#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/26/2202637.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202637_Fobs loop_ _publ_author_name 'Dale, Sophie H.' 'Elsegood, Mark R. J.' _publ_section_title ; Benzene-1,2,4,5-tetracarboxylic acid dimethyl sulfoxide disolvate: a redetermination at 150K ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1205 _journal_page_last o1207 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 80.510 _cell_angle_beta 81.124 _cell_angle_gamma 75.474 _cell_length_a 7.3283 _cell_length_b 7.3331 _cell_length_c 8.9456 _exptl_crystal_F_000 214.00 _reflns_d_resolution_high 0.7319 _[local]_cod_data_source_file fl6049Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shd32 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 92.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 884.53 920.84 5.58 o 2 0 0 240.22 232.61 1.66 o 3 0 0 87.03 90.53 1.40 o 4 0 0 112.81 111.87 1.22 o 5 0 0 249.31 233.53 2.14 o 6 0 0 126.33 123.88 1.57 o 7 0 0 7.42 8.40 1.03 o 8 0 0 21.27 22.37 1.45 o 9 0 0 25.36 24.64 1.71 o -9 1 0 114.99 123.38 3.63 o -8 1 0 0.07 0.12 0.60 o -7 1 0 42.18 41.79 1.87 o -6 1 0 84.99 82.15 1.62 o -5 1 0 16.22 17.15 0.57 o -4 1 0 3.80 3.10 0.31 o -3 1 0 132.13 158.21 1.44 o -2 1 0 428.15 442.88 2.91 o -1 1 0 552.20 585.33 5.21 o 0 1 0 467.61 463.44 2.89 o 1 1 0 907.32 935.18 9.58 o 2 1 0 90.79 83.01 0.86 o 3 1 0 1021.27 1038.55 6.25 o 4 1 0 25.61 29.18 0.67 o 5 1 0 32.72 39.91 0.76 o 6 1 0 6.31 4.76 0.55 o 7 1 0 60.17 63.55 1.49 o 8 1 0 0.62 0.40 0.60 o 9 1 0 17.44 20.55 1.52 o -8 2 0 117.47 118.99 2.40 o -7 2 0 12.46 12.70 0.78 o -6 2 0 78.51 80.69 1.68 o -5 2 0 279.67 266.07 3.15 o -4 2 0 2.78 1.79 0.29 o -3 2 0 491.90 506.64 3.53 o -2 2 0 4.01 4.16 0.26 o -1 2 0 62.36 55.62 0.66 o 0 2 0 594.88 569.28 4.16 o 1 2 0 3962.09 3886.25 36.52 o 2 2 0 901.94 934.69 9.26 o 3 2 0 4.21 4.77 0.34 o 4 2 0 47.98 63.47 1.64 o 5 2 0 853.23 867.87 15.96 o 6 2 0 392.23 375.25 3.98 o 7 2 0 6.86 5.42 1.30 o 8 2 0 37.13 36.41 1.83 o 9 2 0 5.66 8.26 1.20 o -8 3 0 150.54 151.04 4.09 o -7 3 0 5.42 5.76 1.06 o -6 3 0 81.83 78.78 1.75 o -5 3 0 2.73 3.10 0.52 o -4 