#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:02:05 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180946 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/26/2202618.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202618_Fobs loop_ _publ_author_name 'Spirlet, Marie-Rose' 'Graulich, Amaury' 'Li\'egeois, Jean-Francois' _publ_section_title ; 8-Methyl-6-(4-methylpiperazin-1-yl)-11H-pyrido[2,3-b][1,4]benzodiazepine ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1990 _journal_page_last o1991 _journal_volume 59 _journal_year 2003 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.0331 _cell_length_b 15.6103 _cell_length_c 16.5137 _exptl_crystal_F_000 1312.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file dn6096Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Jl18 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 255.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10046.95 9703.80 290.52 o 4 0 0 7008.72 6949.42 118.69 o 6 0 0 2800.76 2729.29 90.95 o 8 0 0 284.74 343.85 31.75 o 10 0 0 2770.75 2702.91 83.03 o 12 0 0 832.18 882.70 50.18 o 14 0 0 4.79 29.71 48.30 o 2 1 0 29897.25 28442.85 950.78 o 4 1 0 3371.95 3312.06 58.31 o 6 1 0 4621.81 4435.19 99.90 o 8 1 0 927.87 909.04 29.85 o 10 1 0 36.49 32.82 20.55 o 12 1 0 17.33 13.42 28.62 o 14 1 0 1.37 -32.95 35.99 o 0 2 0 45047.09 42669.73 3552.33 o 2 2 0 149.73 161.16 18.05 o 4 2 0 7943.59 7734.76 133.71 o 6 2 0 1.98 12.73 19.34 o 8 2 0 1832.69 2024.18 138.00 o 10 2 0 816.51 901.09 52.66 o 12 2 0 56.47 67.01 43.92 o 14 2 0 57.32 37.54 52.86 o 2 3 0 3341.83 3436.96 76.39 o 4 3 0 297.19 302.18 22.57 o 6 3 0 5271.47 5264.37 100.05 o 8 3 0 1268.95 1191.35 48.53 o 10 3 0 387.00 372.84 37.92 o 12 3 0 958.42 896.26 64.69 o 14 3 0 248.63 300.94 63.92 o 0 4 0 54317.78 53221.68 3739.18 o 2 4 0 8736.10 8778.41 107.05 o 4 4 0 3.07 22.67 17.72 o 6 4 0 347.85 339.84 27.67 o 8 4 0 1678.39 1737.22 75.23 o 10 4 0 361.19 400.32 38.52 o 12 4 0 14.85 -23.82 45.98 o 14 4 0 623.47 878.74 129.25 o 2 5 0 468.97 475.72 27.67 o 4 5 0 111.56 120.75 22.89 o 6 5 0 984.42 973.13 38.83 o 8 5 0 101.24 80.15 29.87 o 10 5 0 5825.30 5589.29 169.53 o 12 5 0 1.73 9.70 45.98 o 14 5 0 442.17 599.22 91.94 o 0 6 0 6500.39 6398.57 100.05 o 2 6 0 2868.17 3043.51 104.98 o 4 6 0 108.74 159.14 26.25 o 6 6 0 5556.04 5632.24 104.97 o 8 6 0 2139.35 2143.59 81.96 o 10 6 0 870.77 835.61 45.39 o 12 6 0 3.38 -33.62 47.72 