1 -5 2 8.89 9.18 0.55 o 2 -5 2 20.28 24.21 1.25 o -5 -4 2 2.65 4.01 1.04 o -4 -4 2 73.01 63.40 1.17 o -3 -4 2 0.12 1.25 0.53 o -2 -4 2 207.49 193.28 5.63 o -1 -4 2 58.48 58.03 1.06 o 0 -4 2 9.37 9.77 0.49 o 1 -4 2 20.10 23.02 0.72 o 2 -4 2 0.25 0.39 1.04 o 3 -4 2 34.11 32.08 1.28 o -6 -3 2 22.33 21.88 1.07 o -5 -3 2 26.82 24.59 1.02 o -4 -3 2 21.87 25.89 0.97 o -3 -3 2 0.24 0.06 0.44 o -2 -3 2 162.35 184.47 4.25 o -1 -3 2 117.46 120.81 2.15 o 0 -3 2 111.52 113.65 1.64 o 1 -3 2 47.06 49.76 0.75 o 2 -3 2 11.12 12.81 0.52 o 3 -3 2 30.05 27.77 0.78 o 4 -3 2 12.10 11.81 0.63 o -6 -2 2 26.12 27.36 0.89 o -5 -2 2 36.75 37.36 0.92 o -4 -2 2 34.45 35.21 0.81 o -3 -2 2 0.30 2.71 0.42 o -2 -2 2 12.48 13.92 0.34 o -1 -2 2 526.51 517.15 5.98 o 0 -2 2 26.64 28.81 0.44 o 1 -2 2 5.78 4.07 0.30 o 2 -2 2 270.46 275.09 3.47 o 3 -2 2 0.12 0.01 0.57 o 4 -2 2 108.41 100.38 1.72 o 5 -2 2 2.34 5.52 0.84 o -6 -1 2 17.93 20.46 0.79 o -5 -1 2 56.68 57.33 2.70 o -4 -1 2 17.45 20.02 0.61 o -3 -1 2 227.90 241.36 2.45 o -2 -1 2 193.66 182.40 3.56 o -1 -1 2 6.35 5.32 0.19 o 0 -1 2 1243.77 1181.88 13.35 o 1 -1 2 906.44 914.52 10.44 o 2 -1 2 331.55 331.24 4.19 o 3 -1 2 68.48 61.80 1.11 o 4 -1 2 0.99 1.92 0.63 o 5 -1 2 4.79 5.78 0.49 o -6 0 2 12.94 12.43 0.66 o -5 0 2 7.12 8.02 0.54 o -4 0 2 4.45 7.15 0.46 o -3 0 2 14.68 20.13 0.74 o -2 0 2 1146.67 1112.26 13.67 o -1 0 2 345.03 305.37 3.57 o 0 0 2 324.72 283.16 4.46 o 1 0 2 47.80 36.36 0.89 o 2 0 2 172.58 164.76 2.11 o 3 0 2 3.90 4.74 0.34 o 4 0 2 26.47 25.31 0.54 o 5 0 2 170.57 163.30 2.45 o -5 1 2 18.40 17.31 0.85 o -4 1 2 7.92 8.42 0.48 o -3 1 2 110.49 112.15 1.66 o -2 1 2 64.48 62.19 1.15 o -1 1 2 96.31 89.78 1.48 o 0 1 2 391.31 347.29 3.91 o 1 1 2 49.35 48.26 0.56 o 2 1 2 83.68 88.97 1.00 o 3 1 2 3.41 2.47 0.26 o 4 1 2 144.01 143.03 1.67 o 5 1 2 105.09 105.17 1.75 o 6 1 2 0.69 1.27 0.81 o -5 2 2 33.47 31.92 1.57 o -4 2 2 69.79 66.69 2.29 o -3 2 2 13.53 11.00 0.48 o -2 2 2 281.92 272.89 3.89 o -1 2 2 347.45 387.29 3.73 o 0 2 2 53.66 57.08 0.78 o 1 2 2 34.95 35.77 0.51 o 2 2 2 505.34 545.03 5.19 o 3 2 2 7.82 7.38 0.30 o 4 2 2 13.70 13.87 0.42 o 5 2 2 23.64 