#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/26/2202686.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202686_Fobs loop_ _publ_author_name 'Candiota, Rafael O.' 'Comerlato, Nadia M.' 'Howie, R. Alan' 'Wardell, James L.' _publ_section_title ; Bis(tetraphenylphosphonium) bis(2-oxo-1,3-dithiole-4,5-dithiolato)zincate(II) ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m599 _journal_page_last m601 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 88.567 _cell_angle_beta 74.540 _cell_angle_gamma 87.380 _cell_length_a 16.5321 _cell_length_b 17.3265 _cell_length_c 17.9862 _exptl_crystal_F_000 2272.00 _reflns_d_resolution_high 0.7678 _[local]_cod_data_source_file lh6083Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Ph4P]2{Zn(dmio)2] (Z=4, P-1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 361.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 221.65 266.69 11.13 o 4 0 0 8084.72 7470.44 213.04 o 5 0 0 64.59 69.21 9.06 o 6 0 0 21580.17 23317.15 1209.36 o 7 0 0 2.70 8.01 14.42 o 8 0 0 3581.36 3517.68 96.97 o 9 0 0 2856.10 2766.62 84.66 o 10 0 0 19.06 29.51 51.26 o 11 0 0 695.66 611.51 145.76 o 12 0 0 1857.61 1938.58 286.72 o 13 0 0 4.85 70.82 30.43 o 14 0 0 26.29 128.14 67.28 o 15 0 0 5834.21 5804.62 498.16 o 16 0 0 214.59 291.38 64.07 o 17 0 0 1020.30 963.90 189.01 o 18 0 0 4432.50 4084.42 429.28 o 19 0 0 765.04 984.77 118.78 o 20 0 0 388.68 513.90 190.61 o -20 1 0 66.25 89.10 89.85 o -19 1 0 1272.34 1154.50 130.01 o -18 1 0 126.23 239.15 168.19 o -17 1 0 925.90 1039.96 172.99 o -16 1 0 3891.95 3935.85 207.68 o -15 1 0 433.69 392.37 265.90 o -14 1 0 69.47 84.87 24.72 o -13 1 0 10972.17 10258.29 333.17 o -12 1 0 2328.87 2357.07 192.22 o -11 1 0 1950.16 1893.84 75.39 o -10 1 0 1396.86 1263.71 80.09 o -9 1 0 236.70 232.45 32.04 o -8 1 0 15445.17 15040.81 591.06 o -7 1 0 404.66 373.85 28.83 o -6 1 0 14797.44 13882.14 295.09 o -5 1 0 36605.31 35570.18 746.11 o -4 1 0 28465.90 30702.91 709.60 o -3 1 0 68.52 80.09 6.80 o 3 1 0 741.49 715.04 62.47 o 4 1 0 25517.18 25546.33 538.78 o 5 1 0 20260.01 20099.52 1300.66 o 6 1 0 3835.44 4043.11 90.53 o 7 1 0 2836.37 2924.23 144.16 o 8 1 0 18094.91 17229.61 1063.60 o 9 1 0 1439.12 1182.03 37.72 o 10 1 0 1.28 9.19 18.13 o 11 1 0 232.52 302.05 70.48 o 12 1 0 4231.38 3879.32 135.50 o 13 1 0 1430.26 1210.08 63.32 o 14 1 0 586.48 561.06 49.25 o 15 1 0 1862.57 2338.00 156.98 o 16 1 0 1495.79 1668.56 98.94 o 17 1 0 39.31 114.34 86.50 o 18 1 0 486.67 635.94 134.55 o 19 