#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/26/2202663.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202663_Fobs loop_ _publ_author_name 'Zeng, Ju-Lan' 'Jiang, Yi-Min' 'Yu, Kai-Bei' _publ_section_title ; A new one-dimensional coordination polymer: {[Cu(C~10~H~9~NO~5~S)(H~2~O)]·H~2~O}~n~ ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1137 _journal_page_last m1139 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.690 _cell_angle_gamma 90.000 _cell_length_a 8.5890 _cell_length_b 17.5850 _cell_length_c 9.4790 _exptl_crystal_F_000 724.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file hg6004Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C:\XSCANS\Y1467 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 314.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2100.65 2085.46 17.40 o 2 0 0 10781.28 11000.86 57.97 o 3 0 0 455.11 470.39 15.03 o 4 0 0 422.71 451.92 18.78 o 5 0 0 274.51 332.74 20.01 o 6 0 0 358.33 351.53 23.14 o 7 0 0 751.06 830.05 35.68 o 8 0 0 698.10 704.02 38.17 o 9 0 0 206.49 220.05 28.76 o 1 1 0 10698.74 10939.34 41.26 o 2 1 0 1026.79 1010.59 18.26 o 3 1 0 1203.38 1247.94 24.52 o 4 1 0 1282.53 1301.77 29.51 o 5 1 0 2572.67 2728.58 47.24 o 6 1 0 1078.13 1053.43 35.09 o 7 1 0 1683.58 1698.73 48.30 o 8 1 0 42.31 47.50 21.25 o 9 1 0 379.47 386.47 33.77 o 0 2 0 17794.47 16702.08 135.73 o 1 2 0 6193.87 6457.36 30.03 o 2 2 0 97.58 73.16 6.88 o 3 2 0 9020.71 8497.50 63.23 o 4 2 0 77.89 82.51 12.50 o 5 2 0 436.05 393.59 20.65 o 6 2 0 680.57 588.45 28.80 o 7 2 0 9.15 6.25 17.50 o 8 2 0 1263.91 1234.84 48.87 o 9 2 0 235.92 237.57 30.63 o 1 3 0 2486.78 2746.92 20.45 o 2 3 0 8561.37 8604.16 49.35 o 3 3 0 74.87 72.52 8.75 o 4 3 0 5917.30 6111.57 63.19 o 5 3 0 23.45 20.00 11.87 o 6 3 0 7.69 -0.62 13.75 o 7 3 0 955.21 939.38 38.20 o 8 3 0 237.34 281.34 27.51 o 9 3 0 269.12 255.09 31.26 o 0 4 0 15426.13 14750.35 49.91 o 1 4 0 599.70 625.20 11.30 o 2 4 0 923.20 966.80 16.96 o 3 4 0 1862.59 1933.51 29.61 o 4 4 0 423.10 481.90 18.78 o 5 4 0 56.11 50.00 13.75 o 6 4 0 120.55 150.02 17.50 o 7 4 0 70.73 51.88 20.63 o 8 4 0 192.56 186.30 26.26 o 9 4 0 64.84 59.37 25.62 o 1 5 0 10246.52 10099.99 47.80 o 2 5 0 955.55 1081.36 18.21 o 3 5 0 556.14 625.72 17.54 o 4 5 0 215.54 218.25 14.38 o 5 5 0 265.84 305.19 18.76 o 6 5 0 631.38 644.66 28.79 o 7 5 0 465.30 417.24 28.78 o 8 5 0 45.95 68.12 20.00 o 9 5 0 129.57 100.01 26.88 o 0 6 0 13.71 15.62 5.00 o 1 6 0 759.42 769.90 14.43 o 2 6 0 1159.65 1150.32 20.10 o 3 6 0 879.09 998.22 21.95 o 4 6 0 319.96 336.55 16.89 o 5 6 0 22.49 41.25 14.37 o 6 6 0 15.16 7.50 