#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/25/2202547.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202547_Fobs loop_ _publ_author_name 'Lozano Diz, Enrique' 'Therrien, Bruno' 'S\"uss-Fink, Georg' _publ_section_title ; Decacarbonyltetra-\m-hydrido-bis(tricyclohexylphosphine)-tetrahedro-tetraruthenium ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m431 _journal_page_last m433 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.545 _cell_angle_gamma 90.000 _cell_length_a 12.4610 _cell_length_b 23.9340 _cell_length_c 18.5410 _exptl_crystal_F_000 2528.00 _reflns_d_resolution_high 0.8133 _[local]_cod_data_source_file cv6193Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' EL005 EN P 21/C' _shelx_refln_list_code 4 _shelx_f_calc_maximum 602.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 124557.41 128814.48 2256.26 o 3 0 0 33156.31 32463.13 1018.78 o 4 0 0 529.26 915.40 630.11 o 5 0 0 1859.81 1225.16 511.77 o 6 0 0 35738.32 35069.34 901.64 o 7 0 0 239.93 218.48 581.52 o 8 0 0 9822.99 9525.30 1038.45 o 9 0 0 20617.49 21632.32 635.06 o 10 0 0 8860.37 9185.77 627.41 o 11 0 0 478.61 290.77 812.88 o 12 0 0 10949.55 11178.49 769.88 o 13 0 0 2046.36 1908.69 623.90 o 14 0 0 767.50 1052.63 882.45 o 15 0 0 8974.75 9661.02 1557.17 o 2 1 0 171.54 554.55 555.20 o 3 1 0 29475.17 28688.46 665.55 o 4 1 0 59059.18 57817.62 990.47 o 5 1 0 33977.98 33867.91 845.53 o 6 1 0 721.93 1163.96 341.56 o 7 1 0 21057.54 20486.49 494.19 o 8 1 0 34412.88 34746.22 881.00 o 9 1 0 11892.49 12795.38 531.41 o 10 1 0 992.10 1033.28 485.17 o 11 1 0 1044.11 1023.54 495.61 o 12 1 0 706.40 514.61 612.62 o 13 1 0 1317.71 789.00 557.85 o 14 1 0 15.99 986.62 677.17 o 15 1 0 1253.71 1685.89 945.62 o 1 2 0 4983.83 5692.33 776.15 o 2 2 0 36148.36 35186.61 855.01 o 3 2 0 58514.77 57003.96 887.65 o 4 2 0 30511.22 32150.21 671.94 o 5 2 0 10452.53 9458.45 454.07 o 6 2 0 39418.98 37867.32 585.19 o 7 2 0 14118.99 13968.36 473.59 o 8 2 0 9449.33 9389.77 408.16 o 9 2 0 1745.45 2074.51 481.20 o 10 2 0 0.59 189.84 356.24 o 11 2 0 609.60 328.29 608.05 o 12 2 0 2179.77 1837.02 505.71 o 13 2 0 4486.93 5296.06 627.02 o 14 2 0 4507.98 4647.65 638.31 o 15 2 0 2586.26 2804.44 953.13 o 1 3 0 35336.85 34670.45 807.61 o 2 3 0 8260.49 8300.44 554.56 o 3 3 0 676.74 618.88 395.81 o 4 3 0 15921.97 15034.51 504.69 o 5 3 0 55944.00 58233.51 720.42 o 6 3 0 590.10 572.63 370.74 o 7 3 0 14.24 215.70 