#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:01:49 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180945 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/25/2202554.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202554_Fobs loop_ _publ_author_name 'Thamotharan, S.' 'Parthasarathi, V.' 'Gupta, P.' 'Jindal, D. P.' 'Piplani, P.' 'Linden, Anthony' _publ_section_title ; 2-[(2-Oxopyrrolidin-1-yl)carbonylmethyl]-2,3-dihydro-1H-isoindole-1,3-dione: an antiamnesic agent ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1012 _journal_page_last o1013 _journal_volume 59 _journal_year 2003 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.7480 _cell_length_b 8.3280 _cell_length_c 27.9084 _exptl_crystal_F_000 1136.00 _reflns_d_resolution_high 0.8101 _cod_data_source_file cv6202Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PP-3/DPJ (EX0205)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 220.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' 'x-1/2, y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 19867.82 17829.65 364.38 o 4 0 0 12559.25 11640.44 226.26 o 6 0 0 1551.99 1614.06 35.52 o 8 0 0 1.57 -11.84 11.84 o 10 0 0 182.75 182.85 27.62 o 12 0 0 19.28 1.32 28.94 o 4 1 0 76.09 76.30 5.26 o 6 1 0 0.10 3.95 5.26 o 8 1 0 757.34 770.86 26.31 o 10 1 0 32.59 31.57 11.84 o 12 1 0 90.59 98.66 23.68 o 0 2 0 10750.55 9423.91 210.47 o 2 2 0 1672.68 1794.28 24.99 o 4 2 0 684.29 591.95 11.84 o 6 2 0 3.09 1.32 6.58 o 8 2 0 1.78 6.58 9.21 o 10 2 0 412.97 407.79 22.36 o 12 2 0 35.11 28.94 21.05 o 2 3 0 1316.67 1344.39 19.73 o 4 3 0 1209.88 1379.91 22.36 o 6 3 0 550.96 602.48 17.10 o 8 3 0 896.10 811.63 24.99 o 10 3 0 209.00 189.43 18.42 o 12 3 0 37.14 48.67 23.68 o 0 4 0 539.58 559.07 14.47 o 2 4 0 23.42 19.73 3.95 o 4 4 0 11984.32 13132.17 171.01 o 6 4 0 1750.62 1764.02 38.15 o 8 4 0 705.90 747.18 27.62 o 10 4 0 119.44 139.44 19.73 o 12 4 0 0.79 -2.63 22.36 o 2 5 0 19.07 13.15 3.95 o 4 5 0 0.00 -2.63 6.58 o 6 5 0 1889.95 1946.87 49.99 o 8 5 0 747.11 802.43 28.94 o 10 5 0 2.39 36.83 18.42 o 0 6 0 16.85 15.79 6.58 o 2 6 0 268.85 294.66 10.52 o 4 6 0 31.67 15.79 10.52 o 6 6 0 339.20 323.60 19.73 o 8 6 0 424.15 402.53 32.89 o 10 6 0 22.55 35.52 24.99 o 2 7 0 360.87 345.96 14.47 o 4 7 0 645.27 694.56 28.94 o 6 7 0 245.39 268.35 23.68 o 8 7 0 63.08 53.93 22.36 o 0 8 0 433.15 444.62 22.36 o 2 8 0 1022.58 1177.33 42.09 o 4 8 0 84.50 99.97 17.10 o 6 8 0 131.27 132.86 21.05 o 8 8 0 0.00 6.58 26.31 o 2 9 0 117.53 131.55 21.05 o 4 9 0 234.11 272.30 27.62 o 6 9 0 3.38 -6.58 27.62 o 0 10 0 380.23 386.74 61.83 o 2 10 0 153.70 182.85 52.62 o 1 1 1 4116.04 3785.87 43.41 o 2 1 1 8565.84 8134.76 92.08 o 3 1 1 7910.64 7567.80 84.19 o 4 1 1 2367.01 2321.77 24.99 o 5 1 1 57.33 55.25 3.95 o 6 1 1 303.86 242.04 7.89 o 7 1 1 905.77 969.49 18.42 o 8 1 1 7.19 3.95 6.58 o 9 1 1 28.17 35.52 7.89 o 10 1 1 192.93 221.00 11.84 o 11 