#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:02:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180947 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/27/2202717.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202717_Fobs loop_ _publ_author_name 'Bolte, Michael' 'Brusko, Vasiliy' 'B\"ohmer, Volker' _publ_section_title ; A new pseudopolymorph of 5,11,17,23,29,35,41,47-octabromo-49,50,51,52,53,54,55,56-octamethoxycalix[8]arene ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1691 _journal_page_last o1693 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.287 _cell_angle_gamma 90.000 _cell_length_a 9.0636 _cell_length_b 26.2897 _cell_length_c 15.1205 _exptl_crystal_F_000 1728.00 _reflns_d_resolution_high 0.8286 _cod_data_source_file lh6121Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' boeh9 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 490.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 41577.60 45463.06 2464.73 o 4 0 0 10327.50 11634.12 619.16 o 6 0 0 23990.00 26911.96 248.87 o 8 0 0 810.70 943.68 64.80 o 10 0 0 71.78 140.95 61.84 o 1 1 0 3086.80 3138.66 156.53 o 2 1 0 19358.20 21924.94 1091.04 o 3 1 0 25339.54 27597.64 1232.36 o 4 1 0 93.95 142.44 71.59 o 5 1 0 1715.22 1808.68 84.05 o 6 1 0 503.23 478.81 52.00 o 7 1 0 716.03 895.39 52.83 o 8 1 0 249.50 350.29 47.37 o 9 1 0 22.20 70.49 48.36 o 10 1 0 234.36 288.35 41.41 o 1 2 0 2390.69 3362.36 133.15 o 2 2 0 11015.37 13234.79 575.25 o 3 2 0 10430.21 10702.18 408.07 o 4 2 0 875.14 982.51 68.02 o 5 2 0 690.85 547.67 57.30 o 6 2 0 5296.89 5719.42 298.80 o 7 2 0 2018.69 2282.51 117.78 o 8 2 0 180.83 189.67 53.23 o 9 2 0 162.13 222.45 44.73 o 10 2 0 833.14 661.46 44.05 o 1 3 0 10341.91 11430.61 246.01 o 2 3 0 7682.87 8411.32 268.25 o 3 3 0 2185.20 2404.30 96.18 o 4 3 0 541.66 727.04 66.65 o 5 3 0 27229.35 28835.81 1439.13 o 6 3 0 835.69 989.37 64.71 o 7 3 0 840.00 900.99 59.82 o 8 3 0 11.25 3.18 46.46 o 9 3 0 0.01 -18.75 47.93 o 10 3 0 6.57 44.65 44.44 o 0 4 0 21160.20 25707.83 276.08 o 1 4 0 9846.99 10822.57 340.81 o 2 4 0 11563.24 11733.48 514.21 o 3 4 0 1.29 49.86 77.96 o 4 4 0 531.76 470.35 65.03 o 5 4 0 192.23 164.22 63.88 o 6 4 0 7386.79 7084.32 297.74 o 7 4 0 435.03 466.03 60.76 o 8 4 0 4460.77 4845.73 170.13 o 9 4 0 143.00 147.41 46.77 o 10 4 0 38.11 86.39 47.81 o 1 5 0 32427.72 35341.80 1447.69 o 2 5 0 30850.41 32734.70 1180.02 o 3 5 0 111.34 98.91 60.06 o 4 5 0 