#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:02:05 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180946 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/26/2202667.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202667_Fobs loop_ _publ_author_name 'Lee, Uk' 'Jung, Yeon-Hwa' 'Joo, Hea-Chung' 'Park, Ki-Min' _publ_section_title ; A new decavanadate with a tricobalt(II) cation and 18-crown-6, tris{hexaaquacobalt(II)} decavanadate bis(18-crown-6) decahydrate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m421 _journal_page_last m424 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 101.330 _cell_angle_beta 92.628 _cell_angle_gamma 84.261 _cell_length_a 12.2850 _cell_length_b 13.9240 _cell_length_c 11.1200 _exptl_crystal_F_000 1103.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file lh6059Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CoV10Crown' _shelx_refln_list_code 4 _shelx_f_calc_maximum 275.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 39680.67 27720.68 118.75 o 2 0 0 5237.11 5667.05 48.38 o 3 0 0 31346.32 30166.88 139.21 o 4 0 0 18628.07 17516.42 118.29 o 5 0 0 4610.26 4017.07 65.91 o 6 0 0 761.83 900.06 37.65 o 7 0 0 41.50 9.73 19.19 o 8 0 0 1768.00 1698.02 55.78 o 9 0 0 7.91 18.33 19.86 o 10 0 0 6283.53 6193.45 114.56 o 11 0 0 6.77 33.92 24.99 o 12 0 0 0.16 2.47 24.86 o 13 0 0 1269.56 1297.91 65.44 o 14 0 0 0.08 26.59 29.26 o 15 0 0 0.04 68.57 28.99 o -15 1 0 243.54 318.21 42.72 o -14 1 0 844.90 1032.14 63.11 o -13 1 0 892.76 922.72 58.64 o -12 1 0 196.90 168.80 34.39 o -11 1 0 2251.04 2248.75 77.04 o -10 1 0 7501.37 7640.90 129.35 o -9 1 0 191.45 208.59 28.19 o -8 1 0 837.20 792.23 41.52 o -7 1 0 1057.18 1101.45 43.05 o -6 1 0 317.74 361.00 28.46 o -5 1 0 814.43 534.26 28.12 o -4 1 0 2212.78 1780.79 40.85 o -3 1 0 19057.61 19131.00 108.56 o -2 1 0 3065.13 3172.26 37.19 o -1 1 0 36131.06 30518.21 123.95 o 1 1 0 3313.60 3440.49 28.19 o 2 1 0 650.75 910.12 23.46 o 3 1 0 24.17 88.50 18.99 o 4 1 0 121.74 101.89 20.66 o 5 1 0 3464.89 3404.04 59.58 o 6 1 0 0.17 28.46 19.39 o 7 1 0 518.39 591.71 33.59 o 8 1 0 15.73 -9.00 21.53 o 9 1 0 0.80 28.86 21.33 o 10 1 0 754.63 742.05 45.45 o 11 1 0 1053.47 1012.28 54.98 o 12 1 0 493.40 472.09 42.78 o 13 1 0 329.96 248.97 39.12 o 14 1 0 443.65 373.99 45.45 o 15 1 0 106.37 76.37 31.79 o -15 2 0 478.58 537.26 50.31 o -14 2 0 735.75 775.24 61.38 o -13 2 0 218.28 256.17 37.52 o -12 2 0 422.04 352.13 40.58 o -11 2 0 149.82 131.15 27.79 o -10 2 0 1203.27 1264.12 57.18 o -9 2 0 1170.21 1113.11 51.05 o -8 2 0 4721.39 4529.41 