#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/24/2202417.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202417_Fobs loop_ _publ_author_name 'Jones, Matthew D.' 'Almeida Paz, Filipe A.' 'Davies, John E.' 'Johnson, Brian F. G.' _publ_section_title ; (R)-(+)-2,2'-Diamino-1,1'-binaphthyl ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o910 _journal_page_last o912 _journal_volume 59 _journal_year 2003 _space_group_IT_number 96 _symmetry_space_group_name_Hall 'P 4nw 2abw' _symmetry_space_group_name_H-M 'P 43 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.0388 _cell_length_b 7.0388 _cell_length_c 30.0684 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file cf6256Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bj0322 in P4(3)2(1)2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 78.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+3/4' 'y+1/2, -x+1/2, z+1/4' '-x+1/2, y+1/2, -z+3/4' 'x+1/2, -y+1/2, -z+1/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 626.88 652.93 23.23 o 0 2 0 886.59 878.01 18.58 o 1 2 0 1230.69 1152.82 18.68 o 2 2 0 1024.92 991.81 23.66 o 1 3 0 144.71 147.75 2.53 o 2 3 0 190.14 197.46 3.87 o 3 3 0 761.00 705.25 19.16 o 0 4 0 18.83 24.79 0.85 o 1 4 0 13.54 15.77 0.65 o 2 4 0 415.93 432.14 8.79 o 3 4 0 100.64 106.32 2.12 o 4 4 0 0.05 0.14 0.93 o 1 5 0 1746.38 1750.97 29.82 o 2 5 0 149.88 129.72 3.45 o 3 5 0 22.19 24.46 1.41 o 4 5 0 13.12 14.02 1.12 o 5 5 0 17.61 18.07 1.75 o 0 6 0 76.20 84.02 3.04 o 1 6 0 236.11 233.16 6.32 o 2 6 0 54.76 57.41 1.94 o 3 6 0 384.24 391.27 10.68 o 4 6 0 1.73 0.95 1.15 o 5 6 0 0.11 -1.43 2.86 o 6 6 0 136.64 144.59 10.39 o 1 7 0 21.00 22.67 1.64 o 2 7 0 10.35 11.25 1.33 o 3 7 0 9.60 5.11 1.69 o 4 7 0 1.96 1.09 1.83 o 5 7 0 46.64 44.07 3.15 o 0 8 0 7.95 10.37 3.71 o 1 8 0 23.84 18.96 1.54 o 2 8 0 0.02 1.17 1.55 o 3 8 0 122.43 119.69 8.16 o 4 8 0 11.44 5.58 2.64 o 1 9 0 178.03 190.19 11.65 o 1 1 1 151.82 132.23 3.27 o 0 2 1 3431.40 3394.61 54.90 o 1 2 1 994.44 946.79 11.89 o 2 2 1 138.20 129.55 2.85 o 0 3 1 5.35 4.29 0.28 o 1 3 1 832.19 847.72 9.88 o 2 3 1 468.41 509.45 6.85 o 3 3 1 3.01 4.86 0.59 o 0 4 1 32.32 32.96 1.00 o 1 4 1 414.92 451.05 5.17 o 2 4 1 426.19 436.33 5.45 o 3 4 1 45.49 47.77 0.86 o 4 4 1 8.62 11.33 0.75 o 0 5 1 62.36 53.18 1.41 o 1 5 1 18.85 20.22 0.72 o 2 5 1 21.58 15.44 0.83 o 3 5 1 739.40 749.71 10.27 o 4 5 1 50.84 50.60 1.20 