#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202651.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202651_Fobs loop_ _publ_author_name 'Olmstead, Marilyn M.' 'Sahbari, Javad J.' _publ_section_title ; Acetylacetone dioxime ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1648 _journal_page_last o1649 _journal_volume 59 _journal_year 2003 _space_group_IT_number 118 _symmetry_space_group_name_Hall 'P -4 -2n' _symmetry_space_group_name_H-M 'P -4 n 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.8520 _cell_length_b 10.8520 _cell_length_c 5.9751 _exptl_crystal_F_000 280.00 _reflns_d_resolution_high 0.8386 _[local]_cod_data_source_file fl6064Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mn877a in P-4n2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 65.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' 'x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, z+1/2' 'y+1/2, x+1/2, -z+1/2' '-y+1/2, -x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 495.19 493.87 6.95 o 0 2 0 393.80 391.54 2.25 o 1 2 0 737.24 732.38 7.60 o 2 2 0 4353.48 4597.51 34.68 o 1 3 0 440.52 432.59 2.25 o 2 3 0 23.21 22.22 0.57 o 3 3 0 4.75 3.78 0.41 o 0 4 0 151.51 183.98 5.56 o 1 4 0 12.49 11.09 0.46 o 2 4 0 300.08 284.50 2.24 o 3 4 0 417.13 420.35 2.94 o 4 4 0 203.91 184.78 3.01 o 1 5 0 35.33 41.82 0.95 o 2 5 0 443.53 424.14 3.11 o 3 5 0 409.31 416.99 3.27 o 4 5 0 158.86 150.85 2.10 o 5 5 0 82.02 79.89 2.36 o 0 6 0 11.91 8.85 0.55 o 1 6 0 779.57 861.40 4.76 o 2 6 0 539.74 569.90 3.97 o 3 6 0 175.71 176.00 2.36 o 4 6 0 10.01 8.52 0.61 o 5 6 0 43.83 43.70 1.35 o 6 6 0 54.44 56.24 2.29 o 1 7 0 37.34 43.71 1.24 o 2 7 0 507.14 524.38 4.36 o 3 7 0 0.39 1.30 0.35 o 4 7 0 77.55 83.25 1.88 o 5 7 0 12.44 14.66 0.88 o 6 7 0 57.89 65.44 1.82 o 7 7 0 165.87 178.33 4.32 o 0 8 0 59.20 61.65 1.63 o 1 8 0 142.88 150.22 2.52 o 2 8 0 70.86 73.33 1.80 o 3 8 0 98.28 99.49 2.14 o 4 8 0 166.16 174.45 2.90 o 5 8 0 322.52 337.27 4.12 o 6 8 0 14.14 15.47 0.93 o 7 8 0 101.25 102.05 2.26 o 8 8 0 104.66 