#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/26/2202697.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202697_Fobs loop_ _publ_author_name 'Siero\'n, Les\/law' _publ_section_title ; catena-Poly[[aqua(diformato-\kO)copper(II)]-\m-1,4-diazabicyclo[2.2.2]octane-\k^2^N:N'] ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m803 _journal_page_last m805 _journal_volume 59 _journal_year 2003 _space_group_IT_number 59 _symmetry_space_group_name_Hall '-P 2ab 2a' _symmetry_space_group_name_H-M 'P m m n :2' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 6.8084 _cell_length_b 12.0705 _cell_length_c 6.4224 _exptl_crystal_F_000 294.00 _reflns_d_resolution_high 0.7571 _[local]_cod_data_source_file lh6095Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title lh6095 _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x, y+1/2, -z' 'x+1/2, -y, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x, -y-1/2, z' '-x-1/2, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13345.19 11520.13 30.27 o 4 0 0 2312.09 1999.07 18.68 o 6 0 0 1440.59 1474.69 20.75 o 8 0 0 741.31 747.89 10.62 o 1 1 0 2158.01 2242.30 9.80 o 3 1 0 11723.44 10824.43 38.56 o 5 1 0 2442.28 2336.92 24.06 o 7 1 0 649.10 573.77 8.00 o 0 2 0 7177.01 6754.01 16.41 o 2 2 0 139.01 111.77 1.66 o 4 2 0 147.16 134.26 2.04 o 6 2 0 345.55 364.41 5.17 o 8 2 0 167.77 180.20 3.15 o 1 3 0 29.32 47.61 0.86 o 3 3 0 745.61 665.05 7.83 o 5 3 0 125.44 128.72 2.15 o 7 3 0 232.01 223.78 3.47 o 0 4 0 2792.69 2794.15 15.17 o 2 4 0 1035.15 926.75 10.32 o 4 4 0 1507.80 1500.87 16.99 o 6 4 0 727.86 742.09 8.77 o 8 4 0 83.57 84.27 2.25 o 1 5 0 7399.12 7430.30 28.80 o 3 5 0 3976.42 4085.55 25.89 o 5 5 0 656.33 644.54 8.19 o 7 5 0 699.76 685.23 8.89 o 0 6 0 6921.15 7510.02 30.91 o 2 6 0 3316.04 3193.65 22.12 o 4 6 0 2572.38 2584.60 23.92 o 6 6 0 1041.00 1035.76 13.19 o 8 6 0 142.60 135.55 2.81 o 1 7 0 1684.75 1716.57 16.48 o 3 7 0 1961.76 2057.92 20.51 o 5 7 0 439.20 406.60 5.55 o 7 7 0 381.61 375.43 5.27 o 0 8 0 1749.69 1862.66 18.22 o 2 8 0 354.15 329.14 4.76 o 4 8 0 245.98 263.79 3.85 o 6 8 0 248.89 266.10 3.84 o 1 9 0 88.01 89.61 1.61 o 3 9 0 995.90 1002.61 13.10 o 5 9 0 417.26 430.48 6.12 o 7 9 0 184.84 187.12 3.17 o 0 10 0 2332.24 2363.79 23.66 o 2 10 0 522.09 535.94 7.49 o 4 10 0 133.34 140.61 2.43 o 6 10 0 174.82 170.34 3.03 o 1 11 0 342.01 341.33 4.94 o 3 11 0 1083.85 1058.68 13.08 o 5 11 0 386.69 368.93 5.54 o 0 12 0 1467.87 1448.82 21.25 o 2 12 0 464.64 445.75 6.59 o 4 12 0 250.50 249.50 3.97 o 1 13 0 451.38 434.93 6.30 