1 1 121.19 122.34 13.15 o 12 1 1 0.22 3.95 15.79 o 13 1 1 16.89 -17.10 19.73 o 0 2 1 25140.51 22103.56 352.54 o 1 2 1 18457.94 17745.46 157.85 o 2 2 1 2616.95 2419.12 24.99 o 3 2 1 6843.94 6990.32 69.72 o 4 2 1 1439.57 1620.64 18.42 o 5 2 1 342.43 410.42 7.89 o 6 2 1 30.88 34.20 5.26 o 7 2 1 242.80 243.36 9.21 o 8 2 1 487.66 501.19 14.47 o 9 2 1 20.88 14.47 7.89 o 10 2 1 188.83 184.16 13.15 o 11 2 1 1.60 -10.52 10.52 o 12 2 1 43.13 36.83 15.79 o 13 2 1 68.82 67.09 21.05 o 1 3 1 66.76 52.62 1.32 o 2 3 1 12200.59 12195.56 105.24 o 3 3 1 5376.95 5488.07 52.62 o 4 3 1 1.87 5.26 2.63 o 5 3 1 1624.81 1661.42 21.05 o 6 3 1 553.30 518.29 11.84 o 7 3 1 48.74 39.46 5.26 o 8 3 1 55.86 48.67 6.58 o 9 3 1 159.20 173.64 11.84 o 10 3 1 18.23 14.47 10.52 o 11 3 1 213.34 196.00 15.79 o 12 3 1 8.53 3.95 15.79 o 0 4 1 371.79 326.23 6.58 o 1 4 1 292.30 311.76 3.95 o 2 4 1 1055.52 1040.52 11.84 o 3 4 1 2218.58 2325.72 22.36 o 4 4 1 4488.61 4910.59 47.36 o 5 4 1 828.91 893.19 14.47 o 6 4 1 489.05 443.31 10.52 o 7 4 1 165.43 131.55 7.89 o 8 4 1 76.51 63.14 7.89 o 9 4 1 335.72 322.29 15.79 o 10 4 1 39.98 36.83 10.52 o 11 4 1 0.64 3.95 14.47 o 12 4 1 0.66 -7.89 18.42 o 1 5 1 8.22 10.52 2.63 o 2 5 1 4.97 0.00 2.63 o 3 5 1 1106.65 1170.75 15.79 o 4 5 1 2400.75 2545.40 32.89 o 5 5 1 523.15 530.13 13.15 o 6 5 1 621.77 655.10 15.79 o 7 5 1 3.59 -3.95 7.89 o 8 5 1 10.73 -1.32 9.21 o 9 5 1 45.54 36.83 11.84 o 10 5 1 1.21 -11.84 13.15 o 11 5 1 32.39 -7.89 17.10 o 0 6 1 49.81 40.78 5.26 o 1 6 1 1.55 1.32 3.95 o 2 6 1 49.44 46.04 3.95 o 3 6 1 56.34 46.04 5.26 o 4 6 1 1.34 -5.26 6.58 o 5 6 1 1.25 3.95 7.89 o 6 6 1 1789.86 1958.71 46.04 o 7 6 1 21.66 10.52 10.52 o 8 6 1 31.06 35.52 13.15 o 9 6 1 74.52 92.08 17.10 o 10 6 1 38.43 38.15 17.10 o 1 7 1 126.70 124.97 6.58 o 2 7 1 5.85 9.21 5.26 o 3 7 1 348.73 342.02 9.21 o 4 7 1 1064.13 1152.34 27.62 o 5 7 1 42.64 30.26 10.52 o 6 7 1 2.53 18.42 11.84 o 7 7 1 406.00 395.95 19.73 o 8 7 1 2.14 3.95 14.47 o 9 7 1 191.50 169.69 21.05 o 0 8 1 4.36 3.95 7.89 o 1 8 1 134.96 139.44 7.89 o 2 8 1 142.14 124.97 10.52 o 3 8 1 25.48 7.89 9.21 o 4 8 1 183.97 192.06 13.15 o 5 8 1 11.47 27.62 11.84 o 6 8 1 1.88 -13.15 13.15 o 7 8 1 56.71 34.20 15.79 o 8 8 1 227.22 214.42 24.99 o 1 9 1 21.31 28.94 11.84 o 2 9 1 87.61 86.82 13.15 o 3 9 1 17.69 15.79 14.47 o 4 9 1 7.22 17.10 15.79 o 5 9 1 107.15 65.77 18.42 o 6 9 1 14.66 46.04 21.05 o 0 10 1 161.87 242.04 39.46 o 1 10 1 0.80 -14.47 23.68 o 2 10 1 83.02 101.29 30.26 o 3 10 1 39.67 15.79 30.26 o 1 0 2 9151.38 8287.35 147.33 o 2 0 2 589.64 681.40 11.84 o 3 0 2 1556.61 1594.33 23.68 o 4 0 2 741.08 647.20 11.84 o 5 0 2 820.15 772.17 14.47 o 6 0 2 1556.69 1810.06 30.26 o 7 0 2 3095.37 3326.78 53.93 o 8 0 2 0.51 -1.32 7.89 o 9 0 2 53.96 59.20 10.52 o 10 0 2 79.73 56.56 13.15 o 11 0 2 16.96 59.20 17.10 o 12 0 2 574.06 644.57 35.52 o 13 0 2 15.66 43.41 27.62 o 1 1 2 6544.96 6320.75 65.77 o 2 1 2 