16.25 o 7 6 0 50.84 63.12 19.37 o 8 6 0 33.55 25.62 21.25 o 1 7 0 5119.58 5075.05 39.03 o 2 7 0 154.97 170.09 10.63 o 3 7 0 452.75 458.18 16.27 o 4 7 0 2.09 -1.25 10.62 o 5 7 0 305.13 310.21 20.01 o 6 7 0 133.06 153.15 19.38 o 7 7 0 385.90 368.37 29.39 o 8 7 0 97.62 68.13 22.50 o 0 8 0 10046.23 9403.00 55.39 o 1 8 0 653.53 677.38 16.29 o 2 8 0 2920.64 2882.92 34.12 o 3 8 0 2728.45 3001.58 39.10 o 4 8 0 234.03 201.36 15.63 o 5 8 0 841.44 883.66 30.06 o 6 8 0 723.94 746.13 31.92 o 7 8 0 351.19 326.44 28.77 o 8 8 0 113.81 75.63 24.38 o 1 9 0 1737.67 1434.72 23.90 o 2 9 0 617.11 514.15 16.91 o 3 9 0 1.48 10.00 8.75 o 4 9 0 2974.50 2912.74 45.99 o 5 9 0 292.74 287.67 20.64 o 6 9 0 388.41 376.52 26.27 o 7 9 0 1393.41 1422.54 47.63 o 8 9 0 103.17 108.76 25.00 o 0 10 0 550.27 483.99 15.65 o 1 10 0 2874.78 2867.39 35.97 o 2 10 0 815.61 800.72 21.30 o 3 10 0 6240.35 6052.31 60.44 o 4 10 0 250.96 235.12 16.88 o 5 10 0 845.16 807.76 30.06 o 6 10 0 348.93 388.36 26.27 o 7 10 0 2.88 -1.25 20.00 o 8 10 0 322.38 301.39 33.14 o 1 11 0 3975.28 4029.40 44.92 o 2 11 0 4885.17 4772.12 51.35 o 3 11 0 374.47 365.95 18.14 o 4 11 0 1845.14 1754.71 37.67 o 5 11 0 63.62 55.63 15.00 o 6 11 0 10.06 36.87 16.87 o 7 11 0 780.44 825.50 40.68 o 8 11 0 273.45 281.35 33.14 o 0 12 0 14840.62 14592.96 89.28 o 1 12 0 1086.67 1064.44 26.96 o 2 12 0 252.11 253.89 16.26 o 3 12 0 1791.16 1727.72 35.78 o 4 12 0 0.80 13.12 13.12 o 5 12 0 150.34 166.28 18.75 o 6 12 0 451.26 402.19 28.15 o 7 12 0 195.14 161.91 26.26 o 1 13 0 5875.31 5745.68 59.67 o 2 13 0 85.84 86.26 13.13 o 3 13 0 9.28 21.87 11.25 o 4 13 0 371.74 382.77 21.89 o 5 13 0 1124.30 1065.51 35.70 o 6 13 0 397.31 428.40 28.77 o 7 13 0 457.26 469.70 34.40 o 0 14 0 5062.95 4924.33 58.23 o 1 14 0 162.46 139.41 18.13 o 2 14 0 796.90 721.30 25.67 o 3 14 0 79.70 89.38 15.00 o 4 14 0 105.85 97.51 18.13 o 5 14 0 200.20 172.55 21.88 o 6 14 0 463.02 492.24 31.27 o 7 14 0 111.26 75.00 25.63 o 1 15 0 616.82 577.01 23.78 o 2 15 0 45.18 48.12 13.75 o 3 15 0 347.75 325.20 20.64 o 4 15 0 343.62 347.08 24.39 o 5 15 0 23.16 6.25 18.75 o 6 15 0 53.71 22.50 20.00 o 0 16 0 82.50 43.75 15.00 o 1 16 0 346.41 301.44 20.01 o 2 16 0 59.84 55.62 15.00 o 3 16 0 421.68 449.71 26.27 o 4 16 0 125.03 96.89 20.00 o 5 16 0 68.88 70.00 19.37 o 6 16 0 18.17 18.12 18.75 o 1 17 0 93.69 98.76 16.88 o 2 17 0 89.17 70.63 16.25 o 3 17 0 58.45 56.87 18.12 o 4 17 0 18.41 26.87 17.50 o 5 17 0 0.42 2.50 18.75 o 0 18 0 19.10 21.87 15.62 o 1 18 0 11.96 8.12 15.00 o 2 18 0 159.92 135.65 20.00 o 3 18 0 260.17 275.10 24.38 o 4 18 0 99.33 96.25 20.63 o 5 18 0 7.68 -1.25 17.50 o 1 19 0 11.29 11.25 15.62 o 2 19 0 288.97 253.23 23.76 o 3 19 0 87.20 96.88 21.25 o 4 19 0 198.37 206.92 25.01 o 0 20 0 413.62 434.03 27.52 o 1 20 0 9.61 4.37 15.62 o 2 20 0 230.11 282.58 25.63 o 3 20 0 585.44 612.43 34.41 o 1 21 0 656.70 670.07 33.16 o -9 1 1 5.44 -20.62 20.62 o -8 1 1 0.43 -0.62 18.12 o -7 1 1 52.53 60.00 16.25 o -6 1 1 550.59 530.73 25.03 o -5 1 1 2536.95 2662.84 44.74 o -4 1 1 1026.35 1156.57 26.36 o -3 1 1 1211.48 1329.21 23.90 o -2 1 1 2120.95 2315.66 24.79 o -1 1 1 4852.29 4894.98 25.93 o 0 1 1 151.16 175.73 3.10 o 1 1 1 8282.10 8391.32 46.91 o 2 1 1 958.93 1043.23 20.74 o 3 1 1 3.73 2.50 7.50 o 4 1 1 465.20 506.36 20.03 o 5 1 1 1877.46 1825.69 42.09 o 6 1 1 464.21 449.20 26.28 o 7 1 1 37.66 47.50 19.37 o 8 1 1 106.09 65.00 23.13 o -9 2 1 79.21 110.00 25.63 o -8 2 1 397.56 428.42 28.77 o -7 2 1 404.16 449.12 27.52 o -6 2 1 1033.58 1047.80 34.47 o -5 2 1 798.40 803.22 25.06 o -4 2 1 3293.35 3462.76 44.32 o -3 2 1 20.13 33.12 6.87 o -2 2 1 299.00 318.17 9.39 o -1 2 1 230.32 209.26 5.64 o 0 2 1 17849.30 18159.86 382.65 o 1 2 1 17.87 13.75 3.75 o 2 2 1 456.31 486.19 15.04 o 3 2 1 70.70 60.01 9.38 o 4 2 1 655.05 650.73 23.80 o 5 2 1 304.97 266.44 21.27 o 6 2 1 1184.87 1274.73 40.74 o 7 2 1 247.92 229.47 24.38 o 8 2 1 275.21 313.25 30.64 o -9 3 1 143.38 121.27 25.00 o -8 3 1 4.45 11.25 19.37 o -7 3 1 2644.35 2626.38 57.85 o -6 3 1 102.05 98.14 15.63 o -5 3 1 1164.88 1123.99 30.73 o -4 3 1 9997.27 10239.98 77.22 o -3 3 1 25.41 46.25 8.12 o -2 3 1 3188.16 3049.83 27.45 o -1 3 1 1592.55 1680.45 16.48 o 0 3 1 464.55 520.34 6.21 o 1 3 1 684.63 659.42 11.93 o 2 3 1 1930.51 1955.21 26.52 o 3 3 1 729.43 759.03 21.94 o 4 3 1 2633.23 2479.17 44.12 o 5 3 1 275.98 298.31 20.64 o 6 3 1 262.32 263.25 22.51 o 7 3 1 636.71 540.66 34.42 o 8 3 1 71.07 69.37 24.37 o -9 4 1 69.60 80.62 25.62 o -8 4 1 959.91 912.93 40.07 o -7 4 1 594.93 573.83 31.29 o -6 4 1 1204.19 1101.47 34.48 o -5 4 1 4014.09 4120.46 56.31 o -4 4 1 16.01 23.75 10.00 o -3 4 1 12853.66 12494.02 70.79 o -2 4 1 12619.88 12856.16 59.03 o -1 4 1 10640.67 10324.44 44.40 o 0 4 1 515.89 564.99 7.10 o 1 4 1 657.03 669.56 12.55 o 2 4 1 3699.12 3651.48 34.99 o 3 4 1 6194.66 6098.60 56.95 o 4 4 1 330.48 334.68 19.39 o 5 4 1 2370.45 2488.74 50.32 o 6 4 1 613.27 652.11 32.54 o 7 4 1 12.88 7.50 18.75 o 8 4 1 637.01 596.89 38.79 o -9 5 1 375.21 375.21 33.14 o -8 5 1 86.89 119.38 22.50 o -7 5 1 1929.06 2012.87 51.47 o -6 5 1 74.39 98.76 15.63 o -5 5 1 831.52 844.49 26.94 o -4 5 1 8167.54 8431.32 68.79 o -3 5 1 190.29 173.24 10.63 o -2 5 1 8647.07 8089.98 48.34 o -1 5 1 