#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/24/2202477.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202477_Fobs loop_ _publ_author_name 'Krivokapi\'c, Alexander' 'Faiz, Jonathan A.' 'Anderson, Harry L.' _publ_section_title ; Bis-BBN (9-borabicyclo[3.3.1]nonane) adduct of bis(diethylglyoximato)nickel(II) ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m748 _journal_page_last m749 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90 _cell_angle_beta 94.7398(5) _cell_angle_gamma 90 _cell_length_a 7.4047(1) _cell_length_b 19.2467(2) _cell_length_c 10.5508(2) _[local]_cod_data_source_file ci6244Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma _refln_observed_status 3 0 0 42.25 41.50 0.35 o 4 0 0 6.04 5.15 0.36 o 5 0 0 15.54 16.64 0.31 o 6 0 0 5.52 4.94 0.59 o 7 0 0 54.47 53.59 0.68 o 8 0 0 28.47 28.16 0.43 o 9 0 0 36.27 35.35 0.67 o 2 1 0 8.35 8.13 0.14 o 3 1 0 23.32 22.90 0.17 o 4 1 0 29.47 29.74 0.20 o 5 1 0 20.71 21.85 0.21 o 6 1 0 23.47 23.89 0.24 o 7 1 0 16.50 17.25 0.26 o 8 1 0 22.95 23.59 0.33 o 9 1 0 5.41 6.64 0.95 < 2 2 0 109.82 111.60 0.61 o 3 2 0 55.54 55.73 0.32 o 4 2 0 41.15 42.09 0.26 o 5 2 0 43.28 43.84 0.27 o 6 2 0 29.26 29.98 0.24 o 7 2 0 27.91 26.78 0.29 o 8 2 0 25.38 24.79 0.35 o 9 2 0 12.32 12.85 0.50 o 2 3 0 67.00 68.95 0.36 o 3 3 0 22.68 23.70 0.16 o 4 3 0 -0.89 0.37 4.29 < 5 3 0 14.90 15.23 0.18 o 6 3 0 19.06 19.77 0.23 o 7 3 0 9.41 8.10 0.34 o 8 3 0 6.64 6.64 0.69 o 9 3 0 15.85 16.97 0.46 o 2 4 0 33.27 34.28 0.20 o 3 4 0 36.14 38.13 0.20 o 4 4 0 13.18 14.80 0.16 o 5 4 0 64.00 63.69 0.38 o 6 4 0 23.41 23.73 0.21 o 7 4 0 42.55 42.39 0.36 o 8 4 0 15.27 14.67 0.37 o 9 4 0 20.74 19.56 0.63 o 1 5 0 57.31 57.81 0.36 o 2 5 0 31.24 30.23 0.21 o 3 5 0 42.38 41.09 0.24 o 4 5 0 49.96 48.72 0.30 o 5 5 0 -1.58 0.26 0.95 < 6 5 0 12.01 12.19 0.22 o 7 5 0 9.36 9.54 0.32 o 8 5 0 27.69 28.28 0.39 o 9 5 0 3.81 3.87 2.01 < 0 6 0 35.79 33.36 0.30 o 1 6 0 15.58 15.83 0.14 o 2 6 0 38.27 40.47 0.24 o 3 6 0 49.08 50.11 0.29 o 4 6 0 63.62 65.06 0.37 o 5 6 0 35.13 34.56 0.23 o 6 6 0 76.82 76.41 0.49 o 7 6 0 38.40 37.54 0.32 o 8 6 0 17.51 17.97 0.43 o 9 6 0 39.12 40.48 0.75 o 1 7 0 10.17 9.06 0.15 o 2 7 0 54.22 50.90 0.33 o 3 7 0 19.64 20.28 0.15 o 4 7 0 3.27 3.79 0.29 o 5 7 0 74.38 74.77 0.46 o 6 7 0 6.94 7.29 0.30 o 7 7 0 19.39 20.69 0.29 o 8 7 0 10.19 10.60 0.55 o 9 7 