93.05 52.62 1.32 o 3 1 2 194.22 194.69 3.95 o 4 1 2 65.33 53.93 2.63 o 5 1 2 1322.70 1368.07 15.79 o 6 1 2 2.97 -3.95 3.95 o 7 1 2 0.57 0.00 5.26 o 8 1 2 117.62 123.65 7.89 o 9 1 2 30.32 34.20 7.89 o 10 1 2 689.12 735.34 19.73 o 11 1 2 111.57 109.18 13.15 o 12 1 2 44.31 42.09 13.15 o 13 1 2 12.41 18.42 21.05 o 0 2 2 150.98 207.84 3.95 o 1 2 2 7.25 9.21 1.32 o 3 2 2 4563.25 4756.68 48.67 o 4 2 2 2111.86 2182.34 22.36 o 5 2 2 243.04 278.88 6.58 o 6 2 2 503.19 505.13 10.52 o 7 2 2 8.58 9.21 5.26 o 8 2 2 286.24 257.83 9.21 o 9 2 2 639.55 687.98 18.42 o 10 2 2 0.09 1.32 9.21 o 11 2 2 64.57 52.62 11.84 o 12 2 2 42.27 40.78 14.47 o 1 3 2 108.84 105.24 2.63 o 2 3 2 230.03 231.52 3.95 o 3 3 2 594.63 630.10 7.89 o 4 3 2 13387.90 14246.36 131.55 o 5 3 2 425.62 428.84 7.89 o 6 3 2 1262.42 1329.92 18.42 o 7 3 2 348.67 330.18 10.52 o 8 3 2 21.36 5.26 6.58 o 9 3 2 20.91 19.73 9.21 o 10 3 2 137.39 128.91 11.84 o 11 3 2 86.15 96.03 13.15 o 12 3 2 51.63 31.57 17.10 o 0 4 2 442.06 466.99 7.89 o 1 4 2 882.02 849.78 9.21 o 2 4 2 1685.38 1819.27 17.10 o 3 4 2 44.23 43.41 2.63 o 4 4 2 562.63 594.58 9.21 o 5 4 2 469.94 482.77 10.52 o 6 4 2 1400.44 1400.96 19.73 o 7 4 2 13.13 11.84 3.95 o 8 4 2 279.69 280.19 11.84 o 9 4 2 311.18 330.18 14.47 o 10 4 2 0.26 3.95 10.52 o 11 4 2 0.91 10.52 13.15 o 12 4 2 1.01 13.15 19.73 o 1 5 2 232.76 244.67 5.26 o 2 5 2 1175.82 1270.73 15.79 o 3 5 2 6.68 5.26 3.95 o 4 5 2 634.40 652.46 11.84 o 5 5 2 159.73 148.65 7.89 o 6 5 2 1169.15 1160.23 22.36 o 7 5 2 54.65 46.04 7.89 o 8 5 2 8.68 23.68 9.21 o 9 5 2 1.34 1.32 10.52 o 10 5 2 35.85 22.36 14.47 o 11 5 2 2.08 13.15 15.79 o 0 6 2 1183.24 1277.30 21.05 o 1 6 2 118.31 106.55 5.26 o 2 6 2 91.10 78.93 5.26 o 3 6 2 116.80 102.61 5.26 o 4 6 2 73.61 57.88 6.58 o 5 6 2 63.08 55.25 7.89 o 6 6 2 595.61 584.06 19.73 o 7 6 2 727.36 762.96 22.36 o 8 6 2 1.17 7.89 11.84 o 9 6 2 25.37 27.62 14.47 o 10 6 2 0.06 7.89 17.10 o 1 7 2 13.71 1.32 5.26 o 2 7 2 25.98 23.68 5.26 o 3 7 2 3.57 6.58 5.26 o 4 7 2 212.98 235.47 11.84 o 5 7 2 140.69 113.13 13.15 o 6 7 2 0.79 -1.32 10.52 o 7 7 2 158.99 140.75 15.79 o 8 7 2 277.85 284.14 19.73 o 9 7 2 119.15 88.14 17.10 o 0 8 2 63.21 57.88 9.21 o 1 8 2 1.11 -6.58 6.58 o 2 8 2 117.05 149.96 10.52 o 3 8 2 92.63 102.61 11.84 o 4 8 2 69.52 77.61 11.84 o 5 8 2 38.84 31.57 11.84 o 6 8 2 54.76 38.15 14.47 o 7 8 2 8.66 28.94 15.79 o 8 8 2 98.69 90.77 22.36 o 1 9 2 23.70 15.79 11.84 o 2 9 2 20.21 27.62 11.84 o 3 9 2 213.82 215.73 17.10 o 4 9 2 21.68 21.05 15.79 o 5 9 2 3.88 28.94 17.10 o 6 9 2 0.80 23.68 21.05 o 0 10 2 10.56 -46.04 46.04 o 1 10 2 110.22 80.24 28.94 o 2 10 2 6.96 13.15 27.62 o 1 1 3 51.70 81.56 1.32 o 2 1 3 2114.78 2035.01 18.42 o 3 1 3 6510.81 6715.39 71.03 o 4 1 3 75.27 89.45 3.95 o 5 1 3 115.89 134.18 5.26 o 6 1 3 328.68 324.92 9.21 o 7 1 3 12.65 2.63 3.95 o 8 1 3 256.47 234.15 9.21 o 9 1 3 278.19 285.45 11.84 o 10 1 3 73.22 72.35 10.52 o 11 1 