#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/26/2202620.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202620_Fobs loop_ _publ_author_name 'Chohan, Zahid H.' 'Comerlato, Nadia M.' 'Howie, R. Alan' 'Skakle, Janet M. S.' 'Wardell, James L.' _publ_section_title ; 1,4-Dimethylpyridinium bis(2-oxo-1,3-dithiole-4,5-dithiolato)diphenylantimonate(V) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1006 _journal_page_last m1009 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 94.063 _cell_angle_beta 112.126 _cell_angle_gamma 108.137 _cell_length_a 10.7513 _cell_length_b 12.0130 _cell_length_c 13.5273 _exptl_crystal_F_000 744.00 _reflns_d_resolution_high 0.6617 _[local]_cod_data_source_file dn6098IVsup2.hkl _[local]_cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1,4-diMePy [Sb(dmio)2] P-1, Z=2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 184.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 14914.70 15361.83 280.68 o 2 0 0 1056.29 1129.38 18.53 o 3 0 0 56.62 64.53 8.74 o 4 0 0 874.51 915.74 23.92 o 5 0 0 10870.90 11032.86 94.72 o 6 0 0 1526.14 1543.55 36.74 o 7 0 0 4388.31 4083.47 64.63 o 8 0 0 396.83 336.15 22.33 o 9 0 0 117.46 118.98 17.07 o 10 0 0 42.08 30.59 15.17 o 11 0 0 50.31 8.51 23.30 o 12 0 0 429.41 463.25 48.39 o -12 1 0 454.85 456.98 47.04 o -11 1 0 113.94 83.78 27.33 o -10 1 0 470.35 491.72 29.59 o -9 1 0 328.73 357.00 23.90 o -8 1 0 1011.42 1092.93 36.54 o -7 1 0 5.03 -11.85 11.85 o -6 1 0 212.15 192.92 18.14 o -5 1 0 11094.10 11600.63 95.20 o -4 1 0 14293.10 14927.14 101.69 o -3 1 0 5138.23 5145.84 46.86 o -2 1 0 623.94 666.86 13.35 o -1 1 0 801.09 911.71 18.82 o 0 1 0 4419.27 4511.53 47.94 o 1 1 0 10992.33 11380.58 96.08 o 2 1 0 3516.37 3598.72 36.36 o 3 1 0 1561.94 1565.01 34.05 o 4 1 0 2148.05 2026.97 35.91 o 5 1 0 1904.76 1952.30 38.76 o 6 1 0 2.13 -2.16 9.34 o 7 1 0 241.14 230.67 19.25 o 8 1 0 3.42 5.00 13.22 o 9 1 0 251.54 293.20 39.43 o 10 1 0 246.95 264.79 25.34 o 11 1 0 68.74 62.00 25.76 o -13 2 0 136.70 158.60 36.74 o -12 2 0 233.68 280.91 39.43 o -11 2 0 234.12 252.23 36.74 o -10 2 0 3.85 -6.50 12.04 o -9 2 0 801.75 768.61 32.58 o -8 2 0 1231.23 1198.24 36.81 o -7 2 0 10410.12 10460.41 103.65 o -6 2 0 2344.37 2452.23 51.75 o -5 2 0 123.87 121.93 12.05 o -4 2 0 625.44 604.86 18.40 o -3 2 0 427.36 462.19 13.42 o -2 