0 3.73 3.23 1.73 < 0 8 0 117.99 122.22 1.01 o 1 8 0 116.78 119.83 0.67 o 2 8 0 84.27 86.28 0.44 o 3 8 0 25.42 25.83 0.20 o 4 8 0 65.49 65.37 0.36 o 5 8 0 15.03 14.19 0.16 o 6 8 0 68.29 69.29 0.50 o 7 8 0 24.11 24.57 0.36 o 8 8 0 56.73 56.49 0.68 o 9 8 0 41.92 43.83 0.96 o 1 9 0 24.95 24.49 0.17 o 2 9 0 12.90 12.57 0.17 o 3 9 0 7.39 6.34 0.26 o 4 9 0 8.91 10.44 0.31 o 5 9 0 66.37 66.41 0.47 o 6 9 0 29.13 28.45 0.27 o 7 9 0 9.26 9.51 0.31 o 8 9 0 7.67 7.48 0.59 o 0 10 0 120.36 120.06 0.86 o 1 10 0 101.14 101.06 0.59 o 2 10 0 129.17 128.95 0.80 o 3 10 0 86.90 86.76 0.54 o 4 10 0 98.60 98.23 0.65 o 5 10 0 52.26 53.63 0.39 o 6 10 0 6.81 6.82 0.56 o 7 10 0 14.90 15.61 0.45 o 8 10 0 11.98 13.13 1.12 o 1 11 0 21.43 21.18 0.17 o 2 11 0 42.81 43.02 0.28 o 3 11 0 24.61 24.70 0.24 o 4 11 0 4.58 6.32 0.51 o 5 11 0 -1.58 0.40 1.61 < 6 11 0 20.49 21.28 0.40 o 7 11 0 10.25 9.22 0.59 o 8 11 0 22.17 22.48 0.74 o 0 12 0 33.47 34.42 0.29 o 1 12 0 88.19 86.25 0.51 o 2 12 0 30.59 30.25 0.23 o 3 12 0 86.91 84.91 0.53 o 4 12 0 38.44 38.43 0.30 o 5 12 0 22.34 22.51 0.32 o 6 12 0 2.47 0.41 1.66 < 7 12 0 3.32 3.01 1.82 < 8 12 0 9.87 9.78 1.27 o 1 13 0 36.41 36.51 0.24 o 2 13 0 21.00 19.95 0.19 o 3 13 0 64.49 63.54 0.44 o 4 13 0 2.55 3.92 0.82 < 5 13 0 16.38 17.00 0.34 o 6 13 0 32.99 32.58 0.50 o 7 13 0 17.16 17.16 0.65 o 8 13 0 7.02 7.55 2.14 < 0 14 0 59.17 59.39 0.47 o 1 14 0 45.35 44.95 0.26 o 2 14 0 55.17 56.35 0.33 o 3 14 0 84.35 84.26 0.56 o 4 14 0 24.62 25.34 0.35 o 5 14 0 46.83 47.64 0.49 o 6 14 0 17.90 17.67 0.52 o 7 14 0 13.22 12.58 0.92 o 1 15 0 5.87 6.82 0.31 o 2 15 0 27.33 26.59 0.21 o 3 15 0 13.73 13.53 0.35 o 4 15 0 -2.53 3.14 1.88 < 5 15 0 -2.72 2.08 1.69 < 6 15 0 4.45 4.84 1.34 < 7 15 0 4.23 1.22 2.16 < 0 16 0 42.74 42.81 0.39 o 1 16 0 26.91 28.40 0.22 o 2 16 0 75.03 75.87 0.44 o 3 16 0 33.43 33.44 0.38 o 4 16 0 38.06 39.82 0.47 o 5 16 0 37.67 37.21 0.54 o 6 16 0 30.10 29.34 0.55 o 7 16 0 27.18 28.75 0.73 o 1 17 0 26.92 27.05 0.22 o 2 17 0 2.30 1.89 0.72 < 3 17 0 25.59 24.86 0.40 o 4 17 0 2.86 0.58 1.96 < 5 17 0 19.72 20.39 0.54 o 6 17 0 6.53 0.74 1.79 < 0 18 0 13.34 13.04 0.35 o 1 18 0 7.91 6.80 0.31 o 2 18 0 23.82 23.15 0.25 o 3 18 0 39.83 40.07 0.46 o 4 18 0 42.62 43.72 0.55 o 5 18 0 49.33 48.35 0.66 o 6 18 0 29.77 29.54 0.74 o 1 19 0 26.54 26.73 0.27 o 2 19 0 22.47 21.94 0.28 o 3 19 0 7.28 7.99 0.75 