#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/24/2202404.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202404_Fobs loop_ _publ_author_name 'Liao, Wuping' 'Hu, Chunhua' 'Dronskowski, Richard' _publ_section_title ; Hexaaquabis(dicyanoguanidine)terbium(III) trichloride ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1124 _journal_page_last m1126 _journal_volume 59 _journal_year 2003 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 29.4250 _cell_length_b 9.2613 _cell_length_c 13.6896 _exptl_crystal_F_000 2112.00 _reflns_d_resolution_high 0.7497 _[local]_cod_data_source_file bt6375Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Tb-H2N2 Fdd2 {Tb(H2O)6[NCNC(NH2)2]}Cl3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 815.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 -18 23836.50 22995.47 889.81 o 6 0 -18 8576.03 9109.01 588.95 o 0 2 -18 6936.52 7516.29 514.07 o 1 1 -17 8313.05 8255.57 360.99 o 3 1 -17 17685.51 17864.51 520.83 o 5 1 -17 8407.34 8465.27 302.56 o 7 1 -17 8685.84 9079.37 444.57 o 9 1 -17 15027.00 14907.45 395.13 o 11 1 -17 8321.08 8216.98 312.54 o 13 1 -17 7145.32 6732.05 383.85 o 1 3 -17 6598.08 6943.55 397.34 o 3 3 -17 12356.12 11741.70 389.78 o 5 3 -17 6497.79 6656.33 331.99 o 7 3 -17 4674.71 4577.85 300.08 o 9 3 -17 14453.51 14496.18 499.99 o 0 0 -16 23264.46 22960.79 1189.79 o 4 0 -16 32573.87 31846.61 867.32 o 8 0 -16 28307.96 28005.55 869.21 o 12 0 -16 8313.39 8393.30 433.16 o 16 0 -16 24422.58 24462.48 980.94 o 2 2 -16 28245.51 26873.87 600.36 o 4 2 -16 55.00 99.85 73.95 o 6 2 -16 9605.42 9944.63 320.21 o 8 2 -16 246.45 321.10 83.23 o 10 2 -16 28058.10 28151.72 582.04 o 12 2 -16 34.63 162.33 84.87 o 14 2 -16 27795.65 28052.83 749.67 o 16 2 -16 357.20 393.65 134.21 o 0 4 -16 10046.63 9685.71 513.76 o 2 4 -16 376.00 465.31 96.97 o 4 4 -16 23591.71 23304.85 634.96 o 6 4 -16 567.80 533.43 121.69 o 8 4 -16 17287.96 17409.74 536.48 o 10 4 -16 45.93 207.46 119.24 o 12 4 -16 10493.31 11193.08 788.99 o 14 4 -16 363.78 430.16 182.13 o 1 1 -15 18295.30 17279.07 361.93 o 3 1 -15 28135.37 27991.94 669.04 o 5 1 -15 17896.17 16596.47 389.20 o 7 1 -15 7603.75 7232.08 263.52 o 9 1 -15 15369.75 15299.34 379.73 o 11 1 -15 13017.70 12746.57 345.42 o 13 1 -15 10817.53 9929.81 358.57 o 15 1 -15 22343.91 20895.29 610.94 o 17 1 -15 10316.08 10215.77 437.97 o 19 1 -15 8024.19 8018.67 400.30 o 21 1 -15 13613.21 13616.01 661.87 o 1 3 -15 10114.45 10046.89 303.69 o 3 3 -15 20356.93 19132.32 591.63 o 5 3 -15 12895.02 12515.18 366.02 o 7 3 -15 12536.44 11892.88 358.63 o 9 3 -15 20955.56 21248.72 513.57 o 11 3 -15 13601.32 13356.33 756.60 o 13 3 -15 11658.67 11127.52 512.35 o 15 3 -15 16506.46 17387.35 628.39 o 17 3 -15 8403.37 9367.03 489.60 o 19 3 -15 6921.83 6907.37 435.50 o 1 5 -15 11653.63 13172.71 816.84 o 3 5 -15 15151.18 14864.21 426.31 o 5 5 -15 6983.63 6953.62 339.76 o 7 5 -15 6495.64 6397.85 333.21 o 9 5 -15 13641.53 13243.44 530.47 o 11 5 -15 10350.67 10166.25 488.44 o 13 5 -15 10945.88 11392.34 529.62 o 15 5 -15 10632.61 11124.18 527.30 o 1 7 -15 6550.30 6859.02 373.80 o 2 0 -14 65024.43 62230.92 1198.63 o 6 0 -14 12184.40 11893.71 604.36 o 10 0 -14 33371.43 32903.92 875.65 o 14 0 -14 31774.47 29151.69 1037.34 o 18 0 -14 14229.43 13799.70 714.71 o 22 0 -14 22914.20 21747.75 915.86 o 0 2 -14 31145.41 30011.83 685.60 o 2 2 -14 438.76 460.22 76.90 o 4 2 -14 36412.58 36028.09 598.88 o 6 2 -14 858.17 949.38 105.83 o 8 2 -14 44850.23 43379.21 756.41 o 10 2 -14 203.67 213.48 70.90 o 12 2 -14 20120.53 20130.27 493.84 o 14 2 -14 424.59 374.68 116.13 o 16 2 -14 36245.25 36190.55 940.74 o 18 2 -14 314.19 227.08 111.53 o 20 2 -14 21773.20 21195.59 625.27 o 22 2 -14 537.43 621.96 141.35 o 24 2 -14 11200.40 11048.37 484.99 o 2 4 -14 28373.18 27819.30 547.04 o 4 4 -14 1246.25 1242.50 120.53 o 6 