#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/25/2202536.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202536_Fobs loop_ _publ_author_name 'Jones, Matthew D.' 'Almeida Paz, Filipe A.' 'Davies, John E.' 'Johnson, Brian F. G.' 'Klinowski, Jacek' _publ_section_title ; (\h^3^-Allyl)[(R)-(+)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl]palladium(II) trifluoromethanesulfonate dichloromethane solvate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m538 _journal_page_last m540 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.1814 _cell_length_b 19.7359 _cell_length_c 20.3672 _exptl_crystal_F_000 2040.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file cm6046Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bj0319 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 297.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4316.12 4142.72 186.56 o 4 0 0 2021.89 1601.09 112.99 o 6 0 0 268.92 201.16 103.26 o 8 0 0 655.32 749.95 104.28 o 10 0 0 3598.57 3816.98 257.18 o 12 0 0 476.10 669.21 105.18 o 2 1 0 1892.05 1620.37 483.72 o 3 1 0 5066.85 5343.66 111.15 o 4 1 0 309.89 192.71 65.53 o 5 1 0 564.61 540.84 41.85 o 6 1 0 11887.25 12108.59 237.13 o 7 1 0 19.89 3.86 41.15 o 8 1 0 2373.77 2043.64 117.65 o 9 1 0 0.50 -41.14 45.14 o 10 1 0 4237.47 4462.81 234.47 o 11 1 0 0.42 243.22 113.37 o 12 1 0 1182.05 1611.69 136.71 o 13 1 0 7.19 57.01 81.87 o 2 2 0 75490.78 49627.72 13108.47 o 3 2 0 75903.64 73681.85 1566.00 o 4 2 0 9723.33 8935.80 191.23 o 5 2 0 0.55 122.69 53.23 o 6 2 0 16257.68 16412.72 314.19 o 7 2 0 159.75 208.64 41.99 o 8 2 0 11135.45 11197.58 252.91 o 9 2 0 421.64 502.00 58.07 o 10 2 0 252.76 214.71 827.78 o 11 2 0 1282.59 1174.16 135.38 o 12 2 0 562.03 684.51 87.58 o 13 2 0 0.65 -18.00 106.59 o 1 3 0 1265.86 983.50 381.57 o 2 3 0 3618.52 3903.44 93.92 o 3 3 0 3330.19 3190.85 82.11 o 4 3 0 1298.28 1243.58 45.47 o 5 3 0 814.74 758.32 42.89 o 6 3 0 15255.58 15141.56 318.42 o 7 3 0 1108.11 1010.45 51.23 o 8 3 0 1095.51 1089.55 54.17 o 9 3 0 327.37 322.07 58.32 o 10 3 0 682.39 667.18 65.49 o 11 3 0 2.45 138.85 110.05 o 12 3 0 1463.52 1474.69 138.20 o 13 3 0 203.54 53.80 91.49 o 0 4 0 28711.23 27483.62 825.76 o 1 4 0 484.83 505.34 22.25 o 2 4 0 204.02 309.33 60.69 o 3 4 0 9018.37 9496.21 184.29 o 4 4 0 6313.65 6320.49 125.01 o 5 4 0 587.84 700.01 43.51 o 6 4 0 23650.80 23453.15 447.19 o 7 4 0 2385.19 2238.28 78.47 o 8 4 0 4411.46 3924.14 117.45 o 9 4 0 89.43 136.26 65.34 o 10 4 0 1011.02 1105.20 93.34 o 11 4 0 7.82 54.92 61.43 o 12 4 0 30.18 -77.64 77.64 o 13 4 0 14.33 68.58 82.30 o 1 5 0 56.50 123.47 14.19 o 2 5 0 502.90 687.24 46.59 o 3 5 0 14744.47 14453.82 277.00 o 4 5 0 672.19 912.83 37.99 o 5 5 0 107.80 41.67 32.93 o 6 5 0 781.75 835.29 50.85 o 7 5 0 