#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/25/2202538.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202538_Fobs loop_ _publ_author_name 'Kaludjerovi\'c, Goran N.' 'Heinemann, Frank W.' 'Leovac, Vukadin M.' 'Trifunovi\'c, Sre\'cko R.' 'Sabo, Tibor J.' _publ_section_title ; Ethylenediammonium aquabis(malonato)oxovanadate(IV) ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m541 _journal_page_last m542 _journal_volume 59 _journal_year 2003 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 123.130 _cell_angle_gamma 90.000 _cell_length_a 14.5790 _cell_length_b 11.8660 _cell_length_c 8.7580 _exptl_crystal_F_000 724.00 _reflns_d_resolution_high 0.7331 _[local]_cod_data_source_file cm6048Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Ethylenediammonium aqua-bis(malonato)-oxo-vanadium(IV)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 241.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2364.14 2123.36 10.11 o 4 0 0 14839.92 14707.19 287.50 o 6 0 0 9464.26 9359.64 29.96 o 8 0 0 1870.59 1703.43 48.71 o 10 0 0 710.96 718.98 8.27 o 12 0 0 7741.35 7641.60 119.94 o 14 0 0 1296.67 1280.94 41.52 o 16 0 0 551.51 577.68 11.93 o 1 1 0 15018.87 14361.20 79.27 o 3 1 0 240.97 327.58 3.29 o 5 1 0 4315.18 4545.26 94.13 o 7 1 0 379.67 350.79 8.65 o 9 1 0 2681.22 2733.64 57.11 o 11 1 0 67.76 79.97 7.67 o 13 1 0 3015.60 2953.15 59.06 o 15 1 0 823.78 832.12 25.94 o 0 2 0 1573.55 1450.07 4.56 o 2 2 0 2718.73 2460.88 30.44 o 4 2 0 3816.54 4257.39 196.78 o 6 2 0 645.03 666.96 6.11 o 8 2 0 963.06 1020.00 23.38 o 10 2 0 196.36 200.28 5.42 o 12 2 0 208.23 208.97 6.28 o 14 2 0 10.13 6.70 4.73 o 16 2 0 373.60 366.06 18.02 o 1 3 0 1177.37 1253.72 10.59 o 3 3 0 7865.91 8232.12 49.80 o 5 3 0 121.16 140.28 3.43 o 7 3 0 979.37 1008.40 8.18 o 9 3 0 48.54 50.51 4.13 o 11 3 0 40.97 39.56 4.39 o 13 3 0 530.81 520.90 8.87 o 15 3 0 611.88 612.03 16.93 o 0 4 0 58480.11 56210.32 207.58 o 2 4 0 486.71 629.21 13.52 o 4 4 0 2130.46 2022.91 15.34 o 6 4 0 8326.31 8132.49 53.34 o 8 4 0 2.80 2.33 3.60 o 10 4 0 333.96 341.82 6.63 o 12 4 0 1464.17 1495.76 40.31 o 14 4 0 546.87 559.24 21.07 o 16 4 0 471.92 507.33 10.50 o 1 5 0 5793.32 5725.46 36.04 o 3 5 0 4888.97 4806.04 15.59 o 5 5 0 2066.83 2169.17 29.47 o 7 5 0 2552.58 2427.91 13.26 o 9 5 0 1647.55 1658.48 44.45 o 11 5 0 175.80 173.84 9.86 o 13 5 0 2090.39 2092.47 27.40 o 15 5 0 444.41 445.76 9.73 o 0 6 0 418.97 422.89 18.51 o 2 6 0 10.18 24.79 2.91 o 4 6 0 18.79 28.38 3.27 o 6 6 0 