#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:02:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180947 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/27/2202729.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202729_Fobs loop_ _publ_author_name 'Rabe, Gerd W.' 'Zhang-Pre\&se, Mei' 'Golen, James A.' 'Rheingold, Arnold L.' _publ_section_title ; (\h^8^-Cyclooctatetraene)(2,2'',4,4'',6,6''-hexamethyl-m-terphenyl-\kC^2'^)(tetrahydrofuran-\kO)thulium(III) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1102 _journal_page_last m1103 _journal_volume 59 _journal_year 2003 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.1317 _cell_length_b 15.7090 _cell_length_c 28.5941 _exptl_crystal_F_000 2672.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file lh6136Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rabb42 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 614.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 317972.31 343437.03 13588.36 o 4 0 0 167502.48 174593.17 6946.16 o 6 0 0 2258.87 2485.94 236.87 o 8 0 0 1265.24 1595.07 233.11 o 10 0 0 42095.44 40302.52 1766.61 o 12 0 0 63596.69 64562.62 3915.72 o 14 0 0 19290.70 18859.32 1468.40 o 2 1 0 591.00 607.50 46.77 o 4 1 0 55315.98 54332.96 1394.39 o 6 1 0 128736.48 134804.95 3828.45 o 8 1 0 34966.98 34718.94 1066.67 o 10 1 0 5886.69 5266.17 501.89 o 12 1 0 126.92 186.71 308.58 o 14 1 0 10956.27 12003.84 1879.12 o 0 2 0 377502.41 414103.59 13853.11 o 2 2 0 48205.30 51739.22 1716.69 o 4 2 0 311.83 384.82 72.06 o 6 2 0 93.75 120.80 77.80 o 8 2 0 1589.36 1520.51 161.41 o 10 2 0 23477.56 23263.58 903.25 o 12 2 0 16867.42 16743.90 899.74 o 14 2 0 5878.00 5263.84 812.94 o 2 3 0 46431.99 54353.13 1398.10 o 4 3 0 2432.60 2345.36 137.41 o 6 3 0 3667.75 3675.76 175.54 o 8 3 0 180.48 125.27 115.52 o 10 3 0 1217.14 1424.05 222.46 o 12 3 0 312.23 13.43 254.97 o 14 3 0 265.66 164.23 449.03 o 0 4 0 160498.70 172074.89 5787.05 o 2 4 0 39422.65 44207.52 1503.92 o 4 4 0 36678.97 40902.91 1211.93 o 6 4 0 9461.93 10625.67 335.61 o 8 4 0 5988.08 5285.27 268.90 o 10 4 0 3896.49 3950.60 316.87 o 12 4 0 6172.25 6360.96 350.24 o 14 4 0 779.58 369.87 266.82 o 2 5 0 69281.88 75729.59 2197.50 o 4 5 0 36263.84 36963.48 977.50 o 6 5 0 59447.77 61514.60 1794.29 o 8 5 0 26252.25 26554.12 845.03 o 10 5 0 5035.49 5454.28 311.15 o 12 5 0 504.18 314.50 183.07 o 14 5 0 7120.02 8358.11 609.15 o 0 6 0 145007.45 147645.34 4994.51 o 2 6 0 84355.79 