o 5 5 1 19.58 16.73 1.39 o 0 6 1 1.20 -0.15 0.86 o 1 6 1 100.86 100.61 1.96 o 2 6 1 311.00 293.51 4.54 o 3 6 1 67.01 66.49 1.81 o 4 6 1 9.47 9.86 0.96 o 5 6 1 23.54 24.47 1.53 o 6 6 1 5.70 7.67 2.45 o 0 7 1 21.06 17.45 1.28 o 1 7 1 0.05 0.86 0.80 o 2 7 1 0.74 2.29 0.99 o 3 7 1 66.43 63.96 2.09 o 4 7 1 54.64 55.67 2.05 o 5 7 1 8.70 10.58 1.61 o 0 8 1 1.10 2.41 1.47 o 1 8 1 10.50 11.40 1.21 o 2 8 1 43.49 49.96 2.07 o 3 8 1 23.42 21.05 2.23 o 4 8 1 0.14 0.91 1.63 o 0 9 1 60.76 62.20 3.40 o 1 9 1 14.06 16.19 1.69 o 1 1 2 4622.27 3939.24 130.76 o 0 2 2 6177.00 6014.77 128.89 o 1 2 2 372.63 379.54 5.02 o 2 2 2 2.57 1.01 0.34 o 0 3 2 77.62 72.58 1.38 o 1 3 2 446.85 450.15 5.17 o 2 3 2 27.18 35.78 0.68 o 3 3 2 29.64 27.96 1.05 o 0 4 2 0.30 -0.40 0.40 o 1 4 2 918.07 978.43 10.91 o 2 4 2 61.27 70.24 1.12 o 3 4 2 8.06 8.10 0.54 o 4 4 2 147.95 151.61 3.04 o 0 5 2 62.83 61.07 1.65 o 1 5 2 286.74 283.11 3.59 o 2 5 2 739.94 737.66 10.42 o 3 5 2 410.93 415.34 6.14 o 4 5 2 31.73 31.86 0.98 o 5 5 2 0.03 -0.83 1.05 o 0 6 2 66.14 65.41 1.99 o 1 6 2 324.74 328.01 4.68 o 2 6 2 14.45 14.56 0.92 o 3 6 2 25.99 23.68 1.17 o 4 6 2 28.63 30.18 1.32 o 5 6 2 3.11 4.80 1.04 o 6 6 2 108.40 120.06 7.96 o 0 7 2 6.90 9.65 1.20 o 1 7 2 26.56 25.15 1.18 o 2 7 2 40.43 38.56 1.49 o 3 7 2 30.39 28.44 1.57 o 4 7 2 20.98 19.96 1.57 o 5 7 2 33.86 35.87 2.49 o 0 8 2 18.71 19.28 2.06 o 1 8 2 8.55 4.44 1.18 o 2 8 2 19.60 18.85 1.35 o 3 8 2 38.22 39.08 2.11 o 4 8 2 22.67 20.11 2.10 o 0 9 2 27.82 26.70 2.29 o 1 9 2 5.62 5.62 1.80 o 0 1 3 2521.68 1162.86 59.90 o 0 2 3 369.54 363.73 5.79 o 1 2 3 2103.36 2102.15 27.51 o 2 2 3 640.57 701.56 13.17 o 0 3 3 142.92 158.01 2.57 o 1 3 3 13.03 11.28 0.34 o 2 3 3 601.13 663.95 9.15 o 3 3 3 0.10 -0.24 0.43 o 0 4 3 5.62 6.01 0.52 o 1 4 3 277.71 295.07 3.46 o 2 4 3 846.26 878.78 11.39 o 3 4 3 180.68 175.27 2.79 o 4 4 3 14.80 13.96 0.97 o 0 5 3 430.22 424.70 7.62 o 1 5 3 54.52 54.39 1.04 o 2 5 3 288.76 303.94 4.35 o 3 5 3 11.81 11.52 0.70 o 4 5 3 85.99 77.50 1.46 o 5 5 3 74.73 75.00 2.63 o 0 6 3 23.67 25.80 1.26 o 1 6 3 306.55 306.43 4.48 o 2 6 3 252.04 250.21 4.11 o 3 6 3 24.87 28.90 1.29 o 4 6 3 34.06 31.56 1.19 o 5 6 3 1.83 0.98 1.38 o 6 6 3 34.00 37.19 4.46 o 0 7 3 5.94 7.18 1.43 o 1 7 3 14.90 16.70 1.07 o 2 7 3 52.58 50.66 1.53 o 3 7 3 37.11 34.10 1.65 o 4 7 3 7.75 8.36 1.06 o 5 7 3 18.95 19.24 2.71 o 0 8 3 6.16 5.76 1.57 o 1 8 3 10.43 