o 14 6 0 2.83 105.13 64.54 o 2 7 0 2274.08 2395.38 89.96 o 4 7 0 1856.30 2070.36 127.27 o 6 7 0 35.88 29.09 24.81 o 8 7 0 1727.09 1752.94 56.46 o 10 7 0 1315.86 1336.77 68.98 o 12 7 0 180.94 53.82 86.99 o 14 7 0 72.53 124.04 52.86 o 0 8 0 5.79 40.70 22.57 o 2 8 0 3704.43 3743.62 95.92 o 4 8 0 170.53 158.28 28.30 o 6 8 0 248.81 221.36 116.72 o 8 8 0 0.77 -3.32 31.75 o 10 8 0 347.83 366.29 50.59 o 12 8 0 32.94 23.24 44.21 o 2 9 0 1768.11 1805.16 73.35 o 4 9 0 226.51 216.92 31.13 o 6 9 0 12.33 32.41 27.03 o 8 9 0 811.23 840.33 45.10 o 10 9 0 24.32 20.79 41.54 o 12 9 0 92.47 110.31 51.45 o 0 10 0 1132.36 1210.55 55.46 o 2 10 0 586.17 600.67 39.73 o 4 10 0 45.93 37.85 32.06 o 6 10 0 189.09 204.19 116.72 o 8 10 0 326.84 257.79 48.88 o 10 10 0 99.73 103.43 41.84 o 12 10 0 216.02 202.94 53.97 o 2 11 0 10.44 4.23 30.50 o 4 11 0 265.56 286.64 36.08 o 6 11 0 0.17 -14.39 27.03 o 8 11 0 59.28 -30.74 53.48 o 10 11 0 423.51 411.26 33.62 o 12 11 0 28.00 82.09 49.74 o 0 12 0 288.86 242.13 37.00 o 2 12 0 3653.12 3670.31 96.98 o 4 12 0 3.44 -8.74 35.16 o 6 12 0 133.08 74.38 41.54 o 8 12 0 59.24 43.97 42.43 o 10 12 0 15.91 -17.93 47.72 o 2 13 0 282.22 254.50 37.31 o 4 13 0 50.36 25.45 44.51 o 6 13 0 23.05 44.90 36.08 o 8 13 0 4.37 33.67 43.62 o 10 13 0 100.59 107.58 49.45 o 0 14 0 156.33 138.21 47.72 o 2 14 0 31.45 41.86 44.51 o 4 14 0 1.01 26.85 45.39 o 6 14 0 7.05 19.80 38.22 o 8 14 0 0.97 -7.06 49.16 o 10 14 0 3.48 6.56 48.59 o 2 15 0 11.44 29.26 44.80 o 4 15 0 439.65 464.01 64.69 o 6 15 0 67.51 54.90 45.10 o 8 15 0 0.01 -25.63 49.45 o 0 16 0 335.23 409.36 50.88 o 2 16 0 99.39 167.27 41.54 o 4 16 0 15.62 1.57 54.25 o 6 16 0 37.16 4.35 44.21 o 2 17 0 14.79 16.15 53.97 o 4 17 0 139.99 139.33 54.25 o 6 17 0 1.87 25.12 44.51 o 0 18 0 0.77 54.93 45.68 o 2 18 0 87.90 33.96 58.10 o 1 1 1 4478.80 4210.44 55.89 o 2 1 1 1857.27 1826.90 39.50 o 3 1 1 468.61 444.80 11.73 o 4 1 1 2172.35 2134.50 36.80 o 5 1 1 40.83 26.93 10.74 o 6 1 1 394.14 447.69 25.36 o 7 1 1 1068.11 1055.26 20.44 o 8 1 1 1141.05 1257.95 32.13 o 9 1 1 69.16 75.35 14.96 o 10 1 1 792.23 763.27 24.56 o 11 1 1 191.94 229.43 18.31 o 12 1 1 190.77 183.46 23.38 o 13 1 1 320.88 327.58 27.72 o 14 1 1 9.38 34.40 25.24 o 15 1 1 2.95 -4.73 28.30 o 0 2 1 931.05 847.50 34.54 o 1 2 1 2157.47 2194.89 45.50 o 2 2 1 12432.42 12318.68 131.46 o 3 2 1 265.22 267.22 15.89 o 4 2 1 0.18 9.08 12.67 o 5 2 1 1069.28 1142.41 45.71 o 6 2 1 341.23 