#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/26/2202671.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202671_Fobs loop_ _publ_author_name 'Sakai, Ken' 'Kurashima, Mai' _publ_section_title ; [\m-2,3,5,6-Tetrakis(2-pyridyl)pyrazine]bis[chloroplatinum(II)] bis[trichloro(dimethyl sulfoxide-\kS)platinate(II)] ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m411 _journal_page_last m413 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 94.085 _cell_angle_beta 105.321 _cell_angle_gamma 100.954 _cell_length_a 10.0868 _cell_length_b 12.9476 _cell_length_c 16.5057 _exptl_crystal_F_000 1468.00 _reflns_d_resolution_high 0.8994 _[local]_cod_data_source_file lh6065Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tpp4 in P-1 2003/05/14 13:33:08 000 KENX 2003/05/14 13:48:40 010 KENX' _shelx_refln_list_code 4 _shelx_f_calc_maximum 583.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 24841.71 26976.46 831.52 o 2 0 0 67318.50 71635.62 1826.92 o 3 0 0 89.21 713.62 903.32 o 4 0 0 67623.88 68396.01 2481.20 o 5 0 0 55297.41 55091.09 2517.27 o 6 0 0 8554.22 9984.88 1478.33 o 7 0 0 26482.48 28285.07 2442.03 o 8 0 0 1000.42 -207.80 1862.66 o 9 0 0 14612.81 15095.21 3362.78 o 10 0 0 1026.15 5941.82 2506.39 o -10 1 0 31.90 4082.17 2198.82 o -9 1 0 5884.26 8414.26 2680.91 o -8 1 0 9983.03 8578.91 2542.72 o -7 1 0 8977.36 8932.40 2046.41 o -6 1 0 10794.11 9678.91 1462.82 o -5 1 0 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