11.84 1.59 o 2 8 3 57.64 58.62 2.35 o 3 8 3 30.52 27.95 2.09 o 4 8 3 20.54 23.28 1.99 o 0 9 3 54.81 50.09 3.21 o 1 9 3 73.81 76.69 3.52 o 0 1 4 797.38 676.25 14.56 o 1 1 4 17.27 18.06 0.48 o 0 2 4 2754.72 2706.49 48.89 o 1 2 4 1074.38 1074.13 13.49 o 2 2 4 692.91 720.90 13.22 o 0 3 4 122.08 125.27 2.16 o 1 3 4 399.10 415.39 5.29 o 2 3 4 597.61 665.52 10.15 o 3 3 4 11.02 12.46 0.64 o 0 4 4 0.02 0.77 0.48 o 1 4 4 42.10 35.47 0.60 o 2 4 4 128.32 120.81 1.78 o 3 4 4 70.78 76.51 1.36 o 4 4 4 226.62 229.10 4.23 o 0 5 4 245.09 248.15 4.16 o 1 5 4 12.02 13.95 0.61 o 2 5 4 55.37 52.64 1.12 o 3 5 4 370.79 386.52 5.84 o 4 5 4 76.01 77.00 1.43 o 5 5 4 109.51 107.43 3.17 o 0 6 4 241.62 236.43 4.88 o 1 6 4 163.62 158.11 2.58 o 2 6 4 153.53 149.69 2.68 o 3 6 4 15.02 15.92 1.01 o 4 6 4 9.00 7.69 0.94 o 5 6 4 21.78 20.22 1.51 o 6 6 4 76.17 66.93 6.06 o 0 7 4 55.35 56.29 2.39 o 1 7 4 28.72 27.17 1.33 o 2 7 4 2.16 3.79 1.16 o 3 7 4 67.81 65.50 2.14 o 4 7 4 44.93 51.06 1.75 o 5 7 4 8.29 8.51 2.16 o 0 8 4 3.06 3.84 1.95 o 1 8 4 46.64 44.17 2.04 o 2 8 4 38.02 37.65 1.91 o 3 8 4 3.80 2.08 2.48 o 4 8 4 10.34 10.12 1.93 o 0 9 4 46.64 40.61 3.80 o 1 9 4 89.96 88.37 3.11 o 0 1 5 4108.63 2992.87 119.25 o 0 2 5 2528.07 2471.64 52.95 o 1 2 5 5155.63 5169.94 78.11 o 2 2 5 165.69 181.95 3.31 o 0 3 5 1135.11 1161.33 19.54 o 1 3 5 425.71 432.49 5.62 o 2 3 5 149.38 175.82 2.83 o 3 3 5 99.12 98.77 2.09 o 0 4 5 329.80 359.95 6.48 o 1 4 5 91.99 81.87 1.14 o 2 4 5 133.17 134.54 2.00 o 3 4 5 73.01 74.46 1.29 o 4 4 5 818.85 834.92 16.45 o 0 5 5 56.63 51.92 1.34 o 1 5 5 56.46 54.22 0.98 o 2 5 5 17.02 16.28 0.70 o 3 5 5 220.47 213.76 3.39 o 4 5 5 20.47 21.94 0.87 o 5 5 5 6.69 5.88 1.21 o 0 6 5 757.39 784.76 14.82 o 1 6 5 176.76 169.30 2.62 o 2 6 5 6.79 8.72 0.92 o 3 6 5 31.23 31.83 1.20 o 4 6 5 75.13 75.57 2.01 o 5 6 5 18.03 16.35 1.78 o 6 6 5 2.93 5.71 3.86 o 0 7 5 1023.51 1050.04 20.16 o 1 7 5 33.81 36.53 1.25 o 2 7 5 46.56 45.70 1.82 o 3 7 5 13.94 11.68 1.17 o 4 7 5 54.98 57.88 2.06 o 5 7 5 27.59 30.77 1.94 o 0 8 5 13.67 15.84 2.10 o 1 8 5 37.15 39.07 2.32 o 2 8 5 65.76 64.72 2.35 o 3 8 5 9.98 11.31 1.78 o 4 8 5 65.17 61.66 2.47 o 0 9 5 0.60 3.86 2.92 o 1 9 5 64.61 73.58 3.33 o 0 1 6 193.95 170.00 3.39 o 1 1 6 5.18 7.70 0.39 o 0 2 6 985.00 933.81 17.34 o 1 2 6 1519.01 1535.24 19.21 o 2 2 6 33.61 47.06 1.07 o 0 3 6 428.87 463.27 8.40 o 1 3 6 2451.45 2582.67 32.00 o 2 3 6 163.40 