86688.63 2880.26 o 4 6 0 66041.02 66913.16 1585.81 o 6 6 0 3.51 -124.21 82.81 o 8 6 0 15935.64 16158.75 551.39 o 10 6 0 41318.70 39928.26 1250.06 o 12 6 0 26188.53 26364.17 900.91 o 14 6 0 8941.94 9196.37 524.75 o 2 7 0 63545.61 64031.81 2154.46 o 4 7 0 140243.97 142120.67 3312.40 o 6 7 0 88980.95 89463.82 2335.17 o 8 7 0 68509.43 65814.70 1738.97 o 10 7 0 14133.35 13043.56 514.36 o 12 7 0 7.49 -121.55 144.95 o 14 7 0 8875.78 9064.26 460.69 o 0 8 0 57569.45 58532.88 2044.33 o 2 8 0 80937.76 83686.96 2418.60 o 4 8 0 2024.88 1906.00 141.23 o 6 8 0 1692.15 1911.84 170.79 o 8 8 0 12602.98 13270.95 399.66 o 10 8 0 21030.08 19786.01 677.90 o 12 8 0 13341.36 13242.50 537.82 o 14 8 0 7047.83 6654.30 449.07 o 2 9 0 7366.84 7068.37 248.15 o 4 9 0 20156.25 21909.32 823.37 o 6 9 0 1719.49 1707.55 138.47 o 8 9 0 6846.86 6885.42 346.34 o 10 9 0 2309.36 2386.66 211.74 o 12 9 0 30.34 -82.02 141.71 o 0 10 0 4744.57 4132.36 271.77 o 2 10 0 3551.47 3287.66 196.56 o 4 10 0 6062.05 5987.19 386.93 o 6 10 0 26.09 19.43 110.20 o 8 10 0 784.32 663.71 116.40 o 10 10 0 1859.08 1870.81 212.56 o 12 10 0 1565.69 1509.18 204.36 o 2 11 0 6154.93 5797.12 276.12 o 4 11 0 10957.21 10449.32 500.37 o 6 11 0 7886.51 7700.43 657.34 o 8 11 0 9448.48 9360.97 365.23 o 10 11 0 2093.90 2101.71 238.53 o 12 11 0 36.94 108.30 269.30 o 0 12 0 66481.07 67648.63 2399.99 o 2 12 0 53886.73 53464.74 1651.56 o 4 12 0 9168.58 8914.30 413.09 o 6 12 0 2252.30 1994.55 232.83 o 8 12 0 13965.50 14028.59 486.78 o 10 12 0 18403.42 18246.43 674.66 o 2 13 0 15102.67 14985.34 553.73 o 4 13 0 32365.57 32042.12 1079.90 o 6 13 0 27444.23 25489.76 1028.07 o 8 13 0 25078.35 23604.49 1021.64 o 10 13 0 3006.64 3201.58 347.69 o 0 14 0 32832.24 33262.42 1460.67 o 2 14 0 35347.70 34434.34 1367.01 o 4 14 0 8240.90 7785.06 394.01 o 6 14 0 23.40 193.23 189.53 o 8 14 0 9413.65 9011.45 448.94 o 10 14 0 13894.71 13114.19 675.50 o 2 15 0 3130.58 3176.17 322.27 o 4 15 0 7670.25 7885.06 410.40 o 6 15 0 11142.09 10987.17 699.72 o 8 15 0 3262.17 2793.88 288.94 o 0 16 0 551.80 1668.44 485.21 o 2 16 0 132.66 234.80 184.25 o 4 16 0 18.31 93.99 176.52 o 6 16 0 144.38 341.02 180.85 o 8 16 0 146.48 98.79 198.48 o 2 17 0 1610.73 1249.92 433.05 o 4 17 0 2723.64 2654.44 291.58 o 6 17 0 4394.66 4693.55 498.72 o 2 18 0 8887.46 9293.57 480.25 o 4 18 0 2699.71 2627.95 299.75 o 1 1 1 49129.83 51321.84 843.74 o 2 1 1 2739.91 2670.74 72.43 o 3 1 1 5856.33 5489.25 137.82 o 4 1 1 33552.27 33385.44 