#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/24/2202446.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202446_Fobs loop_ _publ_author_name 'Jones, Matthew D.' 'Almeida Paz, Filipe A.' 'Davies, John E.' 'Johnson, Brian F. G.' 'Klinowski, Jacek' _publ_section_title ; trans-Bis[(S)-({-})-2-aminomethyl-1-ethylpyrrolidine-\k^2^N]palladium(II) dichloride methanol trisolvate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1031 _journal_page_last m1034 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.3092 _cell_length_b 12.9075 _cell_length_c 26.3277 _exptl_crystal_F_000 1112.00 _reflns_d_resolution_high 0.7708 _[local]_cod_data_source_file cf6288Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bj0318 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 211.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5244.80 5339.83 120.58 o 4 0 0 381.55 377.62 61.60 o 6 0 0 1.06 42.81 48.53 o 8 0 0 276.18 465.04 115.18 o 2 1 0 37393.78 37104.39 556.43 o 3 1 0 3693.66 4028.61 65.84 o 4 1 0 8688.61 8671.75 166.35 o 5 1 0 3.46 18.96 17.94 o 6 1 0 10649.16 10540.84 294.38 o 7 1 0 1240.40 1202.01 88.71 o 8 1 0 1686.48 1717.27 159.22 o 9 1 0 317.90 353.48 78.46 o 1 2 0 2312.95 1692.03 151.56 o 2 2 0 9003.72 9319.73 131.92 o 3 2 0 8440.24 8947.33 132.79 o 4 2 0 3858.63 3831.72 70.71 o 5 2 0 1604.41 1497.63 45.27 o 6 2 0 602.28 558.31 32.95 o 7 2 0 457.47 387.07 53.02 o 8 2 0 995.17 938.71 103.48 o 9 2 0 1162.43 1016.63 150.91 o 1 3 0 637.16 624.23 21.84 o 2 3 0 2496.30 2549.42 42.15 o 3 3 0 654.97 703.95 21.11 o 4 3 0 104.75 116.60 13.19 o 5 3 0 7675.93 7789.97 156.43 o 6 3 0 15.17 -6.18 24.71 o 7 3 0 3588.38 3631.88 167.35 o 8 3 0 2309.97 2329.99 129.14 o 9 3 0 719.79 735.45 147.21 o 0 4 0 1425.77 1238.06 45.64 o 1 4 0 41651.99 40189.27 812.79 o 2 4 0 1025.16 910.98 24.75 o 3 4 0 3055.78 3022.49 51.45 o 4 4 0 455.12 420.61 15.81 o 5 4 0 585.12 561.33 19.88 o 6 4 0 128.75 111.62 16.49 o 7 4 0 63.12 51.11 35.02 o 8 4 0 63.86 39.73 79.77 o 9 4 0 650.66 596.55 135.20 o 1 5 0 1010.89 864.77 26.20 o 2 5 0 4650.14 4187.70 77.01 o 3 5 0 11031.95 11026.92 192.47 o 4 5 0 498.50 561.32 22.08 o 5 5 0 9773.03 10138.24 231.05 o 6 5 0 608.11 606.68 33.53 o 7 5 0 2866.16 2960.28 164.46 o 8 5 0 523.61 419.67 55.41 o 9 5 0 530.14 617.49 115.49 o 0 6 0 22035.29 22988.44 666.79 o 1 6 0 11321.61 11285.12 233.09 o 2 6 0 5065.97 4944.15 95.14 o 3 6 0 10995.00 12222.47 242.41 o 4 6 0 6912.91 7043.75 146.24 o 5 6 0 56.15 30.67 13.22 