1 0 373.52 276.86 60.45 o 20 1 0 703.70 700.92 131.35 o -20 2 0 2500.35 2616.99 216.36 o -19 2 0 45.45 104.94 92.45 o -18 2 0 25.77 79.97 58.48 o -17 2 0 192.67 141.48 49.71 o -16 2 0 779.94 842.27 72.12 o -15 2 0 42.46 97.65 28.35 o -14 2 0 2145.93 2049.76 201.83 o -13 2 0 68.80 169.79 36.00 o -12 2 0 738.32 712.99 78.49 o -11 2 0 8738.77 8995.06 264.62 o -10 2 0 3162.79 3006.34 251.48 o -9 2 0 6631.43 6668.91 189.01 o -8 2 0 476.12 484.45 40.05 o -7 2 0 628.49 733.57 56.06 o -6 2 0 2211.01 2491.12 59.23 o -5 2 0 18323.51 19074.40 459.51 o -4 2 0 27272.92 28135.38 657.73 o -3 2 0 57213.28 62212.54 1707.74 o -2 2 0 1132.35 -8.24 8.24 o 2 2 0 244.56 -5.33 5.33 o 3 2 0 60202.14 61833.38 1830.86 o 4 2 0 21278.34 21418.65 438.33 o 5 2 0 1717.23 2119.27 41.86 o 6 2 0 111.67 130.15 16.02 o 7 2 0 111.52 235.48 13.59 o 8 2 0 15.34 35.51 13.03 o 9 2 0 1444.67 1391.69 169.79 o 10 2 0 18161.58 16579.67 914.63 o 11 2 0 356.77 465.09 44.85 o 12 2 0 128.72 161.64 24.21 o 13 2 0 648.71 1001.50 99.31 o 14 2 0 1290.81 1105.62 71.03 o 15 2 0 2340.10 2534.22 174.60 o 16 2 0 1139.33 1494.32 101.59 o 17 2 0 480.22 505.78 63.47 o 18 2 0 1591.09 1712.08 121.58 o 19 2 0 45.87 113.02 59.57 o 20 2 0 32.91 -20.44 70.37 o -20 3 0 282.64 394.37 92.55 o -19 3 0 707.96 699.73 144.16 o -18 3 0 77.90 173.55 76.18 o -17 3 0 599.16 427.10 50.96 o -16 3 0 60.03 152.69 88.10 o -15 3 0 2783.85 2851.54 138.89 o -14 3 0 2733.67 2756.51 118.69 o -13 3 0 7.32 276.84 51.85 o -12 3 0 10863.26 9490.37 693.58 o -11 3 0 40.73 114.26 22.92 o -10 3 0 47.22 13.88 20.82 o -9 3 0 1083.40 1277.10 80.09 o -8 3 0 5752.43 5154.38 154.75 o -7 3 0 3068.06 3681.90 111.29 o -6 3 0 3633.91 3474.86 94.82 o -5 3 0 36216.72 36114.75 827.40 o -4 3 0 18170.47 19996.88 477.91 o -3 3 0 19645.62 21721.35 616.11 o -2 3 0 10263.96 12018.40 296.10 o -1 3 0 28337.00 27433.23 902.17 o 0 3 0 59.19 9.61 12.81 o 1 3 0 41262.57 39818.24 1065.35 o 2 3 0 7379.34 8256.13 258.24 o 3 3 0 19433.96 19554.49 515.85 o 4 3 0 30340.77 30599.34 624.63 o 5 3 0 4454.94 4720.86 110.75 o 6 3 0 4205.28 4020.81 118.53 o 7 3 0 607.76 786.63 25.98 o 8 3 0 45.46 43.02 9.61 o 9 3 0 258.61 293.76 16.88 o 10 3 0 1209.18 1091.29 44.88 o 11 3 0 9001.34 9008.28 1002.73 o 12 3 0 346.73 415.28 92.90 o 13 3 0 3908.45 3324.91 233.86 o 14 3 0 3531.49 3360.18 146.72 o 15 3 0 1672.46 1836.93 126.54 o 16 3 0 2.10 107.85 59.27 o 17 3 0 45.82 35.58 83.29 o 18 3 0 632.82 623.60 83.29 o 19 3 0 505.28 604.27 96.11 o 20 3 0 905.79 1082.89 109.71 