#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/26/2202624.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202624_Fobs loop_ _publ_author_name 'Fischer, Andreas' 'Palladino, Giuseppe' _publ_section_title ; Trisodium citrate dihydrate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1080 _journal_page_last m1082 _journal_volume 59 _journal_year 2003 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.584 _cell_angle_gamma 90.000 _cell_length_a 15.7040 _cell_length_b 12.5010 _cell_length_c 11.2840 _exptl_crystal_F_000 1200.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file dn6103Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound X' _shelx_refln_list_code 4 _shelx_f_calc_maximum 256.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1308.79 1271.23 35.26 o 6 0 0 729.55 693.22 25.07 o 8 0 0 1240.69 1224.87 38.55 o 10 0 0 6467.40 6329.34 161.64 o 12 0 0 365.16 296.04 22.95 o 14 0 0 19028.21 20154.76 567.75 o 16 0 0 522.99 583.96 110.60 o 18 0 0 182.65 -35.51 141.67 o 5 1 0 2400.72 1899.96 39.63 o 7 1 0 11367.18 12446.25 202.29 o 9 1 0 6368.08 6270.11 108.52 o 11 1 0 1950.64 1949.36 46.49 o 13 1 0 1541.76 1527.33 54.74 o 15 1 0 2410.19 2615.54 95.01 o 17 1 0 322.49 234.79 97.30 o 19 1 0 44.48 10.51 105.56 o 4 2 0 18352.65 18616.40 387.26 o 6 2 0 20.23 48.71 7.66 o 8 2 0 905.10 823.68 27.20 o 10 2 0 2804.87 2717.47 71.92 o 12 2 0 254.94 242.03 27.91 o 14 2 0 329.82 260.87 46.13 o 16 2 0 118.43 121.86 47.99 o 18 2 0 148.41 116.83 82.08 o 1 3 0 801.39 783.96 25.22 o 3 3 0 85.96 104.03 10.71 o 5 3 0 29762.70 31299.53 688.56 o 7 3 0 7122.90 7087.88 143.61 o 9 3 0 63.46 74.92 10.31 o 11 3 0 674.81 657.43 38.23 o 13 3 0 935.90 879.67 53.66 o 15 3 0 237.42 216.06 35.24 o 17 3 0 572.08 592.97 73.76 o 19 3 0 600.52 793.19 192.61 o 0 4 0 15204.82 15955.82 457.69 o 2 4 0 9927.65 10566.75 233.79 o 4 4 0 5407.99 5011.93 100.48 o 6 4 0 2137.71 1954.93 81.65 o 8 4 0 2417.51 2627.43 61.48 o 10 4 0 62.37 49.96 10.47 o 12 4 0 2008.49 1993.25 96.56 o 14 4 0 51.37 87.96 35.21 o 16 4 0 80.46 125.01 46.68 o 18 4 0 345.70 263.76 166.61 o 1 5 0 18969.25 17981.17 358.38 o 3 5 0 25089.52 25234.75 567.41 o 5 5 0 4438.35 4431.41 105.68 o 7 5 0 215.53 200.74 17.00 o 9 5 0 2037.92 1940.01 59.42 o 11 5 0 4526.52 4785.37 120.17 o 13 5 0 3102.54 3301.20 122.33 o 15 5 0 65.64 42.78 38.60 o 17 5 0 343.47 528.43 71.29 o 0 6 0 2963.78 3094.68 122.99 o 2 6 0 