8415.77 8163.86 42.71 o 0 5 1 267.56 259.84 5.75 o 1 5 1 719.68 625.53 13.18 o 2 5 1 2813.44 2723.92 31.01 o 3 5 1 4300.04 4439.52 48.25 o 4 5 1 4853.29 4988.69 60.26 o 5 5 1 619.28 610.92 28.17 o 6 5 1 937.68 938.17 37.58 o 7 5 1 906.39 949.78 41.95 o 8 5 1 556.88 528.61 38.79 o -9 6 1 62.58 71.87 25.00 o -8 6 1 6.34 14.37 17.50 o -7 6 1 424.36 468.50 27.52 o -6 6 1 2472.14 2485.64 50.93 o -5 6 1 3260.22 3240.40 49.83 o -4 6 1 2780.09 2868.83 41.00 o -3 6 1 9124.85 9387.12 62.81 o -2 6 1 4536.61 4747.73 38.30 o -1 6 1 516.44 609.73 13.16 o 0 6 1 5702.72 5364.94 106.59 o 1 6 1 3.52 1.87 4.37 o 2 6 1 1092.68 964.25 19.46 o 3 6 1 6910.63 7155.24 60.79 o 4 6 1 989.64 1000.31 28.20 o 5 6 1 2534.77 2362.56 49.69 o 6 6 1 1860.35 1900.28 51.46 o 7 6 1 523.40 447.29 33.78 o 8 6 1 333.96 387.69 35.02 o -9 7 1 105.23 133.13 30.00 o -8 7 1 89.72 81.25 22.50 o -7 7 1 1393.30 1445.43 45.13 o -6 7 1 2636.11 2641.54 52.83 o -5 7 1 3837.40 3695.93 54.31 o -4 7 1 7499.15 7234.99 65.26 o -3 7 1 2741.18 2831.92 35.35 o -2 7 1 4650.03 4595.24 40.15 o -1 7 1 937.81 738.76 15.69 o 0 7 1 547.45 582.37 9.75 o 1 7 1 43.20 21.88 6.25 o 2 7 1 33.42 32.50 7.50 o 3 7 1 1055.57 1147.59 25.71 o 4 7 1 2407.89 2319.94 41.53 o 5 7 1 3134.08 3181.24 56.05 o 6 7 1 1842.26 1761.98 50.83 o 7 7 1 1088.01 1036.50 45.09 o 8 7 1 296.71 264.48 32.51 o -9 8 1 75.34 90.00 25.62 o -8 8 1 20.38 21.87 18.12 o -7 8 1 553.79 539.31 31.91 o -6 8 1 1097.71 1050.71 35.09 o -5 8 1 3982.29 3865.04 56.84 o -4 8 1 858.87 813.88 24.44 o -3 8 1 7970.93 7804.54 60.98 o -2 8 1 4317.54 4717.75 42.57 o -1 8 1 1759.73 1752.51 25.18 o 0 8 1 374.53 533.00 13.77 o 1 8 1 469.22 489.59 14.40 o 2 8 1 127.67 93.78 10.00 o 3 8 1 3667.59 3629.19 44.88 o 4 8 1 290.85 323.96 18.76 o 5 8 1 1718.96 1783.43 42.67 o 6 8 1 551.17 518.68 29.41 o 7 8 1 286.35 245.73 28.14 o 8 8 1 254.04 222.57 31.89 o -8 9 1 5.89 4.37 20.62 o -7 9 1 1241.92 1279.37 41.98 o -6 9 1 0.69 -6.87 16.25 o -5 9 1 166.11 163.17 17.51 o -4 9 1 3442.98 3296.10 47.33 o -3 9 1 207.58 166.34 11.88 o -2 9 1 4270.00 4235.18 43.13 o -1 9 1 106.90 105.65 9.38 o 0 9 1 566.90 579.08 11.07 o 1 9 1 71.75 40.00 8.75 o 2 9 1 1109.74 1090.06 23.83 o 3 9 1 1264.62 1307.79 29.48 o 4 9 1 2405.80 2379.59 44.02 o 5 9 1 139.90 146.28 19.38 o 6 9 1 20.72 24.37 17.50 o 7 9 1 219.51 211.94 26.26 o 8 9 1 572.31 538.60 41.29 o -8 10 1 82.30 98.13 23.75 o -7 10 1 486.20 483.54 30.65 o -6 10 1 2.94 10.62 15.00 o -5 10 1 5.70 15.00 12.50 o -4 10 1 280.52 300.19 16.89 o -3 10 1 557.34 550.22 19.40 o -2 10 1 1477.31 1501.96 27.63 o -1 10 1 549.50 542.19 17.53 o 0 10 1 