o 3 13 0 636.61 620.06 8.42 o 5 13 0 182.63 173.05 3.13 o 0 14 0 442.38 413.53 6.11 o 2 14 0 206.58 200.52 3.43 o 4 14 0 300.72 311.12 4.91 o 1 15 0 158.12 156.59 2.94 o 3 15 0 158.17 158.15 3.01 o 0 0 1 1577.08 1512.48 8.28 o 1 0 1 1194.66 1164.39 8.56 o 2 0 1 12.11 15.75 0.56 o 3 0 1 4734.11 4536.30 24.55 o 4 0 1 4.54 3.49 0.53 o 5 0 1 1173.96 1114.97 15.52 o 6 0 1 81.58 96.39 1.88 o 7 0 1 517.50 464.42 6.84 o 8 0 1 67.08 77.91 2.04 o 0 1 1 8501.87 8284.66 19.94 o 1 1 1 25.61 19.51 0.51 o 2 1 1 905.82 853.44 9.24 o 3 1 1 1027.44 957.45 11.72 o 4 1 1 498.38 473.76 6.87 o 5 1 1 244.83 244.44 3.84 o 6 1 1 471.57 472.85 6.66 o 7 1 1 123.40 120.75 2.25 o 8 1 1 194.32 204.85 3.48 o 0 2 1 4297.61 4541.26 16.42 o 1 2 1 33.67 37.11 0.73 o 2 2 1 1551.00 1616.00 12.66 o 3 2 1 916.11 872.09 10.89 o 4 2 1 863.91 801.51 9.75 o 5 2 1 165.96 158.45 2.40 o 6 2 1 309.77 285.66 3.93 o 7 2 1 155.96 149.26 2.62 o 8 2 1 49.32 50.75 1.89 o 0 3 1 1069.36 993.63 8.68 o 1 3 1 4064.72 4251.00 18.88 o 2 3 1 6.98 6.98 0.47 o 3 3 1 951.54 906.97 11.37 o 4 3 1 100.24 90.98 1.64 o 5 3 1 70.46 81.55 1.51 o 6 3 1 143.55 137.25 2.25 o 7 3 1 177.75 169.02 2.79 o 8 3 1 30.17 30.52 1.53 o 0 4 1 1.51 2.70 0.38 o 1 4 1 346.05 303.27 4.01 o 2 4 1 163.30 164.73 2.32 o 3 4 1 1002.68 910.31 11.87 o 4 4 1 937.01 912.81 10.83 o 5 4 1 141.99 133.01 2.07 o 6 4 1 266.12 250.14 3.59 o 7 4 1 203.23 200.71 3.23 o 8 4 1 1.58 6.19 1.11 o 0 5 1 2801.77 2871.99 18.05 o 1 5 1 767.38 823.00 10.04 o 2 5 1 641.96 595.35 7.52 o 3 5 1 32.66 30.38 0.90 o 4 5 1 759.98 746.84 10.24 o 5 5 1 38.11 37.16 1.18 o 6 5 1 491.95 502.64 6.79 o 7 5 1 113.52 123.55 2.37 o 8 5 1 102.30 102.83 2.44 o 0 6 1 8.06 9.40 0.56 o 1 6 1 949.09 917.00 11.43 o 2 6 1 57.38 43.93 0.97 o 3 6 1 1594.96 1616.24 17.42 o 4 6 1 721.05 707.10 8.96 o 5 6 1 355.32 351.88 4.98 o 6 6 1 294.21 303.46 4.36 o 7 6 1 317.37 315.07 4.47 o 8 6 1 0.99 3.53 1.06 o 0 7 1 1971.63 2119.89 18.43 o 1 7 1 984.76 1051.50 13.18 o 2 7 1 478.69 472.12 6.62 o 3 7 1 497.77 529.62 6.73 o 4 7 1 389.71 380.47 5.25 o 5 7 1 47.78 47.71 1.41 o 6 7 1 284.27 299.33 4.26 o 7 7 1 160.77 166.22 2.81 o 8 7 1 81.20 84.28 2.29 o 0 8 1 1032.22 1027.16 13.87 o 1 8 1 212.90 204.92 3.03 o 2 8 1 386.12 400.23 5.28 o 3 8 1 685.31 687.54 9.06 o 4 8 1 309.79 315.66 4.44 o 5 8 1 177.61 181.24 2.88 o 6 8 1 147.09 140.86 2.48 o 7 8 1 132.00 137.24 2.66 o 0 9 1 937.10 960.60 14.39 o 1 9 1 123.21 136.67 2.25 o 2 9 1 182.85 181.26 2.75 o 3 9 1 316.60 293.79 4.22 o 4 9 1 99.11 102.67 1.90 o 5 9 1 69.92 71.94 1.75 o 6 9 1 