37548.88 38514.52 759.41 o 4 6 0 9711.43 9472.47 216.92 o 6 6 0 3.79 18.03 16.93 o 8 6 0 1895.90 1856.79 57.43 o 10 6 0 0.13 19.19 24.89 o 12 6 0 601.64 630.24 34.18 o 14 6 0 245.24 308.01 56.30 o 16 6 0 1488.49 1431.80 215.69 o 18 6 0 1441.71 1747.09 260.84 o 1 7 0 20450.39 21151.22 451.09 o 3 7 0 6673.47 6563.46 170.49 o 5 7 0 1.63 36.85 24.35 o 7 7 0 732.13 743.10 39.55 o 9 7 0 1667.97 1855.39 115.12 o 11 7 0 5118.23 5162.07 124.39 o 13 7 0 3098.65 3183.32 92.50 o 15 7 0 1580.18 1562.93 113.28 o 17 7 0 1085.47 703.66 111.90 o 0 8 0 33.59 -6.36 57.46 o 2 8 0 253.34 264.98 33.11 o 4 8 0 0.12 27.46 23.60 o 6 8 0 1502.71 1685.91 59.27 o 8 8 0 597.45 563.06 61.42 o 10 8 0 1858.93 1731.34 56.43 o 12 8 0 33.69 41.52 26.42 o 14 8 0 23.85 -26.25 62.47 o 16 8 0 409.54 639.71 150.07 o 1 9 0 57.13 3.88 23.29 o 3 9 0 226.63 270.08 35.38 o 5 9 0 152.27 202.38 32.15 o 7 9 0 1722.27 1945.07 77.92 o 9 9 0 933.41 998.59 60.95 o 11 9 0 166.39 189.69 35.53 o 13 9 0 227.30 246.10 88.02 o 15 9 0 222.73 165.62 103.51 o 0 10 0 499.31 412.15 92.34 o 2 10 0 281.10 282.09 42.47 o 4 10 0 1782.47 1598.13 75.98 o 6 10 0 1631.93 1875.50 77.70 o 8 10 0 2224.29 2153.42 89.63 o 10 10 0 3482.89 3261.84 116.73 o 12 10 0 25.31 -25.70 54.25 o 14 10 0 19.41 30.32 106.82 o 1 11 0 336.99 387.09 52.04 o 3 11 0 238.28 146.33 40.48 o 5 11 0 1838.77 1817.23 78.77 o 7 11 0 0.57 -41.40 51.71 o 9 11 0 1222.86 1286.05 89.81 o 11 11 0 184.82 203.05 69.01 o 13 11 0 129.07 -1.90 149.11 o 0 12 0 7712.49 8403.43 296.86 o 2 12 0 1232.90 1043.89 71.22 o 4 12 0 1227.20 1106.62 87.32 o 6 12 0 655.93 752.78 73.06 o 8 12 0 6.24 49.61 61.10 o 10 12 0 506.19 621.26 86.90 o 12 12 0 197.69 39.81 122.46 o 1 13 0 219.68 199.73 104.37 o 3 13 0 172.31 124.07 62.10 o 5 13 0 386.81 272.40 76.20 o 7 13 0 81.91 54.45 53.31 o 9 13 0 82.88 63.49 83.02 o 11 13 0 17.17 -14.59 195.69 o 0 14 0 605.28 591.36 124.77 o 2 14 0 0.00 81.76 85.37 o 4 14 0 9.56 68.79 66.45 o 6 14 0 10.60 142.47 101.96 o 8 14 0 853.91 1082.22 142.46 o 10 14 0 80.71 44.41 79.86 o 1 15 0 76.31 168.24 116.34 o 3 15 0 159.72 196.08 101.93 o 5 15 0 743.31 1072.86 163.94 o 7 15 0 19.19 -41.27 193.55 o 0 16 0 26.28 -165.57 163.67 o 2 16 0 166.33 3.93 230.72 o -19 1 1 38.74 81.89 157.33 o -17 1 1 179.19 96.60 66.32 o -15 1 1 1101.09 1186.99 107.85 o -13 1 1 150.08 138.76 20.39 o -11 1 1 2186.42 2214.30 75.43 o -9 1 1 28.09 5.26 10.82 o -7 1 1 377.78 560.14 