4 -14 18375.14 17956.89 512.34 o 8 4 -14 70.28 64.89 90.30 o 10 4 -14 29656.60 29372.83 931.17 o 12 4 -14 52.04 177.97 119.35 o 14 4 -14 24109.73 23334.00 737.61 o 16 4 -14 8.36 -51.52 105.11 o 18 4 -14 12674.77 12635.90 765.04 o 20 4 -14 607.69 1005.20 195.45 o 0 6 -14 19555.05 21279.46 862.66 o 2 6 -14 1766.25 1817.87 225.52 o 4 6 -14 19615.44 19707.82 759.44 o 6 6 -14 232.68 248.21 162.80 o 8 6 -14 16520.88 15897.65 564.71 o 10 6 -14 309.07 335.58 125.10 o 12 6 -14 16118.40 15530.18 583.74 o 14 6 -14 21.00 172.47 114.39 o 16 6 -14 18012.97 18938.67 958.72 o 1 1 -13 18672.08 17833.44 325.02 o 3 1 -13 34751.82 33218.05 507.14 o 5 1 -13 23394.17 22716.38 415.50 o 7 1 -13 19846.91 19440.31 411.75 o 9 1 -13 20066.89 19145.35 411.52 o 11 1 -13 16573.62 15747.29 430.16 o 13 1 -13 16252.86 15243.02 432.99 o 15 1 -13 24183.99 22945.34 613.38 o 17 1 -13 16903.17 16385.55 504.26 o 19 1 -13 7226.20 7897.69 374.74 o 21 1 -13 16257.90 15255.42 505.60 o 23 1 -13 10058.32 9874.72 438.60 o 25 1 -13 8217.02 8144.46 412.30 o 27 1 -13 14861.88 14432.42 535.60 o 1 3 -13 24885.84 23436.56 465.27 o 3 3 -13 38775.22 38332.52 668.35 o 5 3 -13 13717.36 13754.06 330.62 o 7 3 -13 15099.39 14747.51 378.43 o 9 3 -13 20471.33 19949.62 464.80 o 11 3 -13 24962.21 25361.18 616.08 o 13 3 -13 26974.52 26548.38 772.23 o 15 3 -13 18504.25 18888.10 633.04 o 17 3 -13 14673.23 14206.02 539.70 o 19 3 -13 7640.99 7705.19 430.86 o 21 3 -13 16719.07 15938.36 599.93 o 23 3 -13 13395.35 13583.40 589.31 o 25 3 -13 5690.27 6359.33 428.52 o 1 5 -13 11036.76 10909.37 298.26 o 3 5 -13 20668.40 21462.46 506.12 o 5 5 -13 10370.81 10810.25 593.42 o 7 5 -13 15539.19 15361.05 627.76 o 9 5 -13 17900.41 16762.02 566.03 o 11 5 -13 5514.64 5644.57 347.24 o 13 5 -13 8436.46 8249.03 755.70 o 15 5 -13 13704.11 13698.03 534.57 o 17 5 -13 8937.91 9118.75 459.25 o 19 5 -13 11871.54 11489.81 523.90 o 21 5 -13 9186.52 9913.82 499.83 o 1 7 -13 13281.93 12798.77 520.12 o 3 7 -13 9463.83 9515.69 646.48 o 5 7 -13 9103.02 8601.08 637.86 o 7 7 -13 4403.95 4850.90 358.59 o 9 7 -13 11667.12 11242.29 624.69 o 11 7 -13 14279.14 14539.06 1103.08 o 13 7 -13 11331.98 11455.63 752.10 o 15 7 -13 11474.22 11811.94 693.37 o 0 0 -12 28154.85 26170.96 1074.05 o 4 0 -12 55230.44 50982.78 984.56 o 8 0 -12 74316.43 71440.57 1537.16 o 12 0 -12 57372.38 53690.05 1232.00 o 16 0 -12 33132.02 34428.82 1128.35 o 20 0 -12 36694.16 34747.93 2121.95 o 24 0 -12 17213.74 16950.73 765.68 o 28 0 -12 23902.92 23805.96 2332.18 o 2 2 -12 76493.49 71824.64 935.98 o 4 2 -12 1378.10 1459.42 105.63 o 6 2 -12 40484.09 39383.07 616.68 o 8 2 -12 150.74 137.62 60.50 o 10 2 -12 60662.29 60408.09 954.11 o 12 2 -12 257.07 261.59 78.91 o 14 2 -12 57912.78 56354.99 1380.32 o 16 2 -12 439.74 464.21 126.21 o 18 2 -12 30446.46 30178.57 919.96 o 20 2 -12 204.94 298.51 108.38 o 22 2 -12 30733.07 29698.18 764.20 o 24 2 -12 16.54 113.89 105.58 o 26 2 -12 25494.08 25351.56 712.38 o 28 2 -12 382.48 559.76 161.09 o 0 4 -12 52338.37 49013.04 1129.99 o 2 4 -12 2032.19 2015.58 192.27 o 4 4 -12 55616.99 53776.91 862.81 o 6 4 -12 2152.16 2242.90 139.10 o 8 4 -12 34654.82 33472.58 621.75 o 10 4 -12 666.82 775.30 144.04 o 12 4 -12 34506.43 31793.69 855.82 o 14 4 -12 1096.30 1225.13 176.11 o 16 4 -12 45537.14 44531.11 1125.82 o 18 4 -12 1328.73 1262.92 190.81 o 20 4 -12 24900.70 23884.91 901.88 o 22 4 -12 1197.74 1456.32 217.40 o 24 4 -12 19402.94 19352.28 883.54 o 26 4 -12 430.63 643.85 168.49 o 2 6 -12 26881.84 27416.68 795.82 o 4 6 -12 1303.00 1217.35 127.36 o 6 6 -12 29912.18 29703.57 732.57 o 8 6 -12 1086.24 1264.11 152.55 o 10 6 -12 22486.49 21000.17 828.83 o 12 6 -12 125.75 185.91 113.50 o 14 6 -12 19884.27 18631.83 616.66 o 16 6 -12 767.81 976.59 170.74 o 18 6 -12 17383.03 17998.82 626.68 o 20 6 -12 355.83 299.23 227.55 o 22 6 -12 17096.61 