1450.80 1328.27 76.75 o 5 5 0 1936.41 1907.83 93.20 o 6 5 0 8.53 1.27 57.89 o 7 5 0 1814.78 1840.31 91.05 o 8 5 0 152.22 156.79 55.11 o 9 5 0 24.78 13.14 49.12 o 10 5 0 0.03 81.10 45.21 o 0 6 0 1734.29 2027.58 240.05 o 1 6 0 57559.52 56762.31 2117.73 o 2 6 0 1380.59 1519.67 69.97 o 3 6 0 2183.54 2658.85 108.60 o 4 6 0 4706.50 4502.96 236.33 o 5 6 0 5198.91 5108.02 245.60 o 6 6 0 523.43 442.76 62.22 o 7 6 0 158.81 210.17 65.96 o 8 6 0 152.64 158.49 50.80 o 9 6 0 434.02 355.38 52.35 o 10 6 0 639.93 632.25 46.73 o 1 7 0 13852.71 14158.84 469.35 o 2 7 0 2899.35 2822.82 82.70 o 3 7 0 17550.17 17460.61 660.54 o 4 7 0 129.89 157.46 59.86 o 5 7 0 4668.07 4802.51 306.22 o 6 7 0 2057.08 2015.42 103.17 o 7 7 0 447.69 509.61 53.09 o 8 7 0 318.97 292.64 52.28 o 9 7 0 55.23 131.08 48.15 o 10 7 0 158.68 191.76 44.96 o 0 8 0 89425.11 96567.81 4658.79 o 1 8 0 2773.45 2616.62 150.71 o 2 8 0 18464.71 19095.63 490.56 o 3 8 0 10.39 77.64 70.12 o 4 8 0 10298.17 11378.50 424.38 o 5 8 0 1262.88 1333.68 63.42 o 6 8 0 2889.99 2846.50 147.40 o 7 8 0 345.00 400.79 58.98 o 8 8 0 420.13 333.45 56.44 o 9 8 0 10.15 -47.85 47.85 o 10 8 0 91.92 176.89 48.22 o 1 9 0 5057.75 5266.23 268.90 o 2 9 0 286.45 406.72 74.81 o 3 9 0 8327.40 8532.79 222.83 o 4 9 0 2030.56 2070.70 98.60 o 5 9 0 1295.28 1448.58 77.40 o 6 9 0 2657.63 2786.03 157.49 o 7 9 0 17.51 33.45 57.66 o 8 9 0 0.62 26.46 50.94 o 9 9 0 108.78 133.92 51.44 o 10 9 0 110.22 151.58 44.79 o 0 10 0 6080.85 6168.01 937.57 o 1 10 0 2360.82 2326.63 254.61 o 2 10 0 3034.16 2914.21 123.58 o 3 10 0 4262.75 4268.88 77.06 o 4 10 0 2751.82 2973.39 89.64 o 5 10 0 841.95 879.04 55.72 o 6 10 0 788.11 755.24 68.98 o 7 10 0 3085.78 3259.55 168.53 o 8 10 0 172.27 214.82 52.67 o 9 10 0 175.69 187.94 50.60 o 10 10 0 517.81 414.58 41.90 o 1 11 0 475.66 571.39 111.54 o 2 11 0 13894.05 13594.31 616.01 o 3 11 0 35.24 80.46 52.70 o 4 11 0 1970.47 2008.54 72.38 o 5 11 0 6035.34 6020.94 166.55 o 6 11 0 26.31 37.88 49.61 o 7 11 0 1511.69 1593.90 99.32 o 8 11 0 285.03 325.47 52.14 o 9 11 0 0.84 74.37 41.58 o 10 11 0 20.15 42.72 43.54 o 0 12 0 18266.96 23002.27 788.22 o 1 12 0 4305.98 3939.66 185.20 o 2 12 0 3296.94 3300.51 216.18 o 3 12 0 1580.46 1728.66 61.66 o 4 12 0 2003.56 2130.98 70.96 o 5 12 0 3980.87 3814.11 116.01 o 6 12 0 6.04 93.81 56.34 o 7 12 0 632.81 573.36 48.74 o 8 12 0 1003.58 1026.29 53.28 o 9 12 0 22.88 150.42 53.02 o 10 12 0 105.74 141.83 42.61 o 1 13 0 1660.36 