#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/24/2202451.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202451_Fobs loop_ _publ_author_name 'Almeida Paz, Filipe A.' 'Neves, Marcia C.' 'Trindade, Tito' 'Klinowski, Jacek' _publ_section_title ; The first dinuclear zinc(II) dithiocarbamate complex with butyl substituent groups ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1067 _journal_page_last m1069 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.104 _cell_angle_gamma 90.000 _cell_length_a 16.0358 _cell_length_b 16.6039 _cell_length_c 18.4868 _exptl_crystal_F_000 2016.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file cf6295Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' JK0318 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 323.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 307.37 672.30 54.86 o 5 0 0 115.66 126.68 6.78 o 6 0 0 12292.27 13516.89 349.87 o 7 0 0 24.77 19.78 4.99 o 8 0 0 1199.04 706.71 40.60 o 9 0 0 59.47 51.54 7.64 o 10 0 0 1009.08 673.73 17.86 o 11 0 0 465.56 399.23 21.74 o 12 0 0 10090.38 10089.48 230.00 o 13 0 0 2131.79 2321.07 62.61 o 14 0 0 34361.98 36790.01 1684.21 o 15 0 0 1806.34 2197.58 62.65 o 16 0 0 2891.51 3507.48 181.57 o 17 0 0 203.81 274.63 24.97 o 18 0 0 372.93 197.23 15.43 o 19 0 0 108.91 126.06 33.81 o 20 0 0 636.10 482.74 52.23 o 3 1 0 10922.07 11763.73 251.62 o 4 1 0 3234.98 3101.89 54.27 o 5 1 0 19113.47 18427.63 309.68 o 6 1 0 37.67 49.81 4.31 o 7 1 0 1746.88 1950.37 34.14 o 8 1 0 656.02 471.21 12.42 o 9 1 0 80.88 28.35 5.16 o 10 1 0 89.16 61.28 11.12 o 11 1 0 2252.38 2489.52 53.96 o 12 1 0 415.30 346.71 10.41 o 13 1 0 5933.45 5885.76 95.61 o 14 1 0 1150.46 1182.34 37.84 o 15 1 0 2148.19 2410.47 47.69 o 16 1 0 72.62 88.72 8.32 o 17 1 0 1.58 28.15 12.17 o 18 1 0 6.34 1.98 16.67 o 19 1 0 383.59 382.33 30.57 o 20 1 0 0.96 21.87 27.03 o 2 2 0 28557.55 13429.61 1453.69 o 3 2 0 1577.56 1852.47 34.49 o 4 2 0 3068.72 3248.63 48.29 o 5 2 0 16.75 53.73 6.42 o 6 2 0 3203.63 2846.18 47.24 o 7 2 0 0.46 6.57 4.40 o 8 2 0 5731.05 6037.17 102.55 o 9 2 0 878.01 1029.45 19.92 o 10 2 0 2817.61 2822.95 49.04 o 11 2 0 639.70 647.77 14.41 o 12 2 0 2046.56 2014.17 41.49 o 13 2 0 77.74 87.90 13.99 o 14 2 0 1595.96 1695.88 37.44 o 15 2 0 131.50 134.27 14.24 o 16 2 0 1302.51 1472.08 