193.62 2.76 o 3 3 6 64.27 75.14 1.75 o 0 4 6 70.13 71.55 1.54 o 1 4 6 386.61 409.86 5.45 o 2 4 6 140.54 151.34 2.33 o 3 4 6 109.46 102.47 1.70 o 4 4 6 664.99 698.97 13.31 o 0 5 6 73.88 71.35 1.54 o 1 5 6 23.25 25.57 0.77 o 2 5 6 67.03 62.51 1.37 o 3 5 6 5.33 5.12 0.64 o 4 5 6 410.99 398.65 5.79 o 5 5 6 55.41 66.54 2.56 o 0 6 6 44.71 44.79 1.54 o 1 6 6 37.85 40.85 1.19 o 2 6 6 85.42 84.91 2.02 o 3 6 6 31.01 29.27 1.08 o 4 6 6 31.42 33.97 1.44 o 5 6 6 138.48 149.63 4.54 o 6 6 6 119.21 127.85 8.58 o 0 7 6 393.75 403.29 8.17 o 1 7 6 42.88 46.50 1.76 o 2 7 6 12.74 14.06 1.28 o 3 7 6 28.96 31.78 1.46 o 4 7 6 10.69 12.77 1.29 o 5 7 6 53.56 51.24 3.00 o 0 8 6 198.09 190.25 6.41 o 1 8 6 36.28 34.13 2.11 o 2 8 6 6.69 6.65 1.52 o 3 8 6 41.96 51.05 2.22 o 4 8 6 60.05 53.11 2.75 o 0 9 6 107.25 104.01 4.67 o 0 1 7 0.77 1.33 0.28 o 1 1 7 166.07 139.69 3.30 o 0 2 7 1590.26 1623.43 22.97 o 1 2 7 198.56 193.68 2.79 o 2 2 7 3195.70 3393.79 62.15 o 0 3 7 688.38 741.32 14.13 o 1 3 7 2057.15 2171.13 27.63 o 2 3 7 849.02 878.21 11.58 o 3 3 7 115.39 135.85 2.78 o 0 4 7 15.76 13.28 0.63 o 1 4 7 43.01 36.45 0.81 o 2 4 7 40.62 40.46 0.88 o 3 4 7 9.78 10.38 0.56 o 4 4 7 476.23 489.00 10.14 o 0 5 7 51.51 57.78 1.41 o 1 5 7 0.93 1.59 0.49 o 2 5 7 141.65 148.43 2.34 o 3 5 7 42.43 45.05 1.23 o 4 5 7 119.40 129.27 2.40 o 5 5 7 280.42 277.13 7.46 o 0 6 7 479.29 469.58 8.57 o 1 6 7 99.28 99.57 1.89 o 2 6 7 1.74 1.24 0.84 o 3 6 7 10.70 9.45 0.97 o 4 6 7 142.30 139.81 2.83 o 5 6 7 42.97 38.26 1.79 o 6 6 7 79.01 73.31 6.63 o 0 7 7 1.82 2.08 1.01 o 1 7 7 388.27 402.25 7.98 o 2 7 7 105.78 100.69 2.77 o 3 7 7 15.33 21.19 1.30 o 4 7 7 35.31 33.39 1.63 o 5 7 7 1.90 1.40 1.49 o 0 8 7 6.44 9.28 2.23 o 1 8 7 41.83 38.94 1.90 o 2 8 7 26.55 26.37 2.19 o 3 8 7 0.48 -1.59 1.59 o 4 8 7 14.15 20.06 2.23 o 0 1 8 173.81 147.68 3.37 o 1 1 8 465.72 463.80 8.22 o 0 2 8 16.14 11.57 0.43 o 1 2 8 130.00 133.11 1.83 o 2 2 8 953.29 1010.29 17.82 o 0 3 8 100.61 98.39 2.00 o 1 3 8 991.21 1121.84 13.84 o 2 3 8 862.75 904.68 12.01 o 3 3 8 28.16 27.36 0.92 o 0 4 8 9.15 8.08 0.60 o 1 4 8 672.19 691.17 10.19 o 2 4 8 309.08 313.20 4.61 o 3 4 8 2.32 2.02 0.45 o 4 4 8 90.87 78.92 2.20 o 0 5 8 93.85 96.72 2.10 o 1 5 8 5.12 6.53 0.52 o 2 5 8 29.01 30.80 0.91 o 3 5 8 83.88 83.87 1.71 o 4 5 8 126.63 113.20 2.26 o 5 5 8 516.88 529.02 11.98 o 0 6 8 659.74 662.34 12.28 o 1 6 8 37.38 40.77 1.11 o 2 6 8 61.47 