o 6 6 0 0.07 -22.01 22.01 o 7 6 0 993.27 913.58 77.39 o 8 6 0 268.70 297.33 67.77 o 1 7 0 1846.04 1914.64 52.64 o 2 7 0 895.92 862.97 30.25 o 3 7 0 1191.25 1143.42 54.47 o 4 7 0 5925.90 5916.57 139.39 o 5 7 0 1255.13 1241.74 42.58 o 6 7 0 6428.47 6942.80 245.99 o 7 7 0 236.08 281.80 67.45 o 8 7 0 2897.62 2896.74 196.98 o 0 8 0 4902.27 4666.13 151.74 o 1 8 0 119.56 140.27 23.69 o 2 8 0 8268.14 8603.05 191.74 o 3 8 0 137.40 101.66 21.94 o 4 8 0 1462.84 1483.23 66.13 o 5 8 0 81.68 58.47 20.35 o 6 8 0 961.28 983.56 74.22 o 7 8 0 119.24 202.65 71.45 o 8 8 0 469.98 492.31 117.18 o 1 9 0 2205.28 2193.28 68.69 o 2 9 0 1854.48 1997.12 59.10 o 3 9 0 1556.90 1479.08 65.06 o 4 9 0 1582.57 1545.88 51.57 o 5 9 0 97.36 91.08 23.16 o 6 9 0 1601.80 1660.49 97.33 o 7 9 0 13.38 79.46 91.47 o 0 10 0 10407.48 10076.17 420.40 o 1 10 0 9014.58 8762.13 256.14 o 2 10 0 1280.50 1386.53 60.79 o 3 10 0 829.20 832.28 51.00 o 4 10 0 895.80 929.63 59.32 o 5 10 0 7.28 17.47 34.19 o 6 10 0 284.21 267.01 79.00 o 7 10 0 1.57 63.75 71.76 o 1 11 0 408.54 372.25 44.80 o 2 11 0 1531.36 1367.23 124.23 o 3 11 0 3078.62 2780.95 128.18 o 4 11 0 1034.83 1055.87 64.25 o 5 11 0 4551.01 4692.92 174.13 o 6 11 0 318.14 368.20 62.96 o 7 11 0 2368.60 2501.07 255.31 o 0 12 0 394.37 593.47 89.93 o 1 12 0 4871.52 4901.25 220.15 o 2 12 0 207.62 208.90 39.30 o 3 12 0 5175.56 4924.49 258.36 o 4 12 0 611.76 563.89 54.94 o 5 12 0 371.72 453.97 49.04 o 6 12 0 0.40 52.33 73.38 o 1 13 0 194.83 101.71 45.21 o 2 13 0 492.23 495.44 63.37 o 3 13 0 1079.13 954.59 84.78 o 4 13 0 312.86 239.93 82.08 o 5 13 0 1417.64 1621.78 110.74 o 0 14 0 4747.36 5029.86 298.43 o 1 14 0 981.16 902.54 95.24 o 2 14 0 1817.20 1554.27 109.18 o 3 14 0 1163.37 826.78 105.06 o 4 14 0 36.16 149.32 114.26 o 5 14 0 205.91 177.66 82.53 o 1 15 0 76.05 133.65 63.79 o 2 15 0 422.99 315.33 87.69 o 3 15 0 39.27 -16.40 114.11 o 4 15 0 1509.39 1365.39 153.95 o 0 16 0 1693.26 1902.68 191.56 o 1 16 0 79.01 60.65 73.40 o 2 16 0 1223.38 1292.63 125.20 o 2 0 1 28908.39 27915.99 510.74 o 3 0 1 25556.24 25709.19 511.55 o 4 0 1 13712.42 13865.28 236.91 o 5 0 1 225.29 224.13 24.45 o 6 0 1 3133.62 3077.85 95.31 o 7 0 1 482.12 514.99 83.46 o 8 0 1 608.56 622.14 115.03 o 9 0 1 500.16 445.26 75.63 o -9 1 1 1917.13 1863.25 214.66 o -7 1 1 2164.25 1957.57 94.12 o -6 1 1 514.36 522.04 39.49 o -5 1 1 6320.31 6436.16 139.05 o -4 1 1 4174.32 4251.30 85.94 o -3 1 1 13127.68 13024.98 198.22 o -2 1 1 29822.33 29109.15 419.38 o 2 1 1 