2 0 19506.66 20194.17 351.47 o -1 2 0 380.35 411.73 12.99 o 0 2 0 25583.07 25436.45 157.03 o 1 2 0 9136.27 9949.78 67.00 o 2 2 0 5345.06 5410.00 38.15 o 3 2 0 32.65 27.06 8.48 o 4 2 0 22.68 8.06 12.10 o 5 2 0 3420.92 3419.64 53.81 o 6 2 0 637.72 626.00 27.78 o 7 2 0 50.44 51.74 14.09 o 8 2 0 58.24 72.93 15.37 o 9 2 0 27.60 42.31 14.41 o 10 2 0 81.16 108.87 19.01 o 11 2 0 12.91 -6.72 21.06 o -14 3 0 4.00 29.12 32.71 o -13 3 0 0.04 29.12 26.43 o -12 3 0 515.66 571.22 50.63 o -11 3 0 1157.66 1075.69 65.41 o -10 3 0 1352.03 1372.72 69.44 o -9 3 0 977.66 970.23 35.53 o -8 3 0 471.91 475.02 36.51 o -7 3 0 845.66 823.47 27.88 o -6 3 0 33.82 44.50 9.57 o -5 3 0 3146.21 3332.51 69.67 o -4 3 0 5046.65 5093.86 50.81 o -3 3 0 10039.54 10666.42 112.00 o -2 3 0 14042.63 15208.45 329.07 o -1 3 0 112.12 152.33 12.54 o 0 3 0 22399.15 23258.34 180.10 o 1 3 0 289.73 282.32 9.05 o 2 3 0 6546.15 6813.75 112.28 o 3 3 0 3471.05 3501.32 81.82 o 4 3 0 210.39 212.97 14.61 o 5 3 0 157.13 146.51 14.64 o 6 3 0 1017.77 1022.41 33.55 o 7 3 0 673.92 675.10 30.36 o 8 3 0 495.19 525.83 28.83 o 9 3 0 460.93 429.66 27.85 o 10 3 0 315.80 297.04 39.43 o 11 3 0 73.87 45.70 28.23 o -14 4 0 243.78 342.73 47.49 o -13 4 0 201.87 191.75 36.74 o -12 4 0 6.49 25.54 24.64 o -11 4 0 94.21 104.39 28.23 o -10 4 0 163.65 129.03 28.23 o -9 4 0 1316.11 1416.18 65.86 o -8 4 0 47.83 42.21 11.99 o -7 4 0 237.83 224.23 15.60 o -6 4 0 2614.11 2539.87 42.71 o -5 4 0 229.06 250.89 19.71 o -4 4 0 101.08 109.95 10.33 o -3 4 0 1836.51 2011.82 26.93 o -2 4 0 186.19 152.77 13.44 o -1 4 0 1798.02 1904.52 41.22 o 0 4 0 3035.20 3232.89 59.14 o 1 4 0 1221.29 1211.90 18.88 o 2 4 0 942.75 983.24 18.31 o 3 4 0 99.37 106.82 9.24 o 4 4 0 587.54 581.28 22.69 o 5 4 0 8.08 16.41 10.97 o 6 4 0 1030.59 967.81 33.78 o 7 4 0 829.64 825.99 42.34 o 8 4 0 305.55 320.30 24.61 o 9 4 0 206.90 228.04 36.29 o 10 4 0 127.97 128.58 30.91 o 11 4 0 106.49 230.28 42.11 o 12 4 0 131.76 165.77 40.32 o -14 5 0 0.00 6.27 26.88 o -13 5 0 1.43 0.45 25.54 o -12 5 0 88.77 79.75 27.78 o -11 5 0 597.60 568.09 49.73 o -10 5 0 492.85 518.36 44.35 o -9 5 0 335.20 304.65 33.60 o -8 5 0 198.07 187.84 16.36 o -7 5 0 130.23 97.22 19.71 o -6 5 0 64.61 59.11 10.44 o -5 5 0 906.62 844.22 23.10 o -4 5 0 4384.33 4447.63 50.57 o -3 5 0 466.74 488.90 15.68 o -2 5 0 9.82 0.00 11.20 o -1 