373.86 18.78 o 7 2 1 1379.53 1342.19 33.27 o 8 2 1 412.40 425.06 24.35 o 9 2 1 204.36 198.86 23.56 o 10 2 1 227.82 292.95 24.35 o 11 2 1 2932.95 2975.25 67.35 o 12 2 1 788.70 773.29 43.15 o 13 2 1 39.16 36.20 32.04 o 14 2 1 104.55 78.12 37.72 o 15 2 1 85.51 144.38 37.61 o 1 3 1 13101.89 12543.39 277.02 o 2 3 1 670.26 694.49 20.95 o 3 3 1 1311.55 1300.60 49.76 o 4 3 1 12.48 14.56 13.03 o 5 3 1 148.94 161.18 15.44 o 6 3 1 102.06 114.02 15.80 o 7 3 1 1461.20 1389.13 64.30 o 8 3 1 197.38 194.72 21.05 o 9 3 1 842.94 915.61 32.56 o 10 3 1 422.40 449.18 27.90 o 11 3 1 423.92 393.28 39.85 o 12 3 1 56.86 85.09 29.56 o 13 3 1 773.65 662.82 48.62 o 14 3 1 11.77 78.12 47.59 o 15 3 1 30.06 61.09 37.29 o 0 4 1 1130.28 1097.77 27.84 o 1 4 1 16648.26 16151.38 263.93 o 2 4 1 42.57 54.27 15.44 o 3 4 1 5804.52 5768.40 77.10 o 4 4 1 157.86 165.32 15.80 o 5 4 1 247.96 261.96 16.83 o 6 4 1 20.63 37.06 14.75 o 7 4 1 161.06 173.21 17.97 o 8 4 1 472.45 441.98 25.15 o 9 4 1 1130.24 1174.92 35.55 o 10 4 1 1948.05 1876.41 53.72 o 11 4 1 1205.15 1264.41 53.05 o 12 4 1 236.44 250.98 36.53 o 13 4 1 23.91 31.23 31.95 o 14 4 1 29.74 33.52 38.92 o 15 4 1 7.51 -0.72 36.36 o 1 5 1 710.78 692.61 14.58 o 2 5 1 1601.53 1561.63 50.86 o 3 5 1 559.29 591.94 20.84 o 4 5 1 3748.93 3769.83 69.98 o 5 5 1 605.89 710.06 42.08 o 6 5 1 18.13 15.54 14.98 o 7 5 1 53.16 53.86 16.26 o 8 5 1 38.21 9.08 23.15 o 9 5 1 62.08 69.41 22.50 o 10 5 1 592.36 629.71 30.49 o 11 5 1 751.67 745.04 44.51 o 12 5 1 58.94 67.10 31.65 o 13 5 1 14.37 11.40 34.25 o 14 5 1 7.78 27.69 36.19 o 0 6 1 224.33 236.90 16.60 o 1 6 1 1189.85 1140.78 21.70 o 2 6 1 1246.41 1314.81 58.56 o 3 6 1 10514.55 10827.16 186.17 o 4 6 1 63.11 50.10 16.38 o 5 6 1 1509.56 1463.10 34.80 o 6 6 1 100.00 98.73 17.18 o 7 6 1 0.54 -17.62 17.62 o 8 6 1 1233.12 1174.12 34.57 o 9 6 1 1.67 -1.90 22.32 o 10 6 1 55.13 52.87 22.09 o 11 6 1 256.23 217.47 36.21 o 12 6 1 29.69 1.15 34.57 o 13 6 1 170.34 164.96 37.07 o 14 6 1 6.53 89.61 49.91 o 1 7 1 14.81 25.60 10.93 o 2 7 1 5375.26 5426.63 80.57 o 3 7 1 59.60 88.33 17.75 o 4 7 1 821.11 819.76 26.83 o 5 7 1 36.51 55.90 16.84 o 6 7 1 62.50 102.00 32.29 o 7 7 1 86.93 120.55 29.66 o 8 7 1 52.53 37.88 22.50 o 9 7 1 293.00 306.39 25.71 o 10 7 1 723.47 638.01 42.60 o 11 7 1 368.08 371.30 39.55 o 12 7 1 20.88 87.04 52.19 o 13 7 1 141.95 154.10 36.64 o 14 7 1 18.02 7.83 41.41 o 0 8 1 557.65 552.98 22.77 o 1 8 1 1859.98 2051.51 94.65 