1611.16 108.79 o 2 13 0 14481.24 15874.11 589.98 o 3 13 0 35.01 17.11 53.39 o 4 13 0 3705.61 3600.33 104.19 o 5 13 0 3981.26 3921.42 135.18 o 6 13 0 590.21 584.92 51.26 o 7 13 0 750.14 743.40 59.50 o 8 13 0 125.37 176.26 50.64 o 9 13 0 2.89 45.75 40.81 o 0 14 0 8049.68 9909.92 246.88 o 1 14 0 19111.65 18724.57 936.05 o 2 14 0 1047.74 1005.77 70.70 o 3 14 0 1365.55 1469.19 51.04 o 4 14 0 1250.35 1103.04 50.71 o 5 14 0 5398.25 5205.17 235.59 o 6 14 0 1042.70 1013.81 50.81 o 7 14 0 157.11 97.99 59.23 o 8 14 0 355.50 359.28 51.55 o 9 14 0 95.24 113.22 42.51 o 1 15 0 907.96 959.49 81.37 o 2 15 0 21.07 -20.14 58.31 o 3 15 0 904.46 927.67 45.00 o 4 15 0 3638.36 3764.38 140.24 o 5 15 0 4.87 4.75 44.43 o 6 15 0 309.29 338.90 41.98 o 7 15 0 331.31 322.42 45.24 o 8 15 0 352.04 237.44 49.88 o 9 15 0 27.09 86.24 41.32 o 0 16 0 14254.66 15661.44 910.69 o 1 16 0 208.20 243.41 57.88 o 2 16 0 2935.72 3164.18 121.77 o 3 16 0 1000.72 1081.94 49.85 o 4 16 0 3119.25 3155.28 138.93 o 5 16 0 1888.37 1931.74 92.83 o 6 16 0 44.67 35.54 46.27 o 7 16 0 191.74 208.77 42.66 o 8 16 0 39.39 60.93 43.98 o 9 16 0 5.40 13.49 40.56 o 1 17 0 4786.99 4968.80 163.20 o 2 17 0 346.93 343.13 46.13 o 3 17 0 7794.33 7814.32 283.21 o 4 17 0 3096.62 2794.02 112.13 o 5 17 0 3487.50 3192.95 195.85 o 6 17 0 462.58 468.53 42.25 o 7 17 0 50.75 33.99 43.45 o 8 17 0 15.53 7.10 47.27 o 9 17 0 9.30 16.92 41.88 o 0 18 0 7196.02 7064.69 440.43 o 1 18 0 66.90 71.63 52.88 o 2 18 0 1778.23 1821.02 63.01 o 3 18 0 1084.25 1090.76 47.24 o 4 18 0 3.29 -4.65 40.70 o 5 18 0 7.08 70.73 47.26 o 6 18 0 146.89 173.16 49.45 o 7 18 0 561.19 541.75 44.54 o 8 18 0 66.82 69.24 42.24 o 1 19 0 679.54 768.12 51.54 o 2 19 0 3654.16 3712.54 181.96 o 3 19 0 308.92 370.80 43.21 o 4 19 0 547.53 581.08 52.45 o 5 19 0 63.01 98.82 43.25 o 6 19 0 480.61 459.59 45.19 o 7 19 0 403.90 380.01 37.82 o 8 19 0 298.80 176.32 47.25 o 0 20 0 835.87 816.87 89.64 o 1 20 0 270.58 351.27 49.52 o 2 20 0 458.79 521.85 52.89 o 3 20 0 450.85 457.25 46.55 o 4 20 0 3972.11 3556.37 188.24 o 5 20 0 864.71 880.01 46.19 o 6 20 0 7.03 27.00 40.26 o 7 20 0 6.52 18.48 40.49 o 8 20 0 214.97 211.39 43.57 o 1 21 0 0.61 40.60 43.20 o 2 21 0 3017.53 3039.24 131.88 o 3 21 0 558.15 508.46 43.60 o 4 21 0 436.93 415.66 44.51 o 5 21 0 1618.61 1548.06 97.24 o 6 21 0 110.93 100.13 35.61 o 7 21 0 426.48 300.19 35.64 o 8 21 0 141.15 56.07 41.22 o 0 22 0 192.94 250.81 54.32 o 1 22 0 1781.59 1749.09 