66.55 o 17 2 0 126.25 167.64 30.31 o 18 2 0 66.51 73.82 12.63 o 19 2 0 4.51 38.58 33.82 o 20 2 0 195.41 80.87 48.01 o 2 3 0 5306.20 4055.24 76.84 o 4 3 0 73.49 98.77 9.22 o 5 3 0 8958.16 8589.89 148.22 o 6 3 0 599.25 408.84 13.87 o 7 3 0 6119.91 6516.75 95.76 o 8 3 0 56.59 104.46 17.23 o 9 3 0 9200.79 8783.55 146.04 o 10 3 0 500.09 460.51 11.14 o 11 3 0 14605.26 15992.88 284.94 o 12 3 0 1026.06 1045.36 21.19 o 13 3 0 4643.52 4758.94 86.54 o 14 3 0 1023.04 1098.68 32.39 o 15 3 0 4136.57 4212.87 96.52 o 16 3 0 717.89 845.08 35.12 o 17 3 0 1100.63 1410.83 61.87 o 18 3 0 106.46 161.09 14.58 o 19 3 0 19.57 0.93 22.40 o 20 3 0 89.36 22.29 26.65 o 0 4 0 11032.64 8161.51 205.27 o 1 4 0 4191.93 4455.50 79.12 o 2 4 0 24876.38 24646.77 482.59 o 3 4 0 28.86 314.66 10.47 o 4 4 0 7004.48 8024.85 137.39 o 5 4 0 56.68 116.22 5.79 o 6 4 0 24.78 56.99 19.14 o 7 4 0 3530.89 3473.41 61.99 o 8 4 0 7623.45 8889.32 139.77 o 9 4 0 284.42 253.33 19.46 o 10 4 0 360.36 557.50 11.75 o 11 4 0 528.86 685.14 19.58 o 12 4 0 786.40 774.32 16.06 o 13 4 0 58.91 63.26 5.20 o 14 4 0 639.45 626.46 14.86 o 15 4 0 367.43 405.48 13.51 o 16 4 0 970.39 1054.80 47.24 o 17 4 0 195.14 204.36 23.56 o 18 4 0 218.81 299.99 19.59 o 19 4 0 0.89 8.51 18.27 o 20 4 0 195.83 172.29 80.44 o 1 5 0 1394.59 1938.28 34.46 o 2 5 0 1107.32 1079.15 20.40 o 3 5 0 40669.29 42175.91 804.31 o 4 5 0 674.59 1050.88 19.29 o 5 5 0 14302.27 15210.19 249.32 o 6 5 0 1177.91 1412.69 64.27 o 7 5 0 2516.46 4002.91 76.98 o 8 5 0 2931.30 3200.67 75.60 o 9 5 0 6815.42 7279.83 138.56 o 10 5 0 528.02 533.81 15.48 o 11 5 0 4277.09 3813.26 93.71 o 12 5 0 139.97 91.07 11.95 o 13 5 0 4108.06 4286.55 125.70 o 14 5 0 173.08 184.91 35.73 o 15 5 0 23.77 5.58 21.44 o 16 5 0 104.33 126.58 40.87 o 17 5 0 8.01 17.06 19.36 o 18 5 0 8.07 15.96 20.14 o 19 5 0 34.95 1.65 22.47 o 20 5 0 23.54 58.25 21.42 o 0 6 0 39349.69 35036.97 899.84 o 1 6 0 1942.26 2079.50 39.47 o 2 6 0 39239.68 38282.84 676.65 o 3 6 0 3525.96 4062.55 72.56 o 4 6 0 19579.57 19771.59 370.14 o 5 6 0 90.86 122.03 12.39 o 6 6 0 13.08 46.41 24.10 o 7 6 0 686.42 905.64 18.03 o 8 6 0 2052.71 1693.90 38.41 o 9 6 0 268.68 341.89 19.66 o 10 6 0 11536.33 11625.44 293.04 o 11 6 0 6.01 -6.94 25.77 o 12 6 0 5495.47 5758.80 183.94 o 13 6 0 911.87 909.49 43.97 o 14 6 0 3683.26 4001.83 