3 0 125.66 114.69 1.87 o -3 3 0 98.54 99.29 2.40 o -2 3 0 244.89 264.91 2.15 o -1 3 0 0.24 2.14 0.30 o 0 3 0 539.23 512.97 3.39 o 1 3 0 298.79 309.63 2.22 o 2 3 0 503.30 546.05 3.59 o 3 3 0 54.75 53.76 1.04 o 4 3 0 1292.82 1354.62 10.31 o 5 3 0 177.65 171.76 2.34 o 6 3 0 147.35 136.07 2.19 o 7 3 0 4.49 4.59 0.79 o 8 3 0 14.21 14.25 1.27 o 9 3 0 27.54 31.04 1.87 o -7 4 0 46.62 40.04 2.08 o -6 4 0 11.18 12.98 1.19 o -5 4 0 128.60 126.24 2.23 o -4 4 0 0.59 0.58 0.39 o -3 4 0 222.88 211.95 2.07 o -2 4 0 488.12 476.13 4.68 o -1 4 0 97.78 110.99 1.27 o 0 4 0 2.74 2.65 0.25 o 1 4 0 66.10 65.27 0.87 o 2 4 0 164.72 161.83 1.71 o 3 4 0 1041.75 1071.95 8.43 o 4 4 0 5.50 7.16 1.14 o 5 4 0 3.66 5.41 1.15 o 6 4 0 377.93 377.86 4.25 o 7 4 0 208.95 208.53 3.09 o 8 4 0 34.36 38.71 1.39 o 9 4 0 4.95 3.83 1.30 o -6 5 0 45.67 40.86 2.10 o -5 5 0 7.66 9.26 1.19 o -4 5 0 6.05 7.59 0.71 o -3 5 0 194.97 183.58 2.69 o -2 5 0 79.70 77.63 1.31 o -1 5 0 125.15 134.56 1.56 o 0 5 0 44.15 40.42 0.78 o 1 5 0 26.84 29.02 0.65 o 2 5 0 461.29 450.18 4.31 o 3 5 0 133.38 130.53 2.00 o 4 5 0 87.35 83.15 1.63 o 5 5 0 731.33 731.15 13.89 o 6 5 0 9.20 9.82 0.70 o 7 5 0 1.93 1.46 0.52 o 8 5 0 2.10 1.77 0.61 o 9 5 0 93.42 95.73 3.33 o -5 6 0 24.18 23.87 1.64 o -4 6 0 138.71 128.89 3.50 o -3 6 0 6.21 5.82 0.94 o -2 6 0 269.53 265.93 3.32 o -1 6 0 9.61 10.05 0.60 o 0 6 0 112.36 99.06 1.38 o 1 6 0 0.03 -0.21 0.26 o 2 6 0 1.83 0.66 0.58 o 3 6 0 780.16 773.70 6.91 o 4 6 0 0.94 0.67 0.39 o 5 6 0 83.54 84.49 1.84 o 6 6 0 3.92 4.07 0.62 o 7 6 0 40.83 39.13 1.41 o 8 6 0 190.53 196.17 3.39 o -4 7 0 3.95 1.85 0.91 o -3 7 0 69.14 71.84 2.59 o -2 7 0 0.05 -0.24 0.57 o -1 7 0 278.96 273.96 3.49 o 0 7 0 4.23 3.23 0.41 o 1 7 0 31.25 33.59 1.09 o 2 7 0 41.42 40.17 1.21 o 3 7 0 73.67 74.14 1.69 o 4 7 0 78.76 76.28 2.48 o 5 7 0 22.32 21.33 1.02 o 6 7 0 47.74 49.63 1.58 o 7 7 0 97.89 101.76 2.36 o -3 8 0 53.48 50.74 2.34 o -2 8 0 10.37 8.43 1.21 o -1 8 0 23.64 21.73 1.42 o 0 8 0 40.76 36.42 1.81 o 1 8 0 76.62 76.01 2.42 o 2 8 0 100.86 96.64 2.31 o 3 8 0 99.62 107.64 2.31 o 4 8 0 75.36 76.23 1.89 o 5 8 0 4.83 4.89 0.72 o 6 8 0 45.65 48.78 1.65 o 2 9 0 0.93 