3 25.29 18.42 11.84 o 12 1 3 2.43 -10.52 17.10 o 13 1 3 66.82 111.81 21.05 o 0 2 3 9898.57 9035.85 107.87 o 1 2 3 3970.08 3825.34 34.20 o 2 2 3 11680.00 11183.98 105.24 o 3 2 3 241.84 256.51 3.95 o 4 2 3 2.47 2.63 2.63 o 5 2 3 116.78 144.70 5.26 o 6 2 3 6.16 6.58 3.95 o 7 2 3 834.07 939.23 18.42 o 8 2 3 653.93 698.51 15.79 o 9 2 3 191.00 214.42 11.84 o 10 2 3 21.00 21.05 9.21 o 11 2 3 29.70 39.46 11.84 o 12 2 3 0.94 -5.26 15.79 o 1 3 3 605.90 545.91 6.58 o 2 3 3 113.92 153.91 3.95 o 3 3 3 575.97 578.80 7.89 o 4 3 3 0.01 3.95 2.63 o 5 3 3 500.36 548.54 7.89 o 6 3 3 19.88 18.42 3.95 o 7 3 3 128.23 117.08 7.89 o 8 3 3 3.30 6.58 6.58 o 9 3 3 45.00 43.41 7.89 o 10 3 3 313.95 352.54 15.79 o 11 3 3 9.79 10.52 13.15 o 12 3 3 38.12 18.42 17.10 o 0 4 3 621.91 588.01 9.21 o 1 4 3 316.65 323.60 5.26 o 2 4 3 36.69 35.52 2.63 o 3 4 3 59.77 84.19 3.95 o 4 4 3 2.19 -2.63 3.95 o 5 4 3 438.14 466.99 10.52 o 6 4 3 464.65 486.72 11.84 o 7 4 3 37.03 30.26 5.26 o 8 4 3 1668.77 1869.26 35.52 o 9 4 3 40.59 56.56 10.52 o 10 4 3 19.23 17.10 11.84 o 11 4 3 46.54 39.46 14.47 o 12 4 3 15.62 -14.47 18.42 o 1 5 3 860.62 878.72 11.84 o 2 5 3 6.87 5.26 2.63 o 3 5 3 13.02 13.15 3.95 o 4 5 3 1594.39 1656.16 22.36 o 5 5 3 428.09 394.64 10.52 o 6 5 3 2569.20 2759.82 43.41 o 7 5 3 1304.98 1382.54 28.94 o 8 5 3 50.69 26.31 10.52 o 9 5 3 217.02 193.37 15.79 o 10 5 3 23.42 17.10 11.84 o 11 5 3 9.27 2.63 15.79 o 0 6 3 486.30 469.62 11.84 o 1 6 3 14.74 19.73 3.95 o 2 6 3 5.26 3.95 3.95 o 3 6 3 18.55 15.79 5.26 o 4 6 3 159.91 147.33 7.89 o 5 6 3 1029.77 1027.37 23.68 o 6 6 3 1323.44 1508.82 34.20 o 7 6 3 189.21 165.75 13.15 o 8 6 3 56.11 60.51 11.84 o 9 6 3 129.09 99.97 15.79 o 10 6 3 28.04 36.83 17.10 o 1 7 3 20.23 22.36 5.26 o 2 7 3 0.10 5.26 5.26 o 3 7 3 28.86 24.99 6.58 o 4 7 3 38.98 34.20 9.21 o 5 7 3 9.47 13.15 9.21 o 6 7 3 166.13 156.54 14.47 o 7 7 3 161.27 90.77 14.47 o 8 7 3 357.12 301.24 19.73 o 9 7 3 18.31 31.57 19.73 o 0 8 3 59.60 78.93 9.21 o 1 8 3 0.63 1.32 6.58 o 2 8 3 0.09 -6.58 7.89 o 3 8 3 0.06 -7.89 9.21 o 4 8 3 74.94 90.77 11.84 o 5 8 3 16.75 34.20 13.15 o 6 8 3 0.18 9.21 14.47 o 7 8 3 1.43 34.20 17.10 o 8 8 3 0.03 -2.63 18.42 o 1 9 3 20.19 17.10 14.47 o 2 9 3 205.85 201.26 15.79 o 3 9 3 1.19 -7.89 13.15 o 4 9 3 33.45 5.26 15.79 o 5 9 3 73.05 101.29 21.05 o 6 9 3 36.53 38.15 19.73 o 0 10 3 629.02 869.51 84.19 o 1 10 3 0.13 -5.26 35.52 o 2 10 3 86.78 127.60 39.46 o 0 0 4 18837.46 16532.61 520.92 o 1 0 4 2615.94 2525.67 32.89 o 2 0 4 516.74 505.13 9.21 o 3 0 4 3142.22 3036.07 46.04 o 4 0 4 1774.91 1691.67 27.62 o 5 0 4 22.54 19.73 3.95 o 6 0 4 7.04 3.95 5.26 o 7 0 4 1214.39 1379.91 30.26 o 8 0 4 146.19 176.27 11.84 o 9 0 4 34.17 59.20 11.84 o 10 0 4 67.76 53.93 13.15 o 11 0 4 542.75 641.94 28.94 o 12 0 4 324.03 405.16 27.62 o 13 0 4 100.60 134.18 27.62 o 1 1 4 1260.51 1101.03 10.52 o 2 1 4 752.62 716.92 6.58 o 3 1 4 105.65 99.97 2.63 o 4 1 4 327.00 