235.00 222.66 71.66 o 8 5 0 1423.47 1561.13 94.91 o 9 5 0 548.45 511.08 58.69 o 10 5 0 2935.36 2643.48 123.26 o 11 5 0 643.00 554.60 77.98 o 12 5 0 778.77 1088.59 190.02 o 0 6 0 62227.06 57725.19 2327.17 o 1 6 0 223.98 341.55 42.73 o 2 6 0 26598.33 27211.93 477.63 o 3 6 0 9191.03 9427.06 192.43 o 4 6 0 53.84 66.64 63.75 o 5 6 0 2640.98 2714.95 64.94 o 6 6 0 1211.21 1385.33 50.90 o 7 6 0 140.88 60.26 43.87 o 8 6 0 4439.84 4372.32 208.18 o 9 6 0 1983.10 1985.38 102.35 o 10 6 0 3867.42 3979.04 145.07 o 11 6 0 88.97 170.89 60.39 o 12 6 0 313.30 159.29 91.87 o 1 7 0 18320.61 17385.05 266.61 o 2 7 0 2520.33 2680.70 60.51 o 3 7 0 810.24 766.12 40.34 o 4 7 0 854.51 1187.55 43.40 o 5 7 0 5877.12 6674.21 136.88 o 6 7 0 62.34 198.78 58.18 o 7 7 0 157.44 290.37 98.41 o 8 7 0 1313.81 1512.17 98.25 o 9 7 0 2575.07 2520.59 101.65 o 10 7 0 2539.44 2865.46 130.41 o 11 7 0 669.57 912.69 226.40 o 12 7 0 826.39 1192.65 193.60 o 0 8 0 2348.71 2346.91 65.57 o 1 8 0 12258.72 12539.05 206.46 o 2 8 0 12160.64 12033.66 200.67 o 3 8 0 4060.19 4389.22 72.04 o 4 8 0 12055.78 11927.93 206.59 o 5 8 0 1496.58 1476.54 50.49 o 6 8 0 6601.93 6530.01 156.38 o 7 8 0 29.22 15.54 45.06 o 8 8 0 2815.94 2877.89 92.93 o 9 8 0 2783.64 2790.89 95.39 o 10 8 0 1758.93 1929.08 147.48 o 11 8 0 24.36 85.58 160.79 o 12 8 0 230.27 253.77 102.05 o 1 9 0 7.50 167.84 48.79 o 2 9 0 749.19 834.77 59.14 o 3 9 0 17436.42 17136.75 270.41 o 4 9 0 2201.47 2041.52 51.41 o 5 9 0 3857.03 3627.48 82.37 o 6 9 0 51.26 47.54 26.45 o 7 9 0 9183.70 9246.65 239.99 o 8 9 0 677.98 709.95 56.88 o 9 9 0 662.18 736.82 67.48 o 10 9 0 3040.96 3184.59 145.28 o 11 9 0 542.75 643.21 140.99 o 12 9 0 571.38 463.63 117.23 o 0 10 0 751.38 839.41 31.61 o 1 10 0 6834.98 7419.15 140.20 o 2 10 0 3776.14 4164.64 125.86 o 3 10 0 977.85 1126.58 33.65 o 4 10 0 6524.35 6486.85 113.91 o 5 10 0 56.52 46.77 18.81 o 6 10 0 1125.85 1094.73 79.30 o 7 10 0 2259.75 2283.15 76.66 o 8 10 0 1152.60 1119.57 91.66 o 9 10 0 697.18 671.02 52.26 o 10 10 0 2105.28 2125.45 126.03 o 11 10 0 1192.29 1208.89 94.15 o 12 10 0 0.84 -15.34 64.55 o 1 11 0 1325.84 1307.12 37.82 o 2 11 0 246.08 269.42 47.78 o 3 11 0 5587.24 4992.75 114.97 o 4 11 0 1035.67 1084.44 31.11 o 5 11 0 6024.57 6060.56 114.21 o 6 11 0 2400.87 2363.45 72.52 o 7 11 0 2504.70 2718.37 117.21 o 8 11 0 1121.27 1026.54 54.17 o 9 11 0 2471.13 2672.58 123.96 o 10 11 0 345.56 417.94 70.87 o 11 11 0 264.98 371.04 178.50 o 0 12 0 606.93 505.36 34.63 o 1 12 0 1011.76 842.32 46.08 o 2 12 0 902.41 781.66 62.57 o 3 12 0 252.46 280.18 56.29 o 4 12 0 2666.96 2785.09 73.58 o 5 12 0 61.24 56.15 39.16 o 6 12 0 2422.48 2449.38 73.97 o 7 12 0 402.03 360.75 112.83 o 8 12 0 165.45 139.67 42.59 o 9 12 0 3530.03 3699.07 145.58 o 10 12 0 1482.39 1826.02 155.71 