67.75 93.99 4.54 o 8 6 0 1594.29 1695.13 33.97 o 10 6 0 37.13 45.55 4.65 o 12 6 0 2324.49 2307.39 17.31 o 14 6 0 111.97 104.70 6.63 o 1 7 0 2184.48 2273.33 15.83 o 3 7 0 935.90 931.07 10.84 o 5 7 0 196.39 204.16 5.08 o 7 7 0 3.38 -0.51 4.04 o 9 7 0 145.39 158.13 5.85 o 11 7 0 5.84 13.81 4.56 o 13 7 0 362.09 357.00 8.70 o 15 7 0 567.85 561.97 21.31 o 0 8 0 12687.01 13237.66 28.41 o 2 8 0 738.70 735.47 7.66 o 4 8 0 343.15 371.00 6.37 o 6 8 0 1677.01 1678.49 12.40 o 8 8 0 14.53 20.37 4.29 o 10 8 0 51.86 48.91 6.09 o 12 8 0 1533.52 1507.86 15.24 o 14 8 0 333.97 312.86 9.13 o 1 9 0 2176.41 2276.39 13.26 o 3 9 0 2730.49 2723.46 14.90 o 5 9 0 355.32 357.85 6.72 o 7 9 0 1948.98 1970.56 34.22 o 9 9 0 565.91 576.16 24.48 o 11 9 0 372.48 367.27 8.44 o 13 9 0 716.87 707.21 22.16 o 0 10 0 5.65 7.18 3.79 o 2 10 0 477.79 450.33 7.23 o 4 10 0 1327.77 1327.98 37.14 o 6 10 0 2256.44 2203.88 29.96 o 8 10 0 1501.01 1509.91 28.13 o 10 10 0 225.46 231.41 7.43 o 12 10 0 950.59 958.13 13.26 o 1 11 0 106.07 112.00 5.08 o 3 11 0 1029.74 1011.94 10.85 o 5 11 0 330.71 334.09 10.11 o 7 11 0 167.29 155.41 8.77 o 9 11 0 576.80 582.83 16.80 o 11 11 0 106.70 103.62 6.72 o 0 12 0 839.50 818.00 10.07 o 2 12 0 67.51 74.28 4.99 o 4 12 0 11.53 0.53 4.64 o 6 12 0 1187.42 1199.94 13.00 o 8 12 0 56.49 64.04 5.86 o 10 12 0 104.59 89.85 6.89 o 1 13 0 569.90 594.75 9.47 o 3 13 0 1037.70 1019.90 12.23 o 5 13 0 491.36 463.25 17.17 o 7 13 0 1025.33 1033.62 13.43 o 9 13 0 265.92 240.80 8.52 o 0 14 0 424.51 449.98 10.11 o 2 14 0 187.89 222.89 13.15 o 4 14 0 359.87 356.34 8.95 o 6 14 0 410.62 446.92 11.81 o 8 14 0 518.44 528.09 11.19 o 1 15 0 194.34 203.45 7.75 o 3 15 0 900.68 930.16 36.17 o 5 15 0 590.41 585.99 11.19 o 0 16 0 10.61 9.72 5.59 o 2 16 0 152.09 159.74 14.13 o -17 1 1 456.18 443.54 15.83 o -15 1 1 63.92 65.34 5.34 o -13 1 1 1309.83 1318.37 31.90 o -11 1 1 1371.94 1297.37 10.85 o -9 1 1 1638.54 1712.49 47.61 o -7 1 1 14591.97 15398.20 274.84 o -5 1 1 73.60 52.40 2.41 o -3 1 1 958.83 1247.14 10.35 o -1 1 1 6592.33 6692.26 62.47 o 1 1 1 1133.21 1251.95 14.86 o 3 1 1 9751.58 9024.39 75.38 o 5 1 1 358.87 308.76 14.13 o 7 1 1 2944.82 3191.34 55.16 o 9 1 1 174.44 191.85 5.34 o 11 1 1 2398.89 2373.65 86.21 o 13 1 1 850.46 868.03 11.93 o 15 1 1 1334.29 1362.17 47.00 o -16 2 1 309.69 300.79 8.77 o -14 2 1 1292.13 1308.41 13.17 o -12 2 1 75.14 74.09 6.33 o -10 2 1 88.89 81.62 5.48 o -8 2 1 4321.48 4134.07 101.07 o -6 2 1 8872.61 9358.68 159.52 o -4 2 1 8471.26 8644.26 