391.61 o 8 3 0 2164.31 2391.48 480.74 o 9 3 0 17.37 113.12 388.54 o 10 3 0 2609.29 2300.62 366.04 o 11 3 0 5700.44 5359.62 610.97 o 12 3 0 157.42 339.42 545.20 o 13 3 0 528.57 846.55 505.76 o 14 3 0 64.83 596.53 677.90 o 15 3 0 397.95 845.62 845.00 o 0 4 0 290.29 526.99 984.20 o 1 4 0 10693.31 10028.42 560.10 o 2 4 0 15264.36 14591.32 542.18 o 3 4 0 27918.34 29615.89 751.58 o 4 4 0 42112.89 40257.58 559.27 o 5 4 0 548.48 454.21 551.53 o 6 4 0 3433.10 3327.97 468.02 o 7 4 0 572.88 560.81 390.90 o 8 4 0 28920.28 28483.06 857.01 o 9 4 0 5605.32 5885.45 457.92 o 10 4 0 15954.93 16556.88 483.30 o 11 4 0 1237.14 1333.36 480.35 o 12 4 0 13442.73 13843.72 584.37 o 13 4 0 12042.90 11621.06 702.74 o 14 4 0 2721.27 2322.67 767.71 o 15 4 0 367.51 939.11 770.66 o 1 5 0 141.67 186.08 586.30 o 2 5 0 13437.92 13436.16 575.47 o 3 5 0 37485.89 37686.15 681.66 o 4 5 0 64005.60 61725.11 845.53 o 5 5 0 5075.67 4316.47 432.14 o 6 5 0 10335.25 10208.32 497.10 o 7 5 0 1469.31 1609.84 374.70 o 8 5 0 19616.47 20775.24 452.25 o 9 5 0 6107.52 6171.62 490.17 o 10 5 0 1052.08 1130.59 390.27 o 11 5 0 1749.40 1645.55 488.85 o 12 5 0 1334.86 1288.83 535.04 o 13 5 0 6891.35 7099.90 616.72 o 14 5 0 4741.02 4716.74 902.12 o 15 5 0 145.16 166.19 1383.92 o 0 6 0 53584.93 57421.39 1266.31 o 1 6 0 8078.02 8431.73 546.31 o 2 6 0 1874.71 2053.10 388.08 o 3 6 0 12298.51 13147.80 470.36 o 4 6 0 4039.79 3439.10 429.77 o 5 6 0 3773.45 3223.52 416.70 o 6 6 0 15224.04 14583.03 429.98 o 7 6 0 1202.21 1240.05 434.47 o 8 6 0 3314.30 3211.58 430.95 o 9 6 0 8916.03 9195.53 375.01 o 10 6 0 218.63 354.73 418.23 o 11 6 0 972.61 712.90 488.72 o 12 6 0 281.12 671.75 596.06 o 13 6 0 2865.98 2341.01 590.97 o 14 6 0 1371.31 1306.93 615.19 o 1 7 0 20.09 101.75 408.53 o 2 7 0 293.08 349.41 359.51 o 3 7 0 6367.64 6312.16 413.77 o 4 7 0 9831.42 8981.76 428.56 o 5 7 0 35357.28 35811.23 606.71 o 6 7 0 7597.69 7392.75 401.05 o 7 7 0 7.85 333.33 432.03 o 8 7 0 618.08 839.20 350.88 o 9 7 0 126.98 385.63 381.54 o 10 7 0 1874.42 2365.08 357.77 o 11 7 0 7558.95 7561.43 548.03 o 12 7 0 14.03 480.84 485.79 o 13 7 0 3792.44 3206.03 738.47 o 14 7 0 1148.47 795.07 531.37 o 0 8 0 249.44 371.86 455.79 o 1 8 0 4066.70 4351.39 484.91 o 2 8 0 36977.58 36779.00 595.29 o 3 8 0 104753.20 104266.13 949.79 o 4 8 0 18300.17 16343.73 545.98 o 5 8 0 19911.96 19874.60 521.26 o 6 8 0 3702.23 4215.31 406.18 o 7 8 0 1834.87 1513.92 346.19 o 8 8 