108.73 110.26 2.30 o 7 9 1 38.78 44.55 1.75 o 0 10 1 400.40 378.00 5.18 o 1 10 1 85.71 90.12 1.75 o 2 10 1 52.31 57.23 1.44 o 3 10 1 413.30 428.00 6.05 o 4 10 1 12.18 14.19 1.05 o 5 10 1 127.57 128.75 2.38 o 6 10 1 27.45 26.29 1.41 o 0 11 1 546.93 594.69 8.18 o 1 11 1 37.53 39.86 1.26 o 2 11 1 121.28 126.04 2.22 o 3 11 1 220.23 204.17 3.32 o 4 11 1 95.41 100.87 2.10 o 5 11 1 85.60 89.79 2.14 o 6 11 1 105.11 114.04 2.55 o 0 12 1 289.45 307.60 4.53 o 1 12 1 172.74 175.04 2.94 o 2 12 1 107.62 112.41 2.11 o 3 12 1 359.92 359.42 5.47 o 4 12 1 104.94 112.42 2.30 o 5 12 1 102.79 103.05 2.40 o 0 13 1 516.64 515.61 7.32 o 1 13 1 144.23 159.55 2.79 o 2 13 1 205.93 208.57 3.32 o 3 13 1 111.18 112.95 2.35 o 4 13 1 209.41 210.29 3.55 o 5 13 1 15.16 13.31 1.29 o 0 14 1 30.65 31.12 1.46 o 1 14 1 203.32 209.23 3.48 o 2 14 1 23.91 23.92 1.31 o 3 14 1 257.92 253.15 4.01 o 4 14 1 90.18 93.68 2.37 o 0 15 1 133.96 129.84 2.62 o 1 15 1 96.21 92.92 2.26 o 2 15 1 36.56 33.67 1.60 o 0 0 2 218.15 225.16 3.32 o 1 0 2 1255.22 1281.57 11.43 o 2 0 2 706.54 706.42 9.57 o 3 0 2 1753.55 1641.69 16.57 o 4 0 2 1333.84 1267.72 16.48 o 5 0 2 279.14 265.28 4.04 o 6 0 2 430.94 426.21 6.35 o 7 0 2 297.00 297.09 4.41 o 8 0 2 22.86 25.42 1.41 o 0 1 2 3083.23 3262.02 17.44 o 1 1 2 2296.02 2350.30 15.59 o 2 1 2 840.13 767.51 10.12 o 3 1 2 552.01 518.45 7.75 o 4 1 2 941.58 884.09 11.43 o 5 1 2 77.03 87.60 1.72 o 6 1 2 464.68 457.69 6.77 o 7 1 2 190.47 187.62 3.23 o 8 1 2 72.70 71.14 2.12 o 0 2 2 982.56 1084.89 10.40 o 1 2 2 1414.60 1394.87 12.36 o 2 2 2 527.99 521.59 6.90 o 3 2 2 1077.81 1072.06 13.60 o 4 2 2 498.29 506.23 6.71 o 5 2 2 152.39 153.09 2.65 o 6 2 2 171.64 170.92 2.82 o 7 2 2 349.17 355.59 5.09 o 8 2 2 13.60 14.32 1.34 o 0 3 2 95.45 75.52 1.31 o 1 3 2 399.58 433.33 5.90 o 2 3 2 51.23 26.23 0.76 o 3 3 2 555.33 585.35 8.28 o 4 3 2 845.90 853.05 11.22 o 5 3 2 95.01 87.19 1.71 o 6 3 2 440.73 458.31 6.23 o 7 3 2 50.17 47.31 1.68 o 8 3 2 17.54 16.69 1.36 o 0 4 2 1676.21 1941.50 15.47 o 1 4 2 703.41 701.09 9.59 o 2 4 2 231.76 216.95 3.13 o 3 4 2 285.98 299.66 4.34 o 4 4 2 37.49 38.94 1.14 o 5 4 2 5.50 7.44 0.78 o 6 4 2 54.69 63.51 1.66 o 7 4 2 204.91 215.67 3.47 o 8 4 2 45.10 43.08 1.75 o 0 5 2 684.53 738.04 10.21 o 1 5 2 32.65 28.50 0.77 o 2 5 2 254.14 237.14 3.44 o 3 5 2 724.22 755.42 9.98 o 4 5 2 1089.32 1031.34 12.72 o 5 5 2 309.11 312.69 4.52 o 6 5 2 466.52 465.15 6.35 o 7 5 2 79.01 82.26 2.04 o 8 5 2 4.83 7.12 1.20 o 0 6 2 1723.61 1896.56 17.41 o 1 6 2 2156.95 2160.15 18.88 o 2 6 2 421.79 468.46 6.61 o 3 6 2 