54.05 o 2 22 0 230.63 251.35 55.45 o 3 22 0 91.23 174.01 38.87 o 4 22 0 113.55 124.45 40.04 o 5 22 0 1015.54 919.75 58.21 o 6 22 0 295.47 291.73 40.77 o 7 22 0 106.17 99.57 38.99 o 1 23 0 360.57 352.52 44.85 o 2 23 0 205.58 215.17 40.62 o 3 23 0 185.20 228.96 42.26 o 4 23 0 212.66 204.97 41.88 o 5 23 0 6.48 -4.71 36.42 o 6 23 0 5.08 33.11 32.08 o 7 23 0 9.90 44.13 35.05 o 0 24 0 664.05 664.53 73.52 o 1 24 0 1.44 7.29 44.33 o 2 24 0 166.08 161.93 40.78 o 3 24 0 1.57 14.44 37.66 o 4 24 0 7.94 -40.24 40.24 o 5 24 0 33.55 38.42 34.68 o 6 24 0 15.77 31.16 38.45 o 7 24 0 93.24 64.20 41.78 o 1 25 0 2811.45 2720.44 91.05 o 2 25 0 2.79 -8.98 37.25 o 3 25 0 4696.00 4213.09 187.24 o 4 25 0 23.04 26.26 34.45 o 5 25 0 370.94 342.49 38.04 o 6 25 0 188.43 154.35 38.51 o 0 26 0 595.33 625.09 61.42 o 1 26 0 314.58 337.82 46.82 o 2 26 0 261.50 236.17 36.36 o 3 26 0 528.53 468.89 40.31 o 4 26 0 150.36 167.92 40.29 o 5 26 0 91.28 77.42 34.81 o 6 26 0 15.51 5.81 33.65 o 1 27 0 201.55 291.35 42.62 o 2 27 0 350.87 373.53 34.32 o 3 27 0 213.20 120.28 42.03 o 4 27 0 3.30 31.11 41.12 o 5 27 0 123.51 129.22 38.22 o 0 28 0 0.93 38.96 46.18 o 1 28 0 4.42 13.01 39.69 o 2 28 0 216.16 222.67 38.68 o 3 28 0 97.88 92.04 37.29 o 4 28 0 1005.23 925.36 86.28 o 5 28 0 1.43 46.05 43.91 o 1 29 0 0.11 2.97 40.93 o 2 29 0 131.14 71.25 32.94 o 3 29 0 119.48 70.12 37.76 o 4 29 0 24.76 72.88 32.27 o 0 30 0 75.51 30.09 45.03 o 1 30 0 254.47 214.57 38.03 o 2 30 0 107.11 132.24 31.84 o 3 30 0 15.49 8.65 35.89 o 1 31 0 139.51 136.74 37.33 o 2 31 0 458.23 350.85 39.52 o -9 0 1 117.39 154.33 59.36 o -7 0 1 196.83 137.67 84.90 o -5 0 1 1402.57 1490.85 137.62 o -3 0 1 35.64 117.23 89.78 o -1 0 1 9073.30 9489.26 168.36 o 1 0 1 5005.78 4579.16 152.93 o 3 0 1 2782.20 3129.12 154.64 o 5 0 1 10110.33 11273.81 261.26 o 7 0 1 1165.85 1133.79 71.43 o 9 0 1 24.64 62.75 65.61 o -10 1 1 3.81 11.91 42.52 o -9 1 1 772.76 953.32 46.59 o -8 1 1 224.67 291.15 53.83 o -7 1 1 848.99 866.00 63.78 o -6 1 1 180.01 268.88 59.08 o -5 1 1 1882.58 2405.50 120.04 o -4 1 1 2861.23 2849.88 115.24 o -3 1 1 12779.84 13442.06 561.17 o -2 1 1 13160.71 12365.46 242.46 o -1 1 1 1851.79 1813.89 110.16 o 1 1 1 820.13 903.27 100.83 o 2 1 1 27772.11 28377.53 369.12 o 3 1 1 117.68 97.30 67.43 o 4 1 1 34139.56 38159.91 1758.34 o 5 1 1 3686.83 3661.68 207.53 o 6 1 1 633.71 615.73 57.97 o 7 1 1 1103.49 1303.49 56.09 o 8 1 1 90.05 125.64 48.30 o 9 1 1 5.70 -18.21 