73.55 o -2 2 1 20841.34 20143.07 132.49 o 0 2 1 4270.52 4240.63 45.99 o 2 2 1 5656.14 5743.53 109.35 o 4 2 1 1853.48 2591.68 71.36 o 6 2 1 2752.98 2522.22 44.69 o 8 2 1 4335.11 4463.84 89.74 o 10 2 1 5.22 8.15 9.74 o 12 2 1 3380.75 3455.86 49.93 o 14 2 1 196.10 233.15 7.40 o -17 3 1 53.13 54.64 6.11 o -15 3 1 410.76 399.48 10.72 o -13 3 1 3401.12 3352.54 35.92 o -11 3 1 573.65 557.65 7.92 o -9 3 1 1170.91 1100.02 31.30 o -7 3 1 1045.79 1075.63 8.01 o -5 3 1 269.77 238.35 3.70 o -3 3 1 2177.79 2006.18 50.17 o -1 3 1 34269.14 31526.66 486.72 o 1 3 1 9162.31 9820.58 86.70 o 3 3 1 422.75 394.87 12.06 o 5 3 1 57.22 123.76 8.16 o 7 3 1 2183.83 2358.39 46.88 o 9 3 1 1124.38 1106.36 30.08 o 11 3 1 2743.30 2713.49 32.76 o 13 3 1 3.21 14.79 4.56 o 15 3 1 761.98 804.58 13.52 o -16 4 1 5.98 12.23 5.25 o -14 4 1 530.71 506.14 9.25 o -12 4 1 1.78 -2.58 3.95 o -10 4 1 2605.77 2669.81 49.44 o -8 4 1 441.40 449.16 6.37 o -6 4 1 874.67 959.93 7.32 o -4 4 1 312.60 275.43 11.45 o -2 4 1 52.08 30.94 2.49 o 0 4 1 1857.60 1794.87 29.57 o 2 4 1 560.20 558.90 20.58 o 4 4 1 1188.51 1354.85 37.51 o 6 4 1 342.26 336.27 5.77 o 8 4 1 475.06 516.35 7.41 o 10 4 1 308.71 307.43 6.80 o 12 4 1 91.44 91.87 6.82 o 14 4 1 210.81 208.01 7.66 o -15 5 1 123.21 114.91 6.36 o -13 5 1 995.67 989.24 11.53 o -11 5 1 723.38 694.65 9.38 o -9 5 1 357.64 363.89 6.46 o -7 5 1 2501.44 2570.03 126.52 o -5 5 1 1864.23 2017.14 10.42 o -3 5 1 10682.39 10725.00 145.03 o -1 5 1 2621.69 2500.15 28.62 o 1 5 1 376.41 458.34 4.99 o 3 5 1 2501.72 2788.17 13.64 o 5 5 1 333.44 337.35 5.97 o 7 5 1 988.23 973.85 20.21 o 9 5 1 1379.53 1379.57 35.31 o 11 5 1 651.19 602.73 9.56 o 13 5 1 495.96 495.59 9.73 o -16 6 1 802.59 802.74 12.57 o -14 6 1 885.65 886.08 35.68 o -12 6 1 648.29 652.57 9.47 o -10 6 1 282.31 310.92 6.54 o -8 6 1 5198.61 5126.57 77.45 o -6 6 1 5622.32 5464.37 38.97 o -4 6 1 11229.31 11599.60 182.78 o -2 6 1 9674.16 9896.92 21.53 o 0 6 1 13419.33 13222.92 166.67 o 2 6 1 2370.71 2270.82 19.12 o 4 6 1 488.20 475.19 6.37 o 6 6 1 2903.67 2844.94 40.43 o 8 6 1 4295.85 4340.64 112.03 o 10 6 1 477.78 493.99 13.39 o 12 6 1 2248.66 2271.68 24.23 o 14 6 1 590.81 614.13 16.32 o -15 7 1 517.89 509.98 10.50 o -13 7 1 1500.38 1485.36 14.64 o -11 7 1 2.74 12.30 4.26 o -9 7 1 4743.99 4718.37 58.45 o -7 7 1 5430.71 5381.42 56.99 o -5 7 1 3041.82 2985.55 14.38 o -3 7 1 799.02 718.10 7.06 o -1 7 1 8949.76 9140.04 39.33 o 1 7 1 451.32 369.09 5.42 o 3 7 1 6287.32 6524.53 26.42 o 5 7 1 4911.42 4819.17 