0 17346.96 17647.36 597.10 o 9 8 0 13485.70 13745.69 455.29 o 10 8 0 221.23 614.33 461.32 o 11 8 0 2863.39 2846.08 484.65 o 12 8 0 7080.41 7234.09 614.78 o 13 8 0 14323.78 14253.06 769.82 o 14 8 0 1933.64 1318.80 688.46 o 1 9 0 2739.75 3073.04 359.51 o 2 9 0 8221.38 8561.92 469.90 o 3 9 0 737.06 981.49 391.67 o 4 9 0 23350.79 23159.03 517.75 o 5 9 0 4995.76 5053.21 445.44 o 6 9 0 1491.50 1369.70 444.15 o 7 9 0 4223.13 4012.27 478.40 o 8 9 0 25496.52 26202.78 575.24 o 9 9 0 17378.13 17357.92 487.28 o 10 9 0 4425.72 4227.56 590.17 o 11 9 0 8443.19 7675.75 469.74 o 12 9 0 5360.77 5058.64 500.84 o 13 9 0 2673.01 2210.13 609.22 o 14 9 0 4107.87 4503.91 809.01 o 0 10 0 55704.66 54794.84 1065.40 o 1 10 0 64983.53 64252.49 722.24 o 2 10 0 68023.20 67603.90 775.87 o 3 10 0 13773.22 13478.79 421.92 o 4 10 0 11416.77 10558.74 428.65 o 5 10 0 6333.67 6359.29 324.19 o 6 10 0 3335.29 3619.50 404.42 o 7 10 0 489.16 444.70 332.24 o 8 10 0 60.97 283.95 355.14 o 9 10 0 1474.58 1347.75 471.43 o 10 10 0 1176.10 1605.60 517.35 o 11 10 0 26.25 532.18 582.43 o 12 10 0 137.88 267.59 528.06 o 13 10 0 289.50 1256.96 592.03 o 14 10 0 225.44 513.69 812.37 o 1 11 0 8782.63 8514.07 521.98 o 2 11 0 27566.79 26625.41 589.08 o 3 11 0 10717.44 10759.24 425.53 o 4 11 0 110.41 333.54 397.71 o 5 11 0 43.34 243.97 388.48 o 6 11 0 8726.53 8691.27 420.27 o 7 11 0 22961.72 22391.63 452.93 o 8 11 0 30797.40 30617.21 641.85 o 9 11 0 4934.33 5197.75 400.21 o 10 11 0 37.75 398.72 473.92 o 11 11 0 230.79 1022.57 522.24 o 12 11 0 1664.56 1473.28 541.13 o 13 11 0 4055.51 3975.59 677.17 o 14 11 0 3862.20 4420.41 764.57 o 0 12 0 100761.28 103117.73 1248.98 o 1 12 0 65712.95 65117.20 932.61 o 2 12 0 17075.53 16836.59 467.29 o 3 12 0 2228.39 2298.65 417.35 o 4 12 0 102.67 193.62 310.85 o 5 12 0 11062.31 11425.49 435.01 o 6 12 0 4120.36 3447.78 481.69 o 7 12 0 3404.12 3248.54 369.49 o 8 12 0 1613.61 1582.24 419.40 o 9 12 0 10953.42 10998.19 459.79 o 10 12 0 2241.08 2268.60 473.46 o 11 12 0 235.37 358.36 527.65 o 12 12 0 277.71 560.13 642.83 o 13 12 0 1009.52 1439.37 522.56 o 1 13 0 1925.55 2175.27 323.96 o 2 13 0 11845.44 12129.18 394.36 o 3 13 0 19421.43 18726.70 467.15 o 4 13 0 38248.83 40068.44 595.02 o 5 13 0 24672.14 26400.03 577.64 o 6 13 0 8269.42 8532.67 459.34 o 7 13 0 118.24 229.38 375.85 o 8 13 0 795.50 735.50 466.82 o 9 13 0 74.60 174.52 476.61 o 10 13 0 3293.70 2695.38 588.68 o 11 13 0 2756.78 