1269.20 1245.55 16.31 o 4 6 2 132.13 138.13 2.25 o 5 6 2 89.49 91.38 1.85 o 6 6 2 145.55 145.23 2.59 o 7 6 2 325.62 329.89 4.86 o 8 6 2 107.97 111.27 2.60 o 0 7 2 1550.56 1575.97 16.91 o 1 7 2 386.71 397.98 5.53 o 2 7 2 609.22 630.50 8.06 o 3 7 2 697.35 675.04 8.88 o 4 7 2 958.21 949.05 13.05 o 5 7 2 239.08 245.28 3.66 o 6 7 2 508.06 500.90 6.88 o 7 7 2 103.16 98.55 2.29 o 0 8 2 576.42 586.08 7.87 o 1 8 2 295.24 316.60 4.82 o 2 8 2 238.65 245.88 3.63 o 3 8 2 500.28 498.58 7.24 o 4 8 2 194.77 200.71 3.09 o 5 8 2 81.22 87.18 1.91 o 6 8 2 102.82 97.21 2.19 o 7 8 2 174.04 182.74 3.11 o 0 9 2 247.45 242.58 3.63 o 1 9 2 220.15 225.85 3.36 o 2 9 2 20.48 27.66 1.07 o 3 9 2 97.13 98.09 1.83 o 4 9 2 75.15 79.35 1.77 o 5 9 2 2.53 5.00 0.97 o 6 9 2 85.86 85.10 2.15 o 7 9 2 31.03 31.87 1.66 o 0 10 2 18.48 18.39 0.97 o 1 10 2 87.38 90.28 1.72 o 2 10 2 22.32 17.75 1.00 o 3 10 2 258.16 250.24 3.70 o 4 10 2 130.39 137.13 2.36 o 5 10 2 43.78 46.41 1.62 o 6 10 2 57.22 65.43 1.98 o 0 11 2 763.89 747.19 10.55 o 1 11 2 161.11 154.71 2.60 o 2 11 2 294.92 287.84 4.37 o 3 11 2 63.70 69.28 1.79 o 4 11 2 293.89 292.85 4.41 o 5 11 2 4.77 6.71 1.08 o 6 11 2 191.37 189.71 3.24 o 0 12 2 141.29 150.66 2.65 o 1 12 2 538.78 537.77 7.26 o 2 12 2 106.60 102.67 2.11 o 3 12 2 502.59 494.18 6.96 o 4 12 2 166.13 160.94 2.80 o 5 12 2 109.61 102.97 2.49 o 0 13 2 207.64 200.31 3.39 o 1 13 2 152.91 152.08 2.77 o 2 13 2 101.78 101.74 2.21 o 3 13 2 161.33 165.18 2.90 o 4 13 2 234.24 240.65 3.93 o 0 14 2 187.34 178.25 3.20 o 1 14 2 78.48 83.47 2.10 o 2 14 2 67.66 64.46 1.91 o 3 14 2 53.50 49.86 1.87 o 0 15 2 38.86 34.85 1.65 o 1 15 2 5.76 8.20 1.11 o 2 15 2 15.03 14.74 1.31 o 0 0 3 3540.69 3795.03 23.13 o 1 0 3 994.75 1117.39 13.01 o 2 0 3 1707.23 1657.94 16.89 o 3 0 3 17.61 14.78 0.82 o 4 0 3 2411.08 2287.18 23.99 o 5 0 3 53.68 55.34 1.52 o 6 0 3 940.92 918.47 13.08 o 7 0 3 2.50 5.15 1.16 o 8 0 3 53.21 55.24 1.98 o 0 1 3 327.04 333.97 4.95 o 1 1 3 4000.80 4112.51 24.89 o 2 1 3 11.67 13.77 0.69 o 3 1 3 2209.65 2206.00 21.41 o 4 1 3 175.93 172.20 2.83 o 5 1 3 239.07 230.77 3.73 o 6 1 3 16.85 18.04 1.27 o 7 1 3 517.98 499.54 7.14 o 8 1 3 12.62 15.17 1.51 o 0 2 3 2201.23 2361.55 18.66 o 1 2 3 0.72 1.07 0.52 o 2 2 3 938.42 857.06 12.35 o 3 2 3 130.92 134.57 2.20 o 4 2 3 1517.29 1474.34 19.56 o 5 2 3 44.32 44.63 1.41 o 6 2 3 706.67 725.86 9.60 o 7 2 3 0.21 4.27 1.08 o 8 2 3 59.68 52.10 2.06 o 0 3 3 707.48 801.34 11.16 o 1 3 3 977.10 951.89 12.50 o 2 3 3 303.61 313.93 4.45 o 3 3 3 1094.14 1149.73 15.75 o 4 3 3 82.96 77.12 1.62 o 5 3 