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3064.10 52.85 o -3 3 0 18.87 27.59 17.53 o -2 3 0 123.19 116.69 17.13 o -1 3 0 13340.08 13069.70 78.97 o 0 3 0 7667.44 7200.87 56.05 o 1 3 0 21058.45 20992.23 99.23 o 2 3 0 27535.12 26110.42 121.75 o 3 3 0 1965.76 2155.91 39.98 o 4 3 0 1018.27 1144.10 34.65 o 5 3 0 1609.59 1619.12 43.25 o 6 3 0 1436.30 1409.06 45.05 o 7 3 0 2185.91 2194.17 58.71 o 8 3 0 5443.08 5233.95 94.63 o 9 3 0 1010.44 1028.61 47.98 o 10 3 0 126.67 47.58 27.19 o 11 3 0 305.36 338.94 35.52 o 12 3 0 204.45 166.54 32.45 o 13 3 0 1640.22 1385.21 71.17 o 14 3 0 308.53 317.01 43.38 o 15 3 0 1469.32 1379.48 75.50 o -15 4 0 5.51 0.00 31.59 o -14 4 0 295.68 296.22 42.92 o -13 4 0 298.21 254.97 38.19 o -12 4 0 147.83 182.06 32.85 o -11 4 0 646.68 600.77 47.45 o -10 4 0 129.44 102.43 27.92 o -9 4 0 6.08 -8.33 22.32 o -8 4 0 1512.41 1498.56 54.38 o -7 4 0 91.71 81.30 20.59 o -6 4 0 759.80 729.86 35.45 o -5 4 0 1483.02 1251.79 40.18 o -4 4 0 454.91 407.45 24.66 o -3 4 0 183.73 177.40 19.19 o -2 4 0 788.43 777.17 27.26 o -1 4 0 1412.90 1425.46 32.25 o 0 4 0 13488.59 13720.86 88.70 o 1 4 0 14544.10 13617.16 88.90 o 2 4 0 96.55 132.82 17.66 o 3 4 0 34117.71 33795.17 161.81 o 4 4 0 23343.11 21653.11 141.61 o 5 4 0 20870.68 19916.44 145.21 o 6 4 0 1617.88 1762.33 50.38 o 7 4 0 4572.59 4476.97 81.84 o 8 4 0 11885.10 12266.21 145.48 o 9 4 0 4395.65 4242.72 94.10 o 10 4 0 239.72 249.11 31.85 o 11 4 0 375.61 328.81 35.19 o 12 4 0 207.97 230.98 34.72 o 13 4 0 3040.02 3020.79 98.56 o 14 4 0 1978.80 1969.32 84.37 o 15 4 0 2372.22 2320.32 93.70 o -14 5 0 12.63 -29.52 29.52 o -13 5 0 480.72 538.46 52.65 o -12 5 0 32.34 82.04 29.19 o -11 5 0 11.84 32.52 27.59 o -10 5 0 335.11 396.05 36.72 o -9 5 0 1168.49 1099.78 52.51 o -8 5 0 340.90 310.02 30.85 o -7 5 0 2.90 -13.39 19.19 o -6 5 0 6.21 -13.13 18.73 o -5 5 0 27.79 -3.87 18.19 o -4 5 0 0.33 14.13 16.93 o -3 5 0 999.30 896.86 32.19 o -2 5 0 3619.68 3426.63 53.98 o -1 5 0 7444.98 6866.13 72.11 o 0 5 0 303.23 182.00 18.39 o 1 5 0 4957.96 4774.79 59.31 o 2 5 0 525.39 430.50 23.19 o 3 5 0 37352.40 36484.41 179.47 o 4 5 0 34907.06 32741.70 184.93 o 5 5 0 24123.05 23738.72 164.74 o 6 5 0 15.85 30.32 17.73 o 7 5 0 595.23 631.56 36.05 o 8 5 0 6365.83 6733.24 110.29 o 9 5 0 1499.93 1507.89 58.44 o 10 5 0 87.67 102.69 25.79 o 11 5 0 387.98 320.88 36.99 o 12 5 0 92.45 48.18 30.66 o 13 5 0 2844.87 2721.30 95.30 o 14 5 0 358.29 343.74 44.32 o 15 5 0 364.40 258.24 44.78 o -14 6 0 58.42 19.59 31.65 o -13 6 0 463.51 507.54 49.18 o -12 6 0 48.09 -4.20 30.59 o -11 6 0 3.52 42.92 27.26 o -10 6 0 203.06 204.72 