2755.66 527.76 o 12 13 0 461.43 674.10 588.35 o 13 13 0 320.49 228.81 686.08 o 0 14 0 4100.31 4303.49 445.74 o 1 14 0 2159.65 2242.34 322.73 o 2 14 0 1053.04 846.41 347.25 o 3 14 0 1484.37 1616.27 480.11 o 4 14 0 6821.11 6952.80 414.68 o 5 14 0 7012.50 7377.42 419.86 o 6 14 0 12272.05 11742.97 517.41 o 7 14 0 5017.09 4788.77 379.34 o 8 14 0 1390.31 1352.60 355.61 o 9 14 0 153.85 342.47 521.66 o 10 14 0 460.87 687.38 484.36 o 11 14 0 3348.44 2933.22 574.98 o 12 14 0 4290.34 3496.25 617.18 o 13 14 0 6403.48 6666.29 821.44 o 1 15 0 8144.17 8547.98 508.46 o 2 15 0 27981.88 28895.70 502.58 o 3 15 0 9372.17 10273.27 436.13 o 4 15 0 589.98 634.23 353.18 o 5 15 0 1194.61 1288.07 412.63 o 6 15 0 1208.96 1444.47 384.79 o 7 15 0 219.00 466.01 462.39 o 8 15 0 599.78 677.29 515.25 o 9 15 0 1614.30 928.49 524.84 o 10 15 0 18176.93 17854.99 551.61 o 11 15 0 9539.32 9095.72 669.92 o 12 15 0 2792.77 2016.34 669.30 o 13 15 0 7.12 808.99 745.07 o 0 16 0 3455.18 3884.56 561.63 o 1 16 0 23.47 336.47 348.51 o 2 16 0 476.63 958.13 415.72 o 3 16 0 4392.20 4263.30 434.57 o 4 16 0 1434.01 1425.53 384.70 o 5 16 0 9499.58 9784.67 423.46 o 6 16 0 17243.04 17687.65 415.42 o 7 16 0 18166.86 18379.71 459.51 o 8 16 0 713.31 589.34 585.82 o 9 16 0 680.64 605.81 413.44 o 10 16 0 28.31 241.11 595.44 o 11 16 0 751.21 1518.00 831.13 o 12 16 0 355.74 1132.80 597.11 o 1 17 0 2124.34 2079.91 468.97 o 2 17 0 229.00 368.68 376.25 o 3 17 0 1289.45 1697.27 465.11 o 4 17 0 10099.85 10490.22 499.29 o 5 17 0 14303.41 15467.29 518.35 o 6 17 0 5301.76 4866.13 431.29 o 7 17 0 108.51 280.52 578.61 o 8 17 0 2.38 850.48 579.26 o 9 17 0 2566.86 2282.41 492.14 o 10 17 0 6615.61 6005.96 614.19 o 11 17 0 4341.89 5246.35 748.08 o 12 17 0 439.74 750.31 730.52 o 0 18 0 10.47 386.77 646.12 o 1 18 0 640.28 582.48 417.43 o 2 18 0 878.60 1405.18 351.64 o 3 18 0 889.44 806.18 462.37 o 4 18 0 4491.66 4552.79 475.50 o 5 18 0 6768.50 6458.45 408.42 o 6 18 0 4535.77 4544.67 529.81 o 7 18 0 4917.97 5207.52 593.63 o 8 18 0 6430.26 5858.42 497.19 o 9 18 0 714.22 720.29 419.82 o 10 18 0 1018.78 827.77 544.58 o 11 18 0 32.02 398.70 658.35 o 12 18 0 610.65 342.17 909.09 o 1 19 0 511.67 358.47 456.80 o 2 19 0 8076.03 8545.25 489.83 o 3 19 0 398.04 279.46 351.16 o 4 19 0 7403.25 7219.54 406.24 o 5 19 0 7567.54 7424.38 598.89 o 6 19 0 2849.75 2967.41 481.19 o 7 19 0 2568.81 2390.08 452.66 o 8 19 0 1452.05 1108.37 525.21 o 9 19 0 