650.79 o 5 1 1 6031.05 5888.77 155.40 o 6 1 1 25489.71 25501.10 619.75 o 7 1 1 1528.21 1835.27 148.48 o 8 1 1 16027.44 15613.68 382.96 o 9 1 1 1406.15 1479.07 126.03 o 10 1 1 1417.07 1524.87 159.92 o 11 1 1 5572.56 5492.67 388.26 o 12 1 1 13.23 -117.75 152.65 o 13 1 1 3944.31 4093.35 312.19 o 14 1 1 690.31 744.04 218.84 o 15 1 1 1097.84 652.88 253.76 o 0 2 1 115289.59 130605.01 3106.61 o 1 2 1 10123.11 11319.68 240.81 o 2 2 1 113899.70 122259.27 2194.56 o 3 2 1 62468.29 63303.26 1145.95 o 4 2 1 5228.74 5416.44 142.57 o 5 2 1 115915.20 121495.42 2176.88 o 6 2 1 519.93 640.65 65.05 o 7 2 1 58204.55 57910.63 1125.88 o 8 2 1 13485.97 12848.29 329.02 o 9 2 1 17302.01 15537.53 454.82 o 10 2 1 6844.28 7113.42 287.24 o 11 2 1 211.63 124.04 121.13 o 12 2 1 14626.63 14126.02 564.91 o 13 2 1 1177.76 1509.26 225.26 o 14 2 1 4293.62 4501.21 351.49 o 15 2 1 5113.13 5193.10 394.12 o 1 3 1 52466.77 55425.79 1199.86 o 2 3 1 6148.97 6343.12 143.78 o 3 3 1 24831.14 23903.47 456.43 o 4 3 1 49608.47 49149.95 950.04 o 5 3 1 3329.00 3042.64 110.64 o 6 3 1 95770.98 98459.78 1778.72 o 7 3 1 17015.50 17296.73 358.23 o 8 3 1 30651.72 31508.65 735.31 o 9 3 1 23904.06 22817.31 654.19 o 10 3 1 2849.73 2991.36 180.87 o 11 3 1 31182.37 29248.04 724.55 o 12 3 1 826.31 1103.49 161.33 o 13 3 1 14208.11 14700.21 619.02 o 14 3 1 2216.71 2738.58 286.19 o 15 3 1 4326.93 3935.06 299.66 o 0 4 1 617.32 727.15 58.00 o 1 4 1 3149.77 3480.92 97.32 o 2 4 1 55436.10 57999.31 1190.38 o 3 4 1 7332.02 7131.81 162.65 o 4 4 1 15601.10 14489.61 298.52 o 5 4 1 113062.32 115951.66 2493.43 o 6 4 1 88.44 134.64 60.10 o 7 4 1 63656.26 65391.73 1349.49 o 8 4 1 16283.04 15864.60 365.64 o 9 4 1 18691.81 18552.48 485.62 o 10 4 1 20893.02 20721.89 540.63 o 11 4 1 92.76 115.59 114.58 o 12 4 1 11781.66 11864.26 376.59 o 13 4 1 2253.67 2195.63 246.66 o 14 4 1 5387.59 5722.63 322.66 o 15 4 1 5027.70 5249.29 329.42 o 1 5 1 50623.19 52160.96 852.24 o 2 5 1 7268.32 6784.42 162.36 o 3 5 1 86054.75 92184.99 1677.33 o 4 5 1 16624.98 17002.77 344.38 o 5 5 1 2434.19 2428.06 108.83 o 6 5 1 41291.28 41637.20 880.80 o 7 5 1 986.06 938.80 91.98 o 8 5 1 13438.80 13821.42 331.60 o 9 5 1 15544.41 16217.02 408.23 o 10 5 1 2397.47 2374.87 170.37 o 11 5 1 9586.49 9541.65 322.61 o 12 5 1 1167.86 822.44 132.50 o 13 5 1 4271.80 4239.56 234.01 o 14 5 1 434.26 555.62 184.06 o 15 5 1 1510.18 1512.92 220.05 o 0 6 1 4541.70 4681.39 150.04 o 1 6 1 28.01 43.58 34.71 o 2 6 1 22333.26 24604.59 