31.92 o -9 6 0 79.17 95.96 25.66 o -8 6 0 2736.20 2561.83 72.17 o -7 6 0 51.59 68.97 21.13 o -6 6 0 34.16 35.12 20.19 o -5 6 0 6628.97 6771.83 96.10 o -4 6 0 3478.76 3514.80 66.04 o -3 6 0 1564.17 1539.82 42.92 o -2 6 0 1849.31 1671.77 42.85 o -1 6 0 2718.82 2261.27 46.92 o 0 6 0 1281.69 827.75 30.52 o 1 6 0 1252.08 1242.33 35.32 o 2 6 0 135.91 153.21 18.93 o 3 6 0 20152.71 19450.41 138.35 o 4 6 0 893.06 963.83 36.05 o 5 6 0 10652.96 10582.31 114.76 o 6 6 0 4795.89 4589.66 81.84 o 7 6 0 283.78 395.78 32.85 o 8 6 0 262.33 296.95 31.45 o 9 6 0 61.63 21.39 23.19 o 10 6 0 19.15 62.04 25.59 o 11 6 0 444.51 352.53 39.32 o 12 6 0 25.98 -1.53 25.32 o 13 6 0 317.51 301.75 40.32 o 14 6 0 431.95 445.36 50.58 o 15 6 0 94.33 89.23 35.85 o -13 7 0 36.67 22.99 28.79 o -12 7 0 755.76 749.12 59.51 o -11 7 0 4.56 -24.06 24.06 o -10 7 0 84.18 140.88 28.32 o -9 7 0 20.56 9.46 21.99 o -8 7 0 171.82 215.12 28.32 o -7 7 0 1634.05 1678.83 59.04 o -6 7 0 377.58 385.92 31.85 o -5 7 0 5373.99 5267.07 88.77 o -4 7 0 4.74 18.13 17.33 o -3 7 0 313.21 339.20 26.46 o -2 7 0 230.01 212.59 21.26 o -1 7 0 46.75 68.11 16.99 o 0 7 0 9.10 57.18 15.59 o 1 7 0 1452.15 1448.72 40.38 o 2 7 0 2295.58 2215.16 50.05 o 3 7 0 3885.24 3761.37 65.51 o 4 7 0 340.21 372.79 25.92 o 5 7 0 3669.60 3730.38 72.11 o 6 7 0 1089.76 952.50 42.18 o 7 7 0 2786.84 2864.71 71.71 o 8 7 0 153.49 156.21 27.06 o 9 7 0 92.13 100.56 24.79 o 10 7 0 15.31 -21.66 23.99 o 11 7 0 441.12 461.36 43.38 o 12 7 0 135.10 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1593.35 1549.74 68.24 o -3 13 0 616.04 583.91 45.32 o -2 13 0 33.90 24.92 22.66 o -1 13 0 1607.68 1575.40 63.18 o 0 13 0 927.11 892.46 49.51 o 1 13 0 216.10 198.26 29.12 o 2 13 0 340.37 405.91 36.32 o 3 13 0 736.97 810.63 46.85 o 4 13 0 247.81 258.17 32.72 o 5 13 0 888.32 985.36 52.38 o 6 13 0 440.45 411.51 39.72 o 7 13 0 132.07 187.20 31.59 o 8 13 0 23.71 47.45 26.26 o 9 13 0 183.57 171.27 34.39 o 10 13 0 0.21 16.19 26.86 o 11 13 0 11.64 -3.60 30.79 o -8 14 0 376.97 418.71 45.98 o -7 14 0 478.12 503.21 47.05 o -6 14 0 46.79 44.65 30.32 o -5 14 0 29.87 78.50 26.59 o -4 14 0 1710.52 1739.34 74.51 o -3 14 0 94.21 107.29 27.26 o -2 14 0 49.60 33.19 25.66 o -1 14 0 598.40 726.46 45.78 o 0 14 0 25.78 29.26 24.52 o 1 14 0 3.91 -22.12 22.12 o 2 14 0 730.03 761.44 47.58 o 3 14 0 77.84 70.24 25.52 o 4 14 0 165.78 189.06 30.19 o 5 14 0 407.62 484.62 43.32 o 6 14 0 101.47 63.18 29.92 o 7 14 0 45.90 25.79 24.19 o 8 14 0 18.46 -1.67 26.52 o 9 14 0 6.24 -27.92 27.92 o 10 14 0 1.00 27.92 25.66 o -7 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