0.63 0.85 o 3 9 0 86.14 98.84 2.28 o 4 9 0 3.58 2.45 0.66 o 5 9 0 55.13 57.20 2.56 o -5 -9 1 13.22 10.27 1.39 o -4 -9 1 51.84 50.26 2.33 o -3 -9 1 0.03 0.39 0.91 o -2 -9 1 47.87 60.20 2.56 o -6 -8 1 51.29 47.34 2.28 o -5 -8 1 6.28 7.12 1.03 o -4 -8 1 163.55 167.84 3.73 o -3 -8 1 70.61 66.39 1.75 o -2 -8 1 2.75 2.93 0.99 o -1 -8 1 28.75 28.62 1.67 o 2 -8 1 24.92 27.16 1.73 o 3 -8 1 23.24 18.80 1.59 o -7 -7 1 0.37 0.11 0.54 o -6 -7 1 2.22 1.48 0.55 o -5 -7 1 100.38 99.82 2.16 o -4 -7 1 110.63 112.10 2.19 o -3 -7 1 12.18 9.49 1.19 o -2 -7 1 4.26 3.58 0.93 o -1 -7 1 221.67 210.57 4.13 o 0 -7 1 1.71 2.41 0.73 o 1 -7 1 1.32 0.54 0.40 o 2 -7 1 31.36 27.50 1.58 o 3 -7 1 5.27 4.65 0.95 o 4 -7 1 44.68 46.56 2.25 o -8 -6 1 42.81 43.14 2.41 o -7 -6 1 89.19 88.80 2.13 o -6 -6 1 2.91 1.57 0.56 o -5 -6 1 9.46 9.06 0.75 o -4 -6 1 28.57 28.43 1.05 o -3 -6 1 252.42 247.62 5.00 o -2 -6 1 313.77 305.18 4.80 o -1 -6 1 23.37 26.05 0.71 o 0 -6 1 217.68 202.50 4.70 o 1 -6 1 14.82 11.85 0.66 o 2 -6 1 233.31 221.23 4.31 o 3 -6 1 23.01 21.20 1.39 o 4 -6 1 20.20 18.80 1.42 o 5 -6 1 49.83 47.10 2.23 o -9 -5 1 132.95 142.11 4.11 o -8 -5 1 33.87 32.25 1.33 o -7 -5 1 99.65 103.24 2.41 o -6 -5 1 97.62 99.31 2.03 o -5 -5 1 534.70 537.42 5.44 o -4 -5 1 969.42 954.94 10.34 o -3 -5 1 42.41 42.44 1.12 o -2 -5 1 3.93 2.89 0.41 o -1 -5 1 19.07 23.72 0.61 o 0 -5 1 88.78 86.99 1.19 o 1 -5 1 150.19 146.78 1.67 o 2 -5 1 0.88 0.48 0.28 o 3 -5 1 41.58 36.01 1.61 o 4 -5 1 94.22 90.04 2.72 o 5 -5 1 7.17 8.00 1.10 o 6 -5 1 27.53 25.42 1.70 o -8 -4 1 15.32 13.51 0.90 o -7 -4 1 0.11 0.59 0.44 o -6 -4 1 394.18 379.46 5.32 o -5 -4 1 0.45 0.23 0.35 o -4 -4 1 189.79 185.40 2.46 o -3 -4 1 153.14 157.24 2.11 o -2 -4 1 1.92 3.32 0.42 o -1 -4 1 436.26 415.16 3.03 o 0 -4 1 278.89 302.94 2.67 o 1 -4 1 34.36 30.36 0.74 o 2 -4 1 40.10 32.42 0.71 o 3 -4 1 731.30 690.50 10.39 o 4 -4 1 6.16 6.78 0.92 o 5 -4 1 11.21 9.49 1.11 o 6 -4 1 75.59 73.86 2.61 o 7 -4 1 14.91 17.27 1.43 o -9 -3 1 21.21 24.13 1.74 o -8 -3 1 44.65 43.50 2.09 o -7 -3 1 224.51 223.94 3.15 o -6 -3 1 180.98 182.01 2.62 o -5 -3 1 20.18 16.73 0.77 o -4 -3 1 20.47 20.16 0.74 o -3 -3 1 235.43 