58.17 1.65 o 3 6 8 2.33 1.45 0.79 o 4 6 8 156.65 153.96 3.39 o 5 6 8 136.99 143.04 3.86 o 6 6 8 188.81 184.91 11.00 o 0 7 8 38.46 40.60 2.08 o 1 7 8 269.37 269.60 4.66 o 2 7 8 38.03 42.80 1.94 o 3 7 8 42.97 47.60 1.69 o 4 7 8 13.39 12.39 1.52 o 5 7 8 15.95 17.03 1.84 o 0 8 8 225.93 244.93 14.22 o 1 8 8 72.99 66.36 2.68 o 2 8 8 54.40 55.68 2.76 o 3 8 8 59.86 69.00 2.95 o 4 8 8 3.70 5.02 3.11 o 0 1 9 58.86 50.78 1.54 o 1 1 9 78.04 72.75 1.39 o 0 2 9 14.56 11.59 0.38 o 1 2 9 1862.46 1947.32 22.49 o 2 2 9 8.18 13.10 0.76 o 0 3 9 29.33 38.21 0.94 o 1 3 9 158.85 143.69 1.82 o 2 3 9 721.57 741.48 9.74 o 3 3 9 6.65 4.83 0.63 o 0 4 9 228.97 229.65 4.30 o 1 4 9 135.66 138.80 2.24 o 2 4 9 474.77 506.69 7.80 o 3 4 9 24.00 26.89 0.89 o 4 4 9 0.21 0.40 0.92 o 0 5 9 9.17 11.34 0.81 o 1 5 9 16.90 19.64 0.68 o 2 5 9 45.54 46.21 1.04 o 3 5 9 75.82 75.40 1.71 o 4 5 9 41.42 45.34 1.35 o 5 5 9 504.45 545.36 16.04 o 0 6 9 164.94 145.55 3.16 o 1 6 9 112.42 107.85 2.01 o 2 6 9 23.62 25.34 1.04 o 3 6 9 38.30 36.90 1.43 o 4 6 9 277.99 268.18 5.91 o 5 6 9 23.08 27.98 1.67 o 6 6 9 144.83 121.64 9.40 o 0 7 9 260.09 294.05 6.94 o 1 7 9 348.39 333.46 5.72 o 2 7 9 145.78 146.54 3.68 o 3 7 9 5.71 6.50 1.52 o 4 7 9 15.33 14.02 1.45 o 5 7 9 4.17 4.43 1.45 o 0 8 9 65.89 64.01 3.58 o 1 8 9 7.31 9.38 1.60 o 2 8 9 20.93 25.21 1.84 o 3 8 9 2.58 3.96 1.49 o 0 1 10 0.98 2.53 0.38 o 1 1 10 1.44 2.10 0.32 o 0 2 10 933.72 899.03 15.33 o 1 2 10 332.56 335.05 3.98 o 2 2 10 2600.64 2757.30 54.43 o 0 3 10 1336.08 1331.50 24.33 o 1 3 10 329.76 365.59 4.10 o 2 3 10 57.13 43.52 0.80 o 3 3 10 8.76 11.87 0.68 o 0 4 10 137.13 163.25 2.99 o 1 4 10 431.96 432.25 6.03 o 2 4 10 181.59 188.77 3.43 o 3 4 10 82.98 81.00 1.64 o 4 4 10 87.07 71.94 2.85 o 0 5 10 78.88 75.93 1.67 o 1 5 10 13.89 14.61 0.64 o 2 5 10 199.23 201.03 3.27 o 3 5 10 58.36 62.76 1.61 o 4 5 10 384.15 365.16 8.49 o 5 5 10 43.62 40.95 3.02 o 0 6 10 152.81 181.93 3.99 o 1 6 10 95.23 95.79 1.88 o 2 6 10 42.89 41.97 1.20 o 3 6 10 119.47 122.36 2.46 o 4 6 10 10.09 12.39 1.38 o 5 6 10 6.78 7.61 1.34 o 6 6 10 9.48 4.94 3.10 o 0 7 10 49.13 33.53 2.40 o 1 7 10 369.05 379.98 6.98 o 2 7 10 35.64 40.09 2.17 o 3 7 10 46.84 48.04 2.42 o 4 7 10 18.07 18.68 1.66 o 5 7 10 9.00 8.62 1.88 o 0 8 10 69.43 76.15 4.43 o 1 8 10 45.99 44.62 2.05 o 2 8 10 32.61 31.74 1.79 o 3 8 10 62.28 71.85 2.62 o 0 1 11 0.05 1.17 0.47 o 1 1 11 383.57 419.90 7.85 