5 0 1923.17 2107.02 48.39 o 0 5 0 1177.58 1121.39 38.53 o 1 5 0 6546.51 6639.30 78.28 o 2 5 0 3072.25 3047.23 52.02 o 3 5 0 7749.50 7702.21 96.33 o 4 5 0 1479.37 1583.93 68.55 o 5 5 0 135.25 138.33 15.94 o 6 5 0 210.15 217.92 19.16 o 7 5 0 1101.82 1077.41 39.28 o 8 5 0 1288.99 1315.38 71.23 o 9 5 0 362.48 402.77 46.59 o 10 5 0 52.29 24.64 28.23 o 11 5 0 75.93 109.32 34.50 o -15 6 0 23.94 48.83 32.71 o -14 6 0 93.60 163.08 37.63 o -13 6 0 513.79 560.47 56.45 o -12 6 0 148.48 170.69 34.50 o -11 6 0 42.38 55.11 27.33 o -10 6 0 47.51 38.08 23.30 o -9 6 0 724.99 648.28 46.59 o -8 6 0 219.11 236.10 30.91 o -7 6 0 186.59 187.57 14.91 o -6 6 0 4464.29 4407.91 58.06 o -5 6 0 995.91 1056.52 47.04 o -4 6 0 632.68 625.82 25.31 o -3 6 0 2831.42 2768.37 38.80 o -2 6 0 1183.27 1128.55 37.63 o -1 6 0 16175.30 15654.60 161.29 o 0 6 0 1948.69 1919.75 55.11 o 1 6 0 613.70 654.84 24.85 o 2 6 0 1665.94 1664.54 27.27 o 3 6 0 1116.89 1064.45 23.10 o 4 6 0 1131.89 1139.93 35.09 o 5 6 0 1095.42 1080.31 35.63 o 6 6 0 1769.27 1704.82 47.69 o 7 6 0 75.87 41.67 25.54 o 8 6 0 47.24 44.80 27.78 o 9 6 0 41.13 27.33 27.33 o 10 6 0 51.57 54.66 30.91 o 11 6 0 87.75 112.00 37.19 o -15 7 0 1.70 12.10 31.36 o -14 7 0 0.90 -26.88 26.88 o -13 7 0 96.00 86.02 32.26 o -12 7 0 16.88 17.02 25.98 o -11 7 0 383.17 363.34 42.11 o -10 7 0 0.88 -8.96 18.82 o -9 7 0 13.24 -4.48 19.71 o -8 7 0 0.35 -15.68 15.68 o -7 7 0 3.84 -3.76 11.20 o -6 7 0 3161.53 3100.00 64.07 o -5 7 0 2655.27 2741.35 53.31 o -4 7 0 3067.39 3225.59 94.31 o -3 7 0 91.44 81.99 17.02 o -2 7 0 822.97 897.38 37.63 o -1 7 0 3043.68 2914.35 70.34 o 0 7 0 1366.14 1296.56 48.83 o 1 7 0 5948.90 5767.17 67.41 o 2 7 0 607.68 609.23 18.61 o 3 7 0 846.44 848.77 45.92 o 4 7 0 239.68 239.03 19.16 o 5 7 0 27.06 6.12 13.78 o 6 7 0 491.44 491.92 47.04 o 7 7 0 156.71 116.48 31.81 o 8 7 0 205.98 195.34 36.29 o 9 7 0 62.95 65.41 29.57 o 10 7 0 18.53 39.87 32.26 o -14 8 0 32.27 68.55 32.26 o -13 8 0 152.38 142.47 37.63 o -12 8 0 371.40 344.52 43.91 o -11 8 0 9.39 6.72 22.85 o -10 8 0 1.77 1.34 18.82 o -9 8 0 325.48 308.24 37.19 o -8 8 0 2773.06 2726.63 92.74 o -7 8 0 1953.62 1807.30 71.23 o -6 8 0 7.76 -1.07 10.44 o -5 8 0 141.64 121.99 12.83 o -4 8 0 827.16 789.12 25.18 o -3 8 0 1906.44 1986.95 56.90 o -2 8 0 3244.54 3133.88 73.47 o -1 8 0 3087.95 2979.31 73.47 o 0 8 0 