o -20 4 0 24.46 20.44 64.65 o -19 4 0 898.46 906.51 117.73 o -18 4 0 1987.63 2062.76 189.68 o -17 4 0 3036.73 3343.37 203.14 o -16 4 0 1059.60 816.95 172.99 o -15 4 0 4.03 -6.22 44.85 o -14 4 0 1436.26 1535.83 83.91 o -13 4 0 10342.18 9464.61 381.23 o -12 4 0 306.56 358.81 42.36 o -11 4 0 2595.72 2571.92 100.91 o -10 4 0 7752.62 7394.63 218.78 o -9 4 0 72.46 42.10 23.07 o -8 4 0 25.32 92.55 30.43 o -7 4 0 18676.18 18657.14 585.71 o -6 4 0 156.65 261.33 23.70 o -5 4 0 406.34 441.05 60.87 o -4 4 0 16786.65 16815.43 460.77 o -3 4 0 19.75 27.23 11.33 o -2 4 0 3564.30 4017.00 92.55 o -1 4 0 10370.39 11329.02 549.42 o 0 4 0 60106.60 64871.28 1581.77 o 1 4 0 7517.29 8202.73 185.38 o 2 4 0 2073.94 2430.26 78.49 o 3 4 0 399.78 436.25 40.05 o 4 4 0 2816.76 3197.90 83.87 o 5 4 0 5633.01 5269.23 116.93 o 6 4 0 8577.47 9086.54 352.40 o 7 4 0 9346.60 9200.69 218.91 o 8 4 0 459.41 501.41 43.25 o 9 4 0 16288.43 15707.83 423.98 o 10 4 0 50.88 38.44 11.71 o 11 4 0 5491.63 5023.41 165.91 o 12 4 0 234.28 291.89 94.51 o 13 4 0 9169.13 8816.45 1265.42 o 14 4 0 9.71 116.91 43.25 o 15 4 0 238.62 370.79 102.52 o 16 4 0 2933.48 2801.36 159.04 o 17 4 0 121.90 76.49 49.45 o 18 4 0 2049.86 2102.84 147.52 o 19 4 0 131.59 108.86 54.64 o 20 4 0 7.27 105.00 88.10 o -20 5 0 109.37 266.84 164.99 o -19 5 0 1080.66 965.85 107.58 o -18 5 0 1562.77 1759.27 164.99 o -17 5 0 662.89 609.73 83.84 o -16 5 0 1625.39 1702.11 119.82 o -15 5 0 4263.83 3956.24 196.03 o -14 5 0 1026.38 1266.00 92.90 o -13 5 0 1534.46 1543.31 139.36 o -12 5 0 1934.08 1893.08 83.38 o -11 5 0 6585.66 6590.49 228.35 o -10 5 0 196.85 297.32 168.19 o -9 5 0 1014.23 1011.85 53.84 o -8 5 0 3521.64 3999.69 124.80 o -7 5 0 14.83 45.00 23.70 o -6 5 0 15.92 39.76 32.04 o -5 5 0 1433.55 1234.01 96.11 o -4 5 0 1249.00 1260.35 37.33 o -3 5 0 272.67 247.40 41.65 o -2 5 0 4908.73 5453.57 135.69 o -1 5 0 856.79 958.12 25.98 o 0 5 0 76.59 113.93 9.06 o 1 5 0 547.66 499.15 30.43 o 2 5 0 5634.69 5831.87 132.73 o 3 5 0 558.74 658.46 81.69 o 4 5 0 459.56 391.47 60.87 o 5 5 0 352.76 330.29 15.38 o 6 5 0 88.05 22.84 27.23 o 7 5 0 205.81 198.22 18.37 o 8 5 0 13581.57 12624.99 355.56 o 9 5 0 1447.75 1443.68 58.08 o 10 5 0 6992.21 6460.01 191.11 o 11 5 0 10840.59 10200.11 386.03 o 12 5 0 2146.50 1962.72 86.52 o 13 5 0 2055.00 2393.12 152.17 o 14 5 0 647.15 670.70 124.94 o 15 5 0 44.65 49.74 43.25 o 16 5 0 78.68 240.32 92.90 o 17 5 0 372.39 543.69 84.66 o 18 5 0 371.35 371.62 102.52 o 19 5 0 146.19 65.91 72.24 o 20 