o 0 2 11 495.81 512.35 9.19 o 1 2 11 311.81 337.58 4.55 o 2 2 11 882.75 971.28 27.68 o 0 3 11 820.00 958.43 21.63 o 1 3 11 207.43 232.94 3.04 o 2 3 11 49.00 50.65 0.94 o 3 3 11 223.03 228.42 4.39 o 0 4 11 425.77 471.17 7.93 o 1 4 11 255.18 266.23 3.75 o 2 4 11 225.63 233.72 3.83 o 3 4 11 79.60 78.15 1.75 o 4 4 11 433.32 383.54 11.09 o 0 5 11 104.24 104.41 2.28 o 1 5 11 37.31 32.76 0.92 o 2 5 11 136.59 143.14 2.57 o 3 5 11 337.21 343.99 6.35 o 4 5 11 72.77 91.19 2.79 o 5 5 11 197.89 206.82 9.06 o 0 6 11 493.04 470.00 9.07 o 1 6 11 144.39 136.35 2.41 o 2 6 11 10.33 11.73 0.87 o 3 6 11 124.48 121.63 2.49 o 4 6 11 126.26 123.95 3.28 o 5 6 11 50.44 54.16 2.63 o 6 6 11 0.02 -3.93 3.93 o 0 7 11 582.80 579.41 16.06 o 1 7 11 35.65 37.82 1.68 o 2 7 11 60.82 58.76 2.12 o 3 7 11 192.09 202.78 4.66 o 4 7 11 21.78 26.57 3.04 o 5 7 11 0.19 1.49 1.68 o 0 8 11 6.78 5.24 4.14 o 1 8 11 41.65 43.45 2.00 o 2 8 11 17.28 17.32 1.78 o 3 8 11 77.68 72.53 2.39 o 0 1 12 219.19 205.39 6.27 o 1 1 12 148.61 148.66 3.03 o 0 2 12 246.75 246.41 5.82 o 1 2 12 227.50 230.82 2.97 o 2 2 12 216.05 245.17 5.29 o 0 3 12 327.69 370.90 8.28 o 1 3 12 31.02 31.43 0.66 o 2 3 12 907.40 939.07 12.80 o 3 3 12 144.23 154.60 3.28 o 0 4 12 24.71 23.20 1.02 o 1 4 12 299.20 310.21 4.10 o 2 4 12 665.88 681.35 10.68 o 3 4 12 184.94 194.24 3.36 o 4 4 12 44.88 57.80 2.58 o 0 5 12 256.37 259.38 5.28 o 1 5 12 77.94 81.59 1.74 o 2 5 12 73.76 75.34 1.61 o 3 5 12 245.42 237.36 4.19 o 4 5 12 49.03 43.36 1.69 o 5 5 12 226.59 210.23 7.12 o 0 6 12 151.97 155.51 3.74 o 1 6 12 59.18 56.12 1.39 o 2 6 12 25.32 23.82 1.06 o 3 6 12 78.27 83.59 2.14 o 4 6 12 23.01 20.88 1.60 o 5 6 12 15.68 16.57 1.65 o 6 6 12 57.87 51.04 5.61 o 0 7 12 9.30 3.15 2.26 o 1 7 12 22.41 18.51 1.13 o 2 7 12 12.83 12.86 1.13 o 3 7 12 58.70 58.33 2.04 o 4 7 12 53.87 48.32 3.55 o 5 7 12 24.60 30.10 2.14 o 0 8 12 0.22 -0.51 2.96 o 1 8 12 31.14 27.86 1.77 o 2 8 12 22.06 17.66 1.79 o 3 8 12 172.90 180.61 4.96 o 0 1 13 351.32 347.27 7.71 o 1 1 13 380.31 431.63 7.63 o 0 2 13 6.35 4.36 0.51 o 1 2 13 33.83 42.42 0.89 o 2 2 13 73.86 83.17 2.14 o 0 3 13 289.00 311.79 6.61 o 1 3 13 194.65 205.96 2.75 o 2 3 13 146.49 156.87 2.50 o 3 3 13 2.25 4.16 0.67 o 0 4 13 65.83 65.10 2.05 o 1 4 13 127.80 130.53 1.91 o 2 4 13 76.11 84.50 1.85 o 3 4 13 181.92 185.24 3.30 o 4 4 13 19.24 23.37 1.60 o 0 5 13 488.50 456.61 9.26 o 1 5 13 145.44 145.89 2.60 o 