30169.98 29090.92 499.19 o 3 1 1 12945.09 12675.74 197.17 o 4 1 1 4077.12 4114.33 89.59 o 5 1 1 6350.84 6633.91 157.11 o 6 1 1 486.72 450.18 43.87 o 7 1 1 2150.71 1875.61 99.82 o 8 1 1 164.90 163.62 59.75 o 9 1 1 1949.88 1745.00 145.30 o -9 2 1 719.33 643.98 135.20 o -8 2 1 830.24 991.07 119.49 o -7 2 1 1602.46 1714.65 84.39 o -6 2 1 2024.75 1969.94 72.17 o -5 2 1 2144.79 1970.33 55.09 o -4 2 1 1548.09 1436.19 32.67 o -3 2 1 2918.73 2957.65 44.04 o -2 2 1 3151.17 3009.87 45.84 o -1 2 1 6892.36 6321.80 301.24 o 1 2 1 6803.08 6536.36 188.78 o 2 2 1 3282.73 3198.02 51.72 o 3 2 1 2955.19 3005.80 53.38 o 4 2 1 1472.32 1339.54 27.60 o 5 2 1 2220.32 2016.81 61.83 o 6 2 1 1966.01 1981.58 76.86 o 7 2 1 1508.88 1429.36 95.59 o 8 2 1 829.45 767.48 91.47 o 9 2 1 718.79 810.28 139.21 o -9 3 1 225.26 107.48 95.47 o -8 3 1 1018.58 1003.08 123.50 o -7 3 1 119.69 221.88 42.59 o -6 3 1 2227.47 2251.00 74.51 o -5 3 1 2933.39 3149.73 71.47 o -4 3 1 2954.57 2903.66 45.76 o -3 3 1 3081.06 2928.31 848.93 o -2 3 1 12259.14 11993.41 197.78 o -1 3 1 2503.28 2384.84 54.22 o 0 3 1 5.89 29.10 17.60 o 1 3 1 2333.84 2252.93 42.69 o 2 3 1 12106.65 11943.88 208.96 o 3 3 1 3086.20 2991.18 49.12 o 4 3 1 3162.62 3207.42 53.92 o 5 3 1 2835.53 2931.40 56.30 o 6 3 1 2394.53 2472.88 75.00 o 7 3 1 127.25 79.46 51.74 o 8 3 1 999.00 1119.55 93.78 o -9 4 1 403.26 135.51 87.77 o -8 4 1 1042.50 824.76 103.79 o -7 4 1 2106.02 2139.72 88.18 o -6 4 1 21.37 27.52 17.31 o -5 4 1 2332.77 2175.56 56.98 o -4 4 1 5010.37 4841.75 82.73 o -3 4 1 1477.15 1245.36 28.37 o -2 4 1 8458.38 8403.72 157.67 o -1 4 1 650.85 644.00 21.41 o 0 4 1 19065.32 18371.57 341.10 o 1 4 1 690.30 665.57 22.97 o 2 4 1 8874.76 8811.48 158.74 o 3 4 1 1446.69 1277.58 48.31 o 4 4 1 5001.43 4835.85 101.20 o 5 4 1 2385.48 2316.63 57.02 o 6 4 1 20.27 28.37 15.52 o 7 4 1 2160.61 2083.29 106.82 o 9 4 1 396.36 388.03 76.37 o -9 5 1 145.61 167.54 123.50 o -8 5 1 1285.02 1409.78 83.29 o -7 5 1 1072.62 1126.25 61.05 o -6 5 1 5445.61 5371.09 158.78 o -5 5 1 2253.74 2299.13 47.82 o -4 5 1 3867.54 3713.06 73.85 o -3 5 1 4195.65 4010.50 74.06 o -2 5 1 3452.52 3488.56 70.36 o -1 5 1 24180.20 24332.50 488.59 o 0 5 1 3863.46 4096.89 85.16 o 1 5 1 24415.03 24425.78 505.10 o 2 5 1 3364.15 3408.06 64.47 o 3 5 1 4263.49 4044.00 74.80 o 4 5 1 3817.54 3818.46 78.70 o 5 5 1 2222.76 2230.65 67.23 o 6 5 1 5358.80 5377.95 131.63 o 7 5 1 1081.81 1011.73 66.06 o 8 5 1 1292.23 1277.02 85.18 o 9 5 1 147.12 119.49 127.50 o -8 6 1 