5 0 217.48 247.58 108.92 o -19 6 0 419.43 370.30 91.86 o -18 6 0 94.87 116.74 55.42 o -17 6 0 14.21 65.80 59.27 o -16 6 0 1148.73 1123.66 280.32 o -15 6 0 30.16 131.99 134.55 o -14 6 0 8136.48 8541.61 304.97 o -13 6 0 10153.86 9560.99 335.82 o -12 6 0 732.68 708.03 75.28 o -11 6 0 6373.78 5921.09 229.87 o -10 6 0 2817.09 3144.14 134.09 o -9 6 0 3982.41 3960.99 197.02 o -8 6 0 851.93 750.47 65.67 o -7 6 0 10809.04 10511.02 506.17 o -6 6 0 5166.87 4723.45 180.07 o -5 6 0 407.65 591.59 94.51 o -4 6 0 1556.91 1384.57 42.33 o -3 6 0 2679.92 3138.16 86.19 o -2 6 0 2161.41 2483.81 116.93 o -1 6 0 6.46 23.14 10.01 o 0 6 0 11495.39 11850.72 244.62 o 1 6 0 223.33 175.32 11.33 o 2 6 0 4631.65 4594.12 116.93 o 3 6 0 7095.42 7549.12 221.05 o 4 6 0 34.84 34.88 10.01 o 5 6 0 600.12 925.80 43.25 o 6 6 0 10065.74 9423.05 687.17 o 7 6 0 47.84 102.96 19.37 o 8 6 0 294.48 343.27 32.04 o 9 6 0 2296.57 2046.31 78.50 o 10 6 0 9390.01 8970.56 288.50 o 11 6 0 2381.18 2706.40 261.09 o 12 6 0 991.20 1220.95 80.76 o 13 6 0 585.61 698.18 75.28 o 14 6 0 6471.29 6809.29 323.29 o 15 6 0 50.56 118.32 72.08 o 16 6 0 3956.96 4221.25 288.32 o 17 6 0 2973.98 3117.61 230.52 o 18 6 0 125.06 113.88 69.24 o 19 6 0 18.20 39.32 92.90 o 20 6 0 13.94 165.42 129.75 o -19 7 0 54.91 120.59 75.26 o -18 7 0 977.17 853.59 125.35 o -17 7 0 313.25 297.39 92.36 o -16 7 0 3080.51 3144.98 267.50 o -15 7 0 8.83 66.73 128.14 o -14 7 0 1788.73 1616.57 93.00 o -13 7 0 965.88 1042.44 74.75 o -12 7 0 380.74 431.30 39.49 o -11 7 0 703.89 844.69 73.90 o -10 7 0 147.17 236.90 78.49 o -9 7 0 75.73 74.75 49.66 o -8 7 0 10478.19 9772.96 362.82 o -7 7 0 511.05 400.78 54.46 o -6 7 0 18947.95 19880.88 606.22 o -5 7 0 10.03 76.61 10.66 o -4 7 0 2578.45 2408.91 83.93 o -3 7 0 26.51 50.40 36.84 o -2 7 0 1000.82 1211.62 37.33 o -1 7 0 2593.86 2592.13 57.73 o 0 7 0 287.36 355.60 16.88 o 1 7 0 3057.50 2877.26 61.04 o 2 7 0 4145.36 4314.16 280.32 o 3 7 0 1131.49 1136.74 39.21 o 4 7 0 2121.19 1669.77 116.93 o 5 7 0 4279.69 5026.96 139.86 o 6 7 0 15868.51 14751.65 397.95 o 7 7 0 2103.06 2023.63 64.65 o 8 7 0 1678.10 1598.47 61.53 o 9 7 0 33.11 53.34 19.74 o 10 7 0 6846.73 6563.72 355.60 o 11 7 0 11303.33 10769.92 385.38 o 12 7 0 523.12 774.50 150.57 o 13 7 0 1.46 300.29 90.06 o 14 7 0 2231.42 2668.89 169.15 o 15 7 0 2841.44 2660.70 179.92 o 16 7 0 0.00 -38.44 57.69 o 17 7 0 445.13 399.39 69.84 o 18 7 0 4.46 -76.89 76.89 o 19 7 0 258.34 363.65 82.80 o -19 8 0 662.03 356.15 95.78 o -18 8 0 234.67 232.72 