16473.35 780.09 o 0 8 -12 23948.63 24552.40 1406.48 o 2 8 -12 1055.44 1387.04 209.52 o 4 8 -12 17918.74 17333.65 635.09 o 6 8 -12 0.16 282.90 135.86 o 8 8 -12 19589.53 18205.11 743.98 o 10 8 -12 802.70 1022.27 270.38 o 12 8 -12 20551.45 20247.38 1280.61 o 14 8 -12 199.38 212.23 228.02 o 1 1 -11 32379.50 30464.47 572.10 o 3 1 -11 19701.97 19179.32 321.88 o 5 1 -11 36210.20 35791.32 513.90 o 7 1 -11 18450.33 18015.20 307.49 o 9 1 -11 35747.15 35201.88 606.55 o 11 1 -11 31092.36 30192.44 613.80 o 13 1 -11 17885.97 17009.49 410.16 o 15 1 -11 29138.64 27308.11 656.65 o 17 1 -11 20147.38 18196.42 885.44 o 19 1 -11 8383.75 8068.80 350.54 o 21 1 -11 18154.88 17443.74 523.19 o 23 1 -11 11712.93 11888.63 436.92 o 25 1 -11 12833.68 12345.02 457.92 o 27 1 -11 12394.68 11980.54 479.63 o 29 1 -11 9964.65 9634.57 472.74 o 31 1 -11 4478.54 5239.51 348.50 o 1 3 -11 28385.83 26993.99 488.81 o 3 3 -11 26563.25 25478.27 468.92 o 5 3 -11 23232.03 22894.33 515.09 o 7 3 -11 34791.88 33435.47 579.58 o 9 3 -11 35860.73 34607.74 597.56 o 11 3 -11 8138.43 8009.55 401.81 o 13 3 -11 10817.47 11333.29 347.58 o 15 3 -11 25498.44 25771.16 735.37 o 17 3 -11 22423.67 21160.70 786.94 o 19 3 -11 23869.21 22607.07 698.53 o 21 3 -11 13339.76 12997.16 634.77 o 23 3 -11 9208.56 9377.57 715.08 o 25 3 -11 10384.73 10774.55 513.52 o 27 3 -11 7955.19 8925.93 483.28 o 29 3 -11 9176.74 9766.36 766.58 o 1 5 -11 28014.72 26773.16 497.34 o 3 5 -11 29186.98 28051.00 513.52 o 5 5 -11 8402.67 8444.12 278.55 o 7 5 -11 7141.02 7153.54 483.91 o 9 5 -11 17388.10 16893.94 469.17 o 11 5 -11 25133.32 25022.24 616.56 o 13 5 -11 21651.85 22271.53 664.70 o 15 5 -11 10896.50 10489.21 430.41 o 17 5 -11 7488.34 8275.18 411.01 o 19 5 -11 9254.69 8930.73 682.00 o 21 5 -11 13100.94 13658.77 699.63 o 23 5 -11 13437.21 14320.11 932.42 o 25 5 -11 9550.07 9679.57 727.90 o 27 5 -11 8845.73 7350.99 808.55 o 1 7 -11 6787.28 6901.46 320.44 o 3 7 -11 15079.68 13583.23 509.43 o 5 7 -11 11744.08 11991.04 471.84 o 7 7 -11 15891.30 15409.34 653.45 o 9 7 -11 12370.84 12897.72 415.30 o 11 7 -11 3440.53 3671.23 348.83 o 13 7 -11 4174.32 3988.83 293.57 o 15 7 -11 9378.76 9977.91 438.35 o 17 7 -11 9738.30 10006.88 774.51 o 19 7 -11 12067.47 11654.46 656.16 o 21 7 -11 7871.94 7996.00 570.00 o 1 9 -11 9537.82 9637.52 625.11 o 3 9 -11 6258.04 7043.40 573.59 o 5 9 -11 5311.71 5252.77 487.24 o 7 9 -11 5217.17 4372.97 441.92 o 9 9 -11 5931.25 6308.99 522.98 o 11 9 -11 12771.01 12889.78 704.01 o 2 0 -10 106905.84 103205.11 1774.52 o 6 0 -10 78549.20 76676.91 1359.05 o 10 0 -10 124031.10 120336.64 2386.77 o 14 0 -10 102444.11 101016.27 2572.50 o 18 0 -10 56372.02 55662.77 1593.63 o 22 0 -10 51991.23 52069.15 1561.88 o 26 0 -10 27281.02 26695.01 1003.12 o 30 0 -10 35021.80 33097.48 1364.61 o 0 2 -10 82266.34 79649.00 1412.04 o 2 2 -10 4276.40 3996.39 130.32 o 4 2 -10 111840.94 106627.99 1889.68 o 6 2 -10 1093.96 1106.29 84.11 o 8 2 -10 71021.15 68344.53 1278.76 o 10 2 -10 35.59 149.30 50.88 o 12 2 -10 71543.07 69767.30 1157.37 o 14 2 -10 1634.29 1709.28 159.03 o 16 2 -10 43712.38 43042.72 914.02 o 18 2 -10 1701.26 1794.02 175.34 o 20 2 -10 62452.27 60479.78 1228.48 o 22 2 -10 122.55 232.33 101.61 o 24 2 -10 33260.73 33087.87 808.25 o 26 2 -10 986.01 1097.51 165.80 o 28 2 -10 24968.16 24568.00 685.87 o 30 2 -10 88.51 244.06 132.82 o 32 2 -10 19397.46 20482.93 1124.98 o 2 4 -10 63737.50 61948.66 938.03 o 4 4 -10 3636.66 3459.55 152.06 o 6 4 -10 93028.20 90542.63 1310.15 o 8 4 -10 77.18 69.48 57.11 o 10 4 -10 58584.25 58859.70 995.49 o 12 4 -10 879.14 904.66 119.65 o 14 4 -10 52126.18 51172.87 1195.34 o 16 4 -10 166.36 72.92 95.66 o 18 4 -10 38690.76 38417.91 985.41 o 20 4 -10 419.58 494.95 135.62 o 22 4 -10 43993.42 40952.20 1069.07 o 24 4 -10 152.85 140.12 111.50 o 26 4 -10 28114.93 29344.36 878.23 o 28 4 -10 