24.06 o -5 1 1 10007.26 9311.77 220.95 o 3 1 1 71.58 95.71 8.28 o 5 1 1 1810.69 2037.13 39.77 o 7 1 1 98.10 98.54 12.18 o 9 1 1 11092.48 11026.61 194.54 o 11 1 1 810.78 842.27 28.76 o 13 1 1 1622.34 1666.99 50.35 o 15 1 1 1096.65 1117.12 39.00 o 17 1 1 468.74 315.18 81.53 o 19 1 1 56.58 85.13 117.78 o -18 2 1 30.97 17.06 80.81 o -16 2 1 2808.32 2770.97 132.25 o -14 2 1 1752.87 1676.82 60.39 o -12 2 1 518.27 475.64 37.22 o -10 2 1 5062.86 5122.70 108.54 o -8 2 1 2542.55 2266.66 55.98 o -6 2 1 32752.25 31434.88 580.22 o -4 2 1 544.41 613.61 17.42 o 2 2 1 1320.63 1222.12 30.99 o 4 2 1 16101.91 17056.12 316.12 o 6 2 1 2813.20 2670.29 52.68 o 8 2 1 22106.71 21697.69 377.46 o 10 2 1 357.56 388.41 20.34 o 12 2 1 82.68 91.03 20.74 o 14 2 1 487.31 502.21 25.70 o 16 2 1 760.82 760.78 107.26 o 18 2 1 911.64 692.24 132.36 o -19 3 1 31.59 19.58 120.53 o -17 3 1 223.23 241.33 158.55 o -15 3 1 3.84 18.29 27.05 o -13 3 1 2433.00 2425.85 84.36 o -11 3 1 1112.39 1061.39 53.86 o -9 3 1 2051.21 1906.57 65.32 o -7 3 1 822.91 1093.73 29.21 o -5 3 1 2929.31 3143.01 65.22 o -3 3 1 15957.85 16008.61 360.91 o -1 3 1 3703.39 3692.32 87.53 o 1 3 1 40069.63 41353.40 1049.93 o 3 3 1 2536.34 2308.95 54.69 o 5 3 1 9671.52 9932.08 206.93 o 7 3 1 7151.47 7120.59 124.74 o 9 3 1 3308.50 3433.80 81.49 o 11 3 1 5797.18 5831.42 116.51 o 13 3 1 0.49 -18.52 13.74 o 15 3 1 280.27 245.21 53.90 o 17 3 1 60.31 254.71 108.34 o 19 3 1 367.73 433.34 192.59 o -18 4 1 50.43 -12.57 111.50 o -16 4 1 864.68 823.96 67.51 o -14 4 1 3583.84 3598.43 134.12 o -12 4 1 1543.14 1620.88 69.52 o -10 4 1 1671.69 1634.97 118.56 o -8 4 1 106.20 162.02 15.16 o -6 4 1 1670.65 1787.41 43.17 o -4 4 1 49471.54 49695.58 1066.93 o -2 4 1 76.66 76.57 13.44 o 0 4 1 34765.76 34143.45 746.84 o 2 4 1 930.41 1168.80 40.99 o 4 4 1 597.87 545.93 34.70 o 6 4 1 1229.56 1431.94 86.56 o 8 4 1 1339.69 1381.91 45.37 o 10 4 1 10385.74 10636.97 228.66 o 12 4 1 0.04 -3.45 12.06 o 14 4 1 493.58 402.26 42.71 o 16 4 1 975.74 1005.31 84.81 o 18 4 1 178.40 406.41 188.48 o -19 5 1 582.54 389.62 219.41 o -17 5 1 91.35 216.95 67.87 o -15 5 1 95.34 117.18 44.00 o -13 5 1 1140.79 1162.50 124.99 o -11 5 1 2687.56 2965.31 70.17 o -9 5 1 185.40 135.81 19.26 o -7 5 1 26.80 35.88 16.21 o -5 5 1 16417.98 16513.05 335.33 o -3 5 1 886.54 656.58 31.60 o -1 5 1 10017.68 9651.53 182.81 o 1 5 1 1117.07 962.10 37.63 o 3 5 1 27.38 23.23 25.71 o 5 5 1 35.86 