o 4 19 0 34.45 34.55 0.54 o 5 19 0 9.31 10.59 0.90 o 6 19 0 19.87 20.39 0.77 o 0 20 0 40.72 40.81 0.52 o 1 20 0 49.77 49.65 0.43 o 2 20 0 17.28 16.98 0.28 o 3 20 0 43.14 43.11 0.57 o 4 20 0 25.81 25.63 0.58 o 5 20 0 17.39 19.67 0.71 o 1 21 0 6.96 9.50 0.66 o 2 21 0 42.73 42.94 0.54 o 3 21 0 3.27 4.40 2.51 < 4 21 0 8.88 10.05 0.98 o 5 21 0 16.07 17.75 0.71 o 0 22 0 26.65 27.42 0.70 o 1 22 0 60.33 59.96 0.74 o 2 22 0 11.05 11.51 0.81 o 3 22 0 22.25 22.15 0.58 o 4 22 0 24.48 24.27 0.64 o 1 23 0 -3.30 2.40 1.88 < 2 23 0 4.43 2.95 1.10 < 3 23 0 8.18 8.05 1.42 < 0 24 0 36.09 35.55 0.91 o 1 24 0 52.76 53.51 0.88 o 2 24 0 34.56 35.15 0.81 o -9 1 1 15.22 13.73 0.51 o -8 1 1 22.70 23.08 0.29 o -7 1 1 11.96 11.69 0.28 o -6 1 1 7.85 6.87 0.27 o -5 1 1 27.02 27.75 0.21 o -4 1 1 92.36 90.22 0.52 o -3 1 1 112.70 113.35 0.65 o 2 1 1 26.36 25.96 0.18 o 3 1 1 35.43 35.69 0.23 o 4 1 1 52.78 54.71 0.30 o 5 1 1 61.96 62.49 0.37 o 6 1 1 56.60 56.59 0.39 o 7 1 1 57.60 57.12 0.43 o 8 1 1 36.97 36.86 0.42 o 9 1 1 31.19 31.06 0.50 o -9 2 1 7.10 6.69 1.01 o -8 2 1 15.83 16.05 0.35 o -7 2 1 41.44 41.08 0.34 o -6 2 1 17.08 17.40 0.22 o -5 2 1 3.46 4.87 0.48 o -4 2 1 48.84 48.84 0.29 o -3 2 1 66.29 65.96 0.39 o -2 2 1 107.76 108.28 0.65 o 2 2 1 19.23 20.70 0.14 o 3 2 1 1.92 1.73 0.42 < 4 2 1 -0.95 0.13 4.93 < 5 2 1 8.69 8.58 0.23 o 6 2 1 5.12 5.15 0.37 o 7 2 1 5.27 5.03 0.53 o 8 2 1 20.01 20.49 0.36 o 9 2 1 11.14 11.41 0.67 o -9 3 1 25.78 25.41 0.57 o -8 3 1 26.62 26.67 0.37 o -7 3 1 34.05 33.54 0.30 o -6 3 1 47.65 49.15 0.32 o -5 3 1 60.30 62.00 0.37 o -4 3 1 65.11 67.30 0.35 o -3 3 1 100.15 102.52 0.60 o -2 3 1 126.96 128.99 0.74 o 2 3 1 49.45 47.08 0.30 o 3 3 1 49.57 50.85 0.28 o 4 3 1 37.14 40.01 0.25 o 5 3 1 40.16 41.84 0.26 o 6 3 1 22.64 22.72 0.21 o 7 3 1 24.32 24.05 0.27 o 8 3 1 4.87 4.05 0.93 < 9 3 1 21.05 20.65 0.52 o -9 4 1 3.70 4.39 1.92 < -8 4 1 14.12 14.19 0.47 o -7 4 1 27.51 27.35 0.31 o -6 4 1 17.73 17.64 0.22 o -5 4 1 28.08 28.56 0.20 o -4 4 1 31.30 30.05 0.19 o -3 4 1 22.55 21.66 0.18 o -2 4 1 30.79 29.08 0.19 o -1 4 1 58.42 58.28 0.33 o 1 4 1 7.73 7.80 0.11 o 2 4 1 65.50 64.64 0.37 o 3 4 1 15.41 15.37 0.14 o 4 4 1 17.56 18.66 0.16 o 5 4 1 31.09 30.29 0.22 o 6 4 1 6.75 7.37 0.29 o 7 4 1 8.86 9.34 0.30 o 8 4 1 19.98 20.67 0.36 o 9 4 1 12.11 11.31 0.57 o -9 5 1 18.20 17.71 0.59 o -8 5 1 30.18 30.00 0.39 o -7 