326.23 5.26 o 5 1 4 1122.91 1077.36 14.47 o 6 1 4 1384.89 1574.60 21.05 o 7 1 4 179.09 155.22 7.89 o 8 1 4 93.94 111.81 7.89 o 9 1 4 115.65 132.86 9.21 o 10 1 4 445.41 493.29 17.10 o 11 1 4 36.83 43.41 10.52 o 12 1 4 15.64 15.79 14.47 o 13 1 4 160.89 177.59 21.05 o 0 2 4 2131.63 2033.69 26.31 o 1 2 4 1324.94 1382.54 13.15 o 2 2 4 835.60 655.10 6.58 o 3 2 4 1633.26 1587.75 15.79 o 4 2 4 5118.57 5547.27 49.99 o 5 2 4 1641.70 1660.10 18.42 o 6 2 4 225.89 199.95 6.58 o 7 2 4 41.54 53.93 6.58 o 8 2 4 12.71 5.26 6.58 o 9 2 4 197.36 197.32 10.52 o 10 2 4 0.20 14.47 9.21 o 11 2 4 0.03 3.95 10.52 o 12 2 4 29.67 40.78 14.47 o 1 3 4 176.65 156.54 2.63 o 2 3 4 1748.36 1849.53 18.42 o 3 3 4 129.36 131.55 3.95 o 4 3 4 8.02 15.79 2.63 o 5 3 4 507.22 513.03 7.89 o 6 3 4 85.66 97.34 5.26 o 7 3 4 130.55 136.81 6.58 o 8 3 4 26.97 30.26 6.58 o 9 3 4 8.55 1.32 7.89 o 10 3 4 200.68 221.00 14.47 o 11 3 4 0.60 35.52 13.15 o 12 3 4 0.22 17.10 15.79 o 0 4 4 40.21 35.52 2.63 o 1 4 4 618.40 644.57 7.89 o 2 4 4 303.67 377.54 5.26 o 3 4 4 955.13 995.80 11.84 o 4 4 4 1051.98 1111.56 14.47 o 5 4 4 2033.88 2204.70 28.94 o 6 4 4 61.45 57.88 6.58 o 7 4 4 0.88 -2.63 3.95 o 8 4 4 195.79 165.75 11.84 o 9 4 4 36.23 10.52 10.52 o 10 4 4 0.01 30.26 11.84 o 11 4 4 12.06 23.68 15.79 o 12 4 4 31.19 18.42 17.10 o 1 5 4 380.43 330.18 5.26 o 2 5 4 1.26 3.95 2.63 o 3 5 4 0.09 1.32 3.95 o 4 5 4 195.85 180.22 6.58 o 5 5 4 154.91 152.59 7.89 o 6 5 4 78.80 68.40 6.58 o 7 5 4 100.45 73.67 9.21 o 8 5 4 18.64 35.52 9.21 o 9 5 4 10.37 -3.95 13.15 o 10 5 4 3.31 -14.47 14.47 o 11 5 4 6.01 1.32 15.79 o 0 6 4 1185.30 1243.10 23.68 o 1 6 4 173.96 153.91 5.26 o 2 6 4 45.82 43.41 5.26 o 3 6 4 13.84 15.79 5.26 o 4 6 4 1.53 0.00 5.26 o 5 6 4 76.92 71.03 7.89 o 6 6 4 11.87 7.89 9.21 o 7 6 4 170.84 157.85 13.15 o 8 6 4 0.55 5.26 13.15 o 9 6 4 3.15 7.89 14.47 o 10 6 4 0.04 24.99 17.10 o 1 7 4 0.10 -1.32 5.26 o 2 7 4 264.66 260.46 9.21 o 3 7 4 89.87 99.97 9.21 o 4 7 4 30.98 19.73 7.89 o 5 7 4 412.24 407.79 17.10 o 6 7 4 284.95 259.14 15.79 o 7 7 4 1.53 -1.32 13.15 o 8 7 4 6.02 -2.63 13.15 o 9 7 4 29.68 15.79 18.42 o 0 8 4 1.80 5.26 9.21 o 1 8 4 1.36 -2.63 6.58 o 2 8 4 52.80 67.09 9.21 o 3 8 4 216.47 228.89 14.47 o 4 8 4 687.79 759.02 24.99 o 5 8 4 34.59 38.15 13.15 o 6 8 4 16.27 28.94 15.79 o 7 8 4 8.50 -10.52 18.42 o 8 8 4 9.85 19.73 18.42 o 1 9 4 1.08 17.10 11.84 o 2 9 4 233.31 236.78 17.10 o 3 9 4 131.51 142.07 18.42 o 4 9 4 75.04 52.62 18.42 o 5 9 4 16.52 -19.73 19.73 o 6 9 4 4.47 0.00 21.05 o 0 10 4 7.94 -52.62 52.62 o 1 10 4 28.39 56.56 28.94 o 2 10 4 2.16 14.47 27.62 o 1 1 5 1189.53 1285.20 11.84 o 2 1 5 3.37 3.95 1.32 o 3 1 5 56.73 56.56 2.63 o 4 1 5 334.38 352.54 6.58 o 5 1 5 313.37 322.29 6.58 o 6 1 5 86.95 88.14 5.26 o 7 1 5 609.98 610.37 13.15 o 8 1 5 123.52 128.91 7.89 o 9 1 5 2.02 -6.58 6.58 o 10 1 5 3.11 -9.21 9.21 o 11 1 5 61.88 38.15 10.52 o 12 1 5 156.95 134.18 15.79 o 13 1 5 74.91 