494.81 o 3 6 1 5668.50 5631.37 154.18 o 4 6 1 6583.73 6939.09 153.68 o 5 6 1 4432.80 4392.99 124.72 o 6 6 1 398.43 448.72 80.36 o 7 6 1 6612.71 6433.79 197.54 o 8 6 1 586.11 563.58 108.11 o 9 6 1 1537.27 1476.24 121.56 o 10 6 1 553.35 523.49 127.99 o 11 6 1 2.17 -45.96 102.06 o 12 6 1 161.89 46.44 102.65 o 13 6 1 116.33 230.22 136.92 o 14 6 1 742.52 654.08 177.48 o 1 7 1 8109.96 7833.41 154.97 o 2 7 1 13.51 -20.03 56.83 o 3 7 1 2193.02 1975.95 91.05 o 4 7 1 2551.06 2386.24 87.87 o 5 7 1 3837.45 3889.74 119.14 o 6 7 1 4687.15 4958.47 151.12 o 7 7 1 504.17 597.44 84.92 o 8 7 1 49.36 73.36 78.77 o 9 7 1 292.57 170.12 84.12 o 10 7 1 10.38 -48.99 95.39 o 11 7 1 3065.60 3111.63 230.92 o 12 7 1 48.49 -32.81 100.86 o 13 7 1 476.50 517.29 121.48 o 14 7 1 39.08 134.38 126.48 o 0 8 1 10295.39 9620.14 275.60 o 1 8 1 2474.45 2626.57 86.04 o 2 8 1 22041.67 21448.22 406.89 o 3 8 1 10598.45 10672.75 255.61 o 4 8 1 7027.26 7555.91 193.76 o 5 8 1 57703.27 59692.89 1115.90 o 6 8 1 689.94 666.86 74.43 o 7 8 1 19475.33 19716.69 416.78 o 8 8 1 3503.51 3413.28 137.13 o 9 8 1 10398.28 10326.51 256.96 o 10 8 1 14341.67 13771.32 353.71 o 11 8 1 37.40 196.54 95.31 o 12 8 1 5657.88 5400.40 214.71 o 13 8 1 482.26 316.09 117.92 o 14 8 1 2343.48 2505.22 202.46 o 1 9 1 39115.14 38922.45 639.68 o 2 9 1 12140.87 12225.78 290.28 o 3 9 1 23329.64 23919.71 605.68 o 4 9 1 47063.44 49207.77 1130.17 o 5 9 1 35.63 64.37 80.40 o 6 9 1 33077.59 31767.25 631.12 o 7 9 1 990.36 807.35 95.20 o 8 9 1 12374.19 12361.91 294.83 o 9 9 1 14344.77 14440.81 335.86 o 10 9 1 4809.33 4559.47 192.13 o 11 9 1 15906.00 15984.18 423.98 o 12 9 1 1.76 47.01 118.62 o 13 9 1 9047.05 8892.61 310.65 o 0 10 1 28207.58 26868.79 718.52 o 1 10 1 1241.43 1356.17 84.69 o 2 10 1 30723.91 30046.70 635.48 o 3 10 1 37098.62 35637.63 997.94 o 4 10 1 3131.33 3353.39 169.44 o 5 10 1 55092.31 55161.03 1266.24 o 6 10 1 351.72 394.24 83.19 o 7 10 1 31940.82 31537.21 638.00 o 8 10 1 10808.04 10366.70 266.76 o 9 10 1 9688.50 10133.17 279.90 o 10 10 1 16591.86 16206.89 453.51 o 11 10 1 77.02 113.50 95.83 o 12 10 1 8789.91 8954.77 298.91 o 13 10 1 1602.89 1491.71 159.43 o 1 11 1 24808.30 25762.30 493.22 o 2 11 1 4705.66 4881.13 178.69 o 3 11 1 7199.38 7031.51 218.83 o 4 11 1 15858.30 15376.45 424.79 o 5 11 1 213.33 244.90 105.38 o 6 11 1 11396.58 11659.68 302.87 o 7 11 1 329.11 382.30 88.80 o 8 11 1 6291.88 6306.08 204.72 o 9 11 1 9831.04 9417.24 266.22 o 10 11 1 1493.11 1677.63 