206.50 o 15 6 0 1319.20 1351.58 61.61 o 16 6 0 2425.93 2712.75 92.00 o 17 6 0 290.83 350.42 31.48 o 18 6 0 9.01 32.17 30.20 o 19 6 0 12.00 44.16 19.74 o 1 7 0 33015.46 32844.04 558.52 o 2 7 0 41.34 21.94 6.00 o 3 7 0 14.47 -1.28 6.79 o 4 7 0 2566.31 3121.25 56.57 o 5 7 0 1941.74 1753.83 29.33 o 6 7 0 1635.29 1584.50 41.95 o 7 7 0 683.89 532.53 11.09 o 8 7 0 102.69 137.41 6.53 o 9 7 0 53.96 100.64 12.90 o 10 7 0 354.60 324.78 16.55 o 11 7 0 442.92 370.66 18.29 o 12 7 0 0.95 -19.48 19.48 o 13 7 0 859.38 1153.43 52.28 o 14 7 0 350.37 295.06 30.04 o 15 7 0 2372.02 2716.04 159.18 o 16 7 0 509.31 545.48 43.95 o 17 7 0 478.84 425.26 36.78 o 18 7 0 32.61 57.27 30.25 o 19 7 0 153.02 119.42 27.07 o 1 8 0 1282.55 1400.42 59.26 o 2 8 0 20736.82 21504.26 355.75 o 3 8 0 1004.22 819.31 34.97 o 4 8 0 2902.12 3190.29 56.39 o 5 8 0 1324.43 1481.20 40.98 o 6 8 0 1274.98 1198.15 35.27 o 7 8 0 322.27 417.29 11.99 o 8 8 0 67.06 58.96 4.10 o 9 8 0 366.04 374.46 25.02 o 10 8 0 415.52 327.06 27.05 o 11 8 0 1276.96 1191.10 98.62 o 12 8 0 2714.35 2384.52 113.96 o 13 8 0 141.71 180.41 24.20 o 14 8 0 2938.41 2851.12 151.54 o 15 8 0 64.97 51.11 38.00 o 16 8 0 667.76 696.33 46.71 o 18 8 0 195.25 135.14 25.74 o 19 8 0 16.92 11.89 31.74 o 2 9 0 65.45 -2.12 10.46 o 3 9 0 543.43 387.08 12.07 o 4 9 0 136.16 309.99 13.13 o 5 9 0 1290.98 1579.33 40.01 o 6 9 0 158.41 237.50 8.05 o 7 9 0 965.90 1025.80 20.20 o 8 9 0 0.09 10.26 8.64 o 9 9 0 17.51 17.68 21.94 o 10 9 0 439.25 577.38 36.68 o 11 9 0 741.88 612.84 47.19 o 12 9 0 152.22 79.25 37.31 o 13 9 0 10243.06 10115.39 522.28 o 14 9 0 819.69 787.83 51.27 o 15 9 0 4213.06 4976.41 303.39 o 16 9 0 277.66 348.61 38.16 o 17 9 0 0.97 21.76 25.05 o 18 9 0 7.13 12.53 23.14 o 0 10 0 5969.67 5896.95 159.46 o 1 10 0 133.96 119.99 11.02 o 2 10 0 4617.61 4233.51 79.19 o 3 10 0 731.32 765.81 21.00 o 4 10 0 1215.06 1410.89 30.88 o 5 10 0 1936.57 1411.45 30.29 o 6 10 0 1185.21 1200.08 26.23 o 7 10 0 178.38 148.38 6.76 o 8 10 0 1724.93 1842.48 36.61 o 9 10 0 1355.55 1583.46 49.23 o 10 10 0 76.56 108.28 23.62 o 11 10 0 45.23 41.98 21.66 o 12 10 0 2099.14 2210.10 107.27 o 13 10 0 225.18 252.28 42.73 o 14 10 0 977.34 1142.18 61.30 o 15 10 0 207.73 181.05 30.94 o 16 10 0 1.92 6.58 24.42 o 17 10 0 43.47 -34.98 34.98 o 18 10 0 117.68 86.68 26.49 o 1 11 0 