1120.67 1159.09 16.41 o 1 10 1 366.88 372.90 14.39 o 2 10 1 47.46 32.50 9.38 o 3 10 1 1329.71 1397.45 31.36 o 4 10 1 116.60 93.14 15.00 o 5 10 1 56.69 54.37 15.62 o 6 10 1 4.90 -10.62 16.25 o 7 10 1 5.11 20.62 19.37 o -8 11 1 66.56 73.12 24.37 o -7 11 1 1.64 15.00 20.00 o -6 11 1 100.58 85.63 18.13 o -5 11 1 763.30 785.68 29.42 o -4 11 1 188.37 145.05 15.63 o -3 11 1 122.54 150.03 13.75 o -2 11 1 119.37 131.90 11.88 o -1 11 1 214.69 227.62 13.13 o 0 11 1 248.19 242.27 9.50 o 1 11 1 412.24 465.52 17.52 o 2 11 1 14.85 24.37 10.62 o 3 11 1 27.32 16.87 11.87 o 4 11 1 220.46 208.21 18.13 o 5 11 1 329.02 332.07 22.51 o 6 11 1 34.46 23.75 17.50 o 7 11 1 0.26 -19.37 19.37 o -8 12 1 96.61 131.88 26.25 o -7 12 1 164.10 166.90 24.38 o -6 12 1 88.90 88.13 20.00 o -5 12 1 150.46 160.66 18.13 o -4 12 1 1075.54 1097.73 31.33 o -3 12 1 589.93 594.59 21.91 o -2 12 1 292.85 273.31 15.01 o -1 12 1 1095.40 1100.83 25.70 o 0 12 1 64.98 62.33 8.36 o 1 12 1 2121.55 2115.41 35.20 o 2 12 1 31.77 35.62 11.87 o 3 12 1 1084.15 1048.30 29.45 o 4 12 1 338.45 324.58 21.26 o 5 12 1 81.92 72.50 20.00 o 6 12 1 357.36 343.32 28.14 o 7 12 1 28.73 45.00 21.25 o -7 13 1 94.96 84.38 20.63 o -6 13 1 137.51 140.64 21.25 o -5 13 1 58.95 43.75 17.50 o -4 13 1 202.12 199.44 18.76 o -3 13 1 32.47 19.37 11.25 o -2 13 1 1070.54 1041.51 27.57 o -1 13 1 217.95 211.97 15.63 o 0 13 1 2017.34 2002.32 25.54 o 1 13 1 702.80 707.46 23.79 o 2 13 1 1028.67 998.06 28.19 o 3 13 1 53.19 64.37 13.12 o 4 13 1 149.20 158.16 18.75 o 5 13 1 78.11 73.13 20.00 o 6 13 1 4.16 13.75 18.12 o -7 14 1 227.32 225.69 26.26 o -6 14 1 454.58 497.25 31.27 o -5 14 1 188.20 246.94 21.88 o -4 14 1 1083.84 1096.23 33.83 o -3 14 1 460.37 451.05 21.90 o -2 14 1 2.44 4.37 10.62 o -1 14 1 38.07 43.75 12.50 o 0 14 1 4223.13 4158.22 53.05 o 1 14 1 1124.57 1146.15 30.71 o 2 14 1 52.37 61.87 14.37 o 3 14 1 111.95 110.64 15.63 o 4 14 1 264.30 266.36 21.88 o 5 14 1 386.67 423.39 27.52 o 6 14 1 166.15 161.28 25.63 o -7 15 1 676.10 613.15 38.17 o -6 15 1 903.32 850.71 38.18 o -5 15 1 1051.83 1151.64 38.83 o -4 15 1 2014.39 1912.26 45.81 o -3 15 1 215.99 230.70 18.13 o -2 15 1 33.47 46.25 12.50 o -1 15 1 412.05 466.02 20.64 o 0 15 1 1194.94 1208.75 22.82 o 1 15 1 1606.15 1577.55 37.01 o 2 15 1 3.49 -2.50 13.75 o 3 15 1 66.72 73.75 16.25 o 4 15 1 315.09 371.44 25.01 o 5 15 1 1057.39 1050.10 41.33 o 6 15 1 109.33 113.13 25.00 o -6 16 1 612.74 666.91 36.29 o -5 16 1 210.36 225.06 23.76 o -4 16 1 290.49 252.61 23.14 o -3 16 1 948.33 978.71 31.93 o -2 16 1 1037.08 999.64 31.94 o -1 16 1 126.46 139.40 15.63 o 0 16 1 1161.02 1191.40 