168.37 o 11 11 1 6656.78 6618.85 262.41 o 12 11 1 93.94 243.43 124.12 o 0 12 1 12712.48 12962.48 423.52 o 1 12 1 9.12 19.24 70.41 o 2 12 1 7872.80 7858.82 245.52 o 3 12 1 2772.95 2802.58 259.91 o 4 12 1 3303.70 3373.11 189.02 o 5 12 1 7519.62 7348.82 292.01 o 6 12 1 964.37 1146.01 125.00 o 7 12 1 11148.36 11159.14 332.54 o 8 12 1 1183.78 1471.41 131.05 o 9 12 1 752.56 804.34 112.98 o 10 12 1 2262.41 2290.82 198.01 o 11 12 1 136.56 38.42 143.71 o 1 13 1 305.99 341.56 95.34 o 2 13 1 72.14 90.03 87.53 o 3 13 1 335.87 365.27 96.76 o 4 13 1 426.12 428.66 105.77 o 5 13 1 31.05 -13.83 122.19 o 6 13 1 475.91 357.67 148.20 o 7 13 1 225.55 43.13 121.13 o 8 13 1 780.70 740.25 140.75 o 9 13 1 348.72 291.49 143.07 o 10 13 1 302.49 172.87 171.90 o 11 13 1 76.26 69.05 224.27 o 0 14 1 2449.17 2646.65 298.72 o 1 14 1 850.86 913.17 103.99 o 2 14 1 3587.62 3663.98 175.95 o 3 14 1 7906.47 7201.35 342.25 o 4 14 1 420.80 594.66 122.96 o 5 14 1 2975.72 3444.84 200.58 o 6 14 1 506.07 642.35 132.93 o 7 14 1 1555.43 1573.81 172.60 o 8 14 1 1111.93 1253.64 156.97 o 9 14 1 2395.79 2160.07 207.15 o 10 14 1 866.83 555.10 235.02 o 1 15 1 18170.11 17416.61 487.50 o 2 15 1 4680.54 4225.04 210.45 o 3 15 1 13536.90 13056.86 387.76 o 4 15 1 8720.31 8345.92 296.30 o 5 15 1 910.69 1102.20 147.15 o 6 15 1 6929.31 7076.38 268.62 o 7 15 1 231.82 152.36 127.46 o 8 15 1 7026.33 6764.62 286.07 o 9 15 1 5201.81 5775.60 443.08 o 0 16 1 9356.33 9380.77 407.76 o 1 16 1 1748.14 1864.17 158.88 o 2 16 1 8559.02 8357.93 386.17 o 3 16 1 9794.75 9261.34 318.44 o 4 16 1 3150.43 3485.97 213.80 o 5 16 1 13283.90 12985.19 383.09 o 6 16 1 30.52 -92.45 121.39 o 7 16 1 13779.63 13662.42 389.48 o 8 16 1 3505.76 3376.69 226.00 o 1 17 1 11537.09 11560.55 460.73 o 2 17 1 4365.81 4198.27 241.06 o 3 17 1 4486.67 4476.27 240.97 o 4 17 1 5215.08 5451.38 272.88 o 5 17 1 370.04 404.98 143.30 o 6 17 1 7631.00 7891.72 308.15 o 1 18 1 477.91 513.08 173.65 o 2 18 1 2548.99 2999.26 344.52 o 3 18 1 1985.27 1973.37 197.76 o 4 18 1 782.74 627.66 162.76 o 1 0 2 39039.11 40185.66 1149.52 o 2 0 2 6012.67 5963.35 160.01 o 3 0 2 112954.74 116554.95 3291.09 o 4 0 2 9.36 -15.90 103.21 o 5 0 2 188177.67 193506.86 5450.09 o 6 0 2 3.86 -27.36 93.69 o 7 0 2 109169.97 118196.95 3377.83 o 8 0 2 4403.68 4700.60 253.18 o 9 0 2 31860.27 31381.98 877.54 o 10 0 2 2773.84 2448.83 257.31 o 11 0 2 5823.17 6039.20 610.77 o 12 0 2 2229.19 2153.11 359.65 o 13 0 2 3261.90 3807.65 976.80 o 14 0 2 689.13 