4255.45 4005.67 77.13 o 2 11 0 556.18 580.70 39.45 o 3 11 0 6642.59 6171.93 126.14 o 4 11 0 1.76 -7.24 7.24 o 5 11 0 1105.39 1062.16 24.99 o 6 11 0 697.15 841.97 25.79 o 7 11 0 693.50 460.33 19.49 o 8 11 0 1918.39 2166.32 73.49 o 9 11 0 1453.37 1215.51 31.35 o 10 11 0 283.59 249.89 32.22 o 11 11 0 1414.70 1457.09 73.83 o 12 11 0 222.50 242.83 38.85 o 13 11 0 710.04 653.23 45.49 o 14 11 0 23.10 -11.20 38.91 o 15 11 0 273.20 219.05 29.03 o 16 11 0 31.81 38.96 25.74 o 17 11 0 126.00 85.35 31.10 o 0 12 0 3263.21 3321.26 99.28 o 1 12 0 4.59 -10.08 11.47 o 2 12 0 9487.51 10526.52 217.59 o 3 12 0 756.53 835.34 21.93 o 4 12 0 6573.18 6922.84 146.31 o 5 12 0 49.18 106.04 19.35 o 6 12 0 35.74 44.36 11.39 o 7 12 0 0.99 5.37 12.55 o 8 12 0 1367.64 1287.26 39.57 o 9 12 0 26.28 41.37 5.16 o 10 12 0 3436.90 3778.02 200.32 o 11 12 0 138.24 162.15 41.56 o 12 12 0 2033.76 2429.68 106.53 o 13 12 0 334.82 330.62 42.25 o 14 12 0 463.40 566.66 50.26 o 15 12 0 75.48 66.77 27.12 o 16 12 0 171.73 124.47 29.78 o 17 12 0 209.59 264.59 33.86 o 1 13 0 1912.50 2449.87 58.62 o 2 13 0 447.75 549.65 17.13 o 3 13 0 21.07 -5.52 9.04 o 4 13 0 103.77 117.94 12.02 o 5 13 0 37.52 115.09 26.49 o 6 13 0 1534.76 1321.58 68.01 o 7 13 0 234.53 147.54 18.36 o 8 13 0 696.26 659.98 28.64 o 9 13 0 12.24 15.24 12.43 o 10 13 0 45.54 53.50 25.74 o 11 13 0 60.89 56.16 36.31 o 12 13 0 20.00 58.17 38.32 o 13 13 0 11.01 37.69 37.05 o 14 13 0 2.75 -17.89 37.74 o 15 13 0 369.62 237.15 41.08 o 16 13 0 244.68 285.24 39.81 o 0 14 0 1190.93 1731.82 78.13 o 1 14 0 874.08 934.38 25.88 o 2 14 0 999.03 1031.04 30.25 o 3 14 0 79.46 90.18 11.88 o 4 14 0 2097.70 1933.97 58.00 o 5 14 0 653.61 574.39 21.36 o 6 14 0 1202.67 1152.29 36.66 o 7 14 0 1344.85 1444.32 45.65 o 8 14 0 345.19 292.07 21.46 o 9 14 0 330.19 403.05 19.97 o 10 14 0 2649.24 2608.03 156.95 o 11 14 0 92.49 86.04 29.78 o 12 14 0 1300.24 1283.05 69.64 o 13 14 0 25.13 -21.18 28.50 o 14 14 0 67.27 -17.25 27.87 o 15 14 0 101.72 173.25 33.17 o 1 15 0 5304.03 4933.11 163.02 o 2 15 0 229.70 156.68 35.47 o 3 15 0 1396.57 1705.89 96.62 o 4 15 0 262.76 194.90 20.98 o 5 15 0 4.03 4.28 13.09 o 6 15 0 0.69 -7.35 11.21 o 7 15 0 154.15 199.54 25.31 o 8 15 0 20.13 17.06 21.12 o 9 15 0 382.15 410.56 34.45 o 10 15 0 5.71 -37.10 41.72 o 11 15 0 344.12 239.91 32.48 o 13 