103.88 3.08 o 1 9 0 63.98 72.49 1.89 o 2 9 0 120.03 117.91 2.42 o 3 9 0 0.24 0.44 0.42 o 4 9 0 60.11 57.24 1.74 o 5 9 0 8.09 6.79 0.65 o 6 9 0 69.70 73.39 1.91 o 7 9 0 98.98 109.12 2.21 o 8 9 0 55.94 56.44 1.47 o 9 9 0 21.55 18.34 1.05 o 0 10 0 65.07 60.08 1.77 o 1 10 0 85.21 89.12 2.16 o 2 10 0 31.82 26.39 1.21 o 3 10 0 0.01 -0.35 0.35 o 4 10 0 50.50 50.76 1.61 o 5 10 0 16.37 18.73 0.97 o 6 10 0 145.21 158.20 2.58 o 7 10 0 169.76 177.40 2.50 o 8 10 0 5.74 5.80 0.45 o 1 11 0 46.00 46.61 1.52 o 2 11 0 5.00 8.36 0.69 o 3 11 0 6.71 7.64 0.64 o 4 11 0 0.04 0.68 0.32 o 5 11 0 2.25 2.44 0.36 o 6 11 0 0.56 0.24 0.27 o 0 12 0 86.23 89.00 1.86 o 1 12 0 7.33 8.47 0.63 o 2 12 0 9.08 8.98 0.62 o 3 12 0 24.47 21.64 0.87 o 4 12 0 10.83 10.81 0.59 o 3 0 1 3467.49 3454.54 32.43 o 5 0 1 514.33 521.78 4.84 o 7 0 1 640.64 681.66 6.66 o 9 0 1 394.55 412.60 6.40 o 11 0 1 15.98 17.35 1.34 o 0 1 1 2011.12 1929.29 12.73 o 1 1 1 392.89 325.86 2.32 o 2 1 1 3006.47 2950.48 26.87 o 3 1 1 593.76 560.31 3.96 o 4 1 1 18.76 20.46 0.87 o 5 1 1 919.73 958.80 6.73 o 6 1 1 266.76 260.58 3.90 o 7 1 1 50.93 54.53 2.01 o 8 1 1 17.59 18.12 1.33 o 9 1 1 40.86 43.05 2.11 o 10 1 1 40.25 42.02 2.13 o 11 1 1 12.03 10.10 1.07 o 12 1 1 17.24 16.77 1.13 o 1 2 1 2996.78 3051.71 27.31 o 2 2 1 1326.96 1266.94 17.93 o 3 2 1 773.19 791.33 5.03 o 4 2 1 108.30 118.39 2.15 o 5 2 1 318.57 307.00 3.89 o 6 2 1 111.83 105.86 2.55 o 7 2 1 122.00 124.20 3.05 o 8 2 1 232.29 239.18 4.62 o 9 2 1 10.15 11.78 1.19 o 10 2 1 31.87 30.40 1.79 o 11 2 1 75.78 82.09 2.73 o 12 2 1 14.98 14.38 1.06 o 0 3 1 3484.87 3622.26 33.22 o 1 3 1 593.31 561.37 3.95 o 2 3 1 774.13 788.44 5.01 o 3 3 1 627.48 631.83 4.86 o 4 3 1 136.03 139.37 2.50 o 5 3 1 41.24 38.56 1.48 o 6 3 1 22.53 20.92 1.24 o 7 3 1 51.08 57.49 2.20 o 8 3 1 12.30 12.90 1.17 o 9 3 1 24.18 23.13 1.59 o 10 3 1 35.47 32.00 1.88 o 11 3 1 4.49 4.91 0.77 o 12 3 1 6.67 6.37 0.71 o 1 4 1 18.96 18.22 0.83 o 2 4 1 107.82 117.25 2.14 o 3 4 1 136.91 145.59 2.54 o 4 4 1 0.34 0.21 0.37 o 5 4 1 171.42 172.35 3.28 o 