3 166.03 162.60 2.81 o 6 3 3 21.96 24.08 1.30 o 7 3 3 316.80 331.20 5.13 o 8 3 3 4.16 6.08 1.21 o 0 4 3 1781.73 1989.09 18.11 o 1 4 3 374.06 426.66 6.15 o 2 4 3 488.23 429.03 5.80 o 3 4 3 123.16 139.81 2.30 o 4 4 3 612.29 605.18 8.06 o 5 4 3 10.62 11.99 0.97 o 6 4 3 385.50 395.31 5.88 o 7 4 3 19.28 22.56 1.43 o 8 4 3 65.35 66.17 2.14 o 0 5 3 34.01 41.64 1.06 o 1 5 3 1376.86 1332.17 15.84 o 2 5 3 11.86 12.20 0.81 o 3 5 3 1752.47 1735.45 20.20 o 4 5 3 23.63 31.46 1.19 o 5 5 3 379.98 378.54 5.30 o 6 5 3 12.31 19.68 1.24 o 7 5 3 306.19 300.91 4.47 o 0 6 3 3801.20 4010.81 28.11 o 1 6 3 138.43 141.75 2.20 o 2 6 3 1474.30 1516.14 18.28 o 3 6 3 75.83 76.78 1.60 o 4 6 3 1018.63 1033.55 14.04 o 5 6 3 51.42 52.86 1.58 o 6 6 3 570.92 554.16 7.98 o 7 6 3 2.50 7.04 1.14 o 0 7 3 28.38 35.16 1.12 o 1 7 3 1478.45 1508.57 18.42 o 2 7 3 61.50 61.67 1.42 o 3 7 3 1607.85 1597.50 20.63 o 4 7 3 39.52 43.63 1.43 o 5 7 3 406.45 420.90 5.85 o 6 7 3 12.55 20.06 1.30 o 7 7 3 351.30 358.28 5.21 o 0 8 3 983.52 934.27 12.29 o 1 8 3 1.02 2.13 0.70 o 2 8 3 401.93 416.29 6.14 o 3 8 3 47.76 45.41 1.42 o 4 8 3 550.29 558.11 7.87 o 5 8 3 28.75 30.32 1.36 o 6 8 3 331.75 330.10 4.71 o 7 8 3 0.39 2.25 1.13 o 0 9 3 523.16 502.92 6.76 o 1 9 3 346.26 367.99 5.43 o 2 9 3 173.55 177.36 2.80 o 3 9 3 305.13 305.01 4.46 o 4 9 3 4.20 3.72 0.93 o 5 9 3 26.45 27.03 1.39 o 6 9 3 6.16 6.44 1.14 o 0 10 3 306.99 307.73 4.61 o 1 10 3 1.40 0.74 0.81 o 2 10 3 155.91 156.83 2.51 o 3 10 3 107.73 104.57 2.09 o 4 10 3 398.59 396.51 5.52 o 5 10 3 95.66 96.24 2.25 o 6 10 3 215.24 214.37 3.51 o 0 11 3 9.28 10.98 1.03 o 1 11 3 765.53 741.51 10.05 o 2 11 3 4.90 5.48 0.94 o 3 11 3 492.77 490.93 6.86 o 4 11 3 32.74 34.29 1.58 o 5 11 3 72.61 75.72 2.12 o 0 12 3 664.89 677.11 9.12 o 1 12 3 71.78 68.03 1.89 o 2 12 3 403.31 380.95 5.78 o 3 12 3 12.59 11.08 1.22 o 4 12 3 554.22 529.32 7.78 o 0 13 3 1.47 4.47 1.06 o 1 13 3 357.44 342.10 5.13 o 2 13 3 3.29 4.53 1.06 o 3 13 3 337.93 341.81 5.42 o 4 13 3 0.24 0.00 1.19 o 0 14 3 216.61 210.93 3.56 o 1 14 3 36.29 40.74 1.68 o 2 14 3 69.48 70.11 2.09 o 0 0 4 1018.43 984.42 13.89 o 1 0 4 703.55 719.75 9.91 o 2 0 4 148.27 160.45 2.66 o 3 0 4 488.56 513.47 7.30 o 4 0 4 122.12 115.12 2.30 o 5 0 4 45.44 49.54 1.58 o 6 0 4 108.71 116.56 2.44 o 7 0 4 250.50 260.07 4.37 o 0 1 4 478.00 492.21 7.06 o 1 1 4 68.77 59.07 1.26 o 2 1 4 197.81 188.93 3.01 o 3 1 4 408.83 390.48 5.88 o 4 1 4 633.92 644.52 8.88 o 5 1 4 83.73 87.12 1.95 o 6 1 4 353.04 364.10 5.59 o 7 1 4 73.05 70.52 2.17 o 0 2 4 690.68 740.73 10.00 o 1 2 4 