25.46 0.61 o 6 2 2 175.42 175.04 2.66 o -4 3 2 2.41 4.14 1.12 o -3 3 2 34.69 33.39 0.82 o -2 3 2 66.74 67.44 0.91 o -1 3 2 20.72 19.84 0.40 o 0 3 2 243.33 257.70 2.56 o 1 3 2 403.28 407.51 7.01 o 2 3 2 25.08 26.01 0.52 o 3 3 2 26.65 27.73 0.51 o 4 3 2 11.51 13.39 0.43 o 5 3 2 421.00 438.52 4.49 o 6 3 2 43.59 48.63 1.15 o -4 4 2 89.05 82.10 1.59 o -3 4 2 78.50 72.51 1.36 o -2 4 2 9.98 10.60 0.40 o -1 4 2 6.90 7.39 0.32 o 0 4 2 471.26 460.76 4.69 o 1 4 2 136.41 129.11 1.41 o 2 4 2 166.69 166.34 3.34 o 3 4 2 154.80 147.23 1.98 o 4 4 2 307.07 303.08 4.23 o 5 4 2 6.99 7.56 0.50 o 6 4 2 21.10 24.37 1.21 o -3 5 2 24.90 22.77 1.00 o -2 5 2 54.35 52.22 1.02 o -1 5 2 84.20 76.32 2.74 o 0 5 2 5.89 6.08 0.33 o 1 5 2 14.34 13.45 0.75 o 2 5 2 220.82 227.19 4.45 o 3 5 2 294.50 283.07 5.35 o 4 5 2 19.31 19.60 1.01 o 5 5 2 0.45 0.46 0.97 o -1 6 2 1.75 2.11 0.90 o 0 6 2 17.44 17.90 0.94 o 1 6 2 116.96 114.21 2.68 o 3 6 2 0.00 0.04 0.69 o 4 6 2 29.25 29.08 1.29 o 5 6 2 0.74 1.28 1.02 o 0 7 2 47.02 47.18 1.70 o 1 7 2 26.91 27.87 1.30 o 2 7 2 5.21 6.42 0.77 o 3 7 2 111.88 108.67 2.84 o 4 7 2 13.57 12.77 1.04 o -3 -6 3 14.38 12.84 0.67 o -2 -6 3 0.86 1.32 0.60 o -1 -6 3 9.65 10.06 0.92 o -4 -5 3 0.69 0.97 1.00 o -3 -5 3 27.23 25.72 0.79 o -2 -5 3 10.51 10.34 0.52 o -1 -5 3 0.02 -0.03 0.50 o 0 -5 3 0.73 1.89 0.63 o 1 -5 3 62.22 66.83 2.01 o -5 -4 3 13.60 11.16 0.80 o -4 -4 3 199.95 183.39 3.64 o -3 -4 3 21.40 22.33 0.68 o -2 -4 3 32.13 29.12 1.54 o -1 -4 3 0.91 0.69 0.45 o 0 -4 3 11.39 10.69 0.52 o 1 -4 3 53.70 52.91 1.54 o 2 -4 3 10.36 12.17 0.85 o 3 -4 3 34.99 32.99 1.37 o -6 -3 3 0.11 -0.34 0.96 o -5 -3 3 170.06 165.23 3.43 o -4 -3 3 5.95 6.47 0.62 o -3 -3 3 13.54 15.40 0.59 o -2 -3 3 1.75 1.62 0.50 o -1 -3 3 137.20 132.33 2.12 o 0 -3 3 104.07 105.48 2.23 o 1 -3 3 0.08 0.29 0.81 o 2 -3 3 167.00 160.09 3.23 o 3 -3 3 94.56 86.46 3.55 o 4 -3 3 4.95 4.21 0.49 o -6 -2 3 51.73 46.80 1.59 o -5 -2 3 4.16 4.16 0.49 o -4 -2 3 0.04 0.21 0.57 o -3 -2 3 0.58 0.47 0.36 o -2 -2 3 2.69 2.82 0.35 o -1 -2 3 506.75 502.03 4.81 o 0 -2 3 33.11 35.95 0.72 o 1 -2 3 6.33 5.99 0.35 o 2 -2 3 0.55 1.06 0.55 o 3 -2 3 20.32 18.74 