176.20 o -17 8 0 311.29 266.31 81.69 o -16 8 0 2245.47 2270.39 185.81 o -15 8 0 1617.49 1634.43 91.40 o -14 8 0 821.99 843.22 67.17 o -13 8 0 2470.16 2111.17 137.75 o -12 8 0 84.34 93.20 33.38 o -11 8 0 7008.23 6768.55 261.73 o -10 8 0 135.23 96.13 80.09 o -9 8 0 8.17 -9.61 30.02 o -8 8 0 5775.29 5991.73 329.97 o -7 8 0 759.53 937.55 49.22 o -6 8 0 9596.05 9738.96 276.48 o -5 8 0 3898.65 3950.03 129.20 o -4 8 0 12922.56 12087.04 453.16 o -3 8 0 7.36 4.37 12.31 o -2 8 0 511.25 508.82 67.28 o -1 8 0 1035.27 908.39 57.66 o 0 8 0 477.70 565.78 57.66 o 1 8 0 439.41 411.72 18.12 o 2 8 0 17.21 25.63 10.66 o 3 8 0 236.59 377.83 25.63 o 4 8 0 8465.48 7505.27 301.14 o 5 8 0 10437.18 10119.85 322.41 o 6 8 0 6456.10 5329.39 174.60 o 7 8 0 249.88 227.00 52.86 o 8 8 0 120.53 148.03 22.92 o 9 8 0 3611.34 3584.90 126.23 o 10 8 0 4299.56 4014.16 147.19 o 11 8 0 8573.72 7680.01 510.97 o 12 8 0 44.56 35.17 47.38 o 13 8 0 9828.65 9908.37 882.59 o 14 8 0 33.06 111.78 131.35 o 15 8 0 33.84 65.24 49.22 o 16 8 0 9.95 0.68 65.67 o 17 8 0 3802.72 4028.68 595.87 o 18 8 0 29.83 78.76 83.29 o 19 8 0 664.46 722.27 100.63 o -18 9 0 34.41 -27.92 76.89 o -17 9 0 183.64 72.78 88.26 o -16 9 0 2.58 -5.61 62.58 o -15 9 0 1325.01 1550.46 217.85 o -14 9 0 1635.92 1543.99 190.61 o -13 9 0 461.38 506.55 91.30 o -12 9 0 6.78 83.29 40.75 o -11 9 0 5410.89 4830.31 220.11 o -10 9 0 0.14 136.52 43.78 o -9 9 0 16865.38 17078.26 546.98 o -8 9 0 30.00 49.98 25.63 o -7 9 0 836.80 766.29 116.93 o -6 9 0 7237.35 6771.24 285.43 o -5 9 0 14.22 16.02 24.61 o -4 9 0 3603.74 3587.89 121.58 o -3 9 0 19302.76 19973.53 679.16 o -2 9 0 518.58 465.74 83.29 o -1 9 0 643.29 746.17 51.26 o 0 9 0 204.78 218.78 19.16 o 1 9 0 3373.24 3441.69 270.70 o 2 9 0 2547.37 2436.33 62.02 o 3 9 0 13720.33 13487.38 394.07 o 4 9 0 9976.59 9037.22 394.04 o 5 9 0 6090.71 5064.96 289.93 o 6 9 0 6745.07 5854.87 155.38 o 7 9 0 3452.09 3393.23 336.38 o 8 9 0 8167.48 7875.40 235.59 o 9 9 0 1541.05 1429.42 69.79 o 10 9 0 113.96 88.41 19.74 o 11 9 0 5985.24 5603.55 536.60 o 12 9 0 17.38 65.35 89.70 o 13 9 0 88.14 163.38 52.10 o 14 9 0 449.08 553.24 140.96 o 15 9 0 185.80 87.30 55.70 o 16 9 0 545.07 619.59 82.36 o 17 9 0 1051.59 1097.69 117.77 o 18 9 0 356.43 193.54 99.31 o 19 9 0 169.79 238.61 152.17 o -18 10 0 963.97 1146.00 172.99 o -17 10 0 1118.53 1241.66 127.68 o -16 10 0 306.54 340.09 72.08 o -15 10 0 45.46 169.90 65.67 o -14 10 0 737.54 641.14 70.37 o -13 10 0 2227.29 2157.42 122.01 o -12 10 0 150.09 167.83 