608.30 568.98 35.84 o 1 8 0 414.90 439.67 21.50 o 2 8 0 45.52 53.31 21.95 o 3 8 0 762.52 735.42 30.88 o 4 8 0 924.06 926.42 35.20 o 5 8 0 546.47 498.19 45.70 o 6 8 0 162.67 153.67 30.47 o 7 8 0 20.71 18.82 21.06 o 8 8 0 2.92 12.99 25.54 o 9 8 0 0.66 41.67 28.23 o 10 8 0 8.94 69.44 32.71 o -14 9 0 66.42 63.62 33.15 o -13 9 0 393.53 399.18 50.18 o -12 9 0 498.82 511.19 52.87 o -11 9 0 399.55 350.80 42.56 o -10 9 0 149.64 138.89 31.36 o -9 9 0 6.22 -1.79 20.61 o -8 9 0 581.92 545.24 45.25 o -7 9 0 1249.56 1102.57 57.35 o -6 9 0 2482.41 2431.88 38.53 o -5 9 0 570.35 609.10 23.76 o -4 9 0 1224.17 1162.84 32.14 o -3 9 0 1498.00 1556.86 54.21 o -2 9 0 153.88 171.14 23.74 o -1 9 0 3080.59 2848.04 79.75 o 0 9 0 138.55 112.91 14.42 o 1 9 0 352.72 401.40 21.96 o 2 9 0 822.25 859.74 54.21 o 3 9 0 253.19 276.87 35.39 o 4 9 0 0.17 -8.51 18.82 o 5 9 0 48.11 39.87 27.33 o 6 9 0 15.20 2.69 24.64 o 7 9 0 3.69 -17.92 25.98 o 8 9 0 65.71 61.83 34.05 o 9 9 0 34.68 4.93 26.43 o -14 10 0 58.37 54.66 35.39 o -13 10 0 93.88 80.19 37.63 o -12 10 0 0.09 -1.34 21.95 o -11 10 0 17.89 15.23 21.50 o -10 10 0 112.92 111.56 30.47 o -9 10 0 199.01 223.56 33.15 o -8 10 0 370.35 392.91 39.87 o -7 10 0 487.52 456.98 40.32 o -6 10 0 38.36 28.14 9.14 o -5 10 0 190.15 171.60 15.84 o -4 10 0 236.41 223.75 17.71 o -3 10 0 604.49 604.82 37.63 o -2 10 0 1312.76 1277.30 55.11 o -1 10 0 1.33 2.69 17.92 o 0 10 0 77.09 103.49 15.15 o 1 10 0 241.63 249.55 30.47 o 2 10 0 156.27 119.62 29.12 o 3 10 0 376.65 315.85 37.19 o 4 10 0 147.92 132.16 29.57 o 5 10 0 112.80 106.18 29.57 o 6 10 0 37.69 22.40 23.74 o 7 10 0 45.93 42.56 29.57 o 8 10 0 17.37 32.71 29.57 o -14 11 0 43.46 63.17 34.05 o -13 11 0 33.92 29.12 29.57 o -12 11 0 142.40 165.77 34.50 o -11 11 0 125.79 114.24 31.36 o -10 11 0 775.41 772.83 60.93 o -9 11 0 32.33 20.61 20.16 o -8 11 0 129.30 91.40 23.74 o -7 11 0 146.06 106.18 23.30 o -6 11 0 218.35 187.72 26.88 o -5 11 0 1221.19 1221.41 37.07 o -4 11 0 373.36 362.75 22.75 o -3 11 0 459.30 419.34 34.95 o -2 11 0 90.58 82.44 22.40 o -1 11 0 6.36 -12.10 17.47 o 0 11 0 268.44 256.27 33.60 o 1 11 0 210.43 227.14 31.81 o 2 11 0 853.04 852.13 56.90 o 3 11 0 110.99 107.97 27.33 o 4 11 0 0.03 -5.82 24.19 o 5 11 0 19.78 44.35 25.54 o 6 11 0 32.35 57.35 30.91 o 7 11 0 94.92 143.81 40.32 o -14 12 0 71.61 90.95 34.50 o -13 12 