818.29 969.12 190.02 o 30 4 -10 19270.93 19143.92 689.06 o 0 6 -10 55033.81 53342.71 1516.92 o 2 6 -10 2888.31 2867.79 170.28 o 4 6 -10 52159.46 52569.61 1044.20 o 6 6 -10 208.84 245.07 86.49 o 8 6 -10 35913.64 36352.08 822.51 o 10 6 -10 1855.65 1728.83 164.17 o 12 6 -10 38997.06 40388.61 872.33 o 14 6 -10 1464.58 1728.29 290.84 o 16 6 -10 39405.25 39634.87 1445.46 o 18 6 -10 219.11 245.00 118.58 o 20 6 -10 22333.70 23069.73 711.65 o 22 6 -10 1243.96 1502.27 512.79 o 24 6 -10 23527.87 23138.09 956.01 o 26 6 -10 735.54 511.62 227.15 o 2 8 -10 29245.08 27596.40 1080.77 o 4 8 -10 1279.92 1158.71 180.32 o 6 8 -10 26201.44 25893.13 766.24 o 8 8 -10 497.19 416.23 158.79 o 10 8 -10 18194.87 17793.97 783.36 o 12 8 -10 84.63 11.02 145.69 o 14 8 -10 19456.52 21366.76 888.69 o 16 8 -10 20.61 -7.16 275.73 o 18 8 -10 20569.44 20002.89 835.76 o 20 8 -10 1192.56 1331.66 254.30 o 0 10 -10 16143.12 15802.53 1098.94 o 2 10 -10 539.14 1099.59 234.30 o 4 10 -10 12271.38 12170.16 709.44 o 6 10 -10 123.03 -6.74 128.43 o 8 10 -10 19147.35 18859.60 864.48 o 1 1 -9 39057.70 35894.18 1033.47 o 3 1 -9 35039.68 33363.72 465.12 o 5 1 -9 55578.13 53734.04 695.25 o 7 1 -9 77204.84 73416.12 1281.26 o 9 1 -9 36101.20 35170.39 530.01 o 11 1 -9 29277.93 28233.24 449.01 o 13 1 -9 21061.42 21097.29 516.54 o 15 1 -9 28030.34 26879.13 623.02 o 17 1 -9 48205.53 47437.29 973.35 o 19 1 -9 23639.81 23319.96 588.66 o 21 1 -9 18590.96 18171.56 511.03 o 23 1 -9 19991.01 19231.15 543.70 o 25 1 -9 13910.57 13268.32 448.67 o 27 1 -9 13517.24 13927.52 481.78 o 29 1 -9 8277.82 9177.62 415.46 o 31 1 -9 14442.40 14701.56 519.74 o 33 1 -9 11610.65 11326.00 482.28 o 1 3 -9 56528.45 55188.13 830.22 o 3 3 -9 19496.58 19530.10 394.46 o 5 3 -9 21083.00 20261.33 523.28 o 7 3 -9 17723.00 17523.40 342.47 o 9 3 -9 26623.25 26856.94 474.61 o 11 3 -9 29989.93 29529.68 558.33 o 13 3 -9 23177.38 23497.35 546.61 o 15 3 -9 16862.36 16048.90 508.78 o 17 3 -9 13282.39 12818.99 455.29 o 19 3 -9 11592.61 10631.41 432.21 o 21 3 -9 17652.37 17964.99 588.81 o 23 3 -9 26986.78 27659.34 803.61 o 25 3 -9 17723.44 17956.23 621.79 o 27 3 -9 7572.49 6549.16 398.10 o 29 3 -9 8848.50 8681.20 464.03 o 31 3 -9 4305.97 4452.35 357.16 o 1 5 -9 9864.35 9251.68 229.02 o 3 5 -9 27674.10 25947.93 464.21 o 5 5 -9 33996.98 33620.81 565.98 o 7 5 -9 46736.66 46388.25 1510.21 o 9 5 -9 41733.40 42027.76 862.92 o 11 5 -9 18154.67 18420.49 514.27 o 13 5 -9 22987.83 23420.81 704.82 o 15 5 -9 13444.96 13336.79 627.89 o 17 5 -9 20786.29 19112.20 593.54 o 19 5 -9 30100.55 30051.85 997.59 o 21 5 -9 13831.04 14715.77 755.09 o 23 5 -9 5316.81 5272.82 345.15 o 25 5 -9 8317.40 9579.80 462.02 o 27 5 -9 7549.23 6641.32 529.70 o 29 5 -9 12983.87 14224.52 1098.75 o 1 7 -9 28203.78 27923.30 774.10 o 3 7 -9 18262.17 16484.77 541.39 o 5 7 -9 7499.62 7625.66 482.71 o 7 7 -9 6989.32 7047.94 284.35 o 9 7 -9 8845.30 8443.64 312.94 o 11 7 -9 17194.79 15877.18 449.33 o 13 7 -9 18533.01 18323.87 499.84 o 15 7 -9 9234.83 8799.86 419.51 o 17 7 -9 6872.80 6358.06 507.01 o 19 7 -9 5992.22 5702.34 451.43 o 21 7 -9 9948.65 9092.95 917.80 o 23 7 -9 10875.98 11303.60 655.49 o 25 7 -9 8465.73 8040.95 581.85 o 1 9 -9 4456.40 4202.55 420.81 o 3 9 -9 9670.72 8327.68 559.41 o 5 9 -9 16277.55 14788.82 1083.23 o 7 9 -9 7061.93 6936.95 516.86 o 9 9 -9 6609.21 6344.44 495.66 o 11 9 -9 5648.04 5481.44 472.12 o 13 9 -9 4663.95 4054.17 414.81 o 15 9 -9 7497.25 8024.02 564.03 o 17 9 -9 7361.97 7084.73 790.46 o 0 0 -8 150032.53 147172.92 3440.92 o 4 0 -8 159072.73 160638.27 2644.70 o 8 0 -8 172308.31 173270.81 2845.68 o 12 0 -8 138201.63 130142.16 2518.06 o 16 0 -8 51519.77 52129.16 1451.13 o 20 0 -8 104079.92 98004.94 2530.25 o 24 0 -8 56667.55 55656.34 1626.36 o 28 0 -8 33140.41 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10 4 1925.55 2076.22 435.61 