492.78 517.57 7.43 o 2 2 4 94.26 91.71 1.69 o 3 2 4 524.05 507.36 7.35 o 4 2 4 59.56 56.66 1.57 o 5 2 4 56.91 58.04 1.68 o 6 2 4 64.95 68.60 1.95 o 7 2 4 132.58 132.98 2.85 o 0 3 4 1031.04 1011.05 14.59 o 1 3 4 188.50 198.49 3.01 o 2 3 4 209.84 207.03 3.21 o 3 3 4 533.95 563.44 7.82 o 4 3 4 151.90 161.60 2.80 o 5 3 4 148.04 148.28 2.68 o 6 3 4 115.16 118.72 2.44 o 7 3 4 76.39 72.92 2.22 o 0 4 4 1446.06 1605.11 18.73 o 1 4 4 90.68 91.00 1.76 o 2 4 4 406.39 428.02 5.99 o 3 4 4 534.85 535.84 7.73 o 4 4 4 156.10 165.39 2.83 o 5 4 4 176.48 174.42 3.08 o 6 4 4 133.84 141.57 2.66 o 7 4 4 97.00 95.12 2.47 o 0 5 4 974.39 1056.41 15.62 o 1 5 4 112.69 111.77 1.99 o 2 5 4 208.62 212.42 3.42 o 3 5 4 551.76 549.70 8.01 o 4 5 4 92.06 93.97 1.95 o 5 5 4 196.80 202.66 3.35 o 6 5 4 127.35 134.38 2.62 o 7 5 4 73.85 77.48 2.32 o 0 6 4 507.84 496.44 7.11 o 1 6 4 135.72 131.65 2.22 o 2 6 4 39.93 46.97 1.35 o 3 6 4 551.60 558.00 7.55 o 4 6 4 3.12 5.40 0.93 o 5 6 4 246.06 254.95 4.15 o 6 6 4 25.91 28.35 1.51 o 7 6 4 148.73 149.09 3.03 o 0 7 4 663.90 700.08 9.71 o 1 7 4 5.58 6.05 0.81 o 2 7 4 241.93 238.08 3.63 o 3 7 4 138.77 124.11 2.25 o 4 7 4 215.73 219.41 3.43 o 5 7 4 41.28 44.20 1.62 o 6 7 4 161.66 162.25 2.96 o 0 8 4 456.61 454.95 6.68 o 1 8 4 344.07 341.83 5.12 o 2 8 4 78.18 85.68 1.82 o 3 8 4 285.68 296.80 4.61 o 4 8 4 22.48 27.62 1.32 o 5 8 4 41.75 38.62 1.65 o 6 8 4 36.48 37.54 1.75 o 0 9 4 153.57 151.99 2.65 o 1 9 4 194.69 204.31 3.31 o 2 9 4 84.19 76.97 1.83 o 3 9 4 379.63 373.76 5.58 o 4 9 4 223.01 215.42 3.63 o 5 9 4 131.47 134.48 2.67 o 6 9 4 113.56 112.41 2.66 o 0 10 4 430.99 428.88 6.12 o 1 10 4 184.76 178.67 3.12 o 2 10 4 165.77 161.47 2.83 o 3 10 4 91.55 94.41 2.17 o 4 10 4 129.13 124.45 2.53 o 5 10 4 2.72 5.09 1.11 o 0 11 4 82.61 90.65 2.04 o 1 11 4 41.90 46.42 1.59 o 2 11 4 47.20 46.81 1.62 o 3 11 4 80.09 77.78 2.05 o 4 11 4 165.72 167.05 2.95 o 0 12 4 25.01 24.64 1.44 o 1 12 4 135.16 130.72 2.53 o 2 12 4 1.25 1.05 0.90 o 3 12 4 162.48 165.65 3.03 o 4 12 4 13.12 12.63 1.36 o 0 13 4 284.31 294.44 4.79 o 1 13 4 20.75 20.65 1.47 o 2 13 4 104.43 103.71 2.42 o 3 13 4 44.95 46.22 1.89 o 0 14 4 140.50 125.44 2.75 o 0 0 5 1208.55 1241.42 17.85 o 1 0 5 911.80 961.45 13.05 o 2 0 5 659.65 654.63 9.68 o 3 0 5 740.28 747.94 10.84 o 4 0 5 290.60 274.69 4.33 o 5 0 5 99.62 110.82 2.34 o 6 0 5 167.79 156.14 2.93 o 7 0 5 177.17 171.63 3.34 o 0 1 5 835.86 820.80 11.92 o 1 1 5 301.05 285.56 4.46 o 2 1 5 287.29 300.31 4.42 o 3 1 5 415.69 394.43 5.66 o 4 1 5 384.02 386.34 5.66 o 5 1 5 182.94 180.00 3.18 o 