2 5 13 267.18 255.21 4.03 o 3 5 13 205.86 220.94 4.06 o 4 5 13 246.51 231.69 4.96 o 5 5 13 66.90 62.39 4.61 o 0 6 13 189.35 182.39 4.95 o 1 6 13 135.98 121.10 2.23 o 2 6 13 87.24 80.86 1.94 o 3 6 13 177.22 172.86 3.38 o 4 6 13 40.02 40.09 2.30 o 5 6 13 10.53 9.73 1.63 o 6 6 13 5.11 3.34 4.10 o 0 7 13 18.91 21.48 2.13 o 1 7 13 41.83 36.60 1.64 o 2 7 13 20.50 22.98 1.37 o 3 7 13 10.98 7.72 1.42 o 4 7 13 38.15 40.73 2.49 o 5 7 13 27.08 27.02 2.27 o 0 8 13 32.21 40.14 5.41 o 1 8 13 11.61 11.90 1.86 o 2 8 13 39.54 37.99 2.52 o 3 8 13 112.46 108.31 3.74 o 0 1 14 911.57 988.27 18.94 o 1 1 14 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19 83.50 78.81 3.33 o 4 6 19 34.93 38.17 4.80 o 5 6 19 5.94 7.03 2.00 o 0 7 19 78.52 64.18 3.90 o 1 7 19 4.62 3.06 1.52 o 2 7 19 52.62 61.44 3.10 o 3 7 19 13.87 15.53 2.30 o 0 1 20 37.40 44.85 1.36 o 1 1 20 42.95 43.11 1.62 o 0 2 20 166.15 177.77 4.45 o 1 2 20 50.83 47.43 1.44 o 2 2 20 302.15 292.73 7.40 o 0 3 20 292.62 271.79 5.93 o 1 3 20 33.30 31.61 1.27 o 2 3 20 1118.86 1112.15 28.89 o 3 3 20 3.21 1.78 1.18 o 0 4 20 48.38 46.06 3.37 o 1 4 20 169.34 158.07 3.84 o 2 4 20 206.39 195.31 4.78 o 3 4 20 17.38 16.94 1.12 o 4 4 20 269.20 266.13 7.67 o 0 5 20 53.51 57.59 2.76 o 1 5 20 44.23 40.81 2.34 o 2 5 20 32.82 27.70 1.48 o 3 5 20 21.45 21.57 2.52 o 4 5 20 0.21 0.68 1.54 o 5 5 20 15.49 16.05 3.03 o 0 6 20 13.80 16.61 2.25 o 1 6 20 91.30 92.40 2.79 o 2 6 20 7.76 11.17 1.31 o 3 6 20 67.08 58.50 2.63 o 4 6 20 10.16 8.67 3.03 o 5 6 20 12.15 12.28 2.34 o 0 7 20 2.04 5.98 3.11 o 1 7 20 1.92 -0.33 1.51 o 2 7 20 24.06 23.20 2.64 o 3 7 20 35.50 23.98 2.89 o 0 1 21 343.43 349.31 6.35 o 1 1 21 1217.86 1234.50 30.29 o 0 2 21 102.87 97.59 2.47 o 1 2 21 380.24 382.24 7.05 o 2 2 21 412.82 400.83 10.79 o 0 3 21 877.72 858.22 17.85 o 1 3 21 135.59 128.61 2.56 o 2 3 21 126.90 127.86 4.07 o 3 3 21 2.40 0.75 1.26 o 0 4 21 509.48 505.05 14.67 o 1 4 21 54.36 53.50 1.78 o 2 4 21 108.20 96.91 2.65 o 3 4 21 63.58 59.79 2.36 o 4 4 21 3.30 -0.84 2.35 o 0 5 21 11.56 8.69 1.57 o 1 5 21 27.10 20.78 1.86 o 2 5 21 40.34 32.08 1.68 o 3 5 21 55.00 51.40 2.90 o 4 5 21 49.62 45.44 2.42 o 0 6 21 12.40 11.62 2.21 o 1 6 21 14.00 14.51 1.72 o 2 6 21 14.50 15.05 1.35 o 3 6 21 14.34 18.62 2.03 o 4 6 21 8.92 8.94 2.28 o 0 7 21 12.29 12.54 3.01 o 1 7 21 7.45 12.90 1.73 o 2 7 21 5.29 7.46 1.65 o 3 7 21 98.78 104.60 5.56 o 0 1 22 19.12 15.59 1.78 