o 6 10 4 15083.01 15070.44 948.44 o 8 10 4 1198.13 1206.31 235.83 o 10 10 4 17652.47 18947.32 797.82 o 12 10 4 116.72 213.06 111.33 o 14 10 4 14768.00 15191.88 1189.52 o 16 10 4 1336.06 1633.39 260.82 o 18 10 4 10661.06 9208.94 799.43 o 20 10 4 496.30 437.52 285.33 o 0 12 4 7061.37 6983.96 782.62 o 2 12 4 529.43 501.67 197.36 o 1 1 5 92755.67 104703.08 2143.24 o 3 1 5 37863.01 39156.85 835.72 o 5 1 5 263349.72 270196.72 7783.17 o 7 1 5 132375.34 140333.27 4148.08 o 9 1 5 74428.61 80331.33 1469.09 o 11 1 5 70720.37 70721.09 1156.87 o 13 1 5 69988.03 70736.86 1168.75 o 15 1 5 60768.72 62911.65 1070.25 o 17 1 5 63166.26 63057.15 1087.31 o 19 1 5 89205.72 90300.83 1507.49 o 21 1 5 25981.49 24887.15 545.53 o 23 1 5 30331.05 29269.84 630.80 o 25 1 5 41394.36 39696.70 807.14 o 27 1 5 9483.92 9205.33 341.18 o 29 1 5 33392.22 32210.72 727.76 o 31 1 5 23504.49 22782.38 897.56 o 33 1 5 14370.74 13673.75 519.85 o 35 1 5 19818.87 18937.41 780.16 o 37 1 5 15884.07 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8972.90 8988.91 591.96 o 1 11 5 6228.41 6973.50 523.84 o 3 11 5 11044.29 10497.10 630.17 o 5 11 5 7418.39 7573.58 543.18 o 7 11 5 9532.81 8889.76 669.20 o 9 11 5 8054.22 7193.70 534.07 o 11 11 5 9962.89 7692.52 856.49 o 13 11 5 9993.13 10521.45 1053.07 o 2 0 6 56462.50 54887.93 1639.93 o 6 0 6 237582.75 246832.39 7138.62 o 10 0 6 117565.25 119672.37 2659.61 o 14 0 6 24610.63 25856.93 747.51 o 18 0 6 123951.88 129064.16 2941.86 o 22 0 6 34379.72 34901.41 1013.09 o 26 0 6 20815.68 19990.26 721.50 o 30 0 6 43201.14 43011.52 1352.21 o 34 0 6 20253.13 19452.89 1189.78 o 0 2 6 201015.25 220193.44 6322.65 o 2 2 6 1044.83 1202.82 132.30 o 4 2 6 90335.70 94712.59 2837.89 o 6 2 6 4892.72 5399.03 308.20 o 8 2 6 95255.16 102857.36 3127.64 o 10 2 6 3363.75 3142.45 128.67 o 12 2 6 99087.91 105037.35 1963.75 o 14 2 6 2913.84 3093.92 176.64 o 16 2 6 43739.73 42275.62 1578.12 o 18 2 6 0.12 30.79 72.60 o 20 2 6 66360.73 67044.66 1379.48 o 22 2 6 709.76 761.02 147.77 o 24 2 6 66257.65 63555.99 1776.48 o 26 2 6 1729.04 1773.18 194.15 o 28 2 6 20054.08 18900.40 736.90 o 30 2 6 1533.59 1654.18 262.32 o 32 2 6 17441.19 16784.08 762.59 o 34 2 6 160.76 118.06 164.58 o 36 2 6 23303.11 24223.95 2659.52 o 4 4 6 9298.88 9354.00 459.01 o 6 4 6 137380.23 147686.80 3568.49 o 8 4 6 3544.86 3331.48 257.14 o 10 4 6 53524.59 54432.23 940.89 o 12 4 6 537.74 520.48 68.73 o 14 4 6 38597.37 37522.40 813.08 o 16 4 6 1201.78 1362.04 186.01 o 18 4 6 65234.94 64456.02 1650.51 o 20 4 6 1362.96 1051.21 197.08 o 22 4 6 23862.18 25161.34 889.00 o 24 4 6 90.81 2.88 115.12 o 26 4 6 21868.16 19891.34 771.40 o 28 4 6 535.83 258.93 170.11 o 30 4 6 21660.65 21770.91 979.24 o 32 4 6 358.73 334.97 195.60 o 34 4 6 15919.37 15833.92 761.72 o 2 6 6 519.27 691.92 219.62 o 4 6 6 38968.65 37543.28 1486.51 o 6 6 6 567.22 538.13 127.09 o 8 6 6 52795.64 51342.73 1226.25 o 10 6 6 294.80 307.35 93.78 o 12 6 6 44129.18 44319.57 984.94 o 14 6 6 3573.30 3452.21 461.24 o 16 6 6 36367.84 34825.17 1832.59 o 18 6 6 1518.68 1355.71 216.36 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2171.03 o 5 1 7 108876.63 118436.29 3519.44 o 7 1 7 136841.64 149927.94 4443.95 o 9 1 7 36335.11 39364.20 1343.27 o 11 1 7 71535.01 75881.82 1779.11 o 13 1 7 62745.08 65100.48 1105.65 o 15 1 7 33701.55 34708.95 777.94 o 17 1 7 57604.74 58757.87 1040.68 o 19 1 7 33945.29 33159.14 668.94 o 21 1 7 30126.16 29741.36 630.42 o 23 1 7 56307.65 57743.11 1078.47 o 25 1 7 29359.67 29647.49 666.75 o 27 1 7 15814.23 14949.06 510.59 o 29 1 7 13825.16 14097.34 508.19 o 31 1 7 20419.88 20396.90 653.46 o 33 1 7 8061.16 8650.07 988.01 o 35 1 7 12050.98 12170.82 755.91 o 1 3 7 32080.87 33231.65 1102.11 o 3 3 7 46694.00 51201.92 1633.64 o 5 3 7 103276.26 113146.17 3409.64 o 7 3 7 86456.33 93504.73 2882.26 o 9 3 7 21851.89 