247.19 1.98 o -2 -3 1 94.64 90.91 0.97 o -1 -3 1 54.05 68.94 1.34 o 0 -3 1 1542.56 1658.40 12.69 o 1 -3 1 24.31 24.79 0.52 o 2 -3 1 1615.45 1596.89 9.52 o 3 -3 1 90.32 93.91 1.21 o 4 -3 1 36.51 32.28 0.76 o 5 -3 1 15.79 16.71 0.78 o 6 -3 1 84.75 81.45 2.58 o 7 -3 1 4.20 6.78 1.12 o 8 -3 1 8.02 7.75 1.36 o -9 -2 1 15.08 20.96 1.59 o -8 -2 1 5.47 7.18 1.07 o -7 -2 1 238.65 238.62 3.18 o -6 -2 1 189.26 186.23 2.57 o -5 -2 1 440.29 446.01 7.33 o -4 -2 1 498.43 509.16 3.55 o -3 -2 1 96.98 118.89 1.86 o -2 -2 1 14.41 16.51 0.36 o -1 -2 1 212.54 253.84 1.82 o 0 -2 1 984.76 934.79 5.59 o 1 -2 1 561.23 621.22 3.92 o 2 -2 1 13.82 17.06 0.42 o 3 -2 1 143.90 127.55 1.69 o 4 -2 1 155.45 157.97 1.65 o 5 -2 1 247.21 230.08 2.25 o 6 -2 1 16.94 15.29 0.76 o 7 -2 1 68.58 71.64 2.44 o 8 -2 1 67.55 64.45 2.47 o -9 -1 1 32.70 32.57 1.92 o -8 -1 1 7.55 8.03 1.11 o -7 -1 1 19.55 19.08 1.29 o -6 -1 1 641.77 658.71 5.92 o -5 -1 1 142.67 129.07 1.46 o -4 -1 1 295.75 305.73 2.40 o -3 -1 1 438.20 461.74 3.12 o -2 -1 1 0.24 2.46 0.94 o -1 -1 1 1936.88 1923.30 11.06 o 0 -1 1 4.24 5.00 0.16 o 1 -1 1 1772.34 1705.80 9.90 o 2 -1 1 9.80 14.70 0.35 o 3 -1 1 344.16 316.98 2.79 o 4 -1 1 50.81 46.13 0.78 o 5 -1 1 0.81 0.95 0.36 o 6 -1 1 1.25 0.79 0.31 o 7 -1 1 252.76 253.89 3.29 o 8 -1 1 14.41 15.12 1.22 o -9 0 1 15.11 18.15 1.50 o -8 0 1 16.23 14.47 1.26 o -7 0 1 5.74 5.78 0.98 o -6 0 1 261.50 268.54 3.22 o -5 0 1 158.64 151.88 1.64 o -4 0 1 972.91 1009.86 6.31 o -3 0 1 7.97 3.79 0.25 o -2 0 1 2480.56 2574.62 14.60 o -1 0 1 733.74 762.50 4.61 o 0 0 1 111.07 113.73 1.03 o 1 0 1 1590.95 1580.28 11.21 o 2 0 1 280.19 260.42 2.67 o 3 0 1 342.52 356.98 3.95 o 4 0 1 372.25 407.75 2.98 o 5 0 1 89.74 85.57 1.16 o 6 0 1 742.39 740.18 5.24 o 7 0 1 1.11 0.48 0.42 o 8 0 1 31.80 29.93 1.63 o 9 0 1 96.31 104.90 3.25 o -8 1 1 28.20 27.74 1.69 o -7 1 1 71.13 71.78 2.88 o -6 1 1 298.33 285.19 9.58 o -5 1 1 0.03 0.00 0.32 o -4 1 1 538.29 560.47 3.90 o -3 1 1 84.13 84.24 0.96 o -2 1 1 1617.97 1709.02 10.97 o -1 1 1 8502.64 8004.61 126.75 o 0 1 1 314.76 309.75 2.02 o 1 1 1 172.97 159.70 1.15 o 2 1 1 408.66 357.17 2.36 o 3 1 1 168.37 197.03 1.57 o 4 1 