o 11 12 0 1764.08 1985.52 172.10 o 1 13 0 8727.27 8734.68 156.98 o 2 13 0 3318.23 3239.57 84.33 o 3 13 0 1515.99 1493.31 59.64 o 4 13 0 562.92 509.86 59.83 o 5 13 0 2260.29 2047.89 47.85 o 6 13 0 1352.20 1351.56 45.29 o 7 13 0 1585.06 1325.60 410.76 o 8 13 0 2.58 -10.61 32.59 o 9 13 0 1852.69 1804.01 106.75 o 10 13 0 6.51 -39.17 62.37 o 11 13 0 987.77 799.73 162.76 o 0 14 0 29.18 -22.79 22.79 o 1 14 0 589.64 544.36 64.74 o 2 14 0 434.29 294.63 74.30 o 3 14 0 147.20 224.71 36.19 o 4 14 0 2548.91 2705.99 91.30 o 5 14 0 1242.15 1400.20 78.15 o 6 14 0 746.07 672.80 31.19 o 7 14 0 598.76 520.76 47.99 o 8 14 0 40.71 50.20 61.32 o 9 14 0 1091.38 1325.58 84.80 o 10 14 0 5.12 341.39 118.24 o 1 15 0 4956.66 4623.72 106.01 o 2 15 0 370.72 340.12 71.89 o 3 15 0 4574.59 4476.81 127.34 o 4 15 0 27.53 41.90 37.12 o 5 15 0 2140.26 2306.04 105.39 o 6 15 0 613.47 558.37 59.62 o 7 15 0 3734.96 4223.63 148.82 o 8 15 0 133.93 248.10 295.78 o 9 15 0 396.61 432.84 205.88 o 10 15 0 30.01 148.10 105.31 o 0 16 0 20.20 29.49 19.31 o 1 16 0 53.53 37.12 65.05 o 2 16 0 352.24 324.29 51.77 o 3 16 0 1104.43 969.63 85.22 o 4 16 0 1003.95 915.54 67.71 o 5 16 0 900.64 947.86 84.88 o 6 16 0 73.76 149.19 84.99 o 7 16 0 946.31 1077.38 83.87 o 8 16 0 261.99 174.44 88.86 o 9 16 0 880.51 880.06 115.12 o 1 17 0 7405.12 7737.51 189.24 o 2 17 0 35.35 24.22 32.01 o 3 17 0 3445.93 3293.30 149.04 o 4 17 0 1897.63 1862.96 101.12 o 5 17 0 2031.81 2187.54 116.83 o 6 17 0 18.09 344.82 66.70 o 7 17 0 1138.27 1420.49 292.12 o 8 17 0 27.93 114.08 111.68 o 9 17 0 3.86 214.01 147.56 o 0 18 0 56.45 113.33 31.77 o 1 18 0 946.39 1133.22 46.60 o 2 18 0 2.52 -39.36 45.05 o 3 18 0 3591.79 3636.41 180.86 o 4 18 0 721.44 802.37 80.87 o 5 18 0 691.44 628.49 83.47 o 6 18 0 1758.06 1749.84 172.55 o 7 18 0 805.11 948.68 98.24 o 8 18 0 409.17 598.28 114.27 o 1 19 0 5196.68 5232.71 197.63 o 2 19 0 7.30 -17.96 37.93 o 3 19 0 1778.30 1893.41 83.71 o 4 19 0 175.04 170.39 59.82 o 5 19 0 914.36 1003.00 76.49 o 6 19 0 3.46 70.68 100.42 o 7 19 0 586.13 1022.45 127.98 o 0 20 0 641.13 799.22 158.67 o 1 20 0 354.61 431.10 72.36 o 2 20 0 610.87 592.63 95.32 o 3 20 0 542.97 478.19 248.49 o 4 20 0 463.83 486.84 93.76 o 5 20 0 2565.85 2793.09 150.33 o 6 20 0 157.91 134.76 94.94 o 1 21 0 2230.42 2547.10 244.65 o 2 21 0 504.78 442.64 211.51 o 3 21 0 695.73 904.10 272.80 o 4 21 0 550.75 508.79 191.93 o 5 21 0 430.29 205.18 82.53 o 0 22 0 1614.63 1263.95 218.29 o 1 22 0 7.00 392.57 174.79 o 2 22 0 1442.56 1562.35 206.78 o 3 22 0 131.50 458.60 150.22 o 4 22 0 744.27 656.93 203.71 o 1 23 0 1234.95 1160.05 193.73 o 2 23 0 1105.18 918.98 145.10 o 2 0 1 2313.54 2320.62 837.97 o 3 0 1 44435.42 43945.05 828.12 o 4 0 1 3792.94 3595.87 82.01 o 5 0 1 2567.93 2460.02 74.25 o 6 0 1 3439.21 