6 4 1 193.88 197.74 3.84 o 7 4 1 3.76 2.97 0.68 o 8 4 1 379.53 389.23 6.19 o 9 4 1 20.17 21.66 1.55 o 10 4 1 50.67 44.69 2.13 o 11 4 1 15.13 15.44 1.17 o 12 4 1 37.03 32.28 1.39 o 0 5 1 516.28 522.91 4.85 o 1 5 1 919.56 953.08 6.71 o 2 5 1 318.65 302.42 3.86 o 3 5 1 40.77 40.80 1.51 o 4 5 1 169.58 168.83 3.25 o 5 5 1 82.38 83.01 2.47 o 6 5 1 10.64 12.38 1.12 o 7 5 1 128.53 128.53 3.50 o 8 5 1 92.56 94.88 3.10 o 9 5 1 167.09 166.30 4.14 o 10 5 1 80.22 94.48 2.92 o 11 5 1 4.64 5.15 0.68 o 1 6 1 266.75 264.46 3.92 o 2 6 1 111.32 105.02 2.54 o 3 6 1 23.33 23.31 1.30 o 4 6 1 193.25 197.97 3.84 o 5 6 1 10.45 9.04 1.03 o 6 6 1 0.00 -0.09 0.49 o 7 6 1 143.20 149.52 3.87 o 8 6 1 101.03 105.87 3.30 o 9 6 1 10.97 9.40 1.12 o 10 6 1 46.58 50.59 2.03 o 11 6 1 15.06 13.13 0.92 o 0 7 1 640.35 674.08 6.97 o 1 7 1 51.00 51.61 1.95 o 2 7 1 121.80 118.92 3.02 o 3 7 1 50.82 54.77 2.14 o 4 7 1 4.11 4.93 0.78 o 5 7 1 128.89 130.16 3.52 o 6 7 1 142.91 144.11 3.80 o 7 7 1 393.47 400.50 6.45 o 8 7 1 10.88 11.64 1.17 o 9 7 1 36.17 35.07 1.80 o 10 7 1 0.05 -0.32 0.37 o 1 8 1 17.45 17.33 1.31 o 2 8 1 232.87 240.01 4.65 o 3 8 1 12.26 23.87 1.56 o 4 8 1 378.57 388.63 6.20 o 5 8 1 92.46 96.65 3.12 o 6 8 1 100.79 107.50 3.34 o 7 8 1 10.85 11.03 1.12 o 8 8 1 11.29 13.07 1.14 o 9 8 1 7.11 7.37 0.80 o 10 8 1 20.67 21.32 1.09 o 0 9 1 394.94 409.99 6.38 o 1 9 1 40.61 43.19 2.08 o 2 9 1 10.23 11.84 1.23 o 3 9 1 24.33 23.16 1.60 o 4 9 1 19.76 22.09 1.56 o 5 9 1 167.58 176.59 4.23 o 6 9 1 10.80 13.24 1.23 o 7 9 1 36.69 40.28 1.89 o 8 9 1 7.16 7.18 0.79 o 9 9 1 62.77 55.81 1.73 o 1 10 1 40.15 39.27 2.06 o 2 10 1 31.21 34.33 1.88 o 3 10 1 35.05 36.36 1.95 o 4 10 1 50.60 53.48 2.28 o 5 10 1 79.80 80.48 2.72 o 6 10 1 46.78 48.43 1.98 o 7 10 1 0.06 0.13 0.31 o 8 10 1 20.96 20.09 1.02 o 0 11 1 15.50 18.57 1.38 o 1 11 1 12.08 10.49 1.12 o 2 11 1 76.35 83.57 2.79 o 3 11 1 4.76 5.44 0.82 o 4 11 1 15.50 14.15 1.09 o 5 11 1 4.69 4.63 0.69 o 6 11 1 14.76 14.71 0.95 o 1 12 1 17.08 17.34 1.14 o 2 12 1 14.89 15.80 1.06 o 3 12 1 6.65 8.40 