21830.57 648.81 o 11 3 7 26576.37 26537.57 597.59 o 13 3 7 39433.43 39619.12 853.27 o 15 3 7 19281.78 19685.88 568.24 o 17 3 7 40706.98 41571.32 915.14 o 19 3 7 64121.52 63564.24 1318.32 o 21 3 7 32588.00 32277.84 986.85 o 23 3 7 21265.61 22303.91 1654.07 o 25 3 7 12925.17 13247.99 589.98 o 27 3 7 7167.10 7219.00 834.54 o 29 3 7 20058.70 18031.76 749.56 o 31 3 7 21918.14 22689.51 886.37 o 33 3 7 10135.30 10350.71 623.73 o 5 5 7 31533.06 33313.06 922.64 o 7 5 7 38868.16 39548.09 1565.75 o 9 5 7 45290.17 43772.70 944.76 o 11 5 7 69784.79 70884.93 1426.42 o 13 5 7 65930.16 67667.14 2158.66 o 15 5 7 25712.60 25832.52 852.16 o 17 5 7 24435.97 25104.18 826.89 o 19 5 7 22037.27 22866.92 791.44 o 21 5 7 14112.44 15102.46 627.54 o 23 5 7 25604.36 24309.65 874.72 o 25 5 7 20717.79 21111.61 816.91 o 27 5 7 7335.71 9179.46 1281.88 o 29 5 7 12389.63 12627.18 682.19 o 31 5 7 12058.34 11877.72 1077.75 o 1 7 7 15256.40 15476.05 1000.43 o 3 7 7 27258.83 28533.21 1256.80 o 5 7 7 46412.89 46192.83 1298.12 o 7 7 7 33913.61 33278.27 798.99 o 9 7 7 18351.45 17589.25 510.62 o 11 7 7 18391.95 17143.78 634.24 o 13 7 7 17418.83 17198.03 651.35 o 15 7 7 10568.63 9871.72 507.69 o 17 7 7 20863.60 20489.47 780.27 o 19 7 7 25061.22 25234.46 898.35 o 21 7 7 17133.47 17812.56 737.81 o 23 7 7 9446.35 10178.16 587.96 o 25 7 7 9088.73 7805.03 543.48 o 27 7 7 7935.67 7776.23 568.21 o 1 9 7 17426.37 17542.16 571.41 o 3 9 7 11482.03 11753.17 541.47 o 5 9 7 17732.64 17555.04 686.34 o 7 9 7 7672.20 8240.67 466.84 o 9 9 7 8913.07 8619.24 482.47 o 11 9 7 16541.66 15542.28 651.15 o 13 9 7 13469.17 13043.14 604.11 o 15 9 7 8868.37 8768.76 525.68 o 17 9 7 5790.54 4820.20 416.01 o 19 9 7 7571.60 8333.17 537.48 o 21 9 7 8340.34 7887.31 549.95 o 1 11 7 8770.40 9136.79 584.09 o 3 11 7 6610.53 6547.18 511.94 o 5 11 7 9720.83 11140.79 773.30 o 7 11 7 6111.31 6289.77 775.73 o 9 11 7 6425.30 7493.07 551.88 o 4 0 8 145390.98 138344.16 4041.38 o 8 0 8 165145.53 171800.75 5074.68 o 12 0 8 144470.91 153142.23 3403.09 o 16 0 8 47431.43 49042.37 1269.08 o 20 0 8 96294.98 100720.12 2406.68 o 24 0 8 64320.42 66664.16 1978.38 o 28 0 8 30938.66 31309.27 1018.96 o 32 0 8 25470.96 25626.23 935.52 o 2 2 8 104119.63 114206.17 2366.81 o 4 2 8 816.60 977.79 76.29 o 6 2 8 111599.60 118763.73 2463.92 o 8 2 8 7136.57 7457.03 407.99 o 10 2 8 66956.87 66775.09 1607.79 o 12 2 8 375.42 335.00 156.26 o 14 2 8 36271.89 35012.35 787.07 o 16 2 8 3079.56 3034.72 201.03 o 18 2 8 89523.00 93370.45 1839.49 o 20 2 8 1258.92 1432.77 160.32 o 22 2 8 51074.68 50700.30 1300.56 o 24 2 8 193.53 394.44 126.57 o 26 2 8 29414.86 29273.57 979.78 o 28 2 8 316.12 325.37 190.76 o 30 2 8 23690.59 24191.98 904.09 o 32 2 8 569.08 551.92 199.52 o 34 2 8 18045.48 18902.14 817.92 o 0 4 8 81603.95 91649.20 2794.44 o 2 4 8 839.46 976.40 168.98 o 4 4 8 70006.27 72149.29 2286.83 o 6 4 8 1477.92 1677.90 228.57 o 8 4 8 78963.98 81752.17 1944.08 o 10 4 8 2228.70 2313.32 219.84 o 12 4 8 75769.33 80384.57 1576.15 o 14 4 8 1491.10 1381.81 192.14 o 16 4 8 56518.93 55479.89 2782.58 o 18 4 8 2006.47 2006.53 347.85 o 20 4 8 32290.36 29153.29 933.73 o 22 4 8 186.77 103.31 141.55 o 24 4 8 32867.37 31702.02 1043.96 o 26 4 8 1014.19 1414.62 255.23 o 28 4 8 21384.92 19941.36 810.78 o 30 4 8 57.98 209.62 177.89 o 32 4 8 19154.80 18560.68 818.55 o 4 6 8 621.57 729.01 160.39 o 6 6 8 83477.84 86177.05 2075.20 o 8 6 8 1758.39 2180.39 246.46 o 10 6 8 54955.96 54223.83 1432.67 o 12 6 8 597.61 697.31 193.36 o 14 6 8 40521.36 40477.39 1174.53 o 16 6 8 1112.09 1220.40 207.95 o 18 6 8 40735.64 42595.18 1259.61 o 20 6 8 1187.62 1428.50 236.30 o 22 6 8 24198.42 25116.58 1268.83 o 24 6 8 753.06 799.45 205.67 o 26 6 8 20059.49 21180.68 970.23 o 28 6 8 1449.73 1631.99 322.17 o 0 8 8 46225.65 48819.88 1966.29 o 2 8 8 703.55 677.80 207.19 o 4 8 8 21566.45 