60.40 o 7 7 1 160.92 165.85 6.33 o 9 7 1 1419.57 1402.84 38.97 o 11 7 1 784.70 833.23 11.28 o 13 7 1 437.53 458.04 9.82 o -14 8 1 424.25 409.19 17.78 o -12 8 1 281.73 281.19 7.66 o -10 8 1 2616.47 2579.11 17.13 o -8 8 1 9.89 6.90 4.04 o -6 8 1 553.93 565.21 7.66 o -4 8 1 947.98 931.39 9.04 o -2 8 1 261.56 266.89 5.25 o 0 8 1 2369.52 2253.43 21.09 o 2 8 1 733.35 748.07 7.92 o 4 8 1 3328.41 3346.34 89.50 o 6 8 1 460.55 433.69 7.41 o 8 8 1 776.84 786.89 10.16 o 10 8 1 380.27 389.16 9.25 o 12 8 1 292.67 272.63 8.35 o -13 9 1 395.68 408.63 9.38 o -11 9 1 1657.46 1675.85 33.37 o -9 9 1 790.02 781.27 10.25 o -7 9 1 254.45 260.42 6.46 o -5 9 1 1907.50 1915.68 31.54 o -3 9 1 380.39 333.97 6.11 o -1 9 1 1572.79 1575.52 11.45 o 1 9 1 1226.68 1199.17 10.35 o 3 9 1 2031.32 2078.06 13.52 o 5 9 1 760.73 731.00 9.13 o 7 9 1 400.97 417.62 8.18 o 9 9 1 231.11 227.03 7.06 o 11 9 1 84.58 85.01 6.63 o -12 10 1 67.03 65.70 10.35 o -10 10 1 13.15 15.22 5.97 o -8 10 1 288.59 310.89 7.32 o -6 10 1 129.47 129.23 5.25 o -4 10 1 230.94 262.53 8.28 o -2 10 1 0.71 -3.41 5.72 o 0 10 1 557.95 577.04 11.92 o 2 10 1 188.03 183.89 5.51 o 4 10 1 8.70 5.84 4.31 o 6 10 1 6.88 -5.60 5.60 o 8 10 1 125.67 120.21 6.03 o 10 10 1 12.84 15.00 12.30 o 12 10 1 162.96 169.77 9.25 o -13 11 1 1179.71 1172.42 15.15 o -11 11 1 97.43 114.99 6.72 o -9 11 1 1185.82 1181.88 25.57 o -7 11 1 565.95 566.11 9.38 o -5 11 1 865.34 853.04 40.43 o -3 11 1 1378.19 1364.87 12.91 o -1 11 1 4308.03 4274.23 52.24 o 1 11 1 268.57 286.74 6.63 o 3 11 1 744.85 765.03 16.93 o 5 11 1 1693.32 1694.82 14.64 o 7 11 1 18.49 18.89 5.08 o 9 11 1 1836.45 1773.86 16.88 o 11 11 1 206.41 213.05 18.87 o -10 12 1 781.74 772.46 11.97 o -8 12 1 28.69 26.63 6.94 o -6 12 1 2.13 2.62 4.56 o -4 12 1 532.78 591.17 16.80 o -2 12 1 143.31 126.19 9.50 o 0 12 1 849.69 828.88 7.28 o 2 12 1 150.17 147.23 5.86 o 4 12 1 1112.12 1082.21 14.00 o 6 12 1 123.40 122.78 8.89 o 8 12 1 705.10 727.08 19.97 o 10 12 1 93.99 97.20 6.97 o -9 13 1 320.30 316.03 8.86 o -7 13 1 10.83 16.20 5.34 o -5 13 1 52.51 53.01 5.25 o -3 13 1 6.62 6.66 4.73 o -1 13 1 57.30 46.01 4.99 o 1 13 1 224.29 220.73 7.06 o 3 13 1 713.84 717.45 10.76 o 5 13 1 271.82 292.38 8.65 o 7 13 1 1.75 11.47 5.42 o -8 14 1 26.49 28.19 6.02 o -6 14 1 5.46 8.68 5.08 o -4 14 1 44.98 50.02 5.68 o -2 14 1 15.54 1.32 5.84 o 0 14 1 3.02 12.84 3.34 o 2 14 1 157.11 174.82 7.15 o 4 14 1 2.64 -0.73 5.51 o 6 14 1 0.28 2.80 5.68 o -7 15 1 418.61 400.97 10.07 o -5 15 1 329.29 326.92 