#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:01:49 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180945 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/25/2202537.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202537_Fobs loop_ _publ_author_name 'Zhang, Yun-Qian' 'Xu, Duan-Jun' 'Su, Jian-Rong' _publ_section_title ; \m~4~-Oxo-hexa-\m~2~-chloro-tetrakis[(benzimidazole-\kN)copper(II)] ethanol disolvate: a reformulation ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m919 _journal_page_last m920 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 68.062 _cell_angle_beta 74.315 _cell_angle_gamma 71.376 _cell_length_a 13.0005 _cell_length_b 13.2362 _cell_length_c 13.8867 _exptl_crystal_F_000 1052.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file cm6047Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yq3 in p -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 306.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5981.45 9.19 3.48 o 2 0 0 2270.45 4066.21 105.51 o 3 0 0 9396.61 10054.34 63.64 o 4 0 0 2597.63 3063.66 89.90 o 5 0 0 621.38 844.03 19.15 o 6 0 0 10327.79 11051.41 42.39 o 7 0 0 118.99 147.67 11.63 o 8 0 0 9934.07 10231.76 185.19 o 9 0 0 1118.53 1034.98 18.70 o 10 0 0 11021.06 11455.99 146.28 o 11 0 0 137.90 212.26 23.01 o 12 0 0 2.97 3.05 23.55 o 13 0 0 530.17 514.06 38.28 o 14 0 0 606.14 682.67 28.64 o 15 0 0 29.83 68.68 28.52 o -15 1 0 2.11 40.01 29.83 o -14 1 0 382.07 365.25 20.30 o -13 1 0 99.70 38.55 36.42 o -12 1 0 129.75 151.28 23.30 o -11 1 0 47.49 55.92 25.38 o -10 1 0 466.17 462.25 53.35 o -9 1 0 59.16 76.75 26.72 o -8 1 0 7126.22 7481.78 104.90 o -7 1 0 230.77 242.76 28.73 o -6 1 0 2475.13 2570.16 14.02 o -5 1 0 2428.33 2484.43 30.52 o -4 1 0 4922.92 4737.83 104.96 o -3 1 0 1019.23 1016.30 7.86 o -2 1 0 2179.87 1571.35 7.51 o -1 1 0 25300.82 25333.08 209.41 o 0 1 0 22269.86 5.92 2.44 o 1 1 0 11542.53 26.67 13.31 o 2 1 0 42994.11 46967.96 1650.97 o 3 1 0 90.01 233.54 10.89 o 4 1 0 282.05 484.39 22.31 o 5 1 0 5677.81 6124.85 41.20 o 6 1 0 359.03 362.94 24.14 o 7 1 0 2069.77 1996.66 31.28 o 8 1 0 846.13 953.96 18.60 o 9 1 0 7056.38 7421.16 160.74 o 10 1 0 2288.81 2360.49 23.97 o 11 1 0 717.46 831.93 30.60 o 12 1 0 12.22 1.75 18.92 o 13 1 0 1278.10 1430.90 41.61 o 14 1 0 523.55 542.05 52.82 o 15 1 0 1.87 -56.01 56.01 o -15 2 0 98.07 109.45 26.53 o -14 2 0 160.00 148.31 23.77 o -13 2 0 21.62 14.82 32.60 o -12 2 0 167.98 179.49 17.79 o -11 2 0 980.42 1006.13 34.04 o -10 2 0 194.43 208.42 20.58 o -9 2 0 106.99 154.65 23.24 o -8 2 0 4207.59 4610.04 20.63 o -7 2 0 1057.94 1016.09 14.19 o -6 2 0 1505.66 1527.39 14.39 o -5 2 0 12119.75 12116.03 334.47 o -4 2 0 2058.39 1737.14 31.00 o -3 2 0 5.84 79.87 22.38 o -2 2 0 