0 0.80 30.02 25.54 o -12 12 0 5.90 -20.16 26.88 o -11 12 0 19.79 33.15 27.33 o -10 12 0 213.38 287.18 40.77 o -9 12 0 165.91 226.25 34.50 o -8 12 0 132.49 91.84 23.74 o -7 12 0 169.22 168.45 28.67 o -6 12 0 177.39 189.51 28.67 o -5 12 0 13.79 6.87 12.80 o -4 12 0 347.77 319.18 18.60 o -3 12 0 281.85 301.07 33.60 o -2 12 0 269.45 247.31 32.71 o -1 12 0 221.41 209.67 30.02 o 0 12 0 115.82 113.35 28.23 o 1 12 0 95.73 114.24 28.67 o 2 12 0 207.81 217.29 37.63 o 3 12 0 85.78 81.54 27.78 o 4 12 0 105.71 140.23 33.60 o 5 12 0 90.02 98.56 32.26 o 6 12 0 3.96 13.89 28.67 o -13 13 0 1.94 -15.23 28.67 o -12 13 0 144.60 133.06 36.74 o -11 13 0 31.24 -2.24 26.43 o -10 13 0 80.92 88.26 31.81 o -9 13 0 115.96 102.15 29.57 o -8 13 0 6.03 20.16 18.37 o -7 13 0 238.83 236.10 34.50 o -6 13 0 283.77 282.25 35.39 o -4 13 0 66.56 58.14 17.07 o -3 13 0 2.43 -0.45 21.95 o -2 13 0 38.42 36.74 23.74 o -1 13 0 41.77 46.59 23.74 o 0 13 0 542.18 541.65 47.94 o 1 13 0 197.26 185.03 34.95 o 2 13 0 64.09 67.65 28.67 o 3 13 0 1.35 0.45 24.64 o 4 13 0 1.55 14.34 29.12 o 5 13 0 86.07 87.81 35.39 o -13 14 0 68.29 34.95 32.26 o -12 14 0 3.14 -8.51 28.67 o -11 14 0 45.84 40.32 30.91 o -10 14 0 117.03 131.27 35.39 o -9 14 0 116.20 142.47 30.47 o -8 14 0 450.23 472.66 48.83 o -7 14 0 9.20 2.69 19.71 o -6 14 0 28.51 16.13 18.82 o -4 14 0 33.13 30.42 16.26 o -3 14 0 279.47 325.71 38.53 o -2 14 0 179.95 217.29 34.05 o -1 14 0 40.77 7.17 24.64 o 0 14 0 15.37 14.34 21.06 o 1 14 0 23.18 27.33 25.98 o 2 14 0 139.52 130.82 34.05 o 3 14 0 28.41 21.50 28.67 o 4 14 0 49.26 41.22 28.67 o -12 15 0 54.28 76.61 35.84 o -11 15 0 17.74 37.19 29.57 o -10 15 0 3.37 91.84 34.50 o -9 15 0 0.78 39.43 25.09 o -8 15 0 62.82 73.92 27.33 o -7 15 0 363.74 388.43 45.70 o -6 15 0 133.04 93.19 25.54 o -3 15 0 0.76 9.86 23.74 o -2 15 0 124.99 124.55 31.81 o -1 15 0 171.23 223.56 36.29 o 0 15 0 61.20 91.40 32.71 o 1 15 0 30.45 31.36 28.67 o 2 15 0 25.92 33.15 29.57 o 3 15 0 0.31 7.17 25.09 o -11 16 0 8.67 4.93 29.12 o -10 16 0 40.22 55.55 30.91 o -9 16 0 59.10 34.95 23.30 o -8 16 0 51.23 33.60 24.64 o -7 16 0 9.22 11.20 21.95 o -6 16 0 18.82 20.61 22.85 o -3 16 0 124.17 148.74 31.81 o -2 16 0 41.08 21.06 28.67 o -1 16 0 2.98 16.13 27.78 o 0 16 0 3.30 30.02 27.33 o 1 16 0 0.37 -1.34 30.47 o -9 17 0 23.35 38.53 28.67 o -8 17 0 64.27 77.06 31.36 