49.66 o -11 10 0 1421.27 1449.53 90.07 o -10 10 0 1964.28 2149.85 112.11 o -9 10 0 143.36 164.57 25.63 o -8 10 0 478.69 351.23 59.27 o -7 10 0 215.28 135.24 46.93 o -6 10 0 320.17 343.34 62.47 o -5 10 0 25.95 57.19 30.52 o -4 10 0 3529.49 3390.69 140.96 o -3 10 0 9458.53 9370.62 376.42 o -2 10 0 3974.35 4219.32 155.37 o -1 10 0 14335.12 15071.33 504.57 o 0 10 0 1061.60 1259.02 47.41 o 1 10 0 6317.41 6236.91 173.28 o 2 10 0 1089.25 1155.01 39.59 o 3 10 0 20386.83 19165.27 625.76 o 4 10 0 339.50 322.36 56.06 o 5 10 0 2765.62 3012.21 257.89 o 6 10 0 740.65 687.24 75.28 o 7 10 0 1018.31 1121.11 44.13 o 8 10 0 4.55 26.83 27.23 o 9 10 0 719.37 650.35 36.11 o 10 10 0 6412.08 6045.37 321.96 o 11 10 0 141.63 170.18 42.65 o 12 10 0 2448.44 2483.10 159.90 o 13 10 0 231.34 325.82 86.50 o 14 10 0 654.20 770.24 73.49 o 15 10 0 3340.56 3472.24 236.53 o 16 10 0 1802.24 1490.28 315.55 o 17 10 0 31.42 20.43 81.54 o 18 10 0 0.79 82.30 61.58 o -17 11 0 1027.78 1141.54 119.80 o -16 11 0 219.20 140.23 54.79 o -15 11 0 465.94 487.42 68.40 o -14 11 0 73.86 37.82 57.66 o -13 11 0 5.52 26.70 57.66 o -12 11 0 194.14 195.75 42.65 o -11 11 0 1605.23 1575.15 184.21 o -10 11 0 153.97 205.03 88.10 o -9 11 0 2581.18 2537.08 246.68 o -8 11 0 3990.03 4146.66 229.06 o -7 11 0 1354.12 1433.48 81.46 o -6 11 0 42.39 129.13 43.78 o -5 11 0 1295.19 1439.27 90.63 o -4 11 0 224.14 277.91 110.52 o -3 11 0 22316.00 21309.82 631.11 o -2 11 0 4735.52 4837.95 157.01 o -1 11 0 3538.36 3937.09 120.68 o 0 11 0 6.33 57.66 15.86 o 1 11 0 6843.43 6322.98 178.91 o 2 11 0 7615.12 7791.37 539.81 o 3 11 0 3.04 62.03 57.66 o 4 11 0 3252.15 3435.46 129.50 o 5 11 0 8309.26 8272.66 336.38 o 6 11 0 2098.88 2133.27 195.42 o 7 11 0 859.25 880.82 39.59 o 8 11 0 4654.57 4450.71 214.64 o 9 11 0 978.56 808.50 53.20 o 10 11 0 1453.58 1631.43 70.22 o 11 11 0 1033.30 1018.14 139.36 o 12 11 0 28.20 -21.36 34.38 o 13 11 0 103.93 257.41 47.75 o 14 11 0 1879.44 2028.49 134.09 o 15 11 0 6.96 27.74 46.09 o 16 11 0 416.48 403.20 104.12 o 17 11 0 1121.54 1209.55 203.43 o 18 11 0 17.20 27.26 68.40 o -17 12 0 382.63 346.37 84.66 o -16 12 0 587.38 463.66 75.85 o -15 12 0 585.94 570.78 80.76 o -14 12 0 903.29 776.20 235.46 o -13 12 0 538.71 491.25 58.64 o -12 12 0 1535.06 1400.77 97.62 o -11 12 0 1558.57 1627.77 354.00 o -10 12 0 729.91 768.30 77.02 o -9 12 0 25.56 19.30 45.14 o -8 12 0 6422.56 6379.25 281.76 o -7 12 0 6.34 36.87 99.31 o -6 12 0 8.94 13.11 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