21524.30 769.64 o 6 8 8 1053.52 1235.79 160.53 o 8 8 8 26665.50 26196.20 860.00 o 10 8 8 1809.31 2165.45 350.72 o 12 8 8 17052.68 18652.95 1499.95 o 14 8 8 2490.30 2822.47 313.88 o 16 8 8 20401.24 18334.24 1434.00 o 18 8 8 87.98 -10.81 312.46 o 20 8 8 15759.74 14896.16 695.76 o 22 8 8 495.67 389.63 188.64 o 24 8 8 19301.05 19356.88 830.37 o 2 10 8 18024.07 19585.04 815.02 o 4 10 8 1249.57 953.17 209.54 o 8 10 8 770.07 575.00 185.99 o 10 10 8 15458.05 15920.27 857.77 o 12 10 8 53.37 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23 3 9 29046.35 28027.29 931.44 o 25 3 9 19156.18 19709.07 763.19 o 27 3 9 6376.27 6433.94 995.92 o 29 3 9 10607.26 10583.37 1050.03 o 31 3 9 5752.89 6033.54 531.33 o 1 5 9 8872.31 9829.83 505.40 o 3 5 9 27657.87 28270.20 1071.85 o 5 5 9 35973.00 33137.95 1236.38 o 7 5 9 47427.48 49754.27 1360.47 o 9 5 9 39850.02 40440.71 3281.71 o 11 5 9 20250.54 20869.77 821.61 o 13 5 9 27453.41 28312.33 883.68 o 15 5 9 12626.73 13630.94 560.14 o 17 5 9 21023.10 21001.49 751.99 o 19 5 9 31366.10 29839.61 1474.73 o 21 5 9 12619.22 13150.06 597.15 o 23 5 9 4951.46 5588.46 439.96 o 25 5 9 8728.83 9343.50 567.28 o 27 5 9 6696.43 6871.74 753.89 o 29 5 9 14059.06 13892.77 729.57 o 1 7 9 28881.53 32464.35 1516.21 o 3 7 9 16212.17 16971.90 625.54 o 5 7 9 9100.62 10395.50 477.72 o 7 7 9 9027.00 8951.22 597.60 o 9 7 9 7547.09 8676.43 460.20 o 11 7 9 18049.53 17983.81 870.97 o 13 7 9 19398.01 19184.90 1032.02 o 15 7 9 8066.85 8160.09 487.50 o 17 7 9 7615.93 7999.34 496.87 o 19 7 9 5803.50 5767.39 549.08 o 21 7 9 9651.23 9167.86 557.86 o 23 7 9 11539.64 12306.42 943.90 o 25 7 9 9025.12 9808.62 612.41 o 1 9 9 5446.16 5281.00 416.42 o 3 9 9 10534.71 11014.40 1011.80 o 5 9 9 16390.14 17347.33 693.63 o 7 9 9 7307.94 7797.52 482.45 o 9 9 9 6416.22 6272.82 491.40 o 11 9 9 6236.33 6263.11 453.08 o 13 9 9 5434.43 5623.01 434.74 o 15 9 9 7476.88 7756.49 512.90 o 17 9 9 8176.89 8240.22 1033.41 o 10 0 10 115547.91 115918.54 3543.18 o 14 0 10 98329.84 99031.88 2321.22 o 18 0 10 62378.15 64216.54 1635.84 o 22 0 10 45374.07 46124.43 1300.79 o 26 0 10 25720.19 25961.67 898.41 o 30 0 10 36862.79 37765.68 1225.42 o 2 2 10 4217.49 4287.29 261.70 o 4 2 10 109388.66 113363.34 3399.12 o 6 2 10 1096.34 1173.42 189.57 o 8 2 10 63640.05 64052.55 2073.23 o 10 2 10 30.78 204.51 134.75 o 12 2 10 79841.63 81120.80 1956.22 o 14 2 10 1699.04 1505.70 162.70 o 16 2 10 41838.17 41326.78 939.94 o 18 2 10 1699.91 1848.54 243.91 o 20 2 10 59638.80 60630.00 1314.43 o 22 2 10 110.26 131.95 116.11 o 24 2 10 38289.79 37905.23 2363.10 o 26 2 10 981.99 1079.86 232.30 o 28 2 10 25051.91 27110.78 1528.80 o 30 2 10 91.02 315.86 171.32 o 32 2 10 17217.56 18030.13 789.41 o 2 4 10 60311.79 65352.55 2085.16 o 4 4 10 3468.30 3633.81 308.98 o 6 4 10 96713.59 106811.52 3316.67 o 8 4 10 82.08 33.41 129.24 o 10 4 10 58482.98 63449.19 1610.91 o 12 4 10 874.80 995.84 172.48 o 14 4 10 51918.45 53653.39 1815.65 o 16 4 10 181.22 341.66 210.03 o 18 4 10 41404.57 40566.73 1193.78 o 20 4 10 404.42 550.26 174.57 o 22 4 10 40684.29 40085.16 1230.43 o 24 4 10 149.22 69.86 165.67 o 26 4 10 27795.72 28507.66 1676.25 o 28 4 10 798.23 822.77 289.59 o 30 4 10 21282.75 23751.22 1216.40 o 2 6 10 2802.21 3060.25 332.72 o 4 6 10 47580.79 56452.93 1953.29 o 6 6 10 209.59 340.11 136.70 o 8 6 10 34960.09 37372.95 1122.50 o 10 6 10 1933.97 1856.00 236.12 o 12 6 10 40622.32 43225.81 1470.90 o 14 6 10 1509.82 1485.85 223.93 o 16 6 10 37688.46 38577.97 1180.08 o 18 6 10 220.39 401.28 178.16 o 20 6 10 20311.82 20712.07 806.43 o 22 6 10 1204.31 1135.41 229.77 o 24 6 10 23605.94 23679.12 986.40 o 26 6 10 705.96 852.02 218.43 o 2 8 10 30826.70 37193.14 1766.52 o 4 8 10 1315.88 1541.61 240.23 o 6 8 10 26224.67 28266.85 945.20 o 8 8 10 524.88 551.07 189.89 o 10 8 10 17405.14 17740.68 973.19 o 12 8 10 