69.72 22.36 o 0 2 5 1667.30 1531.19 23.68 o 1 2 5 2572.24 2391.49 22.36 o 2 2 5 49.04 38.15 1.32 o 3 2 5 0.15 2.63 1.32 o 4 2 5 756.42 719.55 9.21 o 5 2 5 352.67 364.38 6.58 o 6 2 5 109.88 92.08 5.26 o 7 2 5 209.86 213.10 7.89 o 8 2 5 94.62 97.34 7.89 o 9 2 5 216.53 239.41 11.84 o 10 2 5 498.10 489.35 17.10 o 11 2 5 167.33 147.33 14.47 o 12 2 5 43.96 52.62 15.79 o 1 3 5 236.54 211.79 2.63 o 2 3 5 196.34 184.16 3.95 o 3 3 5 1670.44 1800.85 17.10 o 4 3 5 765.95 755.07 10.52 o 5 3 5 931.72 914.24 11.84 o 6 3 5 24.77 19.73 3.95 o 7 3 5 167.84 159.17 7.89 o 8 3 5 833.70 890.56 18.42 o 9 3 5 549.00 585.38 17.10 o 10 3 5 154.50 152.59 13.15 o 11 3 5 66.34 40.78 11.84 o 12 3 5 15.32 7.89 17.10 o 0 4 5 485.47 410.42 7.89 o 1 4 5 1908.06 2012.64 19.73 o 2 4 5 392.81 420.94 5.26 o 3 4 5 0.49 0.00 2.63 o 4 4 5 284.60 253.88 6.58 o 5 4 5 167.80 177.59 6.58 o 6 4 5 46.14 35.52 5.26 o 7 4 5 189.98 155.22 7.89 o 8 4 5 200.96 169.69 11.84 o 9 4 5 23.94 30.26 10.52 o 10 4 5 90.41 94.71 14.47 o 11 4 5 38.00 40.78 14.47 o 12 4 5 0.03 -6.58 18.42 o 1 5 5 350.84 376.22 6.58 o 2 5 5 100.14 102.61 3.95 o 3 5 5 88.55 107.87 5.26 o 4 5 5 66.60 68.40 5.26 o 5 5 5 567.51 540.65 11.84 o 6 5 5 16.43 17.10 6.58 o 7 5 5 213.98 201.26 10.52 o 8 5 5 11.57 1.32 9.21 o 9 5 5 25.92 39.46 13.15 o 10 5 5 8.31 -13.15 13.15 o 11 5 5 60.28 89.45 18.42 o 0 6 5 336.55 345.96 10.52 o 1 6 5 266.09 267.04 6.58 o 2 6 5 230.20 210.47 6.58 o 3 6 5 0.27 3.95 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460.41 7.89 o 4 4 7 1170.98 1186.54 15.79 o 5 4 7 14.61 26.31 3.95 o 6 4 7 44.68 30.26 5.26 o 7 4 7 54.27 48.67 6.58 o 8 4 7 0.26 10.52 9.21 o 9 4 7 23.39 24.99 11.84 o 10 4 7 24.02 10.52 11.84 o 11 4 7 9.44 5.26 14.47 o 1 5 7 515.73 531.44 9.21 o 2 5 7 580.04 599.85 9.21 o 3 5 7 940.80 965.54 14.47 o 4 5 7 74.68 65.77 5.26 o 5 5 7 142.84 124.97 6.58 o 6 5 7 29.08 23.68 6.58 o 7 5 7 27.03 18.42 7.89 o 8 5 7 60.41 34.20 11.84 o 9 5 7 0.55 5.26 11.84 o 10 5 7 11.35 5.26 17.10 o 11 5 7 13.77 30.26 19.73 o 0 6 7 394.50 402.53 13.15 o 1 6 7 985.00 1047.10 14.47 o 2 6 7 6.04 2.63 3.95 o 3 6 7 98.21 82.87 5.26 o 4 6 7 135.45 128.91 7.89 o 5 6 7 107.33 92.08 7.89 o 6 6 7 120.30 99.97 10.52 o 7 6 7 6.46 5.26 9.21 o 8 6 7 281.84 314.39 19.73 o 9 6 7 13.12 5.26 14.47 o 10 6 7 6.68 10.52 17.10 o 1 7 7 3.45 5.26 5.26 o 2 7 7 1.07 1.32 5.26 o 3 7 7 16.38 7.89 6.58 o 4 7 7 641.71 622.21 18.42 o 5 7 7 392.73 386.74 17.10 o 6 7 7 11.66 13.15 13.15 o 7 7 7 23.29 1.32 13.15 o 8 7 7 3.33 7.89 17.10 o 9 7 7 34.12 49.99 19.73 o 0 8 7 266.16 249.94 15.79 o 1 8 7 6.21 0.00 7.89 o 2 8 7 89.97 80.24 10.52 o 3 8 7 90.66 82.87 13.15 o 4 8 7 2.52 9.21 14.47 o 5 8 7 37.66 46.04 19.73 o 6 8 7 29.25 2.63 19.73 o 7 8 7 0.01 3.95 22.36 o 1 9 7 4.69 10.52 17.10 o 2 9 7 168.16 155.22 21.05 o 3 9 7 2.43 -13.15 18.42 o 4 9 7 142.19 178.90 24.99 o 5 9 7 0.28 11.84 23.68 o 0 10 7 117.81 176.27 49.99 o 1 10 