0.76 o 4 12 1 37.55 35.73 1.42 o 0 0 2 2498.97 2459.53 27.08 o 4 0 2 320.38 316.22 3.80 o 6 0 2 557.96 573.97 5.96 o 8 0 2 143.60 146.57 3.73 o 10 0 2 3.97 2.40 0.75 o 12 0 2 40.84 37.54 1.54 o 1 1 2 1081.37 1026.31 17.34 o 2 1 2 233.60 208.37 2.63 o 4 1 2 193.60 174.06 2.85 o 5 1 2 270.44 234.13 3.65 o 6 1 2 229.17 229.58 3.97 o 7 1 2 24.90 23.84 1.45 o 8 1 2 70.69 70.04 2.61 o 9 1 2 81.37 84.48 2.94 o 10 1 2 58.35 61.25 2.51 o 11 1 2 82.96 87.13 2.75 o 12 1 2 51.99 53.51 1.83 o 0 2 2 1052.66 1029.03 12.73 o 1 2 2 231.91 209.49 2.63 o 2 2 2 16.69 16.78 0.82 o 3 2 2 12.66 14.61 0.82 o 4 2 2 80.79 82.37 2.03 o 5 2 2 242.07 228.95 3.71 o 6 2 2 269.27 262.50 4.36 o 7 2 2 518.52 524.68 6.71 o 8 2 2 94.32 96.27 3.07 o 9 2 2 60.07 61.81 2.53 o 10 2 2 73.01 71.66 2.64 o 11 2 2 31.53 25.87 1.53 o 12 2 2 6.80 9.20 0.77 o 1 3 2 1231.35 1242.51 9.78 o 2 3 2 12.16 11.98 0.74 o 3 3 2 528.52 503.85 4.94 o 4 3 2 91.06 92.22 2.26 o 5 3 2 226.14 230.40 3.89 o 6 3 2 68.48 64.92 2.26 o 7 3 2 44.68 44.31 2.02 o 8 3 2 195.97 201.97 4.49 o 9 3 2 16.05 16.15 1.36 o 10 3 2 13.69 17.28 1.40 o 11 3 2 25.81 26.01 1.44 o 12 3 2 6.06 6.02 0.63 o 0 4 2 323.87 316.67 3.80 o 1 4 2 193.17 180.77 2.90 o 2 4 2 81.24 84.40 2.05 o 3 4 2 91.10 92.34 2.27 o 4 4 2 26.58 26.43 1.32 o 5 4 2 233.22 234.31 4.13 o 6 4 2 99.22 95.61 2.85 o 7 4 2 39.28 40.47 1.98 o 8 4 2 16.53 15.60 1.36 o 9 4 2 271.01 282.17 5.32 o 10 4 2 20.56 18.40 1.35 o 11 4 2 0.03 0.07 0.35 o 1 5 2 269.10 239.91 3.70 o 2 5 2 241.25 228.60 3.70 o 3 5 2 227.64 228.30 3.88 o 4 5 2 232.01 243.31 4.23 o 5 5 2 12.85 11.50 1.05 o 6 5 2 6.69 6.64 0.87 o 7 5 2 10.79 10.03 1.12 o 8 5 2 119.87 110.63 3.41 o 9 5 2 10.22 10.40 1.09 o 10 5 2 6.67 5.03 0.75 o 11 5 2 18.62 20.84 1.14 o 0 6 2 563.22 572.65 5.94 o 1 6 2 229.24 222.45 3.91 o 2 6 2 270.13 262.27 4.36 o 3 6 2 68.71 65.38 2.30 o 4 6 2 98.63 100.88 2.96 o 5 6 2 6.75 7.81 0.92 o 6 6 2 32.74 37.23 1.96 o 7 6 2 73.82 73.50 2.80 o 8 6 2 4.31 4.80 0.85 o 9 6 2 10.45 11.60 1.11 o 10 6 2 26.02 26.16 1.39 o 1 7 2 24.63 