3266.69 84.23 o 7 0 1 7741.51 7606.76 190.71 o 8 0 1 557.77 370.37 50.75 o 9 0 1 1494.50 1360.36 62.43 o 10 0 1 2545.93 2836.02 136.54 o 11 0 1 36.96 48.98 78.82 o 12 0 1 989.27 1128.04 311.83 o 13 0 1 69.93 76.92 106.46 o -13 1 1 486.60 609.43 124.76 o -12 1 1 277.67 90.46 257.19 o -11 1 1 30.97 69.95 77.01 o -10 1 1 1069.73 1045.32 67.30 o -9 1 1 774.87 766.03 70.72 o -8 1 1 2820.40 2567.40 107.19 o -7 1 1 4657.21 4770.42 119.56 o -6 1 1 12934.65 12569.19 254.73 o -5 1 1 1821.15 1879.21 122.08 o -4 1 1 11902.75 11218.51 235.29 o -3 1 1 3572.39 3989.16 83.76 o -2 1 1 17354.27 18264.01 554.07 o 2 1 1 16129.30 9617.96 8474.30 o 3 1 1 3076.52 3352.67 84.77 o 4 1 1 11494.07 11000.26 205.59 o 5 1 1 1499.40 1551.27 109.93 o 6 1 1 13111.00 12674.30 251.26 o 7 1 1 4745.61 4931.31 114.67 o 8 1 1 2758.71 2677.18 88.40 o 9 1 1 867.97 721.24 47.39 o 10 1 1 1084.65 1090.67 82.37 o 11 1 1 20.92 -73.11 105.18 o 12 1 1 292.00 325.99 148.56 o 13 1 1 482.77 362.93 116.94 o -13 2 1 180.99 466.80 128.73 o -12 2 1 1837.59 1917.63 159.42 o -11 2 1 354.06 326.83 157.13 o -10 2 1 554.79 561.52 52.43 o -9 2 1 12.12 136.96 58.47 o -8 2 1 91.14 61.80 50.04 o -7 2 1 2041.23 2082.44 68.23 o -6 2 1 4095.05 4011.42 111.74 o -5 2 1 12580.64 12509.09 261.21 o -4 2 1 15255.10 15072.65 282.34 o -3 2 1 913.83 863.81 45.47 o -2 2 1 25299.14 22076.85 1745.70 o 2 2 1 25090.67 22706.13 1801.49 o 3 2 1 847.39 924.51 54.48 o 4 2 1 15244.93 15146.67 294.60 o 5 2 1 12778.46 12275.70 244.87 o 6 2 1 4261.63 4185.27 105.24 o 7 2 1 2190.72 2294.05 89.62 o 8 2 1 142.82 196.76 44.25 o 9 2 1 8.53 135.64 65.23 o 10 2 1 500.76 514.39 1125.20 o 11 2 1 347.09 314.01 159.43 o 12 2 1 1860.51 1630.82 130.65 o 13 2 1 196.10 151.03 133.20 o -13 3 1 209.17 203.41 206.78 o -12 3 1 763.19 1064.75 152.14 o -11 3 1 179.42 114.53 62.72 o -10 3 1 916.89 866.85 171.17 o -9 3 1 810.88 862.58 80.38 o -8 3 1 4606.03 4653.74 176.55 o -7 3 1 2783.65 2679.17 92.97 o -6 3 1 9122.68 9402.44 192.89 o -5 3 1 4077.54 4216.21 94.86 o -4 3 1 9603.52 9600.21 178.76 o -3 3 1 1042.58 1188.65 68.04 o -2 3 1 88283.07 83035.98 3239.40 o -1 3 1 23278.68 12055.09 8009.48 o 1 3 1 23406.81 6529.67 6441.96 o 2 3 1 86771.64 81394.84 2559.24 o 3 3 1 821.87 907.70 65.31 o 4 3 1 9825.04 9880.48 187.88 o 5 3 1 3886.84 3890.73 111.16 o 6 3 1 8976.29 9541.27 187.58 o 7 3 1 2793.39 2885.10 99.81 o 8 3 1 4640.50 4655.10 161.03 o 9 3 1 881.17 884.26 113.88 o 10 3 1 832.82 894.98 74.59 o 11 3 1 150.60 123.72 62.71 o 12 3 1 824.33 1040.75 141.61 o 13 3 1 197.85 448.23 263.97 o -13 4 1 585.27 482.79 84.14 o -12 4 1 2045.70 2022.99 142.76 o -11 4 1 1293.79 1458.06 97.51 o -10 4 1 664.13 503.80 72.84 o -9 4 1 89.38 138.49 103.54 o -8 4 1 1032.04 1122.84 68.11 o -7 4 1 1644.50 1738.21 66.67 