7 24.40 52.62 32.89 o 0 0 8 8057.20 7483.61 128.91 o 1 0 8 4766.40 4477.80 52.62 o 2 0 8 4089.79 3605.66 43.41 o 3 0 8 7432.14 7753.28 105.24 o 4 0 8 1305.17 1379.91 21.05 o 5 0 8 700.99 678.77 14.47 o 6 0 8 186.32 192.06 10.52 o 7 0 8 2836.57 3093.95 63.14 o 8 0 8 463.30 473.56 17.10 o 9 0 8 369.66 381.48 17.10 o 10 0 8 48.54 35.52 11.84 o 11 0 8 250.49 211.79 19.73 o 12 0 8 186.72 243.36 28.94 o 1 1 8 2082.97 1960.02 17.10 o 2 1 8 468.62 445.94 5.26 o 3 1 8 2694.13 2675.63 24.99 o 4 1 8 698.83 681.40 9.21 o 5 1 8 180.54 182.85 5.26 o 6 1 8 1435.88 1483.83 19.73 o 7 1 8 41.33 32.89 5.26 o 8 1 8 159.57 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7.89 o 8 4 8 367.86 361.75 15.79 o 9 4 8 260.87 247.31 15.79 o 10 4 8 16.07 19.73 14.47 o 11 4 8 0.89 3.95 14.47 o 1 5 8 1878.22 1871.89 22.36 o 2 5 8 4.61 2.63 2.63 o 3 5 8 687.85 730.08 10.52 o 4 5 8 55.26 52.62 5.26 o 5 5 8 195.63 177.59 7.89 o 6 5 8 27.16 22.36 6.58 o 7 5 8 69.72 44.73 9.21 o 8 5 8 10.51 -1.32 11.84 o 9 5 8 1.70 1.32 13.15 o 10 5 8 29.18 32.89 14.47 o 11 5 8 45.60 27.62 18.42 o 0 6 8 169.52 164.43 11.84 o 1 6 8 257.67 249.94 6.58 o 2 6 8 125.86 113.13 5.26 o 3 6 8 0.15 3.95 3.95 o 4 6 8 13.80 17.10 5.26 o 5 6 8 23.32 17.10 6.58 o 6 6 8 19.38 -1.32 6.58 o 7 6 8 304.26 313.08 17.10 o 8 6 8 4.17 -10.52 13.15 o 9 6 8 44.93 36.83 15.79 o 10 6 8 2.84 28.94 18.42 o 1 7 8 27.28 15.79 5.26 o 2 7 8 197.99 205.21 7.89 o 3 7 8 354.28 389.37 14.47 o 4 7 8 205.20 223.63 11.84 o 5 7 8 257.14 290.72 15.79 o 6 7 8 169.21 178.90 17.10 o 7 7 8 1.06 15.79 14.47 o 8 7 8 36.20 46.04 18.42 o 9 7 8 11.33 -7.89 18.42 o 0 8 8 366.52 438.05 22.36 o 1 8 8 23.58 18.42 9.21 o 2 8 8 105.28 105.24 14.47 o 3 8 8 25.59 19.73 15.79 o 4 8 8 189.71 227.57 21.05 o 5 8 8 17.33 5.26 17.10 o 6 8 8 8.14 27.62 21.05 o 7 8 8 4.29 -22.36 22.36 o 1 9 8 0.63 0.00 17.10 o 2 9 8 62.35 56.56 23.68 o 3 9 8 12.29 -1.32 22.36 o 4 9 8 3.99 0.00 23.68 o 5 9 8 35.72 69.72 35.52 o 1 1 9 4476.86 4398.87 38.15 o 2 1 9 178.28 171.01 2.63 o 3 1 9 2806.38 2903.20 24.99 o 4 1 9 491.91 474.88 6.58 o 5 1 9 2317.84 2433.59 24.99 o 6 1 9 515.95 530.13 10.52 o 7 1 9 373.03 356.49 10.52 o 8 1 9 64.50 72.35 6.58 o 9 1 9 2.17 1.32 6.58 o 10 1 9 409.92 419.63 15.79 o 11 1 9 6.93 21.05 13.15 o 12 1 9 67.90 80.24 17.10 o 0 2 9 377.51 436.73 7.89 o 1 2 9 74.47 56.56 2.63 o 2 2 9 2933.21 3015.02 26.31 o 3 2 9 3416.18 3596.45 31.57 o 4 2 9 127.40 110.50 2.63 o 5 2 9 49.52 48.67 3.95 o 6 2 9 106.71 98.66 5.26 o 7 2 9 1.72 0.00 5.26 o 8 2 9 255.97 261.78 10.52 o 9 2 9 3.17 -2.63 7.89 o 10 2 9 121.47 115.76 11.84 o 11 2 9 30.45 24.99 13.15 o 12 2 9 4.56 1.32 19.73 o 1 3 9 2030.66 1965.29 18.42 o 2 3 9 77.47 59.20 2.63 o 3 3 9 380.85 418.31 6.58 o 4 3 9 398.41 406.47 6.58 o 5 3 9 0.99 1.32 3.95 o 6 3 9 688.55 712.98 13.15 o 7 3 9 126.74 117.08 7.89 o 8 3 9 28.94 28.94 6.58 o 9 3 9 391.73 426.21 18.42 o 10 3 9 85.55 88.14 14.47 o 11 3 9 