5 1 30.85 30.20 0.30 o -6 5 1 54.78 54.88 0.34 o -5 5 1 19.30 20.09 0.20 o -4 5 1 42.61 45.10 0.24 o -3 5 1 48.60 51.42 0.27 o -2 5 1 83.09 84.05 0.44 o -1 5 1 41.20 43.31 0.23 o 0 5 1 131.32 133.68 0.78 o 1 5 1 87.90 87.27 0.52 o 2 5 1 94.65 96.74 0.63 o 3 5 1 68.78 69.16 0.37 o 4 5 1 36.24 35.34 0.22 o 5 5 1 84.06 86.03 0.47 o 6 5 1 12.11 12.50 0.21 o 7 5 1 52.65 52.49 0.38 o 8 5 1 3.77 4.77 1.10 < 9 5 1 44.01 44.76 0.87 o -9 6 1 3.32 3.63 1.94 < -8 6 1 4.76 4.55 1.02 < -7 6 1 24.92 23.99 0.28 o -6 6 1 12.52 13.50 0.23 o -5 6 1 42.27 41.41 0.26 o -4 6 1 9.47 10.56 0.18 o -3 6 1 10.59 8.16 0.17 o -2 6 1 87.58 85.25 0.47 o -1 6 1 39.51 39.27 0.23 o 0 6 1 46.42 46.69 0.27 o 1 6 1 70.17 70.58 0.43 o 2 6 1 49.02 49.82 0.35 o 3 6 1 36.80 38.77 0.26 o 4 6 1 46.75 46.63 0.28 o 5 6 1 51.66 50.93 0.30 o 6 6 1 12.48 13.46 0.20 o 7 6 1 50.19 50.26 0.38 o 8 6 1 6.68 6.54 0.72 o 9 6 1 4.90 1.74 1.60 < -9 7 1 27.38 28.87 0.58 o -8 7 1 41.63 41.12 0.55 o -7 7 1 39.62 38.69 0.34 o -6 7 1 50.99 51.88 0.37 o -5 7 1 10.59 11.22 0.19 o -4 7 1 77.47 78.40 0.46 o -3 7 1 57.78 59.94 0.31 o -2 7 1 103.08 103.99 0.56 o -1 7 1 117.74 116.79 0.67 o 0 7 1 99.39 101.14 0.56 o 1 7 1 92.17 93.20 0.51 o 2 7 1 69.36 68.60 0.46 o 3 7 1 44.89 44.43 0.29 o 4 7 1 9.84 8.37 0.12 o 5 7 1 47.95 47.27 0.29 o 6 7 1 47.22 46.27 0.33 o 7 7 1 19.69 18.69 0.26 o 8 7 1 61.19 59.62 0.61 o 9 7 1 24.82 25.82 0.76 o -9 8 1 6.63 9.19 1.06 o -8 8 1 4.43 1.60 0.99 < -7 8 1 9.32 9.03 0.35 o -6 8 1 41.06 42.88 0.33 o -5 8 1 11.65 12.48 0.18 o -4 8 1 4.11 3.24 0.33 o -3 8 1 10.61 10.67 0.16 o -2 8 1 25.18 23.50 0.17 o -1 8 1 84.91 82.55 0.49 o 0 8 1 71.97 70.64 0.40 o 1 8 1 54.40 53.71 0.29 o 2 8 1 2.90 4.19 0.67 < 3 8 1 18.80 17.83 0.21 o 4 8 1 46.80 45.53 0.31 o 5 8 1 36.29 36.81 0.26 o 6 8 1 16.64 16.45 0.20 o 7 8 1 4.91 4.21 0.43 o 8 8 1 13.78 14.44 0.46 o -8 9 1 31.82 31.49 0.53 o -7 9 1 3.07 3.94 0.78 < -6 9 1 38.55 37.45 0.33 o -5 9 1 51.62 50.57 0.35 o -4 9 1 46.98 47.80 0.29 o -3 9 1 91.69 91.48 0.53 o -2 9 1 62.13 63.09 0.32 o -1 9 1 117.28 115.97 0.61 o 0 9 1 123.80 123.97 0.66 o 1 9 1 99.22 99.55 0.49 o 2 9 1 85.99 87.22 0.57 o 3 9 1 53.43 53.67 0.40 o 4 9 1 70.24 70.10 0.45 o 5 9 1 27.50 27.56 0.30 o 6 9 1 54.14 54.81 0.51 o 7 9 1 46.16 45.83 0.57 o 8 9 1 45.09 45.76 0.96 o -8 10 1 11.28 11.77 0.52 o -7 10 1 2.17 0.84 0.97 < -6 10 1 2.35 