6 1 5 228.91 231.99 3.99 o 7 1 5 63.94 64.00 2.26 o 0 2 5 217.61 210.36 3.28 o 1 2 5 123.24 131.71 2.21 o 2 2 5 43.91 47.89 1.41 o 3 2 5 380.04 359.42 5.46 o 4 2 5 8.84 12.42 1.12 o 5 2 5 78.32 83.17 2.05 o 6 2 5 17.19 18.66 1.41 o 7 2 5 118.70 118.88 2.89 o 0 3 5 717.82 748.19 10.10 o 1 3 5 0.85 2.57 0.74 o 2 3 5 115.68 119.57 2.15 o 3 3 5 67.09 61.63 1.66 o 4 3 5 91.86 94.51 2.09 o 5 3 5 32.74 35.61 1.54 o 6 3 5 129.84 131.80 2.74 o 7 3 5 8.98 11.94 1.47 o 0 4 5 390.20 388.35 5.67 o 1 4 5 128.04 132.26 2.29 o 2 4 5 123.85 137.37 2.40 o 3 4 5 749.17 749.39 10.02 o 4 4 5 35.78 41.37 1.51 o 5 4 5 286.67 289.08 4.87 o 6 4 5 31.71 34.48 1.66 o 0 5 5 1724.34 1750.86 22.43 o 1 5 5 268.72 264.83 4.04 o 2 5 5 395.99 413.10 6.14 o 3 5 5 360.39 354.45 5.31 o 4 5 5 104.51 111.25 2.26 o 5 5 5 170.58 168.25 3.05 o 6 5 5 130.89 127.98 2.78 o 0 6 5 480.32 472.40 7.09 o 1 6 5 126.46 122.93 2.25 o 2 6 5 266.85 250.10 3.97 o 3 6 5 619.51 602.24 8.56 o 4 6 5 145.21 137.14 2.65 o 5 6 5 202.89 200.15 3.50 o 6 6 5 81.13 81.17 2.33 o 0 7 5 580.32 589.92 8.05 o 1 7 5 115.90 114.06 2.11 o 2 7 5 93.86 97.94 2.05 o 3 7 5 122.01 129.25 2.45 o 4 7 5 51.26 52.38 1.75 o 5 7 5 48.55 48.56 1.80 o 6 7 5 73.43 78.96 2.29 o 0 8 5 71.58 81.64 1.88 o 1 8 5 70.02 73.61 1.81 o 2 8 5 37.18 38.88 1.45 o 3 8 5 224.12 226.62 3.80 o 4 8 5 39.26 38.94 1.61 o 5 8 5 46.68 44.70 1.82 o 0 9 5 266.62 265.97 4.17 o 1 9 5 46.85 49.35 1.62 o 2 9 5 96.43 94.59 2.13 o 3 9 5 58.21 64.45 1.94 o 4 9 5 189.54 190.24 3.21 o 5 9 5 19.40 21.57 1.51 o 0 10 5 116.53 117.90 2.38 o 1 10 5 260.66 254.52 4.24 o 2 10 5 50.76 54.07 1.79 o 3 10 5 241.43 224.58 3.78 o 4 10 5 27.89 27.73 1.64 o 0 11 5 227.65 214.04 3.59 o 1 11 5 30.88 29.92 1.51 o 2 11 5 91.85 91.06 2.33 o 3 11 5 78.81 76.42 2.22 o 0 12 5 148.41 150.79 2.86 o 1 12 5 83.46 79.20 2.19 o 2 12 5 52.53 50.09 1.87 o 0 0 6 522.40 553.86 7.87 o 1 0 6 9.34 9.27 1.00 o 2 0 6 221.16 228.31 3.78 o 3 0 6 109.21 102.39 2.20 o 4 0 6 311.94 321.73 5.36 o 5 0 6 148.88 146.82 2.89 o 6 0 6 215.96 219.63 3.89 o 0 1 6 90.92 91.84 1.95 o 1 1 6 421.70 431.40 6.06 o 2 1 6 19.93 24.21 1.29 o 3 1 6 489.55 496.56 7.48 o 4 1 6 35.38 39.14 1.68 o 5 1 6 109.61 105.88 2.57 o 6 1 6 7.24 8.92 1.42 o 0 2 6 918.40 903.00 12.26 o 1 2 6 237.15 242.27 3.97 o 2 2 6 377.16 367.61 5.47 o 3 2 6 47.57 55.80 1.77 o 4 2 6 343.19 340.78 5.46 o 5 2 6 0.10 1.75 1.07 o 6 2 6 224.85 220.47 4.07 o 0 3 6 153.64 159.88 2.78 o 1 3 6 475.72 452.84 6.74 o 2 3 6 120.34 111.53 2.24 o 3 3 6 660.80 628.47 9.19 o 4 3 6 134.51 125.32 2.57 o 5 