41.84 46.04 17.10 o 12 3 9 0.27 -11.84 19.73 o 0 4 9 1661.76 1704.83 26.31 o 1 4 9 67.05 53.93 2.63 o 2 4 9 440.48 449.88 6.58 o 3 4 9 1033.57 989.22 13.15 o 4 4 9 129.68 118.39 5.26 o 5 4 9 202.35 178.90 6.58 o 6 4 9 302.08 284.14 9.21 o 7 4 9 2.24 2.63 6.58 o 8 4 9 817.76 827.42 26.31 o 9 4 9 64.59 53.93 13.15 o 10 4 9 0.08 -2.63 14.47 o 11 4 9 64.79 49.99 18.42 o 1 5 9 249.71 228.89 5.26 o 2 5 9 376.90 372.27 7.89 o 3 5 9 728.07 711.66 10.52 o 4 5 9 43.75 40.78 5.26 o 5 5 9 178.58 178.90 7.89 o 6 5 9 2446.26 2561.19 42.09 o 7 5 9 233.23 223.63 14.47 o 8 5 9 25.10 9.21 11.84 o 9 5 9 0.32 -14.47 14.47 o 10 5 9 0.47 28.94 18.42 o 11 5 9 30.49 56.56 18.42 o 0 6 9 137.84 110.50 10.52 o 1 6 9 224.67 205.21 7.89 o 2 6 9 932.81 991.85 15.79 o 3 6 9 14.25 17.10 5.26 o 4 6 9 412.58 419.63 11.84 o 5 6 9 34.42 30.26 7.89 o 6 6 9 118.89 111.81 10.52 o 7 6 9 13.02 2.63 11.84 o 8 6 9 23.25 -6.58 14.47 o 9 6 9 4.61 1.32 17.10 o 10 6 9 8.26 -3.95 21.05 o 1 7 9 23.47 10.52 6.58 o 2 7 9 77.46 68.40 6.58 o 3 7 9 178.87 172.32 10.52 o 4 7 9 352.65 359.12 14.47 o 5 7 9 19.81 24.99 10.52 o 6 7 9 96.71 90.77 13.15 o 7 7 9 0.08 7.89 17.10 o 8 7 9 303.32 349.91 28.94 o 9 7 9 6.88 40.78 23.68 o 0 8 9 290.03 310.45 19.73 o 1 8 9 273.27 274.93 15.79 o 2 8 9 0.09 6.58 11.84 o 3 8 9 12.40 -3.95 13.15 o 4 8 9 32.76 43.41 15.79 o 5 8 9 0.57 17.10 18.42 o 6 8 9 241.74 323.60 30.26 o 7 8 9 0.18 -23.68 23.68 o 1 9 9 10.50 0.00 18.42 o 2 9 9 504.74 544.60 38.15 o 3 9 9 12.52 22.36 23.68 o 4 9 9 166.57 173.64 31.57 o 5 9 9 0.97 24.99 27.62 o 0 0 10 7.34 28.94 3.95 o 1 0 10 775.50 816.90 10.52 o 2 0 10 616.04 527.50 7.89 o 3 0 10 8610.70 9310.78 117.08 o 4 0 10 78.43 76.30 5.26 o 5 0 10 725.62 680.09 13.15 o 6 0 10 682.77 703.77 19.73 o 7 0 10 151.71 173.64 10.52 o 8 0 10 207.29 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13 121.12 77.61 18.42 o 3 8 13 0.44 -11.84 17.10 o 4 8 13 14.43 9.21 26.31 o 5 8 13 68.39 59.20 26.31 o 6 8 13 2.44 -10.52 23.68 o 1 9 13 15.39 14.47 19.73 o 2 9 13 204.77 238.10 31.57 o 3 9 13 3.58 -23.68 27.62 o 4 9 13 3.57 27.62 26.31 o 0 0 14 873.40 948.44 17.10 o 1 0 14 11308.54 12463.92 131.55 o 2 0 14 1577.21 1619.32 19.73 o 3 0 14 37.89 89.45 5.26 o 4 0 14 24.74 15.79 5.26 o 5 0 14 1.32 -3.95 5.26 o 6 0 14 10.80 6.58 6.58 o 7 0 14 1818.61 2052.11 47.36 o 8 0 14 156.77 143.38 11.84 o 9 0 14 257.35 260.46 21.05 o 10 0 14 34.64 22.36 14.47 o 11 0 14 80.93 101.29 19.73 o 12 0 14 55.94 26.31 24.99 o 1 1 14 6641.95 7406.00 60.51 o 2 1 14 31.59 31.57 2.63 o 3 1 14 172.59 218.37 5.26 o 4 1 14 29.69 22.36 3.95 o 5 1 14 1149.00 1211.53 18.42 o 6 1 14 0.00 -1.32 5.26 o 7 1 14 0.00 2.63 5.26 o 8 1 14 260.93 252.57 11.84 o 9 1 14 369.05 403.84 17.10 o 10 1 14 190.22 177.59 14.47 o 11 1 14 191.82 157.85 18.42 o 12 1 14 0.03 -14.47 19.73 o 0 2 14 113.20 115.76 3.95 o 1 2 14 1676.68 1828.48 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