15 0 505.39 514.96 52.44 o 14 15 0 188.95 103.61 34.55 o 0 16 0 730.09 1223.33 63.06 o 1 16 0 291.07 319.51 26.47 o 2 16 0 263.33 283.07 42.40 o 3 16 0 691.66 800.07 33.21 o 4 16 0 24.72 64.43 15.51 o 5 16 0 493.75 557.62 47.47 o 6 16 0 412.39 369.57 20.84 o 7 16 0 16.33 7.79 40.37 o 8 16 0 27.49 2.74 21.31 o 9 16 0 150.79 100.79 28.50 o 10 16 0 216.72 124.04 33.17 o 11 16 0 270.27 294.05 41.19 o 12 16 0 39.55 25.90 43.84 o 13 16 0 3.70 30.57 46.50 o 1 17 0 2101.52 2620.18 87.49 o 2 17 0 21.30 2.34 22.68 o 3 17 0 226.32 193.87 17.41 o 4 17 0 101.80 62.13 18.11 o 5 17 0 17.64 24.41 18.98 o 6 17 0 34.12 -14.82 38.59 o 7 17 0 9.15 8.90 54.70 o 8 17 0 219.83 238.27 33.17 o 9 17 0 13.30 -31.21 31.21 o 10 17 0 318.94 342.09 51.17 o 11 17 0 219.36 99.04 31.26 o 12 17 0 80.68 108.38 32.59 o 0 18 0 3135.15 2987.69 202.28 o 1 18 0 110.33 127.86 21.56 o 2 18 0 956.16 969.91 58.31 o 3 18 0 221.66 199.88 20.58 o 4 18 0 15.12 19.74 18.57 o 5 18 0 2.76 -17.17 17.17 o 6 18 0 64.42 112.36 24.12 o 7 18 0 10.35 -3.34 30.57 o 8 18 0 6.98 -31.21 40.50 o 9 18 0 14.58 73.78 29.88 o 10 18 0 4.76 37.90 31.26 o 11 18 0 3.88 15.29 44.59 o 1 19 0 36.46 53.21 24.71 o 2 19 0 108.90 83.54 60.77 o 3 19 0 6.20 40.13 21.39 o 4 19 0 160.96 103.65 23.89 o 5 19 0 11.15 10.95 18.65 o 6 19 0 57.86 55.78 41.19 o 7 19 0 33.65 23.25 30.57 o 8 19 0 245.64 331.10 37.26 o 9 19 0 8.39 -8.65 31.90 o 0 20 0 3.24 2.65 23.30 o 1 20 0 19.21 67.73 62.74 o 2 20 0 196.87 141.39 36.70 o 3 20 0 1.42 8.98 36.65 o 4 20 0 539.11 530.34 68.39 o 5 20 0 3.68 9.98 28.61 o 6 20 0 50.54 111.68 34.55 o 7 20 0 161.97 234.76 50.53 o 1 21 0 75.82 47.49 20.99 o 2 21 0 55.98 23.26 18.35 o 3 21 0 199.91 288.89 25.24 o 4 21 0 77.74 62.53 42.57 o -20 1 1 21.66 13.84 28.69 o -19 1 1 1.20 19.92 23.41 o -18 1 1 374.74 328.58 19.56 o -17 1 1 251.77 302.92 19.99 o -16 1 1 4723.50 4726.04 142.43 o -15 1 1 913.53 872.35 29.51 o -14 1 1 12940.37 14580.42 262.57 o -13 1 1 509.67 520.22 26.32 o -12 1 1 802.75 683.08 14.50 o -11 1 1 18.66 6.49 7.72 o -10 1 1 7501.49 7922.59 139.89 o -9 1 1 541.98 601.64 13.02 o -8 1 1 1140.88 1324.46 23.50 o -7 1 1 9.37 108.26 4.91 o -6 1 1 7954.94 8276.65 142.34 o -5 1 1 27.40 67.85 2.97 o -4 1 1 36139.52 32476.31 747.86 o -3 1 1 1658.76 1263.39 30.87 o 3 1 1 24.62 33.26 4.68 o 5 1 1 678.08 