9140.99 11790.39 32.87 o -1 2 0 1764.07 2244.22 8.53 o 0 2 0 7682.82 8738.67 170.00 o 1 2 0 64.27 271.42 7.44 o 2 2 0 1429.15 1331.88 31.00 o 3 2 0 8887.34 10854.77 20.33 o 4 2 0 2.55 503.01 13.13 o 5 2 0 2428.55 2752.21 161.52 o 6 2 0 2426.13 3122.86 15.07 o 7 2 0 459.11 589.01 14.16 o 8 2 0 1021.08 1144.29 41.48 o 9 2 0 1751.51 1766.68 20.60 o 10 2 0 1040.39 1106.86 21.88 o 11 2 0 3202.19 3165.84 88.02 o 12 2 0 47.63 40.49 22.31 o 13 2 0 646.95 696.30 49.41 o 14 2 0 362.48 415.27 23.09 o 15 2 0 1.56 21.09 31.67 o 16 2 0 77.40 62.71 32.62 o -14 3 0 2.69 22.28 31.15 o -13 3 0 106.05 105.06 21.48 o -12 3 0 367.12 385.93 17.42 o -11 3 0 507.44 495.50 19.18 o -10 3 0 331.75 344.91 14.86 o -9 3 0 23.43 34.96 13.10 o -8 3 0 4395.30 4401.66 40.59 o -7 3 0 2639.97 2542.83 22.09 o -6 3 0 3560.46 3358.10 87.79 o -5 3 0 5203.02 5011.28 21.35 o -4 3 0 772.26 833.50 15.99 o -3 3 0 378.50 396.48 13.04 o -2 3 0 25242.57 28947.81 87.79 o -1 3 0 29690.02 31985.04 126.26 o 0 3 0 10182.38 11527.41 24.55 o 1 3 0 1859.29 1775.17 11.93 o 2 3 0 22.27 124.78 17.74 o 3 3 0 1749.38 2128.06 24.45 o 4 3 0 7718.57 8793.36 27.44 o 5 3 0 1923.46 2533.53 82.35 o 6 3 0 20189.38 22544.07 189.34 o 7 3 0 1645.74 1616.94 25.07 o 8 3 0 32.94 71.37 15.57 o 9 3 0 2.88 6.94 16.56 o 10 3 0 411.28 501.18 18.54 o 11 3 0 484.73 479.06 20.30 o 12 3 0 381.95 386.19 35.99 o 13 3 0 245.16 224.97 23.95 o 14 3 0 6.64 40.93 23.71 o 15 3 0 160.46 154.39 24.91 o 16 3 0 546.99 486.78 52.81 o -14 4 0 8.56 -23.20 23.20 o -13 4 0 2.00 -8.16 24.77 o -12 4 0 71.45 110.58 20.76 o -11 4 0 57.19 63.90 19.00 o -10 4 0 440.64 419.71 19.41 o -9 4 0 146.23 151.83 16.00 o -8 4 0 2113.00 2119.06 25.50 o -7 4 0 752.81 781.06 16.46 o -6 4 0 25.71 79.16 15.62 o -5 4 0 897.18 964.39 25.17 o -4 4 0 204.85 210.41 11.92 o -3 4 0 284.38 358.98 10.04 o -2 4 0 8491.32 10610.52 382.50 o -1 4 0 3730.10 4094.09 29.45 o 0 4 0 14491.89 16399.09 136.32 o 1 4 0 162.21 318.92 15.01 o 2 4 0 3892.74 5389.09 44.05 o 3 4 0 788.06 761.21 81.24 o 4 4 0 4319.65 4501.17 61.43 o 5 4 0 254.13 258.25 17.43 o 6 4 0 2192.91 2334.27 18.56 o 7 4 0 2548.48 2595.58 24.91 o 8 4 0 38.39 64.37 17.00 o 9 4 0 713.52 808.45 38.20 o 10 4 0 128.85 168.26 19.30 o 11 4 0 459.36 446.29 31.50 o 12 4 0 14.31 40.81 22.60 o 13 4 0 417.31 448.56 23.90 o 14 4 0 410.48 412.62 46.81 o 15 4 0 316.85 297.37 25.72 o 16 4 0 583.60 602.50 63.13 o -13 5 0 2.09 17.43 20.68 o -12 5 0 763.88 714.82 21.30 o -11 5 0 648.02 690.96 27.86 o -10 5 0 70.45 74.88 33.23 o -9 5 0 37.62 43.23 16.91 o -8 5 0 391.81 374.78 20.12 o -7 5 0 801.71 837.67 26.49 o -6 5 0 7977.11 7909.10 53.33 o -5 5 0 2676.52 2557.06 35.85 o -4 5 0 981.77 953.55 24.67 o -3 5 0 540.56 593.58 36.93 o -2 5 0 16353.98 18345.20 293.53 o -1 