113.49 30.31 o 7 5 1 4096.78 4238.41 91.81 o 9 5 1 3385.00 3173.77 84.26 o 11 5 1 167.32 164.15 19.15 o 13 5 1 272.30 238.50 23.81 o 15 5 1 155.25 118.35 58.66 o 17 5 1 81.54 220.22 92.41 o -18 6 1 198.84 92.19 117.34 o -16 6 1 28.63 -28.09 45.19 o -14 6 1 275.29 175.53 52.66 o -12 6 1 117.76 150.20 16.79 o -10 6 1 106.83 137.26 17.87 o -8 6 1 398.69 408.34 46.99 o -6 6 1 391.14 391.16 25.13 o -4 6 1 29.93 42.08 15.75 o -2 6 1 80.29 51.79 21.11 o 0 6 1 40.59 87.82 18.82 o 2 6 1 2750.82 2724.86 72.76 o 4 6 1 133.25 190.98 24.88 o 6 6 1 3032.84 3135.80 83.64 o 8 6 1 563.85 550.73 43.14 o 10 6 1 316.88 313.25 25.32 o 12 6 1 4.23 -12.68 18.19 o 14 6 1 197.36 163.31 20.63 o 16 6 1 106.64 -12.13 53.15 o 18 6 1 0.50 -53.88 119.51 o -17 7 1 146.65 190.72 225.34 o -15 7 1 115.13 95.99 71.85 o -13 7 1 928.52 887.23 42.19 o -11 7 1 131.91 75.94 25.60 o -9 7 1 5.15 -3.55 20.76 o -7 7 1 641.98 666.08 37.40 o -5 7 1 460.14 637.76 72.41 o -3 7 1 10487.15 10642.66 214.94 o -1 7 1 2377.83 2467.58 70.80 o 1 7 1 192.29 183.88 25.40 o 3 7 1 730.64 828.37 39.19 o 5 7 1 581.55 476.60 42.83 o 7 7 1 1783.38 1813.77 66.02 o 9 7 1 31.87 30.97 23.91 o 11 7 1 168.90 160.72 29.21 o 13 7 1 324.69 350.23 31.29 o 15 7 1 139.52 225.47 94.62 o 17 7 1 1404.73 1388.20 125.10 o -16 8 1 202.31 289.60 136.05 o -14 8 1 88.13 86.11 87.47 o -12 8 1 11.56 -14.19 31.18 o -10 8 1 1465.10 1431.25 54.94 o -8 8 1 360.64 344.54 31.79 o -6 8 1 674.73 663.54 49.43 o -4 8 1 5088.37 5150.62 124.89 o -2 8 1 1412.57 1465.02 96.83 o 0 8 1 424.51 389.12 33.47 o 2 8 1 147.75 90.60 22.46 o 4 8 1 398.34 356.57 36.08 o 6 8 1 467.79 578.84 50.19 o 8 8 1 31.03 0.56 25.57 o 10 8 1 3699.51 4145.65 115.40 o 12 8 1 1476.62 1438.11 67.89 o 14 8 1 1601.27 1640.77 134.40 o 16 8 1 430.99 174.22 119.48 o -15 9 1 2.12 -58.74 95.95 o -13 9 1 336.49 361.10 51.77 o -11 9 1 1372.19 1551.35 64.82 o -9 9 1 226.96 139.17 30.49 o -7 9 1 1571.75 1728.95 67.20 o -5 9 1 198.09 226.32 33.99 o -3 9 1 1500.82 1450.58 60.04 o -1 9 1 885.75 996.36 52.90 o 1 9 1 3059.30 3136.88 98.30 o 3 9 1 6810.51 7019.38 171.19 o 5 9 1 1.01 52.95 28.90 o 7 9 1 1997.83 2024.91 99.97 o 9 9 1 57.65 18.14 31.78 o 11 9 1 156.44 197.62 36.26 o 13 9 1 54.58 107.16 122.77 o 15 9 1 0.39 -39.16 133.97 o -14 10 1 17.82 123.94 131.52 o -12 10 1 54.25 106.38 61.68 o -10 10 1 517.70 482.51 50.85 o -8 10 1 1578.34 1491.87 105.59 o -6 10 1 1218.15 1206.03 60.01 o -4 10 1 301.21 329.02 38.53 o -2 10 1 376.31 347.67 42.66 o 0 10 1 443.30 448.43 52.13 o 2 10 1 490.86 423.36 47.78 o 4 10 1 953.90 998.33 59.05 o 6 10 1 1455.33 1515.66 89.94 o 8 10 1 1808.87 1822.51 93.23 o 10 10 1 672.63 641.58 92.38 o 12 10 1 390.52 414.29 68.16 o 14 10 1 62.37 -49.15 159.01 o -13 11 1 592.02 563.48 111.04 o -11 11 1 503.58 407.30 56.88 o -9 11 1 22.26 -9.77 53.64 o -7 11 1 288.71 233.65 47.97 o -5 11 1 532.96 448.61 53.91 o -3 11 1 116.87 175.91 49.32 o -1 11 1 6487.39 6607.24 172.99 o 1 11 1 316.77 419.04 55.63 o 3 11 1 119.72 15.40 36.33 o 5 11 1 142.01 197.01 41.43 o 7 11 1 320.15 316.92 63.95 o 9 11 1 200.02 112.48 57.78 o 11 11 1 410.83 348.11 93.15 o 13 11 1 0.92 -84.14 117.55 o -12 12 1 2.32 -174.05 116.04 o -10 12 1 383.24 386.49 62.96 o -8 12 1 2071.10 2155.30 126.47 o -6 12 1 16.60 -11.89 44.04 o -4 12 1 499.55 510.76 64.58 o -2 12 1 93.70 74.59 46.19 o 0 12 1 7.17 84.35 39.80 o 2 12 1 64.25 48.76 49.39 o 4 12 1 546.80 497.13 74.81 o 6 12 1 733.26 613.36 79.13 o 8 12 1 8.25 -4.05 62.69 o 10 12 1 21.97 126.13 75.26 o 12 12 1 5.30 -9.41 171.05 o -11 13 1 101.72 -108.29 93.63 o -9 13 1 95.41 6.11 62.54 o -7 13 1 1.23 12.58 58.44 o -5 13 1 57.84 -6.89 56.39 o -3 13 1 47.97 28.82 68.10 o -1 13 1 768.46 827.86 197.86 o 1 13 1 538.14 611.05 79.86 o 3 13 1 35.29 140.44 88.11 o 5 13 1 512.50 502.08 86.12 o 7 13 1 441.38 418.19 65.87 o 9 13 1 957.14 1167.94 120.58 o 11 13 1 135.94 221.45 203.44 o -10 14 1 24.23 81.37 222.10 o -8 14 1 458.06 338.95 82.98 o -6 14 1 499.50 381.28 104.48 o -4 14 1 627.55 746.60 106.91 o -2 14 1 242.49 326.72 87.67 o 0 14 1 246.18 268.42 79.97 o 2 14 1 247.93 226.58 80.83 o 4 14 1 957.43 772.71 88.46 o 6 14 1 72.85 20.30 76.92 o 8 14 1 408.72 465.59 163.59 o -7 15 1 240.01 438.73 129.80 o -5 15 1 278.92 267.68 108.50 o -3 15 1 261.13 206.74 124.07 o -1 15 1 109.25 73.54 76.82 o 1 15 1 96.57 -23.71 107.97 o 3 15 1 0.07 68.37 88.22 o 5 15 1 302.66 242.89 100.97 o 7 15 1 1045.09 1243.45 133.33 o -2 16 1 52.82 -66.20 115.59 o 0 16 1 164.60 278.33 124.68 o 2 16 1 321.78 281.79 111.11 o -20 0 2 763.68 515.74 186.21 o -18 0 2 140.43 235.86 119.67 o -16 0 2 713.49 410.94 140.75 o -14 0 2 5449.35 5439.58 287.30 o -12 0 2 2767.98 2734.72 176.79 o -10 0 2 157.30 170.03 16.07 o -8 0 2 33742.22 34178.54 864.38 o -6 0 2 8928.04 9663.82 283.05 o -4 0 2 12487.38 11617.56 315.47 o 2 0 2 5176.78 4698.28 124.40 o 4 0 