1 3.80 2.61 0.26 o 5 1 1 621.73 643.08 4.43 o 6 1 1 42.80 39.67 1.10 o 7 1 1 37.49 37.15 1.34 o 8 1 1 142.99 137.08 3.45 o 9 1 1 6.09 9.45 1.22 o -8 2 1 1.44 1.71 0.59 o -7 2 1 99.20 101.05 2.09 o -6 2 1 6.77 6.88 0.67 o -5 2 1 38.37 38.17 1.32 o -4 2 1 27.10 28.56 0.82 o -3 2 1 719.42 726.55 4.73 o -2 2 1 47.36 44.06 0.88 o -1 2 1 3286.44 3335.82 22.99 o 0 2 1 304.29 343.94 2.54 o 1 2 1 1301.43 1321.83 8.72 o 2 2 1 145.93 132.96 1.49 o 3 2 1 1134.15 1183.11 11.01 o 4 2 1 17.63 20.03 0.48 o 5 2 1 83.12 109.39 2.12 o 6 2 1 72.26 76.13 1.54 o 7 2 1 164.82 165.40 2.54 o 8 2 1 53.36 55.94 1.67 o 9 2 1 20.04 21.19 1.53 o -8 3 1 18.74 20.62 1.20 o -7 3 1 59.80 58.47 1.65 o -6 3 1 2.96 4.09 0.72 o -5 3 1 17.53 14.28 1.45 o -4 3 1 43.17 47.37 1.22 o -3 3 1 35.38 28.69 0.65 o -2 3 1 1152.80 1154.03 13.95 o -1 3 1 25.06 20.99 0.45 o 0 3 1 2081.95 2126.28 12.19 o 1 3 1 11.32 9.31 0.30 o 2 3 1 1007.74 1024.75 7.76 o 3 3 1 46.61 59.59 1.09 o 4 3 1 2.09 2.22 0.35 o 5 3 1 356.60 352.97 3.69 o 6 3 1 4.90 6.62 0.63 o 7 3 1 3.31 3.96 0.56 o 8 3 1 57.95 58.50 1.61 o 9 3 1 14.27 11.22 1.05 o -7 4 1 1.54 2.65 0.91 o -6 4 1 29.64 28.37 1.17 o -5 4 1 4.04 4.57 0.94 o -4 4 1 158.13 157.44 2.45 o -3 4 1 28.45 25.82 1.17 o -2 4 1 88.91 79.84 1.07 o -1 4 1 367.59 342.13 2.64 o 0 4 1 2.59 0.95 0.21 o 1 4 1 566.39 559.34 3.79 o 2 4 1 91.81 97.96 1.05 o 3 4 1 683.86 691.79 5.85 o 4 4 1 665.85 679.86 5.94 o 5 4 1 12.56 14.99 0.89 o 6 4 1 56.02 48.41 1.32 o 7 4 1 7.66 8.60 0.76 o 8 4 1 75.71 77.37 1.90 o 9 4 1 104.29 107.28 2.41 o -6 5 1 57.20 55.59 2.42 o -5 5 1 21.62 22.00 1.05 o -4 5 1 17.89 18.43 1.75 o -3 5 1 473.11 480.48 4.96 o -2 5 1 49.11 50.19 1.25 o -1 5 1 471.51 454.11 4.42 o 0 5 1 12.68 9.48 0.51 o 1 5 1 117.90 124.13 1.40 o 2 5 1 86.00 83.25 1.07 o 3 5 1 823.81 833.14 7.03 o 4 5 1 39.66 41.07 1.47 o 5 5 1 84.53 78.16 1.65 o 6 5 1 107.75 103.12 2.83 o 7 5 1 6.93 9.82 0.76 o 8 5 1 60.05 60.32 1.87 o 9 5 1 3.82 2.19 0.99 o -5 6 1 0.93 0.02 0.70 o -4 6 1 90.22 91.72 2.04 o -3 6 1 13.66 15.40 0.85 o -2 6 1 0.05 -0.10 0.34 o -1 6 1 158.34 156.48 2.58 o 0 6 1 9.54 8.59 0.57 o 1 6 1 189.24 182.34 1.94 o 2 6 1 75.76 69.94 