o 2 8 1 915.67 917.94 27.92 o 3 8 1 13.87 13.95 17.04 o 4 8 1 297.83 282.56 22.07 o 5 8 1 474.29 480.17 24.47 o 6 8 1 335.74 322.75 23.33 o 7 8 1 71.35 57.56 20.83 o 8 8 1 771.10 788.02 32.26 o 9 8 1 95.99 136.83 33.23 o 10 8 1 214.01 202.30 33.60 o 11 8 1 26.70 -12.15 33.78 o 12 8 1 7.19 32.53 40.12 o 13 8 1 27.27 54.82 36.63 o 1 9 1 78.28 79.09 13.72 o 2 9 1 29.84 21.84 19.46 o 3 9 1 597.76 634.69 27.39 o 4 9 1 187.04 196.90 23.33 o 5 9 1 54.85 65.01 19.81 o 6 9 1 7.41 -0.52 20.14 o 7 9 1 939.18 860.94 30.95 o 8 9 1 301.35 303.45 24.56 o 9 9 1 34.49 69.68 33.62 o 10 9 1 242.73 263.79 33.98 o 11 9 1 0.25 -19.07 33.24 o 12 9 1 93.45 111.25 37.05 o 13 9 1 151.72 222.90 43.57 o 0 10 1 47.42 63.52 20.04 o 1 10 1 0.43 -14.21 14.21 o 2 10 1 26.11 49.37 20.74 o 3 10 1 113.85 148.85 24.35 o 4 10 1 738.81 762.02 31.07 o 5 10 1 202.57 171.82 21.75 o 6 10 1 214.26 206.94 23.56 o 7 10 1 219.95 156.91 32.06 o 8 10 1 606.64 524.71 39.57 o 9 10 1 216.31 239.11 37.82 o 10 10 1 0.41 12.65 30.62 o 11 10 1 5.07 56.26 33.59 o 12 10 1 23.37 44.51 34.12 o 13 10 1 0.02 15.25 38.62 o 1 11 1 609.25 595.26 20.82 o 2 11 1 1328.86 1260.60 35.88 o 3 11 1 134.49 141.20 25.49 o 4 11 1 331.92 365.76 27.45 o 5 11 1 125.17 128.16 22.43 o 6 11 1 13.59 10.57 18.45 o 7 11 1 81.71 105.63 30.15 o 8 11 1 389.62 357.76 37.59 o 9 11 1 2.67 30.67 32.00 o 10 11 1 158.09 50.05 37.83 o 11 11 1 1.66 -4.13 33.60 o 12 11 1 30.06 12.55 38.99 o 0 12 1 867.23 899.90 32.50 o 1 12 1 38.77 56.00 16.92 o 2 12 1 183.83 154.58 25.70 o 3 12 1 109.92 95.82 26.04 o 4 12 1 166.48 191.47 26.05 o 5 12 1 31.58 -6.22 20.83 o 6 12 1 73.12 101.08 27.28 o 7 12 1 1.86 56.52 26.68 o 8 12 1 96.98 99.22 30.95 o 9 12 1 7.98 39.93 31.83 o 10 12 1 7.68 50.41 30.07 o 11 12 1 32.84 3.83 35.44 o 1 13 1 37.77 70.19 16.98 o 2 13 1 0.00 -34.10 34.10 o 3 13 1 375.75 385.18 42.40 o 4 13 1 81.72 101.55 33.74 o 5 13 1 18.90 53.34 28.22 o 6 13 1 137.05 126.38 29.85 o 7 13 1 21.01 18.02 28.84 o 8 13 1 6.24 61.16 30.89 o 9 13 1 136.04 44.45 38.16 o 10 13 1 7.24 24.85 34.03 o 11 13 1 16.99 -20.07 36.93 o 0 14 1 2.90 5.75 29.96 o 1 14 1 7.71 -11.93 21.74 o 2 14 1 93.20 58.98 33.08 o 3 14 1 339.12 444.43 41.98 o 4 14 1 149.05 113.45 35.56 o 5 14 1 504.45 440.52 39.41 o 6 14 1 34.42 37.64 27.42 o 7 14 1 40.08 7.91 33.80 o 8 14 1 3.22 -8.12 34.14 o 9 14 1 21.03 14.57 34.66 o 10 14 1 1.34 -0.39 35.37 o 1 15 1 219.99 205.11 26.06 o 2 15 1 76.27 87.04 