15.83 o -3 15 1 63.02 74.24 6.36 o -1 15 1 833.57 846.66 12.48 o 1 15 1 41.95 70.28 6.03 o 3 15 1 1173.96 1140.44 14.47 o 5 15 1 511.02 500.21 12.06 o -2 16 1 123.03 116.27 8.52 o 0 16 1 512.30 500.44 7.67 o -18 0 2 24.12 22.54 5.77 o -16 0 2 1962.67 1923.84 18.39 o -14 0 2 3438.43 3321.34 61.98 o -12 0 2 136.61 132.46 4.99 o -10 0 2 14331.57 14022.30 47.49 o -8 0 2 6580.08 6658.21 121.77 o -6 0 2 45240.99 42699.53 740.49 o -4 0 2 32477.33 31059.65 552.11 o -2 0 2 14718.97 13184.24 79.47 o 0 0 2 4286.50 4666.10 45.42 o 2 0 2 3948.76 3668.61 11.11 o 4 0 2 3278.70 2950.55 77.20 o 6 0 2 15546.33 16114.13 290.30 o 8 0 2 8947.44 8480.06 172.91 o 10 0 2 829.82 886.69 22.65 o 12 0 2 17.12 41.29 4.99 o 14 0 2 2279.56 2350.19 30.81 o -17 1 2 51.06 45.68 5.50 o -15 1 2 704.63 698.21 10.72 o -13 1 2 315.88 321.37 6.72 o -11 1 2 2710.38 2790.56 22.77 o -9 1 2 757.24 743.99 7.15 o -7 1 2 12122.26 13188.09 38.72 o -5 1 2 4806.06 4709.84 19.36 o -3 1 2 372.09 478.37 3.85 o -1 1 2 7566.86 7436.31 98.63 o 1 1 2 4226.37 3502.55 701.64 o 3 1 2 24.69 13.20 7.67 o 5 1 2 9780.45 10272.01 349.73 o 7 1 2 4538.49 4798.80 96.81 o 9 1 2 1026.75 986.58 48.22 o 11 1 2 945.02 1009.69 19.85 o 13 1 2 812.58 790.72 14.73 o -18 2 2 56.32 63.12 7.79 o -16 2 2 8.86 0.89 5.08 o -14 2 2 0.95 2.19 4.48 o -12 2 2 285.44 263.11 6.11 o -10 2 2 376.35 415.18 8.28 o -8 2 2 728.32 750.02 6.80 o -6 2 2 358.23 392.21 7.67 o -4 2 2 757.20 701.26 13.52 o -2 2 2 544.35 649.38 11.32 o 0 2 2 470.10 390.53 6.15 o 2 2 2 7977.56 8367.07 81.83 o 4 2 2 78.79 111.38 4.26 o 6 2 2 9.69 4.38 3.62 o 8 2 2 59.62 68.31 4.56 o 10 2 2 269.07 277.72 9.50 o 12 2 2 238.28 242.56 7.05 o 14 2 2 236.64 239.06 8.18 o -17 3 2 53.45 63.51 6.03 o -15 3 2 1.33 7.59 4.29 o -13 3 2 86.00 86.58 4.82 o -11 3 2 2.28 11.26 3.87 o -9 3 2 27.12 29.14 4.38 o -7 3 2 126.46 146.43 3.79 o -5 3 2 2159.12 2246.29 31.42 o -3 3 2 25042.30 26502.20 486.47 o -1 3 2 1755.49 1786.17 30.93 o 1 3 2 4193.83 4899.97 170.60 o 3 3 2 1757.81 1979.45 16.80 o 5 3 2 2038.33 2264.77 62.22 o 7 3 2 1244.97 1302.74 17.66 o 9 3 2 119.46 127.97 5.16 o 11 3 2 21.03 26.64 4.82 o 13 3 2 100.54 104.19 6.37 o -16 4 2 58.42 51.20 5.85 o -14 4 2 658.73 649.19 9.64 o -12 4 2 39.80 43.25 4.39 o -10 4 2 9821.97 9476.25 133.46 o -8 4 2 2842.99 2723.73 52.97 o -6 4 2 6198.42 6177.66 42.25 o -4 4 2 9.02 10.27 2.41 o -2 4 2 69.30 80.03 10.59 o 0 4 2 2664.14 2490.30 47.36 o 2 4 2 2257.72 2159.99 43.23 o 4 4 2 121.91 74.69 7.18 o 6 4 2 1078.22 