1420.65 1538.21 135.05 o -7 6 1 670.99 642.44 95.47 o -6 6 1 2301.06 2332.85 90.15 o -5 6 1 3144.10 3037.64 72.69 o -4 6 1 2154.76 2102.62 46.68 o -3 6 1 7894.53 7935.44 149.19 o -2 6 1 2414.72 2556.04 63.00 o -1 6 1 9401.76 9638.85 195.71 o 0 6 1 20923.16 21636.68 423.18 o 1 6 1 9537.94 9767.26 194.29 o 2 6 1 2374.92 2472.25 55.53 o 3 6 1 7911.39 7983.45 148.33 o 4 6 1 2167.43 2097.48 69.92 o 5 6 1 3111.44 3019.74 90.20 o 6 6 1 2265.40 2294.71 70.99 o 7 6 1 670.08 645.83 87.16 o 8 6 1 1437.34 1414.63 96.96 o -8 7 1 454.85 406.63 85.89 o -7 7 1 988.73 1089.29 165.38 o -6 7 1 1966.96 1970.65 96.86 o -5 7 1 1353.71 1341.63 42.36 o -4 7 1 2908.13 2897.01 65.22 o -3 7 1 7319.96 7571.40 177.52 o -2 7 1 4622.10 4537.33 90.93 o -1 7 1 7627.05 7675.95 151.63 o 0 7 1 2568.72 2440.37 58.33 o 1 7 1 7491.98 7520.17 154.54 o 2 7 1 4669.95 4615.04 98.02 o 3 7 1 7291.83 7542.30 151.64 o 4 7 1 2839.47 2865.39 70.46 o 5 7 1 1356.59 1254.21 56.40 o 6 7 1 1945.82 1833.56 91.64 o 7 7 1 997.99 1193.10 115.18 o 8 7 1 477.42 320.12 74.22 o -8 8 1 1212.03 1221.25 113.57 o -7 8 1 209.41 127.19 59.75 o -6 8 1 2113.94 2068.06 136.13 o -5 8 1 101.01 109.58 22.03 o -4 8 1 1974.30 2039.79 59.20 o -3 8 1 3468.89 3469.91 94.67 o -2 8 1 142.20 150.98 30.90 o -1 8 1 5138.95 5200.42 122.74 o 0 8 1 452.84 459.69 27.42 o 1 8 1 5360.23 5491.21 127.43 o 2 8 1 108.05 119.20 18.88 o 3 8 1 3384.14 3393.03 90.18 o 4 8 1 1810.44 1754.97 52.49 o 5 8 1 104.99 66.85 20.44 o 6 8 1 2118.09 2113.85 138.89 o 7 8 1 195.01 170.62 95.16 o 8 8 1 1226.58 1159.66 108.10 o -7 9 1 1123.62 1261.47 143.52 o -6 9 1 902.84 855.16 96.24 o -5 9 1 2197.63 2115.49 79.11 o -4 9 1 919.35 929.39 40.13 o -3 9 1 493.11 500.68 29.28 o -2 9 1 3281.85 3062.76 93.16 o -1 9 1 2129.78 2149.92 68.66 o 0 9 1 2837.76 2909.23 83.74 o 1 9 1 2051.89 1977.99 73.79 o 2 9 1 3286.21 3010.75 84.08 o 3 9 1 562.66 599.06 35.11 o 4 9 1 959.64 872.61 39.50 o 5 9 1 2198.37 2143.07 76.69 o 6 9 1 901.39 855.47 75.27 o 7 9 1 1173.50 1290.42 135.20 o -7 10 1 154.04 127.50 71.76 o -6 10 1 552.09 512.43 42.29 o -5 10 1 755.22 706.81 48.33 o -4 10 1 2474.71 2372.88 92.13 o -3 10 1 1226.65 1183.09 94.77 o -2 10 1 2261.49 2122.68 71.72 o -1 10 1 3298.70 3153.41 98.05 o 0 10 1 3770.81 3838.59 121.18 o 1 10 1 3223.73 3241.73 205.54 o 2 10 1 2217.25 2170.68 76.77 o 3 10 1 1351.65 1338.25 63.32 o 4 10 1 2480.33 2343.31 112.08 o 5 10 1 775.27 857.66 54.40 o 6 10 1 557.73 494.06 56.81 o 7 10 1 136.78 178.93 75.45 o -7 11 