708.26 723.56 o 15 0 2 16331.71 15711.78 1042.84 o 1 1 2 339108.50 359427.78 5854.49 o 2 1 2 279.97 406.17 29.27 o 3 1 2 2588.40 3333.10 105.63 o 4 1 2 118.88 143.33 54.14 o 5 1 2 93.24 138.06 50.61 o 6 1 2 2340.58 2319.91 137.49 o 7 1 2 12914.16 13343.94 328.46 o 8 1 2 351.65 192.03 88.21 o 9 1 2 24279.71 24310.50 527.15 o 10 1 2 344.89 163.24 115.86 o 11 1 2 56274.09 57710.25 1756.21 o 12 1 2 223.94 534.54 175.02 o 13 1 2 25683.24 24314.00 949.05 o 14 1 2 13.15 64.83 196.04 o 15 1 2 6368.19 6345.34 342.62 o 0 2 2 6703.49 6310.36 180.62 o 1 2 2 2246.90 2419.57 59.94 o 2 2 2 417.58 385.62 39.42 o 3 2 2 33091.28 31868.77 563.76 o 4 2 2 539.97 649.40 57.15 o 5 2 2 66784.97 68441.36 1244.26 o 6 2 2 292.70 424.30 64.15 o 7 2 2 47938.04 46844.80 876.15 o 8 2 2 1117.77 1384.98 108.75 o 9 2 2 7345.96 6699.12 243.37 o 10 2 2 481.72 379.69 126.90 o 11 2 2 638.24 616.13 132.82 o 12 2 2 643.10 211.68 192.90 o 13 2 2 2627.62 2530.70 262.50 o 14 2 2 50.04 158.30 180.98 o 15 2 2 5114.36 5168.66 393.38 o 1 3 2 116.21 154.13 41.54 o 2 3 2 2312.38 2429.94 71.81 o 3 3 2 776.54 1061.22 65.31 o 4 3 2 55.68 117.65 63.52 o 5 3 2 12369.11 13621.00 282.52 o 6 3 2 393.37 418.97 63.81 o 7 3 2 2035.69 2305.08 106.86 o 8 3 2 2.55 -114.46 76.31 o 9 3 2 2037.63 2127.68 168.08 o 10 3 2 51.31 526.67 170.34 o 11 3 2 714.50 566.46 135.02 o 12 3 2 104.12 154.99 153.05 o 13 3 2 187.22 129.20 171.40 o 14 3 2 1.54 300.64 157.80 o 15 3 2 184.18 163.63 175.47 o 0 4 2 475.96 586.30 59.64 o 1 4 2 37639.61 40563.58 790.52 o 2 4 2 1180.15 1354.13 72.74 o 3 4 2 20116.29 21166.25 371.87 o 4 4 2 51.77 114.24 49.37 o 5 4 2 5053.48 4685.47 144.69 o 6 4 2 615.12 833.85 73.80 o 7 4 2 6824.95 6801.86 185.05 o 8 4 2 1968.94 2354.61 125.29 o 9 4 2 4026.62 3930.31 195.31 o 10 4 2 87.17 -20.96 116.11 o 11 4 2 764.37 770.05 135.30 o 12 4 2 59.22 104.33 125.31 o 13 4 2 106.06 52.99 145.94 o 14 4 2 202.82 88.30 154.61 o 15 4 2 1630.74 1935.13 219.34 o 1 5 2 80926.48 79744.84 1405.76 o 2 5 2 159.68 123.46 45.17 o 3 5 2 38159.81 37655.82 747.73 o 4 5 2 677.19 629.11 54.41 o 5 5 2 9920.82 10042.81 231.23 o 6 5 2 1824.01 1795.53 123.25 o 7 5 2 14798.27 15108.45 346.85 o 8 5 2 3189.85 3214.15 164.72 o 9 5 2 25925.60 24918.02 576.34 o 10 5 2 416.45 298.11 116.86 o 11 5 2 28883.69 28713.47 672.05 o 12 5 2 52.12 -105.76 101.36 o 13 5 2 13185.43 13564.70 395.43 o 14 5 2 380.82 213.47 160.39 o 15 5 2 2811.98 2726.85 240.07 o 0 6 2 23217.00 26262.83 612.47 o 1 6 