23.48 1.46 o 2 7 2 517.33 523.11 6.71 o 3 7 2 44.17 42.42 1.99 o 4 7 2 39.36 41.82 2.02 o 5 7 2 11.27 11.97 1.20 o 6 7 2 74.70 70.51 2.76 o 7 7 2 155.67 161.89 4.07 o 8 7 2 53.52 46.69 2.09 o 9 7 2 34.31 34.16 1.65 o 10 7 2 31.73 32.45 1.36 o 0 8 2 143.98 152.92 3.79 o 1 8 2 68.49 65.78 2.53 o 2 8 2 95.14 99.64 3.12 o 3 8 2 195.75 193.27 4.41 o 4 8 2 16.41 15.89 1.34 o 5 8 2 120.45 110.15 3.41 o 6 8 2 4.35 5.02 0.78 o 7 8 2 53.95 57.32 2.29 o 8 8 2 1.65 1.86 0.51 o 9 8 2 2.73 2.65 0.54 o 1 9 2 80.84 81.82 2.93 o 2 9 2 60.08 59.66 2.52 o 3 9 2 16.25 15.85 1.37 o 4 9 2 272.41 261.40 5.18 o 5 9 2 10.03 12.50 1.17 o 6 9 2 10.36 9.87 1.04 o 7 9 2 34.15 35.70 1.68 o 8 9 2 2.63 2.65 0.50 o 0 10 2 4.01 4.72 0.81 o 1 10 2 58.18 60.75 2.49 o 2 10 2 73.15 69.88 2.65 o 3 10 2 13.58 15.91 1.29 o 4 10 2 20.23 20.66 1.44 o 5 10 2 6.57 4.43 0.73 o 6 10 2 25.80 26.47 1.41 o 7 10 2 31.91 29.67 1.31 o 1 11 2 82.95 83.39 2.67 o 2 11 2 32.27 30.30 1.60 o 3 11 2 25.44 25.70 1.44 o 4 11 2 0.02 0.65 0.38 o 5 11 2 18.67 20.04 1.11 o 0 12 2 41.01 39.55 1.60 o 1 12 2 52.03 52.54 1.81 o 2 12 2 6.75 7.69 0.72 o 3 12 2 5.98 6.14 0.65 o 1 0 3 1016.42 1030.88 7.12 o 7 0 3 362.52 346.85 5.78 o 9 0 3 108.01 113.38 3.45 o 11 0 3 4.68 4.32 0.64 o 0 1 3 1018.27 1053.72 7.19 o 1 1 3 11.92 17.71 0.96 o 2 1 3 173.62 175.42 3.00 o 6 1 3 204.87 181.57 3.95 o 7 1 3 161.85 163.62 4.00 o 8 1 3 196.53 194.28 4.46 o 9 1 3 237.74 246.48 5.00 o 10 1 3 70.03 71.02 2.51 o 11 1 3 10.52 11.98 0.94 o 1 2 3 173.69 172.43 2.98 o 2 2 3 385.66 382.51 4.37 o 3 2 3 276.07 289.45 4.19 o 5 2 3 29.12 30.41 1.58 o 6 2 3 6.45 7.16 0.86 o 7 2 3 64.93 65.74 2.56 o 8 2 3 116.43 115.36 3.46 o 9 2 3 19.52 19.08 1.40 o 10 2 3 0.23 0.57 0.49 o 11 2 3 4.80 4.46 0.64 o 0 3 3 12.01 13.02 0.65 o 1 3 3 139.33 143.98 2.03 o 2 3 3 275.53 284.25 4.15 o 3 3 3 33.91 36.82 1.58 o 4 3 3 52.55 48.22 1.91 o 5 3 3 51.67 47.91 2.00 o 6 3 3 233.96 233.81 4.67 o 7 3 3 77.80 69.14 2.66 o 8 3 3 46.15 46.23 2.25 o 9 3 3 56.07 62.07 2.46 o 10 3 3 9.55 9.91 0.95 o 11 3 3 58.49 58.50 