2.92 0.53 < -5 10 1 15.11 14.77 0.17 o -4 10 1 26.07 26.77 0.19 o -3 10 1 29.36 28.42 0.21 o -2 10 1 9.99 8.46 0.17 o -1 10 1 10.05 7.74 0.17 o 0 10 1 31.02 31.06 0.20 o 1 10 1 -0.71 2.35 2.83 < 2 10 1 28.47 29.27 0.19 o 3 10 1 44.50 43.87 0.35 o 4 10 1 2.66 2.18 0.66 < 5 10 1 36.14 34.85 0.35 o 6 10 1 7.89 8.46 0.55 o 7 10 1 3.89 1.27 1.72 < 8 10 1 3.42 4.38 2.46 < -8 11 1 7.52 7.72 1.20 o -7 11 1 8.02 7.32 0.69 o -6 11 1 33.92 33.97 0.39 o -5 11 1 77.55 77.84 0.57 o -4 11 1 75.49 76.03 0.42 o -3 11 1 60.43 60.35 0.36 o -2 11 1 51.24 52.66 0.31 o -1 11 1 28.92 29.65 0.19 o 0 11 1 31.01 32.30 0.20 o 1 11 1 76.52 77.02 0.41 o 2 11 1 40.90 41.39 0.26 o 3 11 1 90.50 92.92 0.63 o 4 11 1 52.89 53.95 0.41 o 5 11 1 23.65 24.28 0.34 o 6 11 1 17.76 17.40 0.51 o 7 11 1 30.98 29.07 0.63 o 8 11 1 11.11 11.20 1.08 o -8 12 1 6.36 6.20 1.32 < -7 12 1 -2.47 2.97 2.67 < -6 12 1 13.42 13.04 0.40 o -5 12 1 11.87 12.44 0.34 o -4 12 1 -2.02 1.44 1.36 < -3 12 1 5.25 3.28 0.24 o -2 12 1 28.41 27.18 0.21 o -1 12 1 13.58 12.31 0.20 o 0 12 1 16.45 15.79 0.16 o 1 12 1 31.95 31.41 0.20 o 2 12 1 17.67 17.71 0.17 o 3 12 1 56.99 55.63 0.41 o 4 12 1 61.35 61.78 0.49 o 5 12 1 1.92 1.96 1.92 < 6 12 1 17.13 16.04 0.67 o 7 12 1 13.99 11.41 0.67 o 8 12 1 -4.29 2.95 2.13 < -8 13 1 8.98 6.38 1.20 o -7 13 1 40.60 39.09 0.61 o -6 13 1 21.20 21.16 0.40 o -5 13 1 57.93 57.90 0.49 o -4 13 1 56.74 56.44 0.42 o -3 13 1 52.28 52.20 0.31 o -2 13 1 29.99 30.68 0.22 o -1 13 1 70.86 72.47 0.42 o 0 13 1 40.04 42.36 0.24 o 1 13 1 47.08 48.00 0.27 o 2 13 1 43.71 44.78 0.28 o 3 13 1 20.89 20.68 0.27 o 4 13 1 3.05 0.73 1.16 < 5 13 1 -2.77 0.01 1.48 < 6 13 1 13.48 14.20 0.78 o 7 13 1 12.93 14.90 0.74 o 8 13 1 25.54 27.73 0.99 o -7 14 1 5.08 4.36 1.44 < -6 14 1 27.18 26.53 0.47 o -5 14 1 16.20 16.14 0.35 o -4 14 1 50.44 51.30 0.40 o -3 14 1 50.86 51.21 0.32 o -2 14 1 1.82 1.53 0.83 < -1 14 1 2.77 3.17 0.63 < 0 14 1 26.69 24.32 0.20 o 1 14 1 23.19 21.97 0.18 o 2 14 1 39.35 36.66 0.27 o 3 14 1 10.71 11.60 0.39 o 4 14 1 26.02 25.85 0.36 o 5 14 1 25.31 24.64 0.42 o 6 14 1 18.48 18.05 0.62 o 7 14 1 8.41 8.19 1.10 o -7 15 1 33.54 32.78 0.60 o -6 15 1 30.71 31.05 0.47 o -5 15 1 37.28 36.57 0.44 o -4 15 1 38.90 40.47 0.39 o -3 15 1 44.26 44.08 0.33 o -2 15 1 57.32 58.46 0.35 o -1 15 1 37.08 38.01 0.25 o 0 15 1 84.51 85.31 0.46 o 1 15 1 69.81 70.19 0.39 o 2 