824.21 17.84 o 6 1 1 44961.06 46255.80 844.98 o 7 1 1 2416.66 1815.67 30.13 o 8 1 1 3778.05 2958.79 51.58 o 9 1 1 588.33 480.51 10.19 o 10 1 1 2046.35 1609.09 27.43 o 11 1 1 595.72 670.97 16.98 o 12 1 1 7125.11 7231.03 112.23 o 13 1 1 539.07 597.66 18.97 o 14 1 1 6638.34 8096.11 156.60 o 15 1 1 238.94 252.87 34.41 o 16 1 1 16.89 88.28 12.80 o 17 1 1 1.28 0.66 12.43 o 18 1 1 1377.42 1510.75 123.64 o 19 1 1 209.39 216.34 87.21 o 20 1 1 980.57 960.48 57.40 o -20 2 1 8.60 -11.43 67.83 o -19 2 1 3.97 5.53 13.13 o -18 2 1 18.81 82.36 20.76 o -17 2 1 1052.23 946.45 29.13 o -16 2 1 242.91 268.85 17.75 o -15 2 1 5779.73 5674.99 121.63 o -14 2 1 1254.69 1284.07 41.22 o -13 2 1 7874.61 8493.75 158.15 o -12 2 1 32.20 49.71 5.66 o -11 2 1 305.45 279.79 14.50 o -10 2 1 994.87 913.79 18.46 o -9 2 1 12052.82 13569.89 235.13 o -8 2 1 127.91 226.19 9.93 o -7 2 1 1907.02 1890.35 32.10 o -6 2 1 2.04 20.09 3.32 o -5 2 1 1705.65 1105.20 20.76 o -4 2 1 3654.50 3329.60 53.33 o -2 2 1 144.32 63.37 22.77 o 2 2 1 209.01 55.79 4.15 o 3 2 1 23.40 387.52 10.34 o 4 2 1 967.67 946.70 15.49 o 5 2 1 15581.38 17401.20 262.39 o 6 2 1 19.80 -3.70 4.22 o 7 2 1 13495.28 14020.25 227.68 o 8 2 1 1358.33 1086.80 19.69 o 9 2 1 15784.28 15670.53 263.01 o 10 2 1 706.18 582.39 15.54 o 11 2 1 11292.70 11288.00 184.21 o 12 2 1 1087.41 1307.41 25.55 o 13 2 1 1849.37 2352.16 77.78 o 14 2 1 714.78 876.52 30.98 o 15 2 1 132.04 197.20 11.06 o 16 2 1 6.09 19.20 22.10 o 17 2 1 92.33 64.00 16.26 o 18 2 1 59.57 46.98 15.07 o 19 2 1 426.92 483.32 36.39 o 20 2 1 164.51 115.61 34.43 o -20 3 1 7.43 -25.48 25.48 o -19 3 1 61.19 19.05 33.34 o -18 3 1 89.12 89.19 15.81 o -17 3 1 40.49 68.46 15.93 o -16 3 1 8.34 16.49 7.81 o -15 3 1 6.20 1.25 9.90 o -14 3 1 90.43 136.40 7.93 o -13 3 1 0.09 -9.43 9.43 o -12 3 1 440.19 377.04 17.66 o -11 3 1 490.98 540.34 15.06 o -10 3 1 639.79 761.39 20.23 o -9 3 1 311.71 259.08 12.04 o -8 3 1 1900.26 1797.49 36.01 o -7 3 1 339.66 320.73 13.54 o -6 3 1 3645.55 4152.06 79.93 o -5 3 1 473.00 335.40 14.41 o -4 3 1 1310.81 1203.02 30.43 o -3 3 1 3654.63 5059.01 120.63 o -2 3 1 47791.97 45894.36 1722.08 o -1 3 1 2.31 50.90 15.65 o 0 3 1 17160.00 15266.79 601.53 o 1 3 1 143.13 288.91 15.31 o 2 3 1 69120.30 66847.86 2443.43 o 3 3 1 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