5 0 3839.53 3951.44 17.45 o 0 5 0 124.00 146.12 18.10 o 1 5 0 657.79 887.87 23.21 o 2 5 0 7812.34 7637.96 222.61 o 3 5 0 1484.91 1403.08 17.18 o 4 5 0 5238.23 5894.12 140.34 o 5 5 0 3324.18 3222.55 78.04 o 6 5 0 31.15 43.76 18.34 o 7 5 0 1410.57 1664.68 40.67 o 8 5 0 2040.42 1942.19 26.98 o 9 5 0 226.53 236.70 32.57 o 10 5 0 432.59 484.07 27.18 o 11 5 0 139.08 223.44 57.30 o 12 5 0 3872.76 3963.22 37.21 o 13 5 0 1999.03 2077.70 34.39 o 14 5 0 26.64 9.40 26.02 o 15 5 0 2.03 -0.79 32.10 o 16 5 0 13.80 16.10 34.16 o -13 6 0 84.29 80.60 38.04 o -12 6 0 282.78 336.49 28.08 o -11 6 0 309.95 298.17 21.00 o -10 6 0 314.73 342.57 19.73 o -9 6 0 140.83 142.77 18.03 o -8 6 0 303.53 280.85 24.23 o -7 6 0 3922.95 3794.97 25.31 o -6 6 0 1876.08 1832.13 26.36 o -5 6 0 1538.33 1401.66 23.73 o -4 6 0 3128.49 2939.55 48.99 o -3 6 0 220.43 292.46 40.49 o -2 6 0 14688.82 15588.94 87.12 o -1 6 0 1715.88 1538.45 29.61 o 0 6 0 1644.19 1862.39 82.83 o 1 6 0 9333.47 9629.90 26.08 o 2 6 0 3511.73 3539.77 20.95 o 3 6 0 1278.16 1535.80 117.70 o 4 6 0 7988.73 7959.78 74.89 o 5 6 0 1663.60 1891.06 27.75 o 6 6 0 3407.10 3475.15 35.38 o 7 6 0 3088.47 3196.37 28.11 o 8 6 0 6245.66 6089.80 30.30 o 9 6 0 202.07 215.92 25.31 o 10 6 0 279.74 307.15 32.52 o 11 6 0 8583.40 8367.52 96.77 o 12 6 0 5085.02 4943.03 61.75 o 13 6 0 139.88 147.94 27.70 o 14 6 0 888.13 868.61 36.32 o 15 6 0 13.44 7.81 49.34 o 16 6 0 3.13 -1.06 39.55 o -12 7 0 125.79 155.35 22.82 o -11 7 0 28.66 30.59 21.51 o -10 7 0 603.01 610.87 27.27 o -9 7 0 406.24 446.63 21.14 o -8 7 0 349.62 373.30 18.60 o -7 7 0 199.29 240.41 21.89 o -6 7 0 1186.73 1187.54 33.11 o -5 7 0 1162.27 1137.39 24.19 o -4 7 0 5.69 15.71 21.51 o -3 7 0 60.11 83.17 19.18 o -2 7 0 3005.90 2822.72 27.31 o -1 7 0 2201.47 2341.45 21.04 o 0 7 0 208.79 236.57 23.00 o 1 7 0 5674.69 5793.06 34.09 o 2 7 0 1985.19 2530.14 63.39 o 3 7 0 4861.97 4756.95 37.55 o 4 7 0 5.50 5.23 26.24 o 5 7 0 456.88 527.09 47.35 o 6 7 0 44.20 34.09 23.34 o 7 7 0 6370.61 6713.53 186.35 o 8 7 0 1862.83 1804.83 67.31 o 9 7 0 1046.26 1100.73 44.12 o 10 7 0 209.24 237.65 32.60 o 11 7 0 2766.72 2730.10 67.62 o 12 7 0 110.02 64.92 36.48 o 13 7 0 786.35 792.98 34.56 o 14 7 0 122.52 103.69 32.57 o 15 7 0 93.12 154.70 31.16 o -11 8 0 9.81 36.82 22.54 o -10 8 0 207.52 164.67 22.18 o -9 8 0 577.37 579.14 21.77 o -8 8 0 170.41 172.73 30.90 o -7 8 0 11.67 -22.18 35.38 o -6 8 0 181.11 183.01 28.99 o -5 8 0 3097.79 3018.34 29.24 o -4 8 0 1.52 16.56 16.01 o -3 8 0 881.85 921.05 43.53 o -2 8 0 0.41 43.80 21.07 o -1 8 0 995.46 967.30 65.92 o 0 8 0 11024.13 11137.82 262.17 o 1 8 0 2280.50 2143.83 44.31 o 2 8 0 200.17 223.86 22.32 o 3 8 0 67.81 101.88 23.07 o 4 8 0 626.92 590.61 24.85 o 5 8 0 2797.29 2782.37 28.09 o 6 8 0 