1.46 o 3 6 1 6.42 7.18 1.56 o 4 6 1 588.50 569.77 5.59 o 5 6 1 98.11 100.82 2.00 o 6 6 1 40.29 41.21 1.35 o 7 6 1 19.46 20.98 1.07 o 8 6 1 33.24 34.98 1.41 o -4 7 1 42.25 43.04 2.19 o -3 7 1 0.58 -0.47 0.56 o -2 7 1 50.81 52.85 1.91 o -1 7 1 17.66 17.38 0.85 o 0 7 1 47.38 42.95 1.23 o 1 7 1 212.72 207.00 4.90 o 2 7 1 301.26 310.35 3.72 o 3 7 1 6.68 6.65 0.68 o 4 7 1 66.35 66.22 1.87 o 5 7 1 272.42 277.95 3.76 o 6 7 1 58.06 59.26 1.70 o 7 7 1 2.20 2.04 0.62 o -3 8 1 25.49 23.22 1.65 o -2 8 1 16.52 15.53 1.34 o -1 8 1 12.19 11.01 0.80 o 0 8 1 13.71 15.76 1.25 o 1 8 1 24.81 26.49 1.57 o 2 8 1 86.51 93.89 2.36 o 3 8 1 0.51 0.92 0.63 o 4 8 1 9.51 11.47 0.86 o 5 8 1 60.74 60.94 1.74 o 6 8 1 64.65 67.57 1.92 o -2 9 1 8.28 5.94 1.18 o 1 9 1 86.08 94.05 3.13 o 2 9 1 7.70 4.09 0.97 o 3 9 1 40.88 44.08 1.52 o 4 9 1 0.16 0.27 0.62 o 5 9 1 15.61 17.17 1.58 o -2 -9 2 5.81 5.15 1.21 o -1 -9 2 106.11 120.34 3.68 o -6 -8 2 73.30 77.65 2.93 o -5 -8 2 82.30 86.45 2.14 o -4 -8 2 0.32 -0.31 0.52 o -3 -8 2 3.24 5.21 1.11 o -2 -8 2 200.57 189.88 4.45 o -1 -8 2 29.59 29.94 1.69 o 0 -8 2 69.79 70.23 2.53 o 2 -8 2 124.21 142.48 3.91 o -7 -7 2 26.52 27.95 1.84 o -6 -7 2 2.19 0.80 0.52 o -5 -7 2 14.18 14.52 2.21 o -4 -7 2 160.15 152.33 2.65 o -3 -7 2 77.97 74.90 1.74 o -2 -7 2 1.73 1.74 0.44 o -1 -7 2 38.85 38.96 1.75 o 0 -7 2 16.24 13.85 0.77 o 1 -7 2 122.30 133.13 2.35 o 2 -7 2 69.53 65.41 2.42 o 3 -7 2 0.73 -0.05 0.74 o -8 -6 2 31.11 33.13 2.07 o -7 -6 2 7.37 7.75 0.88 o -6 -6 2 18.95 17.77 0.99 o -5 -6 2 117.05 112.80 2.21 o -4 -6 2 0.49 0.45 0.47 o -3 -6 2 29.75 30.16 1.05 o -2 -6 2 118.63 103.65 2.30 o -1 -6 2 180.95 188.11 3.76 o 0 -6 2 11.34 8.61 0.60 o 1 -6 2 81.80 71.37 1.88 o 2 -6 2 23.80 21.28 0.99 o 3 -6 2 170.08 168.81 3.98 o 4 -6 2 224.11 228.03 4.95 o 5 -6 2 26.27 26.83 1.80 o -8 -5 2 97.81 99.32 2.34 o -7 -5 2 0.05 -0.21 0.46 o -6 -5 2 118.61 116.13 3.83 o -5 -5 2 171.21 165.99 5.06 o -4 -5 2 101.94 97.30 1.85 o -3 -5 2 270.81 255.33 3.09 o -2 -5 2 390.70 397.55 4.00 o -1 -5 2 101.16 94.63 1.26 o 0 -5 2 16.71 12.44 0.50 o 1 -5 2 9.79 11.85 0.64 o 2 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1.19 