3 6 183.33 180.99 3.34 o 6 3 6 49.17 49.56 2.10 o 0 4 6 875.39 845.29 12.10 o 1 4 6 25.95 25.70 1.28 o 2 4 6 304.41 299.40 4.61 o 3 4 6 22.92 27.56 1.43 o 4 4 6 231.65 223.90 4.02 o 5 4 6 1.36 2.12 1.11 o 0 5 6 3.03 5.17 0.97 o 1 5 6 217.74 224.07 3.68 o 2 5 6 18.42 22.58 1.31 o 3 5 6 426.67 416.89 6.24 o 4 5 6 6.82 9.30 1.16 o 5 5 6 126.63 121.01 2.72 o 0 6 6 510.29 499.76 7.43 o 1 6 6 22.82 22.43 1.26 o 2 6 6 181.50 186.26 3.24 o 3 6 6 2.07 0.00 1.08 o 4 6 6 195.09 196.86 3.56 o 5 6 6 4.43 5.17 1.18 o 0 7 6 4.47 9.46 1.15 o 1 7 6 293.10 306.67 5.06 o 2 7 6 0.60 0.62 1.01 o 3 7 6 343.02 334.06 5.27 o 4 7 6 6.34 8.96 1.27 o 0 8 6 388.52 367.02 5.85 o 1 8 6 61.04 55.86 1.85 o 2 8 6 180.56 175.63 3.03 o 3 8 6 15.33 14.00 1.36 o 4 8 6 240.56 237.58 4.14 o 0 9 6 1.14 2.90 1.03 o 1 9 6 258.45 255.97 4.27 o 2 9 6 8.48 6.14 1.16 o 3 9 6 244.74 241.13 4.06 o 0 10 6 247.98 225.46 3.87 o 1 10 6 41.06 42.99 1.75 o 2 10 6 106.28 101.85 2.49 o 0 11 6 10.59 11.35 1.37 o 1 11 6 122.34 112.42 2.64 o 0 0 7 19.07 21.50 1.35 o 1 0 7 32.30 32.74 1.46 o 2 0 7 5.87 6.96 1.08 o 3 0 7 85.11 84.54 2.27 o 4 0 7 73.87 73.91 2.25 o 5 0 7 21.49 25.78 1.62 o 0 1 7 142.17 146.31 2.71 o 1 1 7 93.32 90.80 2.18 o 2 1 7 48.79 52.10 1.77 o 3 1 7 47.04 47.74 1.80 o 4 1 7 69.80 72.88 2.25 o 5 1 7 0.93 3.24 1.18 o 0 2 7 89.13 99.03 2.20 o 1 2 7 165.26 161.23 2.94 o 2 2 7 38.71 38.77 1.60 o 3 2 7 168.49 162.80 3.06 o 4 2 7 114.73 117.92 2.74 o 0 3 7 169.28 162.48 2.87 o 1 3 7 90.42 90.47 2.19 o 2 3 7 95.49 91.33 2.21 o 3 3 7 113.62 112.26 2.59 o 4 3 7 147.25 140.84 2.94 o 0 4 7 120.92 118.28 2.45 o 1 4 7 126.99 125.57 2.55 o 2 4 7 34.13 30.46 1.54 o 3 4 7 69.91 71.06 2.13 o 4 4 7 57.55 60.79 2.13 o 0 5 7 22.31 23.23 1.39 o 1 5 7 39.15 40.68 1.68 o 2 5 7 20.84 21.10 1.41 o 3 5 7 64.32 65.68 2.10 o 4 5 7 108.05 105.92 2.64 o 0 6 7 65.29 61.21 1.95 o 1 6 7 120.39 120.14 2.59 o 2 6 7 15.32 19.17 1.36 o 3 6 7 57.91 60.13 2.12 o 0 7 7 74.68 66.89 2.10 o 1 7 7 46.97 51.02 1.95 o 2 7 7 56.33 53.41 1.98 o 3 7 7 37.34 37.24 1.81 o 0 8 7 18.82 18.28 1.43 o 1 8 7 96.37 91.24 2.40 o 2 8 7 10.08 9.30 1.32 o 0 9 7 72.40 62.12 2.18 o 0 0 8 58.88 52.31 1.97 o 1 0 8 57.04 56.09 2.03 o 2 0 8 51.33 48.42 1.95 o 0 1 8 194.67 191.43 3.49 o 1 1 8 79.01 83.37 2.35 o 2 1 8 50.03 50.50 1.95 o 0 2 8 20.25 19.13 1.51 o 1 2 8 77.98 77.69 2.29 o 2 2 8 32.51 34.97 1.73 o 0 3 8 196.78 196.03 3.44 o 1 3 8 55.57 54.01 1.98 o 2 3 8 69.18 67.22 2.24 o 0 4 8 0.35 1.05 1.16 o 1 4 8 106.63 105.85 2.60 o 0 5 8 125.35 116.05 2.74 o 1 5 8 96.18 95.34 2.56 o