12395.11 12599.68 547.59 o 10 19 0 27473.80 28400.11 823.36 o 11 19 0 19226.72 20290.40 793.16 o 0 20 0 156.51 573.89 637.88 o 1 20 0 390.51 584.98 322.89 o 2 20 0 13772.22 14089.11 508.34 o 3 20 0 15128.93 15381.77 447.96 o 4 20 0 4354.86 4146.71 532.29 o 5 20 0 518.28 791.43 472.97 o 6 20 0 4882.26 4510.15 490.93 o 7 20 0 2308.60 1812.70 447.32 o 8 20 0 99.14 466.76 533.72 o 9 20 0 563.36 815.82 545.16 o 10 20 0 1032.33 813.23 749.90 o 11 20 0 242.48 419.42 749.86 o 1 21 0 5876.15 5445.12 398.87 o 2 21 0 7244.38 7638.09 437.58 o 3 21 0 5423.44 5040.12 591.70 o 4 21 0 4652.24 4334.30 589.97 o 5 21 0 1716.84 1383.92 484.53 o 6 21 0 8382.17 8014.91 476.45 o 7 21 0 22738.67 23503.85 565.79 o 8 21 0 15310.42 15753.91 690.21 o 9 21 0 12036.90 11972.66 768.02 o 10 21 0 3294.69 3479.33 885.04 o 0 22 0 5366.80 5372.60 599.97 o 1 22 0 1457.74 1017.22 479.81 o 2 22 0 3584.02 3411.03 586.28 o 3 22 0 3100.20 2802.49 482.00 o 4 22 0 138.62 300.42 469.00 o 5 22 0 194.45 451.72 584.98 o 6 22 0 130.07 344.76 477.72 o 7 22 0 1886.73 1456.53 546.27 o 8 22 0 1217.89 1335.64 728.19 o 9 22 0 160.86 658.92 613.57 o 10 22 0 216.92 437.91 833.91 o 1 23 0 5834.37 5659.80 495.82 o 2 23 0 16470.56 16617.40 536.15 o 3 23 0 11535.73 11255.02 520.71 o 4 23 0 3503.14 3361.68 534.15 o 5 23 0 2751.52 2169.86 628.91 o 6 23 0 6214.77 6165.20 658.00 o 7 23 0 4976.48 4322.12 531.49 o 8 23 0 3796.39 3413.85 950.02 o 9 23 0 630.04 1746.17 906.08 o 0 24 0 395.42 492.89 588.77 o 1 24 0 1387.58 1113.90 581.75 o 2 24 0 4868.39 4680.73 494.32 o 3 24 0 3016.12 2921.35 421.37 o 4 24 0 189.56 398.38 414.57 o 5 24 0 2500.66 2284.78 714.73 o 6 24 0 11286.83 10706.11 632.92 o 7 24 0 2603.24 2910.80 665.69 o 8 24 0 7.14 620.53 740.47 o 1 25 0 4686.57 4142.30 596.04 o 2 25 0 2339.85 2275.12 490.03 o 3 25 0 1053.10 1500.09 716.84 o 4 25 0 7.43 526.38 572.47 o 5 25 0 1834.26 857.32 731.50 o 6 25 0 55.95 461.33 594.01 o 7 25 0 204.84 671.55 823.98 o 8 25 0 90.08 399.87 1268.09 o 0 26 0 162.31 1183.75 990.91 o 1 26 0 0.05 491.17 586.37 o 2 26 0 22.59 529.64 715.25 o 3 26 0 0.74 499.67 586.36 o 4 26 0 82.57 309.18 643.43 o 5 26 0 132.47 343.71 556.64 o 6 26 0 123.62 361.87 631.90 o 1 27 0 3277.78 2969.24 605.00 o 2 27 0 3559.53 3196.59 562.33 o 3 27 0 2177.21 1786.88 606.18 o 4 27 0 2072.53 1709.94 741.67 o 5 27 0 88.66 995.42 734.26 o 6 27 0 1140.06 695.22 931.46 o 0 28 0 281.30 576.46 1038.45 o 1 28 0 2936.82 