34.55 o 3 15 1 103.32 139.18 37.18 o 4 15 1 0.89 -35.13 35.13 o 5 15 1 104.21 118.72 31.87 o 6 15 1 45.01 10.30 30.72 o 7 15 1 9.65 15.05 33.71 o 8 15 1 52.69 11.97 37.33 o 9 15 1 52.62 34.19 46.57 o 0 16 1 0.40 34.45 30.80 o 1 16 1 26.14 35.15 24.11 o 2 16 1 8.44 32.79 48.82 o 3 16 1 1.48 47.80 36.05 o 4 16 1 129.36 202.38 40.07 o 5 16 1 42.12 77.20 31.14 o 6 16 1 0.09 -29.39 29.39 o 7 16 1 12.95 5.90 32.95 o 1 17 1 14.60 -23.43 24.36 o 2 17 1 1.35 -11.69 36.09 o 3 17 1 2.85 48.16 35.05 o 4 17 1 1.53 -40.82 40.82 o 5 17 1 0.07 -10.35 30.71 o 6 17 1 39.71 26.59 32.39 o 0 18 1 4.59 -31.50 34.69 o 1 18 1 28.05 25.52 26.18 o 2 18 1 0.14 2.78 36.53 o 3 18 1 18.93 26.03 41.32 o 0 0 2 29692.79 28391.98 1249.75 o 1 0 2 3808.17 3704.86 115.01 o 2 0 2 12120.63 11913.94 366.95 o 3 0 2 1622.47 1507.62 65.20 o 4 0 2 3056.55 2965.31 86.33 o 5 0 2 0.62 14.31 18.05 o 6 0 2 7627.99 7645.95 109.88 o 7 0 2 5447.10 5512.53 101.36 o 8 0 2 299.14 341.70 116.72 o 9 0 2 609.87 618.35 40.64 o 10 0 2 565.14 495.90 37.31 o 11 0 2 0.97 -15.83 28.30 o 12 0 2 1105.62 882.44 111.26 o 13 0 2 807.04 840.43 64.95 o 14 0 2 23.34 95.17 49.16 o 15 0 2 24.53 17.61 53.14 o 1 1 2 8696.79 8030.79 176.29 o 2 1 2 3211.76 3416.11 74.97 o 3 1 2 83.72 98.18 14.16 o 4 1 2 2764.61 2728.70 55.41 o 5 1 2 124.31 128.78 14.63 o 6 1 2 127.52 112.87 16.12 o 7 1 2 46.04 39.01 14.64 o 8 1 2 58.84 87.77 18.44 o 9 1 2 23.61 29.34 21.18 o 10 1 2 37.69 33.20 21.74 o 11 1 2 400.08 356.58 25.82 o 12 1 2 4.01 -26.23 29.50 o 13 1 2 75.82 97.89 35.79 o 14 1 2 0.02 14.43 33.77 o 15 1 2 37.86 42.36 38.44 o 0 2 2 5926.31 5852.12 77.30 o 1 2 2 219.60 204.04 12.28 o 2 2 2 9180.61 9175.32 100.71 o 3 2 2 172.20 176.92 20.96 o 4 2 2 3622.26 3531.78 85.67 o 5 2 2 3959.85 4144.82 129.25 o 6 2 2 2098.69 2190.55 75.00 o 7 2 2 747.74 802.95 40.44 o 8 2 2 96.14 146.79 27.67 o 9 2 2 195.68 217.54 31.75 o 10 2 2 169.92 190.32 33.92 o 11 2 2 306.64 254.22 34.54 o 12 2 2 87.53 54.98 44.51 o 13 2 2 40.89 32.59 48.59 o 14 2 2 25.09 23.49 51.16 o 15 2 2 32.70 -31.42 58.64 o 1 3 2 38938.13 37856.20 1143.30 o 2 3 2 2851.40 2793.63 74.76 o 3 3 2 46.06 35.83 20.31 o 4 3 2 2112.10 1943.73 113.40 o 5 3 2 951.81 950.84 36.08 o 6 3 2 88.60 99.82 23.53 o 7 3 2 2257.67 2280.45 77.07 o 8 3 2 342.79 361.02 33.62 o 9 3 2 947.71 949.03 45.39 o 10 3 2 221.58 210.23 34.85 o 11 3 2 121.88 99.20 45.68 o 12 3 2 194.39 153.77 45.68 o 13 3 2 59.38 68.85 46.56 o 14 3 