o -3 0 10 12.34 11.95 1.31 o -2 0 10 0.27 -0.26 0.77 o -1 0 10 105.87 105.98 3.32 o 0 0 10 39.27 40.88 2.04 o 1 0 10 103.27 101.74 2.17 o 2 0 10 39.97 40.66 1.42 o 3 0 10 0.02 -0.47 0.47 o 4 0 10 6.17 8.07 1.19 o 5 0 10 150.29 144.63 3.26 o 6 0 10 83.93 89.84 3.20 o -3 1 10 18.31 16.31 1.48 o -2 1 10 85.04 86.30 3.07 o -1 1 10 13.34 16.10 1.39 o 0 1 10 51.01 49.14 2.23 o 1 1 10 15.49 13.98 1.27 o 2 1 10 6.66 8.97 0.83 o 3 1 10 0.07 -0.09 0.45 o 4 1 10 150.63 146.00 4.61 o 5 1 10 44.44 47.16 1.76 o 6 1 10 0.15 0.17 0.85 o -2 2 10 147.10 148.95 4.12 o -1 2 10 16.60 17.08 1.42 o 0 2 10 66.11 67.33 2.60 o 1 2 10 34.79 36.88 1.92 o 2 2 10 72.53 78.42 2.75 o 3 2 10 61.79 65.61 1.75 o 4 2 10 1.05 2.85 0.66 o 5 2 10 21.16 18.11 1.10 o -3 3 10 14.62 13.46 1.50 o -2 3 10 39.84 41.52 2.24 o -1 3 10 74.04 69.46 2.74 o 0 3 10 0.62 0.80 0.72 o 1 3 10 97.08 94.34 3.07 o 2 3 10 5.13 2.81 0.89 o 3 3 10 0.70 -0.53 0.63 o 4 3 10 103.03 109.31 2.29 o 5 3 10 0.06 0.78 0.84 o -2 4 10 58.67 61.18 2.69 o -1 4 10 8.72 9.49 0.95 o 0 4 10 13.02 11.80 1.24 o 1 4 10 7.61 6.42 1.06 o 2 4 10 36.92 35.67 1.86 o 3 4 10 111.27 116.26 3.32 o 5 4 10 62.73 69.43 2.71 o -1 5 10 7.20 5.26 0.85 o 0 5 10 49.21 48.98 1.67 o 1 5 10 48.31 48.20 2.24 o 2 5 10 35.56 37.55 1.92 o 0 6 10 9.53 7.30 0.93 o 1 6 10 14.16 14.61 1.86 o 2 6 10 8.45 7.03 1.17 o 0 -2 11 111.26 125.35 3.75 o 1 -1 11 1.10 3.07 0.93 o 2 -1 11 11.48 13.26 1.59 o -1 0 11 28.81 25.23 1.80 o 0 0 11 0.02 0.56 0.88 o 1 0 11 76.31 82.08 3.07 o 2 0 11 14.94 13.96 0.95 o 3 0 11 49.39 45.46 1.85 o -1 1 11 24.56 26.01 1.85 o 0 1 11 28.04 30.20 1.90 o 1 1 11 152.87 157.31 4.28 o 2 1 11 11.02 11.45 1.26 o 3 1 11 28.21 23.76 1.17 o 4 1 11 39.26 36.06 1.47 o 5 1 11 54.77 56.95 2.58 o 0 2 11 7.30 6.23 1.25 o 1 2 11 3.81 2.78 0.94 o 2 2 11 0.58 -0.32 0.68 o 3 2 11 59.05 51.99 2.36 o 4 2 11 133.45 140.90 2.82 o 5 2 11 3.92 1.42 0.88 o 0 3 11 0.51 0.22 0.87 o 1 3 11 41.29 44.17 2.24 o 2 3 11 60.80 62.44 2.61 o 3 3 11 51.49 48.19 2.26 o 4 3 11 22.35 25.10 1.73 o 1 4 11 0.06 -0.68 0.68 o 2 4 11 5.84 3.14 1.02 o 3 4 11 43.70 43.90 2.17 o 1 5 11 3.71 1.12 0.85 o 2 5 11 62.79 65.30 2.71 o