1123.57 28.86 o 8 4 2 1961.90 1864.58 41.52 o 10 4 2 2.65 2.60 7.18 o 12 4 2 284.00 304.19 7.83 o 14 4 2 1025.85 1059.28 38.36 o -17 5 2 334.51 279.65 18.14 o -15 5 2 219.66 240.07 7.23 o -13 5 2 1126.29 1103.25 11.71 o -11 5 2 1700.70 1682.51 12.92 o -9 5 2 906.80 931.59 9.04 o -7 5 2 7063.47 7295.43 62.71 o -5 5 2 3750.09 3626.28 181.19 o -3 5 2 74.22 59.52 6.94 o -1 5 2 8212.17 7993.51 77.45 o 1 5 2 4187.02 4306.54 31.90 o 3 5 2 1221.44 1182.41 8.70 o 5 5 2 3225.28 3078.77 61.74 o 7 5 2 4269.84 4307.77 87.92 o 9 5 2 149.86 150.44 5.68 o 11 5 2 1680.54 1709.80 47.37 o 13 5 2 589.12 602.56 18.51 o -16 6 2 414.87 380.78 11.20 o -14 6 2 442.69 451.56 8.95 o -12 6 2 66.23 63.73 4.91 o -10 6 2 38.25 34.94 5.36 o -8 6 2 65.73 66.71 4.22 o -6 6 2 11.93 8.40 3.27 o -4 6 2 2264.99 2274.18 42.38 o -2 6 2 2655.60 2556.29 13.88 o 0 6 2 1290.53 1553.63 24.16 o 2 6 2 3275.21 3359.95 62.71 o 4 6 2 42.13 71.07 5.60 o 6 6 2 1124.07 1243.18 10.85 o 8 6 2 570.92 557.46 8.61 o 10 6 2 302.82 308.65 7.74 o 12 6 2 99.77 91.95 6.63 o -15 7 2 35.30 54.63 9.38 o -13 7 2 28.29 20.75 4.99 o -11 7 2 4.15 3.88 6.70 o -9 7 2 434.87 461.46 7.49 o -7 7 2 210.64 242.96 5.68 o -5 7 2 1594.81 1716.72 28.74 o -3 7 2 4027.43 4183.95 48.59 o -1 7 2 1238.87 1234.66 25.21 o 1 7 2 77.64 97.44 7.55 o 3 7 2 0.32 11.86 3.60 o 5 7 2 1053.32 1072.17 15.46 o 7 7 2 1463.21 1445.54 49.68 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257.89 6.63 o -6 10 2 28.51 33.30 4.31 o -4 10 2 807.16 810.28 9.56 o -2 10 2 2249.20 2224.43 14.29 o 0 10 2 713.22 647.56 5.94 o 2 10 2 6459.38 6279.05 70.63 o 4 10 2 482.97 460.99 15.83 o 6 10 2 242.61 258.33 7.32 o 8 10 2 765.47 794.47 20.58 o 10 10 2 561.71 576.29 11.02 o -13 11 2 309.31 308.21 9.21 o -11 11 2 71.70 78.04 7.43 o -9 11 2 121.11 130.78 6.11 o -7 11 2 16.58 23.64 8.89 o -5 11 2 124.79 108.32 13.52 o -3 11 2 457.50 461.28 7.83 o -1 11 2 673.45 672.85 8.95 o 1 11 2 140.60 148.47 5.77 o 3 11 2 878.11 841.93 10.50 o 5 11 2 44.19 60.68 5.08 o 7 11 2 78.33 83.90 11.57 o 9 11 2 0.42 -5.68 5.68 o -12 12 2 79.52 93.78 6.80 o -10 12 2 311.15 304.08 12.79 o -8 12 2 538.54 519.19 9.56 o -6 12 2 47.58 62.98 5.06 o -4 12 2 53.11 61.76 4.99 o -2 12 2 7.82 10.34 6.82 o 0 12 2 223.92 227.76 4.66 o 2 12 2 1191.49 1187.16 23.38 o 4 12 2 6.01 10.22 5.97 o 6 12 2 539.90 552.43 10.16 o 8 12 2 423.85 413.35 9.98 o -11 13 2 511.47 498.01 23.01 o -9 13 2 413.30 399.87 13.64 o -7 13 2 699.53 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