2 0.27 59.32 43.92 o 15 3 2 176.58 134.20 33.62 o 0 4 2 2486.69 2356.64 93.60 o 1 4 2 19312.70 18812.65 455.10 o 2 4 2 1218.10 1173.10 41.84 o 3 4 2 253.73 304.41 27.24 o 4 4 2 255.90 253.13 24.49 o 5 4 2 245.43 284.21 25.12 o 6 4 2 25.37 4.93 20.96 o 7 4 2 924.86 808.78 69.99 o 8 4 2 250.55 246.51 29.24 o 9 4 2 408.10 385.62 39.73 o 10 4 2 6.70 28.28 31.44 o 11 4 2 138.64 110.73 48.30 o 12 4 2 152.22 241.54 48.70 o 13 4 2 73.70 79.92 49.45 o 14 4 2 68.34 86.85 54.25 o 15 4 2 0.98 -34.77 56.46 o 1 5 2 620.32 601.83 20.38 o 2 5 2 6404.81 6404.56 103.28 o 3 5 2 307.02 264.53 25.12 o 4 5 2 2111.12 2090.63 74.53 o 5 5 2 419.05 431.20 27.98 o 6 5 2 8.79 -26.74 26.74 o 7 5 2 1055.38 961.20 43.91 o 8 5 2 607.98 581.22 38.22 o 9 5 2 138.53 109.15 35.77 o 10 5 2 167.90 194.05 32.99 o 11 5 2 1186.88 1125.47 70.70 o 12 5 2 91.50 73.72 44.21 o 13 5 2 365.42 369.30 55.64 o 14 5 2 41.21 52.74 53.70 o 0 6 2 245.32 252.85 23.53 o 1 6 2 42.59 26.08 15.11 o 2 6 2 1441.49 1430.24 47.14 o 3 6 2 2673.91 2799.22 86.17 o 4 6 2 172.30 168.77 24.17 o 5 6 2 1046.99 1086.85 40.34 o 6 6 2 161.29 164.44 25.76 o 7 6 2 26.18 35.30 26.40 o 8 6 2 33.90 19.76 27.98 o 9 6 2 0.38 28.63 30.81 o 10 6 2 22.15 -8.03 44.21 o 11 6 2 295.20 284.34 49.74 o 12 6 2 30.46 9.60 49.45 o 13 6 2 193.56 314.51 68.34 o 14 6 2 20.74 25.09 55.36 o 1 7 2 249.82 244.05 18.98 o 2 7 2 4530.42 4633.60 98.53 o 3 7 2 3466.10 3855.13 266.59 o 4 7 2 2684.04 2684.31 86.98 o 5 7 2 43.88 28.69 23.53 o 6 7 2 21.28 16.47 24.81 o 7 7 2 333.90 326.43 31.75 o 8 7 2 772.80 779.07 42.73 o 9 7 2 892.28 876.18 48.01 o 10 7 2 75.83 133.90 40.04 o 11 7 2 12.17 16.55 42.14 o 12 7 2 9.58 57.62 46.85 o 13 7 2 32.05 -30.07 50.59 o 14 7 2 146.73 185.75 32.68 o 0 8 2 1445.36 1447.75 50.31 o 1 8 2 2293.67 2383.33 62.90 o 2 8 2 625.32 683.93 36.39 o 3 8 2 1076.37 1100.74 42.43 o 4 8 2 65.58 99.94 27.03 o 5 8 2 41.08 36.35 25.76 o 6 8 2 144.99 186.92 29.24 o 7 8 2 579.34 566.85 38.83 o 8 8 2 1010.25 1046.23 45.68 o 9 8 2 2148.22 2069.63 81.96 o 10 8 2 26.91 -4.34 39.43 o 11 8 2 100.55 92.96 48.88 o 12 8 2 9.80 12.05 46.85 o 13 8 2 78.05 91.81 52.86 o 1 9 2 292.24 299.40 20.65 o 2 9 2 314.42 256.40 35.00 o 3 9 2 1202.65 1352.65 67.18 o 4 9 2 22.45 55.02 27.98 o 5 9 2 1.45 13.69 28.30 o 6 9 2 46.71 55.07 28.30 o 7 9 2 304.36 289.09 34.23 o 8 9 2 244.71 171.60 39.29 o 9 9 2 1284.03 1301.36 73.59 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