o -6 4 1 2047.74 2076.32 65.74 o -5 4 1 3808.96 3814.28 88.49 o -4 4 1 5789.65 5653.18 162.99 o -3 4 1 15128.07 14628.96 274.57 o -2 4 1 25046.69 25095.58 437.65 o -1 4 1 14426.54 14529.25 267.74 o 0 4 1 14394.64 14303.38 278.40 o 1 4 1 14894.48 14459.35 250.18 o 2 4 1 25327.17 24841.03 479.43 o 3 4 1 15197.30 15115.21 299.09 o 4 4 1 5898.37 5827.56 160.16 o 5 4 1 4024.04 4069.05 94.13 o 6 4 1 1998.08 2088.60 65.66 o 7 4 1 1693.36 1654.33 87.51 o 8 4 1 885.12 883.55 56.09 o 9 4 1 66.08 164.04 64.79 o 10 4 1 601.97 562.26 126.49 o 11 4 1 1299.88 1312.58 92.89 o 12 4 1 2098.74 2195.93 231.09 o 13 4 1 600.15 496.16 201.28 o -12 5 1 277.77 348.06 109.40 o -11 5 1 20.22 76.04 79.79 o -10 5 1 2027.46 2019.42 145.97 o -9 5 1 3279.24 3210.20 106.64 o -8 5 1 1638.12 1521.61 101.87 o -7 5 1 4763.97 4899.64 122.98 o -6 5 1 3357.43 3260.67 87.13 o -5 5 1 9655.06 9467.88 196.08 o -4 5 1 13982.04 13694.25 260.71 o -3 5 1 5769.51 5829.23 115.65 o -2 5 1 23602.75 23198.55 396.06 o -1 5 1 13425.75 13737.08 234.58 o 0 5 1 50606.62 48883.82 819.79 o 1 5 1 13935.97 13916.68 240.79 o 2 5 1 23223.81 22563.85 402.10 o 3 5 1 6062.44 6122.96 127.23 o 4 5 1 14043.94 14062.58 276.21 o 5 5 1 9595.62 9491.71 219.26 o 6 5 1 3420.92 3352.50 84.99 o 7 5 1 4829.02 4780.17 117.78 o 8 5 1 1516.98 1238.13 166.63 o 9 5 1 3225.80 3489.61 127.02 o 10 5 1 1996.98 2093.94 100.91 o 11 5 1 30.55 44.42 54.41 o 12 5 1 317.75 129.25 87.03 o -12 6 1 794.73 780.97 121.52 o -11 6 1 878.86 1001.88 105.74 o -10 6 1 1405.17 1384.83 172.61 o -9 6 1 4770.22 4964.73 141.60 o -8 6 1 1843.86 1710.08 70.41 o -7 6 1 1327.44 1339.12 93.53 o -6 6 1 726.18 728.48 42.62 o -5 6 1 311.96 240.68 32.62 o -4 6 1 4049.76 3858.28 86.18 o -3 6 1 8137.34 7955.89 586.98 o -2 6 1 10033.99 9932.10 197.33 o -1 6 1 19513.00 19382.39 282.46 o 0 6 1 4810.69 4776.01 67.89 o 1 6 1 18927.13 18557.20 296.07 o 2 6 1 10274.84 10151.50 162.85 o 3 6 1 7787.90 7605.87 159.57 o 4 6 1 4040.79 3940.81 85.86 o 5 6 1 232.90 219.50 36.69 o 6 6 1 793.65 825.73 77.64 o 7 6 1 1425.60 1473.06 65.42 o 8 6 1 1698.98 1662.99 88.43 o 9 6 1 4918.89 4975.73 144.89 o 10 6 1 1320.20 1265.29 89.17 o 11 6 1 812.63 821.32 75.59 o 12 6 1 820.21 939.07 112.73 o -12 7 1 145.51 201.17 116.31 o -11 7 1 190.63 125.67 58.34 o -10 7 1 577.23 524.18 84.97 o -9 7 1 4627.49 4630.94 151.42 o -8 7 1 5097.35 4829.57 133.87 o -7 7 1 2901.74 2629.79 91.26 o -6 7 1 3020.27 2843.04 77.56 o -5 7 1 5260.33 5041.07 110.04 o -4 7 1 4799.95 5066.02 98.75 o -3 7 1 3564.81 3566.11 72.11 o -2 7 1 6737.96 6850.82 128.95 o -1 7 1 405.03 409.98 37.88 o 0 7 1 461.71 502.29 32.42 o 1 7 1 357.26 357.88 19.81 o 2 7 1 6386.56 6441.35 96.60 o 3 7 1 3637.53 3712.51 67.39 o 4 7 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