82.81 43.19 135.68 o 14 8 10 19693.56 19541.70 805.32 o 16 8 10 13.41 140.57 164.12 o 18 8 10 21350.71 23072.51 2233.98 o 20 8 10 1180.92 1904.17 658.59 o 0 10 10 15767.00 15945.08 1040.06 o 2 10 10 544.30 1344.78 372.37 o 6 10 10 124.20 -2.20 286.76 o 8 10 10 19477.16 22778.79 884.54 o 7 1 11 17714.69 19528.27 765.06 o 9 1 11 32325.44 33004.60 1191.15 o 11 1 11 31889.99 26459.10 1031.41 o 13 1 11 19493.33 19769.53 655.46 o 15 1 11 28390.47 27271.25 686.17 o 17 1 11 21388.47 21374.28 594.19 o 19 1 11 8194.20 8427.18 367.18 o 21 1 11 13968.19 14048.95 537.84 o 23 1 11 12366.53 12695.55 464.93 o 25 1 11 13523.69 13861.08 502.05 o 27 1 11 10749.26 11851.56 611.22 o 29 1 11 10323.61 11503.86 626.32 o 31 1 11 5318.37 5652.57 499.40 o 7 3 11 38892.02 40237.36 1413.82 o 9 3 11 32993.60 26905.77 1050.58 o 11 3 11 8729.99 9196.07 425.39 o 13 3 11 12711.57 12859.93 651.78 o 15 3 11 22060.25 21397.64 588.49 o 17 3 11 23898.05 24531.34 822.29 o 19 3 11 25377.10 23814.64 1005.26 o 21 3 11 12528.23 12468.21 1464.78 o 23 3 11 9821.47 9760.30 887.67 o 25 3 11 11474.40 11933.24 619.83 o 27 3 11 8005.23 8145.12 758.86 o 29 3 11 9292.76 9798.35 606.11 o 7 5 11 6927.05 7374.98 466.69 o 9 5 11 15959.08 17754.50 655.45 o 11 5 11 26018.44 28518.24 908.83 o 13 5 11 23061.40 24515.37 828.42 o 15 5 11 9788.06 11203.58 531.37 o 17 5 11 7179.48 7667.10 466.59 o 19 5 11 7910.56 8277.86 505.43 o 21 5 11 10549.64 10346.18 578.57 o 23 5 11 13005.54 12834.41 626.57 o 25 5 11 10468.80 10844.57 625.00 o 27 5 11 8260.80 7856.52 868.77 o 3 7 11 15056.58 21052.30 1338.40 o 5 7 11 13574.37 19455.98 1216.76 o 7 7 11 14492.11 16065.85 1063.87 o 9 7 11 10897.31 12412.72 618.52 o 11 7 11 3538.26 4426.70 378.89 o 13 7 11 3899.85 4205.43 376.07 o 15 7 11 9190.49 10320.83 571.57 o 17 7 11 10486.41 11849.86 598.61 o 19 7 11 13013.37 13413.97 686.19 o 21 7 11 7377.27 7094.36 518.16 o 1 9 11 9529.62 14320.02 1248.32 o 3 9 11 5904.09 7412.79 822.83 o 5 9 11 5563.44 6766.75 790.33 o 7 9 11 5417.47 6557.68 764.52 o 9 9 11 5530.85 6672.27 771.90 o 11 9 11 12931.68 16678.06 1127.83 o 16 0 12 31109.75 30559.02 1383.94 o 20 0 12 33138.95 31570.01 1454.73 o 24 0 12 18405.85 19770.39 1115.16 o 28 0 12 23953.48 25351.73 1377.47 o 12 2 12 256.33 291.19 159.00 o 14 2 12 58540.05 58707.84 1536.33 o 16 2 12 453.52 565.79 133.19 o 18 2 12 35203.40 35158.23 870.45 o 20 2 12 202.47 109.54 129.28 o 22 2 12 30393.59 30867.98 1016.34 o 24 2 12 17.37 -70.73 153.84 o 26 2 12 25747.24 26149.03 1173.77 o 28 2 12 386.30 419.84 236.48 o 10 4 12 623.00 658.86 363.95 o 12 4 12 39469.06 42190.91 1678.98 o 14 4 12 1097.24 1206.84 204.57 o 16 4 12 43637.75 43992.87 1287.85 o 18 4 12 1333.81 1713.80 262.60 o 20 4 12 23832.72 22803.75 840.24 o 22 4 12 1143.90 1107.85 230.56 o 24 4 12 21767.70 21759.90 1011.07 o 26 4 12 454.19 602.11 208.77 o 6 6 12 31958.11 46276.38 2238.53 o 8 6 12 1075.30 2023.93 531.14 o 10 6 12 21725.33 25897.49 1448.22 o 12 6 12 123.56 424.08 291.53 o 14 6 12 20329.05 22852.25 1127.35 o 16 6 12 738.99 1072.99 213.44 o 18 6 12 18566.25 20356.49 811.08 o 20 6 12 347.85 525.70 184.61 o 22 6 12 17345.34 17429.43 759.16 o 0 8 12 26453.51 50971.06 2777.11 o 2 8 12 1038.28 3244.74 767.29 o 4 8 12 18152.75 26025.64 1633.26 o 6 8 12 0.24 -127.40 337.04 o 8 8 12 20182.37 25944.63 1535.21 o 10 8 12 807.19 1090.41 388.20 o 12 8 12 20665.68 24072.85 1433.85 o 14 8 12 197.83 88.49 279.06 o 15 1 13 21846.38 22038.49 808.19 o 17 1 13 17739.45 18723.18 563.49 o 19 1 13 7280.18 7703.36 370.29 o 21 1 13 14042.90 14629.49 510.38 o 23 1 13 9982.82 10250.91 457.26 o 25 1 13 8642.08 8747.82 1361.12 o 27 1 13 13559.38 15061.08 694.73 o 13 3 13 27134.98 30059.68 1541.50 o 15 3 13 17331.89 17104.84 1083.64 o 17 3 13 15155.25 15132.41 1014.15 o 19 3 13 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