o 0 2 22 301.16 280.15 7.16 o 1 2 22 22.15 22.26 1.11 o 2 2 22 709.06 681.64 17.62 o 0 3 22 640.59 652.51 16.95 o 1 3 22 861.96 833.74 12.91 o 2 3 22 60.19 68.19 2.80 o 0 4 22 33.32 33.66 2.16 o 1 4 22 14.07 11.94 1.17 o 2 4 22 16.68 14.02 1.34 o 3 4 22 1.89 0.72 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36.67 2.54 o 1 7 23 52.09 57.58 2.73 o 2 7 23 6.83 9.60 2.17 o 0 1 24 52.88 49.05 1.23 o 1 1 24 1.84 0.23 0.73 o 0 2 24 39.91 36.23 1.84 o 1 2 24 36.62 36.10 1.12 o 2 2 24 60.82 62.08 3.59 o 0 3 24 51.51 47.40 2.42 o 1 3 24 314.96 334.31 7.55 o 2 3 24 692.85 685.70 15.03 o 0 4 24 57.65 63.53 3.47 o 1 4 24 51.32 51.02 1.75 o 2 4 24 14.40 13.66 1.40 o 3 4 24 0.91 -1.36 2.29 o 4 4 24 15.75 13.60 2.79 o 0 5 24 88.16 96.74 3.12 o 1 5 24 12.03 9.93 1.64 o 2 5 24 2.51 2.42 1.79 o 3 5 24 7.84 7.78 3.88 o 4 5 24 20.15 21.12 2.62 o 5 5 24 1.82 6.96 3.69 o 0 6 24 17.33 16.93 3.01 o 1 6 24 43.61 50.80 2.60 o 2 6 24 8.93 8.27 2.39 o 3 6 24 0.17 1.55 3.03 o 4 6 24 80.31 94.07 7.47 o 0 7 24 73.32 84.00 4.85 o 1 7 24 30.00 32.04 2.30 o 0 1 25 74.48 77.27 1.86 o 1 1 25 0.06 0.84 1.26 o 0 2 25 338.11 336.76 8.96 o 1 2 25 145.53 159.91 3.04 o 2 2 25 318.52 318.18 9.00 o 0 3 25 507.26 482.97 18.80 o 1 3 25 343.58 319.24 6.04 o 2 3 25 90.15 86.29 2.56 o 0 4 25 66.42 65.57 3.63 o 1 4 25 0.70 2.47 1.10 o 2 4 25 65.90 69.38 2.65 o 3 4 25 17.53 16.53 2.46 o 0 5 25 3.47 5.28 1.60 o 1 5 25 2.81 -0.69 1.25 o 2 5 25 22.56 23.11 2.73 o 3 5 25 23.34 23.00 3.04 o 4 5 25 91.62 82.99 6.74 o 0 6 25 65.01 68.06 5.80 o 1 6 25 12.09 9.19 1.85 o 2 6 25 15.68 15.80 1.91 o 3 6 25 6.13 6.09 2.99 o 0 7 25 41.57 57.69 4.29 o 0 1 26 3.25 3.12 0.98 o 1 1 26 3.27 1.92 1.13 o 0 2 26 471.11 468.78 10.47 o 1 2 26 175.54 175.12 3.60 o 2 2 26 427.35 459.40 12.90 o 0 3 26 598.06 603.99 22.97 o 1 3 26 430.74 424.64 7.39 o 2 3 26 2.54 1.47 1.31 o 3 3 26 9.63 10.87 2.29 o 0 4 26 72.99 74.98 4.72 o 1 4 26 16.50 13.60 1.11 o 2 4 26 2.14 -0.34 1.37 o 3 4 26 3.09 6.18 1.91 o 0 5 26 9.10 8.20 1.56 o 1 5 26 1.62 1.14 1.31 o 2 5 26 33.81 34.75 2.86 o 3 5 26 6.07 6.56 3.04 o 0 6 26 155.32 186.10 8.51 o 1 6 26 7.66 6.79 2.15 o 2 6 26 12.00 6.95 1.78 o 3 6 26 9.67 14.40 3.60 o 0 1 27 180.94 166.24 3.36 o 1 1 27 326.12 317.64 8.70 o 0 2 27 6.30 4.10 1.33 o 1 2 27 189.43 176.15 3.63 o 0 3 27 468.01 515.19 18.76 o 1 3 27 147.44 154.26 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