15 1 91.11 90.80 0.53 o 3 15 1 19.61 19.31 0.33 o 4 15 1 35.44 35.37 0.46 o 5 15 1 17.26 17.24 0.50 o 6 15 1 31.96 32.01 0.58 o 7 15 1 35.87 34.35 0.72 o -7 16 1 17.10 15.92 0.87 o -6 16 1 13.71 13.07 0.58 o -5 16 1 10.62 10.83 0.63 o -4 16 1 1.87 0.81 3.05 < -3 16 1 10.99 11.53 0.22 o -2 16 1 17.05 16.85 0.20 o -1 16 1 48.73 48.47 0.32 o 0 16 1 12.07 11.93 0.21 o 1 16 1 25.99 26.57 0.22 o 2 16 1 9.01 9.22 0.25 o 3 16 1 15.08 15.99 0.39 o 4 16 1 20.31 20.61 0.40 o 5 16 1 2.45 5.98 2.29 < 6 16 1 6.10 2.97 1.79 < 7 16 1 4.10 5.69 3.10 < -7 17 1 39.03 39.55 0.89 o -6 17 1 37.01 37.22 0.57 o -5 17 1 46.39 45.25 0.62 o -4 17 1 23.77 24.09 0.42 o -3 17 1 43.31 42.20 0.34 o -2 17 1 43.80 42.52 0.30 o -1 17 1 22.44 20.29 0.23 o 0 17 1 53.31 51.21 0.33 o 1 17 1 64.24 63.73 0.39 o 2 17 1 44.33 43.40 0.35 o 3 17 1 28.18 27.47 0.37 o 4 17 1 31.05 31.29 0.45 o 5 17 1 8.15 8.12 0.82 o 6 17 1 32.23 32.93 0.69 o -6 18 1 4.10 2.69 2.76 < -5 18 1 18.55 18.56 0.64 o -4 18 1 14.19 13.54 0.52 o -3 18 1 3.38 2.71 0.62 < -2 18 1 31.62 32.09 0.29 o -1 18 1 10.20 10.53 0.28 o 0 18 1 24.76 24.46 0.25 o 1 18 1 27.28 27.64 0.24 o 2 18 1 5.34 6.48 0.43 o 3 18 1 16.38 16.26 0.49 o 4 18 1 9.96 10.33 0.67 o 5 18 1 8.58 8.40 0.77 o 6 18 1 -3.66 0.83 2.72 < -6 19 1 17.29 18.89 0.76 o -5 19 1 53.17 53.55 0.77 o -4 19 1 14.60 14.45 0.63 o -3 19 1 55.90 55.31 0.52 o -2 19 1 14.18 14.17 0.30 o -1 19 1 41.93 41.36 0.32 o 0 19 1 10.96 10.16 0.29 o 1 19 1 33.09 31.78 0.30 o 2 19 1 62.35 60.62 0.52 o 3 19 1 48.48 47.54 0.51 o 4 19 1 57.88 57.22 0.69 o 5 19 1 33.76 33.27 0.59 o 6 19 1 25.15 26.87 0.76 o -5 20 1 14.87 14.72 0.69 o -4 20 1 12.57 13.52 0.67 o -3 20 1 9.05 10.19 0.44 o -2 20 1 27.46 28.95 0.36 o -1 20 1 16.57 16.45 0.33 o 0 20 1 8.99 8.45 0.39 o 1 20 1 23.64 24.95 0.30 o 2 20 1 6.75 7.47 0.50 o 3 20 1 7.84 7.96 0.84 o 4 20 1 11.19 12.12 0.83 o 5 20 1 12.17 12.94 0.78 o -5 21 1 9.59 10.29 0.98 o -4 21 1 26.72 27.07 0.60 o -3 21 1 17.12 16.81 0.43 o -2 21 1 34.78 34.20 0.46 o -1 21 1 51.50 51.29 0.60 o 0 21 1 38.71 38.49 0.53 o 1 21 1 24.55 24.61 0.39 o 2 21 1 23.08 23.54 0.39 o 3 21 1 40.72 40.56 0.65 o 4 21 1 21.91 22.64 0.55 o 5 21 1 34.87 35.44 0.73 o -4 22 1 19.75 20.12 0.73 o -3 22 1 26.36 25.52 0.54 o -2 22 1 3.08 0.01 1.82 < -1 22 1 4.09 5.09 1.32 < 0 22 1 8.80 8.14 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