1482.39 1620.19 28.08 o 7 8 0 967.61 843.08 61.17 o 8 8 0 258.53 306.33 31.57 o 9 8 0 1578.06 1398.84 27.33 o 10 8 0 1009.24 1089.43 35.60 o 11 8 0 991.59 904.47 30.00 o 12 8 0 379.94 458.29 32.96 o 13 8 0 12.34 4.37 41.39 o 14 8 0 0.30 40.86 53.37 o 15 8 0 90.11 132.40 82.42 o -10 9 0 95.17 86.35 27.03 o -9 9 0 177.45 241.29 48.60 o -8 9 0 250.68 271.69 35.22 o -7 9 0 418.03 403.42 39.20 o -6 9 0 2531.68 2481.03 80.87 o -5 9 0 1120.42 1119.56 33.11 o -4 9 0 614.36 604.72 23.27 o -3 9 0 4367.91 4639.16 221.63 o -2 9 0 164.17 165.94 34.40 o -1 9 0 2090.25 2124.35 64.32 o 0 9 0 4318.73 4172.53 29.81 o 1 9 0 265.86 346.85 29.71 o 2 9 0 1471.96 1460.46 36.49 o 3 9 0 15.73 78.34 27.24 o 4 9 0 3141.93 3071.15 113.94 o 5 9 0 2112.69 2179.14 50.24 o 6 9 0 504.49 555.99 29.17 o 7 9 0 75.79 88.11 30.48 o 8 9 0 0.36 -17.81 31.27 o 9 9 0 2223.30 2067.14 57.30 o 10 9 0 3163.58 3021.35 171.49 o 11 9 0 434.63 497.35 31.27 o 12 9 0 0.21 79.81 30.67 o 13 9 0 13.52 5.34 32.60 o 14 9 0 168.47 157.48 46.04 o 15 9 0 15.06 65.27 45.89 o -9 10 0 18.22 79.75 27.76 o -8 10 0 500.33 429.13 30.53 o -7 10 0 46.49 56.29 32.55 o -6 10 0 435.68 356.43 25.02 o -5 10 0 138.55 26.92 43.74 o -4 10 0 2400.65 2416.18 25.38 o -3 10 0 937.69 1087.63 29.27 o -2 10 0 153.75 172.12 27.68 o -1 10 0 151.74 190.88 55.45 o 0 10 0 523.44 555.04 29.33 o 1 10 0 689.33 683.29 30.55 o 2 10 0 466.57 466.03 44.00 o 3 10 0 619.91 617.83 31.07 o 4 10 0 903.48 1036.07 31.69 o 5 10 0 51.40 92.75 40.13 o 6 10 0 2005.77 2055.70 51.17 o 7 10 0 142.58 164.72 73.29 o 8 10 0 14.33 -19.52 34.17 o 9 10 0 381.19 329.99 36.72 o 10 10 0 83.83 104.24 31.41 o 11 10 0 215.75 247.59 32.65 o 12 10 0 40.72 59.82 32.69 o 13 10 0 79.49 41.21 45.12 o 14 10 0 196.00 249.04 47.88 o -8 11 0 846.07 799.77 39.92 o -7 11 0 4.26 -19.67 42.50 o -6 11 0 5.48 -25.76 25.76 o -5 11 0 949.40 946.01 39.36 o -4 11 0 1866.74 1898.07 94.85 o -3 11 0 11.17 42.33 46.16 o -2 11 0 959.02 950.22 64.37 o -1 11 0 1485.70 1467.69 33.87 o 0 11 0 1973.51 1959.73 38.37 o 1 11 0 29.68 -5.54 57.25 o 2 11 0 1208.33 1248.14 56.68 o 3 11 0 14.34 56.89 40.01 o 4 11 0 348.25 341.58 33.99 o 5 11 0 4215.77 4187.70 42.74 o 6 11 0 7271.07 7187.72 145.61 o 7 11 0 273.16 272.15 71.80 o 8 11 0 1271.47 1207.32 40.33 o 9 11 0 376.84 311.85 38.55 o 10 11 0 101.70 88.44 125.85 o 11 11 0 217.75 274.30 61.38 o 12 11 0 27.19 95.95 46.84 o 13 11 0 329.61 383.63 63.39 o 14 11 0 318.64 320.24 41.06 o -7 12 0 10.84 11.18 31.05 o -6 12 0 13.94 57.60 27.87 o -5 12 0 204.05 376.00 101.20 o -4 12 0 14.25 29.11 25.75 o -3 12 0 620.57 655.35 52.40 o -2 12 0 202.49 131.77 34.68 o -1 12 0 1708.43 1743.57 50.55 o 0 12 0 307.04 374.00 86.29 o 1 12 0 1486.52 1468.92 42.09 o 2 12 0 169.79 261.06 35.63 o 3 12 0 