2 6971.37 7101.01 171.51 o 6 0 2 20243.07 19109.23 470.06 o 8 0 2 260.92 213.00 38.25 o 10 0 2 37.86 47.36 22.57 o 12 0 2 3290.73 3369.54 92.74 o 14 0 2 6530.81 6896.09 242.97 o 16 0 2 349.59 380.75 64.50 o 18 0 2 818.49 680.28 187.63 o -19 1 2 18.14 1.31 82.53 o -17 1 2 160.63 301.66 82.74 o -15 1 2 2314.34 2376.18 138.37 o -13 1 2 3093.99 3061.98 99.95 o -11 1 2 424.16 418.53 29.38 o -9 1 2 614.98 611.00 24.77 o -7 1 2 2446.19 2262.03 48.18 o -5 1 2 9182.46 9155.21 161.09 o -3 1 2 189.81 217.91 9.87 o 1 1 2 5570.30 5239.07 119.99 o 3 1 2 11277.36 10914.43 217.61 o 5 1 2 6334.45 6403.09 112.95 o 7 1 2 1694.59 1745.86 39.20 o 9 1 2 2835.27 3077.09 65.46 o 11 1 2 3490.79 3655.36 82.43 o 13 1 2 266.18 272.68 23.60 o 15 1 2 114.57 154.25 29.77 o 17 1 2 75.76 14.66 120.70 o -20 2 2 911.31 891.42 174.23 o -18 2 2 73.67 123.07 125.21 o -16 2 2 150.75 150.65 24.80 o -14 2 2 940.71 870.41 47.87 o -12 2 2 18.55 32.33 16.47 o -10 2 2 2458.44 2337.63 58.60 o -8 2 2 9068.04 8783.08 167.92 o -6 2 2 19304.30 18212.78 329.23 o -4 2 2 9404.52 9479.92 179.50 o -2 2 2 5451.95 5201.53 112.98 o 0 2 2 301.01 281.02 15.87 o 2 2 2 8995.08 8990.97 201.40 o 4 2 2 11264.17 10532.18 206.72 o 6 2 2 271.22 434.77 20.92 o 8 2 2 12795.87 12570.19 243.69 o 10 2 2 23.92 12.95 14.82 o 12 2 2 0.49 15.79 17.15 o 14 2 2 1270.72 1304.76 50.28 o 16 2 2 1456.51 1409.17 100.83 o 18 2 2 222.11 193.93 119.75 o -19 3 2 7.55 3.73 190.26 o -17 3 2 543.39 599.69 76.70 o -15 3 2 502.07 437.14 36.23 o -13 3 2 268.69 250.25 39.85 o -11 3 2 3375.77 3334.85 89.71 o -9 3 2 209.55 246.23 27.22 o -7 3 2 55154.34 55320.34 1070.47 o -5 3 2 16727.09 15592.49 266.81 o -3 3 2 14972.18 14090.63 299.81 o -1 3 2 607.70 584.13 22.36 o 1 3 2 91.02 68.07 12.43 o 3 3 2 775.35 513.64 28.47 o 5 3 2 3835.02 3939.37 79.66 o 7 3 2 9390.53 9047.67 175.72 o 9 3 2 3457.84 3515.43 76.59 o 11 3 2 8168.22 8758.71 178.07 o 13 3 2 5052.67 4965.93 131.92 o 15 3 2 130.87 84.16 29.86 o 17 3 2 1389.93 1293.15 171.93 o -16 4 2 1351.47 1449.30 76.19 o -14 4 2 248.82 327.02 39.85 o -12 4 2 3034.44 2993.44 96.20 o -10 4 2 895.06 762.27 44.66 o -8 4 2 444.44 386.71 16.04 o -6 4 2 3.34 19.03 11.30 o -4 4 2 220.20 332.14 33.70 o -2 4 2 4606.78 4379.44 106.96 o 0 4 2 11432.57 12517.08 267.80 o 2 4 2 2833.04 2408.47 99.45 o 4 4 2 9165.47 9496.87 201.68 o 6 4 2 1661.01 1442.37 40.88 o 8 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