2 12572.10 12541.55 281.57 o 2 6 2 3164.60 3459.77 105.16 o 3 6 2 129546.60 135630.69 2593.45 o 4 6 2 9.22 -26.72 45.72 o 5 6 2 79193.73 80733.38 1417.48 o 6 6 2 235.18 342.58 71.38 o 7 6 2 91787.61 94068.64 1816.46 o 8 6 2 2217.10 2174.89 118.86 o 9 6 2 27301.18 28746.32 627.66 o 10 6 2 389.32 324.49 107.97 o 11 6 2 3306.40 3607.70 221.20 o 12 6 2 501.61 663.45 118.59 o 13 6 2 3739.00 3630.47 218.98 o 14 6 2 246.17 119.30 151.76 o 1 7 2 193743.28 207959.08 3503.51 o 2 7 2 2895.16 3400.08 115.59 o 3 7 2 110607.60 119972.76 2187.39 o 4 7 2 68.03 29.97 61.41 o 5 7 2 6757.46 7022.53 167.19 o 6 7 2 4434.31 4450.09 143.65 o 7 7 2 3916.25 3705.57 157.44 o 8 7 2 313.00 257.77 82.87 o 9 7 2 35153.89 35437.63 702.78 o 10 7 2 70.88 -73.43 94.06 o 11 7 2 37349.68 35986.59 772.06 o 12 7 2 87.73 56.82 103.05 o 13 7 2 18004.67 18411.87 464.07 o 14 7 2 337.84 188.19 135.50 o 0 8 2 13160.85 16265.60 412.64 o 1 8 2 6144.16 6361.75 145.29 o 2 8 2 8645.71 9486.99 207.89 o 3 8 2 66258.38 67727.73 1145.88 o 4 8 2 300.18 451.92 73.28 o 5 8 2 35930.44 36312.44 670.11 o 6 8 2 244.85 390.56 77.72 o 7 8 2 19566.15 20032.76 426.12 o 8 8 2 44.32 -116.11 106.14 o 9 8 2 10818.04 11080.08 268.99 o 10 8 2 1610.19 1725.57 133.63 o 11 8 2 1199.95 1352.29 135.29 o 12 8 2 611.21 604.08 157.85 o 13 8 2 2019.75 2536.32 193.10 o 14 8 2 278.50 47.38 138.21 o 1 9 2 9648.16 9493.39 198.97 o 2 9 2 319.21 313.50 71.10 o 3 9 2 1557.19 1732.15 119.01 o 4 9 2 5.43 -120.24 80.16 o 5 9 2 402.96 391.93 89.26 o 6 9 2 736.44 835.44 94.88 o 7 9 2 1495.43 1435.32 113.89 o 8 9 2 2623.77 2521.96 143.45 o 9 9 2 4516.58 4606.54 181.95 o 10 9 2 114.74 204.18 96.92 o 11 9 2 5238.10 5177.06 232.70 o 12 9 2 219.86 209.95 110.42 o 13 9 2 1943.03 2093.11 171.20 o 0 10 2 19.95 136.98 88.45 o 1 10 2 255.30 193.69 69.99 o 2 10 2 29.58 19.82 76.43 o 3 10 2 807.64 832.52 117.06 o 4 10 2 1579.01 1596.25 131.95 o 5 10 2 969.29 1185.15 114.50 o 6 10 2 435.36 492.59 76.78 o 7 10 2 6292.83 6154.93 191.74 o 8 10 2 655.81 630.28 94.23 o 9 10 2 842.16 984.37 105.45 o 10 10 2 121.89 -12.92 94.23 o 11 10 2 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10 27 572.98 489.09 288.74 o 2 10 27 1813.56 1395.12 316.73 o 3 10 27 7625.81 8937.49 705.25 o 4 10 27 873.11 977.11 266.20 o 1 11 27 7686.12 8496.87 650.58 o 2 11 27 894.73 933.76 431.88 o 0 0 28 3322.06 3473.08 698.02 o 1 0 28 3022.47 3214.79 390.54 o 2 0 28 5181.78 6120.95 492.93 o 3 0 28 12576.26 14032.26 738.85 o 4 0 