1 95.55 307.05 107.79 o -6 11 1 741.91 725.85 62.98 o -5 11 1 277.94 252.10 53.32 o -4 11 1 1609.52 1611.38 87.98 o -3 11 1 2121.65 1879.55 95.37 o -2 11 1 3569.79 3615.56 136.84 o -1 11 1 3725.07 3789.93 169.09 o 0 11 1 2327.64 2341.02 107.83 o 1 11 1 3861.93 3815.96 291.96 o 2 11 1 3515.44 3508.58 154.50 o 3 11 1 2092.58 2037.81 87.75 o 4 11 1 1546.28 1435.80 77.21 o 5 11 1 286.67 287.87 55.15 o 6 11 1 698.23 692.05 160.46 o 7 11 1 84.37 79.46 99.48 o -6 12 1 73.20 107.22 51.44 o -5 12 1 1684.38 1553.66 99.43 o -4 12 1 522.34 430.54 56.22 o -3 12 1 1581.88 1672.00 102.18 o -2 12 1 2796.78 3042.42 138.55 o -1 12 1 12.95 73.53 48.97 o 0 12 1 3983.42 3788.30 241.45 o 1 12 1 19.20 7.07 54.79 o 2 12 1 2763.45 2805.60 112.27 o 3 12 1 1577.60 1414.98 81.12 o 4 12 1 530.18 453.33 54.66 o 5 12 1 1656.54 1663.50 107.93 o 6 12 1 73.64 74.47 65.55 o -5 13 1 871.87 806.81 67.02 o -4 13 1 853.80 845.98 93.62 o -3 13 1 1506.06 1761.06 109.85 o -2 13 1 644.00 485.67 80.50 o -1 13 1 1142.55 1030.07 78.03 o 0 13 1 628.22 588.63 62.83 o 1 13 1 1145.67 1061.25 84.91 o 2 13 1 642.90 590.52 119.96 o 3 13 1 1531.38 1510.05 106.82 o 4 13 1 869.57 823.96 138.89 o 5 13 1 866.16 860.71 75.61 o -5 14 1 287.40 176.44 63.22 o -4 14 1 585.03 583.35 81.10 o -3 14 1 822.17 782.74 87.62 o -2 14 1 695.95 651.33 145.98 o -1 14 1 635.93 615.28 118.72 o 0 14 1 2805.70 2599.49 234.37 o 1 14 1 650.58 508.36 62.84 o 2 14 1 747.34 730.29 82.01 o 3 14 1 858.24 714.03 153.06 o 4 14 1 608.85 613.92 93.37 o 5 14 1 288.62 285.88 83.10 o -4 15 1 113.18 230.75 93.93 o -3 15 1 625.50 665.53 95.81 o -2 15 1 946.37 810.66 89.00 o -1 15 1 258.53 208.75 67.17 o 0 15 1 1540.48 1643.01 134.03 o 1 15 1 263.14 166.13 75.76 o 2 15 1 970.63 945.72 136.74 o 3 15 1 628.72 624.99 80.02 o 4 15 1 107.55 201.86 87.13 o -2 16 1 197.42 267.00 205.27 o -1 16 1 829.25 1029.67 124.69 o 0 16 1 73.81 10.30 70.16 o 1 16 1 806.20 680.04 109.41 o 2 16 1 200.50 389.21 110.56 o 2 0 2 1202.74 1268.28 23.91 o 3 0 2 10968.01 10673.60 191.92 o 4 0 2 108.89 106.65 22.49 o 5 0 2 16073.56 15871.63 362.45 o 6 0 2 1476.61 1449.92 69.41 o 7 0 2 6724.98 6989.10 278.48 o 8 0 2 10.35 19.15 45.69 o 9 0 2 1267.95 1454.26 198.64 o -9 1 2 708.32 635.97 91.47 o -8 1 2 703.55 615.95 95.47 o -7 1 2 519.68 437.13 53.26 o -6 1 2 549.12 517.77 40.86 o -5 1 2 1840.65 1817.75 48.08 o -4 1 2 2030.50 2065.65 36.84 o -3 1 2 14661.65 14646.68 198.33 o -2 1 2 9054.92 8822.76 124.73 o -1 1 2 44301.75 16717.99 4111.53 o 