1.85 o 1 4 3 197.01 202.91 2.57 o 2 4 3 31.69 31.60 1.06 o 3 4 3 52.49 59.42 2.11 o 4 4 3 53.72 47.24 1.98 o 5 4 3 43.40 45.85 2.06 o 6 4 3 68.35 67.40 2.60 o 7 4 3 9.64 8.55 1.07 o 8 4 3 56.07 65.59 2.59 o 9 4 3 3.62 3.59 0.73 o 10 4 3 8.88 10.81 0.98 o 11 4 3 6.64 6.22 0.64 o 0 5 3 221.03 224.52 3.09 o 1 5 3 63.29 61.32 1.52 o 2 5 3 29.87 28.08 1.51 o 3 5 3 50.82 45.93 1.99 o 4 5 3 43.34 41.77 1.96 o 5 5 3 52.48 52.02 2.27 o 6 5 3 35.46 34.26 1.90 o 7 5 3 189.41 178.32 4.30 o 8 5 3 18.28 21.26 1.52 o 9 5 3 16.87 17.71 1.28 o 10 5 3 17.23 18.38 1.12 o 1 6 3 207.29 190.29 4.05 o 2 6 3 6.21 7.07 0.87 o 3 6 3 232.72 223.29 4.57 o 4 6 3 67.85 68.97 2.61 o 5 6 3 35.47 30.02 1.82 o 6 6 3 20.73 18.86 1.46 o 7 6 3 24.62 22.26 1.55 o 8 6 3 16.16 14.30 1.21 o 9 6 3 17.96 19.20 1.22 o 10 6 3 11.43 12.08 0.85 o 0 7 3 363.18 356.38 5.84 o 1 7 3 160.72 161.49 3.95 o 2 7 3 65.09 61.20 2.47 o 3 7 3 77.25 69.89 2.70 o 4 7 3 9.37 6.87 0.98 o 5 7 3 189.17 182.96 4.34 o 6 7 3 24.11 21.79 1.58 o 7 7 3 8.55 8.63 1.01 o 8 7 3 0.03 0.29 0.37 o 9 7 3 64.44 58.17 1.88 o 1 8 3 196.96 195.57 4.49 o 2 8 3 117.16 115.41 3.47 o 3 8 3 46.22 43.08 2.17 o 4 8 3 56.44 59.44 2.47 o 5 8 3 18.22 20.05 1.44 o 6 8 3 16.08 13.95 1.23 o 7 8 3 0.03 0.88 0.35 o 8 8 3 0.53 1.14 0.40 o 0 9 3 107.04 106.51 3.29 o 1 9 3 236.42 238.02 4.89 o 2 9 3 19.67 21.22 1.51 o 3 9 3 56.41 58.78 2.42 o 4 9 3 3.70 3.34 0.73 o 5 9 3 17.31 17.16 1.28 o 6 9 3 17.72 17.83 1.21 o 7 9 3 64.36 58.00 1.86 o 1 10 3 69.51 72.85 2.53 o 2 10 3 0.25 -0.08 0.49 o 3 10 3 9.95 9.58 0.97 o 4 10 3 8.86 8.35 0.85 o 5 10 3 16.90 16.41 1.06 o 6 10 3 11.24 12.23 0.83 o 0 11 3 4.89 4.27 0.67 o 1 11 3 10.52 10.23 0.88 o 2 11 3 4.79 5.33 0.67 o 3 11 3 59.16 54.55 1.81 o 4 11 3 6.52 5.97 0.63 o 0 0 4 388.88 410.36 5.44 o 2 0 4 110.81 108.56 2.87 o 8 0 4 131.98 133.17 3.62 o 10 0 4 8.86 6.47 0.71 o 1 1 4 39.59 41.17 1.78 o 2 1 4 155.94 166.57 3.57 o 3 1 4 95.33 103.12 2.93 o 8 1 4 51.73 50.10 2.24 o 9 1 4 6.09 6.52 0.80 o 10 1 4 59.73 60.03 1.99 o 0 2 4 110.18 101.51 