2506.84 747.00 o 2 28 0 5353.97 4813.37 621.01 o 3 28 0 2047.45 2409.85 733.52 o 4 28 0 122.74 389.50 639.86 o 1 29 0 1315.44 1264.34 742.43 o 2 29 0 1376.80 1180.54 1009.69 o -15 1 1 446.89 539.09 858.70 o -14 1 1 230.55 638.75 684.58 o -13 1 1 527.14 477.28 505.15 o -12 1 1 265.97 296.11 503.86 o -11 1 1 892.27 953.95 412.36 o -10 1 1 933.11 393.18 440.79 o -9 1 1 1799.78 1801.26 402.55 o -8 1 1 5155.50 5486.49 468.19 o -7 1 1 1754.21 1331.78 365.29 o -6 1 1 8015.92 7799.16 491.61 o -5 1 1 31179.67 29873.26 614.40 o -4 1 1 16093.29 16493.47 535.63 o -3 1 1 13011.09 13035.51 631.18 o -2 1 1 1334.58 1318.20 601.51 o -1 1 1 46513.54 41846.72 899.77 o 1 1 1 183.36 368.19 671.83 o 2 1 1 32681.40 34012.39 939.16 o 3 1 1 25286.96 26425.29 699.59 o 4 1 1 4013.56 3779.23 413.77 o 5 1 1 14803.46 13303.42 451.00 o 6 1 1 5816.22 5710.01 397.02 o 7 1 1 15082.54 14350.85 526.72 o 8 1 1 7193.59 7218.58 422.65 o 9 1 1 13073.79 14103.92 452.82 o 10 1 1 20.35 235.59 354.26 o 11 1 1 323.80 485.27 487.50 o 12 1 1 325.22 671.28 423.80 o 13 1 1 635.49 574.99 503.46 o 14 1 1 0.25 918.19 613.52 o 15 1 1 495.92 1225.03 946.05 o -15 2 1 951.42 1511.51 961.43 o -14 2 1 18.75 783.43 679.98 o -13 2 1 4029.24 3971.99 571.05 o -12 2 1 2907.02 2772.84 514.03 o -11 2 1 802.99 647.14 594.58 o -10 2 1 13954.41 14251.69 461.67 o -9 2 1 16653.09 15829.05 471.87 o -8 2 1 21771.64 22993.32 533.61 o -7 2 1 97.58 328.24 329.09 o -6 2 1 215.03 374.71 419.17 o -5 2 1 11282.43 10705.17 379.44 o -4 2 1 9139.79 10436.64 511.45 o -3 2 1 1795.31 1630.32 617.71 o -2 2 1 23631.71 25563.53 921.85 o -1 2 1 128880.37 121293.45 1484.53 o 0 2 1 362537.69 346781.06 3790.50 o 1 2 1 46243.75 49309.21 1220.89 o 2 2 1 4211.11 3352.68 533.63 o 3 2 1 18300.93 20189.86 743.66 o 4 2 1 1945.56 2239.97 416.68 o 5 2 1 21401.66 20420.25 472.63 o 6 2 1 7453.29 6296.52 434.14 o 7 2 1 1053.50 1237.74 329.15 o 8 2 1 6130.24 5907.61 418.93 o 9 2 1 533.26 750.43 419.52 o 10 2 1 168.25 1029.29 350.13 o 11 2 1 19200.30 18700.82 607.44 o 12 2 1 20957.64 22006.93 663.90 o 13 2 1 6022.39 6332.92 648.72 o 14 2 1 184.15 792.70 566.37 o 15 2 1 1616.76 1360.45 775.08 o -15 3 1 22.87 440.60 851.68 o -14 3 1 3600.88 3282.45 698.70 o -13 3 1 6637.92 6377.50 536.16 o -12 3 1 1624.40 1702.97 550.94 o -11 3 1 741.74 1169.43 536.14 o -10 3 1 1036.73 938.05 430.66 o -9 3 1 1733.28 1875.06 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