1 1 2 44604.57 811.61 7493.66 o 2 1 2 9410.37 9093.10 159.94 o 3 1 2 14601.49 14245.12 224.60 o 4 1 2 1978.22 1992.74 76.81 o 5 1 2 1907.18 1881.02 53.96 o 6 1 2 570.56 628.90 48.99 o 7 1 2 493.11 515.35 71.60 o 8 1 2 683.06 676.01 87.47 o 9 1 2 692.89 897.75 135.20 o -9 2 2 1258.16 1209.49 165.85 o -8 2 2 1117.00 1058.25 78.83 o -7 2 2 2698.17 2590.22 112.70 o -6 2 2 1415.02 1446.57 68.77 o -5 2 2 4474.88 4303.33 74.48 o -4 2 2 8798.92 8938.68 136.85 o -3 2 2 6705.42 6536.09 97.30 o -2 2 2 4034.11 3831.81 53.59 o -1 2 2 1657.89 1642.29 33.74 o 0 2 2 627.54 243.09 72.86 o 1 2 2 1633.80 1557.22 117.94 o 2 2 2 4036.57 3805.99 71.92 o 3 2 2 6654.88 6432.04 107.54 o 4 2 2 8944.28 9192.61 147.23 o 5 2 2 4358.08 4170.88 90.38 o 6 2 2 1445.40 1424.48 64.43 o 7 2 2 2602.50 2555.97 119.04 o 8 2 2 1231.30 970.12 127.19 o 9 2 2 1258.00 1247.61 178.93 o -9 3 2 299.71 139.21 103.48 o -8 3 2 292.18 167.23 63.75 o -7 3 2 59.19 48.02 31.20 o -6 3 2 436.28 440.51 15.80 o -5 3 2 1114.53 1091.83 40.78 o -4 3 2 478.69 442.39 15.67 o -3 3 2 3726.88 3867.85 61.49 o -2 3 2 27474.22 26728.37 435.05 o -1 3 2 2489.20 2252.62 52.19 o 0 3 2 435.69 413.57 39.86 o 1 3 2 2365.44 2246.16 43.34 o 2 3 2 28080.94 27489.75 485.86 o 3 3 2 3712.01 3860.79 78.38 o 4 3 2 469.43 430.68 15.71 o 5 3 2 1093.15 1127.75 32.77 o 6 3 2 435.12 406.07 39.02 o 7 3 2 50.39 39.74 47.72 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o 2 6 31 162.48 137.91 82.21 o 0 7 31 1427.41 1180.43 130.98 o 0 0 32 692.32 479.21 112.72 o 1 0 32 196.51 204.85 108.41 o 2 0 32 255.91 314.62 93.87 o 3 0 32 1072.67 1025.97 102.92 o -3 1 32 398.63 373.89 74.01 o -2 1 32 399.48 454.78 91.66 o -1 1 32 1217.11 997.06 118.24 o 0 1 32 11.45 -53.84 53.84 o 1 1 32 1217.33 1094.79 181.09 o 2 1 32 365.24 227.34 89.32 o 3 1 32 422.63 400.78 159.22 o -3 2 32 204.70 218.49 83.81 o -2 2 32 204.66 164.91 56.39 o -1 2 32 1265.42 1301.14 148.91 o 0 2 32 471.59 412.64 81.12 o 1 2 32 1269.43 1406.77 133.32 o 2 2 32 242.58 140.65 80.78 o 3 2 32 225.43 132.47 78.27 o -2 3 32 401.69 351.00 64.01 o -1 3 32 134.82 166.02 61.49 o 0 3 32 427.64 352.05 68.19 o 1 3 32 141.66 200.65 103.33 o 2 3 32 431.41 433.02 75.92 o -2 4 32 319.89 249.98 79.87 o -1 4 32 316.25 233.47 69.74 o 0 4 32 31.68 52.57 58.85 o 1 4 32 308.77 170.10 86.41 o 2 4 32 340.22 282.31 87.64 o -1 5 32 318.15 298.43 96.18 o 0 5 32 596.37 645.42 80.59 o 1 5 32 328.56 363.10 127.81 o 1 0 33 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