0.61 o 4 -2 3 2.97 3.22 0.40 o -6 -1 3 0.40 0.13 0.82 o -5 -1 3 7.91 7.98 0.49 o -4 -1 3 3.57 4.22 0.42 o -3 -1 3 86.17 90.22 1.37 o -2 -1 3 0.30 0.63 0.28 o -1 -1 3 626.03 681.83 6.43 o 0 -1 3 310.31 309.36 5.04 o 1 -1 3 9.44 8.76 0.35 o 2 -1 3 52.43 47.59 0.86 o 3 -1 3 100.40 88.64 1.95 o 4 -1 3 26.53 25.72 0.75 o 5 -1 3 6.58 5.65 0.49 o -6 0 3 2.21 5.53 0.86 o -5 0 3 23.16 23.75 0.79 o -4 0 3 55.64 54.54 1.09 o -3 0 3 89.05 88.24 1.64 o -2 0 3 125.32 132.75 1.77 o -1 0 3 51.05 54.03 0.81 o 0 0 3 119.90 121.69 2.09 o 1 0 3 0.66 0.14 0.38 o 2 0 3 97.24 82.86 1.55 o 3 0 3 351.27 343.14 6.77 o 4 0 3 4.53 4.12 0.31 o 5 0 3 0.05 -0.04 0.51 o -5 1 3 25.94 28.85 0.87 o -4 1 3 69.18 65.75 1.25 o -3 1 3 175.10 169.38 2.32 o -2 1 3 4.42 5.88 0.32 o -1 1 3 3.02 3.20 0.16 o 0 1 3 282.39 293.93 3.37 o 1 1 3 1358.98 1287.56 14.36 o 2 1 3 1536.62 1567.05 14.61 o 3 1 3 240.76 249.37 3.64 o 4 1 3 37.81 38.66 0.95 o 5 1 3 15.69 16.17 0.52 o 6 1 3 43.87 40.44 1.05 o -5 2 3 10.97 11.01 0.64 o -4 2 3 3.04 5.14 0.76 o -3 2 3 67.80 64.32 1.45 o -2 2 3 109.63 112.67 1.25 o -1 2 3 194.92 197.05 1.98 o 0 2 3 208.92 164.08 3.95 o 1 2 3 962.46 1010.50 16.62 o 2 2 3 185.00 213.51 3.18 o 3 2 3 58.24 61.27 1.26 o 4 2 3 17.16 14.51 0.43 o 5 2 3 13.32 13.21 0.47 o 6 2 3 5.41 6.07 0.53 o -4 3 3 10.28 10.64 0.56 o -3 3 3 5.07 6.44 0.47 o -2 3 3 7.81 9.48 0.34 o -1 3 3 1.34 1.05 0.36 o 0 3 3 418.26 441.11 7.71 o 1 3 3 892.01 994.75 16.46 o 2 3 3 223.68 223.09 2.68 o 3 3 3 193.49 198.78 2.12 o 4 3 3 124.63 119.62 1.46 o 5 3 3 3.62 3.89 0.36 o 6 3 3 60.50 64.13 2.05 o -4 4 3 9.13 9.38 0.62 o -3 4 3 44.14 46.48 1.05 o -2 4 3 43.93 44.17 0.96 o -1 4 3 17.60 16.76 0.41 o 0 4 3 74.37 87.94 1.48 o 1 4 3 60.58 62.72 1.55 o 2 4 3 19.09 19.20 0.90 o 3 4 3 16.17 16.77 0.88 o 4 4 3 130.85 135.29 2.10 o 5 4 3 38.60 40.40 1.02 o 6 4 3 1.25 1.93 1.16 o -3 5 3 29.23 30.52 0.91 o -2 5 3 0.18 0.15 0.97 o -1 5 3 47.08 45.53 1.30 o 0 5 3 14.15 12.87 0.50 o 1 5 3 115.23 114.22 1.75 o 2 5 3 39.44 39.55 1.28 o 4 5 3 58.67 57.91 1.71 o 5 5 3 1.41 2.06 0.89 o -1 6 3 11.47 13.73 0.96 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