o -7 17 0 23.91 25.98 24.19 o -6 17 0 47.41 69.44 28.67 o -2 17 0 11.49 31.36 32.71 o -1 17 0 30.06 69.44 32.26 o 6 -18 1 25.22 27.78 25.54 o 0 -17 1 5.90 38.08 35.84 o 1 -17 1 26.88 24.64 31.81 o 2 -17 1 72.86 90.05 32.26 o 6 -17 1 1.65 8.96 21.95 o 7 -17 1 12.64 33.60 26.43 o 8 -17 1 86.82 138.89 37.19 o 9 -17 1 42.13 60.48 31.81 o -2 -16 1 32.30 72.13 32.26 o -1 -16 1 17.40 21.95 29.12 o 0 -16 1 63.85 85.57 32.71 o 1 -16 1 25.65 46.15 29.57 o 2 -16 1 1.62 6.27 25.09 o 3 -16 1 70.97 65.47 20.03 o 6 -16 1 73.75 57.35 25.09 o 7 -16 1 114.69 138.89 32.71 o 8 -16 1 7.31 1.79 23.30 o 9 -16 1 2.09 -4.48 21.95 o 10 -16 1 5.18 57.79 32.26 o 11 -16 1 3.20 41.22 34.50 o -3 -15 1 22.28 16.58 25.54 o -2 -15 1 0.80 60.48 31.81 o -1 -15 1 2.26 -1.79 27.78 o 0 -15 1 6.14 -8.06 26.43 o 1 -15 1 74.77 62.72 27.78 o 2 -15 1 202.39 262.99 40.32 o 3 -15 1 14.49 44.89 17.92 o 4 -15 1 140.05 164.27 22.84 o 6 -15 1 0.35 0.45 20.61 o 7 -15 1 123.31 172.04 34.50 o 8 -15 1 50.39 37.63 24.64 o 9 -15 1 119.24 133.51 34.50 o 10 -15 1 83.79 46.59 28.23 o 11 -15 1 58.81 88.71 35.39 o 12 -15 1 0.05 15.23 31.36 o -4 -14 1 0.16 25.98 25.98 o -3 -14 1 23.92 29.12 25.09 o -2 -14 1 88.79 146.05 34.95 o -1 -14 1 188.87 204.74 38.08 o 0 -14 1 232.98 194.44 36.29 o 1 -14 1 125.87 109.76 29.57 o 2 -14 1 0.55 -15.68 21.50 o 3 -14 1 19.26 9.86 23.30 o 4 -14 1 40.06 75.27 23.30 o 7 -14 1 60.30 56.90 25.09 o 8 -14 1 1.81 -8.06 17.47 o 9 -14 1 12.09 33.60 24.19 o 10 -14 1 8.17 26.88 27.78 o 11 -14 1 168.56 173.83 40.77 o 12 -14 1 83.86 135.30 38.53 o -6 -13 1 27.62 27.78 32.26 o -5 -13 1 61.08 24.19 27.33 o -4 -13 1 20.26 7.62 27.78 o -3 -13 1 226.62 230.73 38.53 o -2 -13 1 82.65 137.09 32.26 o -1 -13 1 0.63 -21.95 21.95 o 0 -13 1 107.16 108.42 29.12 o 1 -13 1 83.96 125.00 27.78 o 2 -13 1 567.60 557.78 45.70 o 3 -13 1 152.54 146.50 27.78 o 4 -13 1 353.95 386.25 34.50 o 5 -13 1 19.84 3.02 14.48 o 7 -13 1 397.97 417.55 44.35 o 8 -13 1 51.16 19.26 22.40 o 9 -13 1 446.34 466.83 50.18 o 10 -13 1 117.81 140.68 35.39 o 11 -13 1 17.00 14.78 23.30 o 12 -13 1 56.55 54.21 32.71 o 13 -13 1 38.92 34.50 28.23 o -7 -12 1 59.66 77.51 32.71 o -6 -12 1 75.87 70.79 33.60 o -5 -12 1 0.33 -25.09 25.09 o -4 -12 1 4.81 -4.48 25.54 o -3 -12 1 102.81 90.50 26.88 o -2 -12 1 420.08 445.78 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