195.49 163.92 46.39 o 4 12 0 1303.16 1230.80 38.28 o 5 12 0 4376.29 4332.35 46.09 o 6 12 0 106.46 177.47 40.44 o 7 12 0 1924.10 1918.97 100.78 o 8 12 0 280.81 334.10 41.41 o 9 12 0 1037.56 890.63 73.40 o 10 12 0 264.29 272.94 106.92 o 11 12 0 105.85 97.50 38.01 o 12 12 0 110.25 87.84 78.55 o 13 12 0 138.22 200.51 52.17 o -5 13 0 303.55 304.77 30.09 o -4 13 0 243.96 262.20 32.67 o -3 13 0 51.80 103.81 45.58 o -2 13 0 7.11 17.16 36.45 o -1 13 0 39.55 83.04 37.49 o 0 13 0 79.92 93.80 46.66 o 1 13 0 466.05 508.37 49.00 o 2 13 0 350.55 288.85 79.69 o 3 13 0 140.69 135.00 39.35 o 4 13 0 493.58 425.42 114.92 o 5 13 0 1.62 20.94 57.56 o 6 13 0 258.20 217.78 48.12 o 7 13 0 86.12 144.73 42.56 o 8 13 0 182.24 -3.10 77.57 o 9 13 0 222.20 252.53 105.79 o 10 13 0 26.46 78.98 46.26 o 11 13 0 12.10 89.46 42.14 o 12 13 0 54.36 -8.67 69.53 o -4 14 0 5.80 10.34 26.46 o -3 14 0 13.90 52.15 40.70 o -2 14 0 940.92 897.54 43.40 o -1 14 0 645.26 661.90 43.30 o 0 14 0 35.52 42.85 104.14 o 1 14 0 3.27 -38.46 54.47 o 2 14 0 0.78 28.25 42.31 o 3 14 0 36.07 51.16 55.24 o 4 14 0 90.10 98.45 44.69 o 5 14 0 68.31 88.83 64.99 o 6 14 0 543.77 612.66 47.07 o 7 14 0 201.14 176.94 61.31 o 8 14 0 198.75 152.65 47.74 o 9 14 0 407.18 443.42 49.77 o 10 14 0 490.57 433.39 51.49 o 11 14 0 233.99 198.15 47.58 o -1 15 0 8.34 59.40 82.99 o 0 15 0 168.72 85.45 48.13 o 1 15 0 31.40 110.30 54.93 o 2 15 0 2.35 -27.96 45.98 o 3 15 0 5.30 45.82 56.98 o 4 15 0 33.93 -32.31 61.91 o 5 15 0 251.97 121.43 49.85 o 6 15 0 1159.71 1152.40 68.61 o 7 15 0 69.54 70.24 65.46 o 8 15 0 580.60 594.63 52.98 o 9 15 0 233.65 295.35 76.28 o -7 -15 1 240.19 234.13 154.37 o -6 -15 1 755.15 756.98 75.10 o -5 -15 1 18.26 0.91 67.41 o -4 -15 1 84.52 32.18 121.83 o -3 -15 1 119.97 145.99 49.63 o -2 -15 1 153.09 216.17 84.18 o -1 -15 1 3.51 78.13 59.15 o 0 -15 1 9.30 -45.62 46.83 o -10 -14 1 86.40 144.16 52.68 o -9 -14 1 33.46 168.17 77.63 o -8 -14 1 151.90 242.73 50.28 o -7 -14 1 572.53 579.86 50.07 o -6 -14 1 52.59 73.62 96.10 o -5 -14 1 231.80 256.31 46.49 o -4 -14 1 91.54 68.61 92.12 o -3 -14 1 30.27 0.21 44.89 o -2 -14 1 10.88 -21.53 43.23 o -1 -14 1 3.54 68.41 81.39 o 0 -14 1 103.31 214.82 42.21 o 1 -14 1 827.49 855.64 55.14 o 2 -14 1 33.85 -9.24 101.56 o 3 -14 1 258.94 283.61 42.14 o -11 -13 1 4.18 41.16 69.63 o -10 -13 1 356.92 344.84 49.01 o -9 -13 1 1342.38 1150.44 51.06 o -8 -13 1 157.80 108.84 62.87 o -7 -13 1 1.64 93.87 61.69 o -6 -13 1 3.20 -46.83 60.86 o -5 -13 1 53.60 -36.71 42.32 o -4 -13 1 2.95 -11.79 41.32 o -3 -13 1 9.14 4.32 91.76 o -2 -13 1 32.43 8.11 72.78 o -1 -13 1 291.93 302.86 39.35 o 0 -13 1 116.61 64.99 48.12 o 1 -13 1 42.84 41.21 50.06 o 2 -13 1 266.56 277.73 38.20 o 3 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