43.52 o 10 1 1 3.90 45.18 37.82 o -10 2 1 0.69 -5.85 43.00 o -9 2 1 95.04 83.72 43.65 o -8 2 1 79.90 90.14 50.38 o -7 2 1 24.35 150.58 54.88 o -6 2 1 77.52 159.35 54.21 o -5 2 1 1346.25 1623.00 77.89 o -4 2 1 5049.06 5469.29 270.78 o -3 2 1 1310.05 1221.06 70.36 o -2 2 1 766.56 876.71 80.75 o -1 2 1 4535.40 4237.67 96.55 o 0 2 1 8893.40 8896.01 202.85 o 1 2 1 1786.30 1827.79 87.91 o 2 2 1 2769.55 2445.08 70.20 o 3 2 1 5165.59 5437.41 151.03 o 4 2 1 2242.11 2520.81 111.07 o 5 2 1 9443.98 10242.65 485.25 o 6 2 1 643.23 639.98 62.07 o 7 2 1 225.52 201.45 59.71 o 8 2 1 407.04 494.37 52.52 o 9 2 1 406.13 434.99 40.67 o 10 2 1 0.75 -9.60 41.67 o -10 3 1 23.63 7.59 49.18 o -9 3 1 307.20 351.41 57.17 o -8 3 1 557.85 616.87 53.60 o -7 3 1 2402.56 2478.47 110.02 o -6 3 1 5785.95 5793.22 298.92 o -5 3 1 968.17 1189.85 58.61 o -4 3 1 4329.46 4519.71 287.41 o -3 3 1 15378.04 14374.39 719.78 o -2 3 1 6275.78 6963.65 176.06 o -1 3 1 14896.92 14869.73 289.07 o 0 3 1 208.18 155.58 78.15 o 1 3 1 896.66 612.97 76.10 o 2 3 1 6691.65 7068.84 103.44 o 3 3 1 19097.67 19526.25 557.85 o 4 3 1 455.90 516.24 68.16 o 5 3 1 2255.64 2247.61 118.50 o 6 3 1 5529.55 5641.42 281.54 o 7 3 1 950.62 957.15 54.44 o 8 3 1 1628.04 1574.35 63.42 o 9 3 1 158.31 148.11 47.43 o 10 3 1 29.52 39.39 43.29 o -10 4 1 134.83 134.32 47.72 o -9 4 1 541.44 639.95 51.27 o -8 4 1 12.93 10.53 53.30 o -7 4 1 4955.04 4793.73 245.04 o -6 4 1 156.32 165.33 55.96 o -5 4 1 1535.09 1578.18 81.96 o -4 4 1 388.71 313.59 65.56 o -3 4 1 25825.19 26310.67 1403.92 o -2 4 1 9182.86 9367.11 240.49 o -1 4 1 62603.11 60598.63 1009.12 o 0 4 1 2698.99 2680.05 89.04 o 1 4 1 31567.44 33732.63 370.73 o 2 4 1 903.90 1071.96 65.32 o 3 4 1 4013.06 4318.02 93.14 o 4 4 1 3174.89 3207.11 151.53 o 5 4 1 200.99 257.63 62.13 o 6 4 1 470.44 479.67 55.44 o 7 4 1 2611.06 2914.30 146.73 o 8 4 1 30.74 -11.60 48.71 o 9 4 1 1430.53 1725.54 71.45 o 10 4 1 138.14 181.74 43.23 o -10 5 1 406.28 542.74 54.48 o -9 5 1 9.23 65.83 47.01 o -8 5 1 203.00 226.96 55.51 o -7 5 1 2757.99 2660.68 98.04 o -6 5 1 2196.44 2205.39 120.89 o -5 5 1 1911.89 2077.40 115.81 o -4 5 1 11764.69 12555.32 654.95 o -3 5 1 6833.48 7455.44 262.88 o -2 5 1 20417.21 21296.57 515.52 o -1 5 1 71668.10 68068.23 2031.93 o 0 5 1 12058.88 13855.03 284.16 o 1 5 1 5163.99 5127.15 95.15 o 2 5 1 1288.19 1309.44 61.15 o 3 5 1 19463.27 19691.08 438.92 o 4 5 1 8094.46 8529.35 374.73 o 5 5 1 4046.83 3743.05 162.38 