2.79 o 1 2 4 154.72 169.79 3.61 o 2 2 4 1.67 1.17 0.54 o 3 2 4 6.84 7.44 0.91 o 4 2 4 5.59 5.06 0.83 o 7 2 4 39.03 40.32 2.08 o 8 2 4 7.73 8.08 0.98 o 9 2 4 4.92 5.13 0.77 o 10 2 4 31.84 28.51 1.37 o 1 3 4 96.45 99.70 2.85 o 2 3 4 7.20 4.89 0.83 o 3 3 4 282.88 271.09 4.95 o 4 3 4 61.77 58.20 2.38 o 6 3 4 2.83 0.50 0.67 o 7 3 4 30.72 29.22 1.78 o 8 3 4 87.32 87.85 2.86 o 9 3 4 20.47 22.50 1.37 o 10 3 4 1.32 0.48 0.36 o 0 4 4 122.37 127.71 3.39 o 1 4 4 73.47 72.82 1.82 o 2 4 4 5.58 5.60 0.83 o 3 4 4 61.60 51.14 2.23 o 4 4 4 0.95 0.87 0.42 o 5 4 4 11.17 7.84 0.99 o 6 4 4 53.57 51.00 2.32 o 7 4 4 50.23 47.60 2.18 o 8 4 4 13.36 10.46 1.10 o 9 4 4 54.88 52.06 1.93 o 1 5 4 235.03 231.06 4.49 o 2 5 4 125.32 125.51 3.70 o 3 5 4 31.95 34.80 1.48 o 4 5 4 11.26 7.65 0.97 o 5 5 4 161.88 161.28 4.08 o 6 5 4 21.09 18.31 1.45 o 7 5 4 1.07 2.55 0.62 o 8 5 4 27.32 24.15 1.41 o 9 5 4 2.50 3.34 0.52 o 0 6 4 171.35 177.28 5.30 o 1 6 4 46.07 47.30 1.56 o 2 6 4 118.49 122.83 2.51 o 3 6 4 2.80 1.79 0.62 o 4 6 4 53.68 51.06 2.30 o 5 6 4 20.95 16.48 1.38 o 6 6 4 1.61 2.15 0.61 o 7 6 4 29.97 27.69 1.52 o 8 6 4 5.47 3.67 0.58 o 1 7 4 14.17 13.26 0.92 o 2 7 4 38.66 36.28 1.98 o 3 7 4 30.82 31.40 1.81 o 4 7 4 49.16 47.75 2.23 o 5 7 4 1.06 1.23 0.52 o 6 7 4 29.89 27.61 1.53 o 7 7 4 14.45 13.47 1.03 o 8 7 4 29.52 27.96 1.23 o 0 8 4 131.52 131.40 3.61 o 1 8 4 51.05 51.49 2.28 o 2 8 4 7.68 7.39 0.92 o 3 8 4 87.43 86.30 2.84 o 4 8 4 13.22 11.10 1.06 o 5 8 4 27.80 23.38 1.39 o 6 8 4 5.52 4.88 0.65 o 7 8 4 29.88 26.68 1.19 o 1 9 4 6.09 7.59 0.86 o 2 9 4 4.72 5.86 0.78 o 3 9 4 20.10 19.92 1.28 o 4 9 4 54.72 50.57 1.89 o 5 9 4 2.53 1.91 0.47 o 0 10 4 9.37 8.99 0.83 o 1 10 4 60.07 65.37 2.05 o 2 10 4 31.88 30.55 1.41 o 3 10 4 1.27 1.27 0.43 o 1 0 5 9.33 10.79 1.15 o 3 0 5 304.90 319.95 5.70 o 0 1 5 9.82 12.61 1.27 o 1 1 5 0.65 4.32 0.76 o 2 1 5 54.11 54.78 2.37 o 3 1 5 151.17 167.89 4.14 o 4 1 5 45.48 46.56 2.21 o 9 1 5 30.09 27.76 1.25 o 1 2 5 54.49 58.50 2.46 o 2 2 5 34.38 33.19 1.85 o 3 2 5 13.42 14.11 1.30 o 4 2 5 14.18 