27.88 o 1 16 1 1280.63 1277.81 35.09 o 2 16 1 751.90 733.58 29.42 o 3 16 1 538.43 579.31 28.78 o 4 16 1 24.89 35.00 16.25 o 5 16 1 847.15 887.52 38.81 o -5 17 1 28.53 42.50 17.50 o -4 17 1 1592.23 1450.55 44.51 o -3 17 1 359.76 367.72 24.39 o -2 17 1 1378.68 1460.88 39.48 o -1 17 1 944.06 988.72 31.93 o 0 17 1 451.46 448.34 38.78 o 1 17 1 263.05 300.75 21.88 o 2 17 1 714.40 709.69 31.29 o 3 17 1 480.79 488.52 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184.68 179.41 27.51 o -10 2 4 21.32 25.62 21.25 o -9 2 4 303.60 361.42 28.14 o -8 2 4 3266.49 3092.87 62.94 o -7 2 4 2367.14 2415.54 52.80 o -6 2 4 7753.17 7639.15 81.07 o -5 2 4 3.25 24.37 11.87 o -4 2 4 321.43 300.31 15.02 o -3 2 4 100.47 61.89 8.13 o -2 2 4 2128.57 2017.46 29.02 o -1 2 4 857.17 809.84 17.56 o 0 2 4 1192.70 1255.98 162.02 o 1 2 4 313.36 352.23 16.27 o 2 2 4 5263.17 5379.47 66.70 o 3 2 4 2271.49 2238.55 49.68 o 4 2 4 341.01 388.39 25.64 o 5 2 4 1060.47 1072.31 44.47 o 6 2 4 2.67 25.62 21.25 o 7 2 4 0.81 15.62 21.87 o -10 3 4 114.00 78.76 25.00 o -9 3 4 170.53 151.28 26.26 o -8 3 4 778.73 779.34 35.05 o -7 3 4 4226.87 4188.92 66.92 o -6 3 4 2202.19 2127.54 44.01 o -5 3 4 1850.15 1911.42 37.71 o -4 3 4 439.52 479.44 18.15 o -3 3 4 52.46 84.38 9.38 o -2 3 4 1285.27 1329.00 23.25 o -1 3 4 1330.43 1290.25 22.00 o 0 3 4 1074.51 1008.95 28.87 o 1 3 4 86.32 111.27 10.00 o 2 3 4 1902.17 1887.00 42.11 o 3 3 4 108.33 97.52 17.50 o 4 3 4 2025.08 1983.69 54.63 o 5 3 4 84.41 85.63 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352.76 327.76 18.14 o -3 10 4 1474.62 1506.51 32.00 o -2 10 4 1176.30 1145.52 27.59 o -1 10 4 4958.32 4942.32 54.49 o 0 10 4 204.59 232.90 25.95 o 1 10 4 79.88 66.25 13.13 o 2 10 4 334.64 330.85 19.39 o 3 10 4 1333.18 1394.58 38.86 o 4 10 4 144.67 150.02 22.50 o 5 10 4 760.09 807.94 40.05 o 6 10 4 14.50 30.62 23.12 o -8 11 4 507.60 492.91 33.15 o -7 11 4 3915.36 3891.99 70.55 o -6 11 4 385.41 369.01 23.77 o -5 11 4 575.83 609.49 26.28 o -4 11 4 1036.10 1097.68 30.07 o -3 11 4 0.51 -5.00 11.87 o -2 11 4 3000.84 2823.28 43.46 o -1 11 4 732.44 714.42 23.79 o 0 11 4 3608.53 3494.59 34.79 o 1 11 4 978.04 979.10 28.82 o 2 11 4 469.89 480.46 23.15 o 3 11 4 142.14 143.15 19.38 o 4 11 4 1073.40 1140.43 41.33 o 5 11 4 7.55 1.25 20.00 o -8 12 4 394.52 460.90 33.77 o -7 12 4 216.04 226.94 23.76 o -6 12 4 2579.22 2633.25 54.66 o -5 12 4 848.58 771.99 30.05 o -4 12 4 657.73 699.75 26.29 o -3 12 4 1128.96 1047.77 30.08 o -2 12 4 28.55 18.12 10.62 o -1 12 4 502.20 490.55 21.27 o 0 12 4 1119.84 1080.17 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