o 6 5 1 10156.85 9727.35 438.24 o 7 5 1 283.21 280.54 56.30 o 8 5 1 1945.22 1886.74 84.80 o 9 5 1 8.70 46.70 59.35 o 10 5 1 99.26 113.67 51.76 o -10 6 1 51.53 106.09 46.45 o -9 6 1 510.25 461.66 53.10 o -8 6 1 105.72 163.36 52.64 o -7 6 1 161.99 169.29 64.90 o -6 6 1 92.27 97.16 66.97 o -5 6 1 2486.33 2689.05 177.14 o -4 6 1 2593.70 2744.93 96.04 o -3 6 1 249.65 378.74 66.69 o -2 6 1 2551.70 2792.74 75.12 o -1 6 1 403.74 492.98 67.63 o 0 6 1 3483.80 3618.65 103.05 o 1 6 1 860.55 1115.59 60.32 o 2 6 1 8257.60 8254.87 159.74 o 3 6 1 10073.71 10958.93 228.34 o 4 6 1 9791.41 10561.23 325.35 o 5 6 1 5588.27 5773.36 228.14 o 6 6 1 2478.03 2533.66 136.74 o 7 6 1 11.72 46.61 51.31 o 8 6 1 91.59 143.99 58.85 o 9 6 1 605.99 574.79 55.79 o 10 6 1 240.14 258.51 56.04 o -10 7 1 206.54 340.45 54.28 o -9 7 1 391.77 427.55 53.20 o -8 7 1 887.93 988.35 71.01 o -7 7 1 24.82 58.39 54.41 o -6 7 1 4179.38 4348.47 279.56 o -5 7 1 2081.00 2176.94 122.04 o -4 7 1 2316.42 2886.04 100.87 o -3 7 1 3252.23 3673.00 137.87 o -2 7 1 1.67 54.03 62.86 o -1 7 1 604.42 711.69 73.59 o 0 7 1 542.59 502.73 69.15 o 1 7 1 609.10 636.29 61.42 o 2 7 1 9156.91 9814.32 206.00 o 3 7 1 184.35 247.42 53.06 o 4 7 1 3714.98 3958.03 119.97 o 5 7 1 1148.65 1128.77 67.73 o 6 7 1 0.88 17.22 56.44 o 7 7 1 65.72 112.40 50.33 o 8 7 1 57.27 44.98 49.08 o 9 7 1 108.65 134.19 55.13 o 10 7 1 80.00 161.29 55.12 o -10 8 1 14.90 55.42 54.69 o -9 8 1 61.18 156.25 56.84 o -8 8 1 14.90 -36.84 48.80 o -7 8 1 166.98 216.50 50.26 o -6 8 1 116.06 177.03 61.17 o -5 8 1 5631.97 5640.62 430.51 o -4 8 1 2098.14 2051.58 73.65 o -3 8 1 448.06 530.79 65.41 o -2 8 1 16803.37 17210.90 573.17 o -1 8 1 35234.49 35417.37 947.45 o 0 8 1 1724.70 1955.67 76.24 o 1 8 1 52917.22 55218.88 1134.59 o 2 8 1 3032.27 3132.23 78.67 o 3 8 1 70.27 104.47 58.34 o 4 8 1 14648.48 15010.60 429.97 o 5 8 1 10371.19 10450.24 406.46 o 6 8 1 645.49 739.34 57.18 o 7 8 1 627.76 597.36 50.84 o 8 8 1 5.83 55.08 49.32 o 9 8 1 17.04 99.75 55.26 o 10 8 1 275.77 265.40 48.24 o -10 9 1 75.81 95.74 43.06 o -9 9 1 58.95 59.80 48.46 o -8 9 1 10.86 83.17 55.48 o -7 9 1 7.69 39.59 52.23 o -6 9 1 36.50 46.39 64.12 o -5 9 1 1237.40 1240.16 62.96 o -4 9 1 4472.38 4004.21 151.76 o -3 9 1 3990.66 4215.20 118.30 o -2 9 1 35212.04 37169.86 1422.94 o -1 9 1 53.10 75.11 63.74 o 0 9 1 20136.46 22881.58 815.30 o 1 9 1 22.34 29.41 76.16 o 2 9 1 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