16.96 1.41 o 9 2 5 19.38 17.19 0.95 o 0 3 5 305.65 313.28 5.67 o 1 3 5 151.10 170.58 4.19 o 2 3 5 13.49 15.35 1.31 o 3 3 5 0.50 -0.30 0.50 o 4 3 5 37.16 38.00 2.00 o 5 3 5 8.83 9.40 1.01 o 8 3 5 1.78 2.32 0.51 o 1 4 5 45.79 46.78 2.21 o 2 4 5 14.04 17.36 1.43 o 3 4 5 37.79 41.07 2.09 o 4 4 5 35.88 30.99 1.84 o 5 4 5 53.52 57.14 2.35 o 7 4 5 9.08 7.64 0.79 o 8 4 5 1.79 2.49 0.46 o 0 5 5 19.59 19.91 1.04 o 1 5 5 22.05 22.22 1.10 o 2 5 5 53.95 52.30 2.01 o 3 5 5 8.42 9.11 1.07 o 4 5 5 53.34 57.53 2.34 o 5 5 5 12.09 10.05 1.02 o 6 5 5 45.02 38.32 1.71 o 7 5 5 8.17 7.32 0.72 o 1 6 5 7.73 8.47 0.70 o 2 6 5 18.76 18.82 0.98 o 3 6 5 18.58 18.02 1.03 o 4 6 5 40.41 34.34 1.24 o 5 6 5 45.31 37.16 1.71 o 6 6 5 41.37 32.34 1.47 o 7 6 5 40.45 36.99 1.40 o 0 7 5 37.68 39.48 1.79 o 1 7 5 17.19 17.47 0.93 o 2 7 5 4.71 5.05 0.54 o 3 7 5 0.56 0.63 0.30 o 4 7 5 9.04 6.69 0.81 o 5 7 5 8.29 6.85 0.71 o 6 7 5 40.28 33.06 1.31 o 1 8 5 9.85 11.89 0.70 o 2 8 5 64.68 64.15 2.80 o 3 8 5 1.82 2.03 0.43 o 4 8 5 1.77 2.13 0.43 o 0 9 5 4.20 5.64 0.43 o 1 9 5 29.94 28.46 1.24 o 2 9 5 19.63 17.07 0.96 o 0 0 6 86.69 90.02 2.96 o 2 0 6 63.65 66.00 2.55 o 4 0 6 11.91 14.71 1.23 o 1 1 6 0.00 0.36 0.49 o 2 1 6 68.77 71.11 2.63 o 3 1 6 9.64 11.46 1.05 o 4 1 6 35.62 42.26 1.89 o 5 1 6 9.13 9.29 0.93 o 0 2 6 63.40 70.10 2.62 o 1 2 6 68.78 77.00 2.71 o 2 2 6 82.33 85.97 2.83 o 3 2 6 0.44 0.08 0.45 o 4 2 6 16.39 17.84 1.24 o 5 2 6 2.57 2.58 0.59 o 1 3 6 9.57 11.05 1.07 o 2 3 6 0.44 0.50 0.37 o 3 3 6 1.47 0.64 0.48 o 4 3 6 24.90 29.70 1.52 o 5 3 6 12.21 14.22 1.03 o 6 3 6 5.66 5.47 0.62 o 0 4 6 12.05 16.69 1.22 o 1 4 6 35.64 40.04 1.85 o 2 4 6 16.48 16.21 1.22 o 3 4 6 25.11 27.73 1.50 o 4 4 6 0.98 0.91 0.52 o 5 4 6 0.87 1.37 0.40 o 1 5 6 8.98 8.37 0.84 o 2 5 6 2.45 2.37 0.52 o 3 5 6 12.35 14.33 1.06 o 4 5 6 0.88 2.03 0.43 o 0 6 6 75.98 76.32 3.63 o 1 6 6 3.90 4.14 0.42 o 2 6 6 0.95 1.46 0.27 o 3 6 6 5.63 4.25 0.59 o 1 0 7 9.42 8.80 0.76 o 0 1 7 9.18 10.19 0.80 o 1 1 7 0.97 0.56 0.36 o 2 1 7 3.50 3.74 0.50 o 1 2 7 3.51 4.16 0.56 o