28 451.83 254.10 304.67 o 5 0 28 12382.75 11815.17 767.47 o 6 0 28 46.91 53.03 288.92 o 7 0 28 7537.10 6769.09 560.23 o 8 0 28 1486.80 1314.81 432.49 o 1 1 28 16487.36 17840.73 608.67 o 2 1 28 920.08 1173.67 238.73 o 3 1 28 7478.81 8461.49 441.46 o 4 1 28 4500.92 4568.29 421.41 o 5 1 28 943.38 956.27 229.25 o 6 1 28 3522.40 2752.79 289.54 o 7 1 28 659.71 723.91 248.33 o 8 1 28 840.63 1264.97 281.32 o 0 2 28 3128.97 3432.40 396.49 o 1 2 28 310.82 -147.99 165.46 o 2 2 28 2165.15 2608.23 253.61 o 3 2 28 3394.59 3449.12 314.16 o 4 2 28 74.20 78.35 208.61 o 5 2 28 3289.10 3360.89 319.95 o 6 2 28 11.16 -196.90 241.54 o 7 2 28 2487.83 2737.93 367.24 o 8 2 28 897.13 900.49 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28 10370.71 10351.90 564.51 o 2 7 28 860.45 1431.18 296.35 o 3 7 28 5015.46 5221.23 743.96 o 4 7 28 3179.96 2754.93 371.67 o 5 7 28 738.22 1029.18 286.09 o 6 7 28 3924.75 2772.85 367.00 o 0 8 28 3235.38 2842.86 838.48 o 1 8 28 1143.23 1429.42 286.64 o 2 8 28 970.38 1423.08 294.61 o 3 8 28 5978.15 6105.94 626.62 o 4 8 28 218.66 277.29 262.34 o 5 8 28 6156.99 6269.86 697.88 o 1 9 28 178.37 70.78 241.43 o 2 9 28 500.37 946.73 285.41 o 3 9 28 252.49 -116.54 314.54 o 4 9 28 1950.86 1684.18 331.03 o 0 10 28 2.00 -98.47 362.99 o 1 10 28 191.66 -67.76 252.17 o 2 10 28 144.72 -173.73 254.51 o 1 1 29 24.62 241.03 246.59 o 2 1 29 1906.33 2160.63 277.08 o 3 1 29 43.47 -144.26 205.48 o 4 1 29 3023.26 3557.27 431.30 o 5 1 29 0.12 -114.03 222.44 o 6 1 29 2197.10 1799.74 298.34 o 7 1 29 101.77 35.01 285.37 o 8 1 29 886.71 940.77 330.98 o 0 2 29 10678.15 12191.08 692.18 o 1 2 29 152.46 313.37 191.22 o 2 2 29 9196.16 10213.13 487.33 o 3 2 29 273.16 83.86 212.81 o 4 2 29 3360.41 3510.47 336.86 o 5 2 29 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29 277.32 427.01 266.26 o 3 7 29 8.13 166.40 244.97 o 4 7 29 490.57 494.85 276.51 o 5 7 29 4.59 -232.03 250.52 o 0 8 29 8503.41 7471.19 1023.62 o 1 8 29 1.35 -158.91 233.33 o 2 8 29 6152.32 7098.58 735.36 o 3 8 29 96.56 117.31 258.59 o 4 8 29 1882.99 2172.79 348.54 o 1 9 29 395.33 655.11 274.07 o 2 9 29 2464.77 2599.35 361.88 o 3 9 29 113.97 262.83 266.37 o 0 0 30 8698.27 9648.85 1055.54 o 1 0 30 1257.01 741.60 390.69 o 2 0 30 5655.17 6914.29 1153.44 o 3 0 30 5682.77 6015.24 991.70 o 4 0 30 2254.47 2402.42 467.04 o 5 0 30 8441.20 7615.79 598.73 o 6 0 30 213.44 70.22 306.30 o 7 0 30 3334.89 3450.25 485.70 o 1 1 30 2920.77 3756.77 331.24 o 2 1 30 5493.36 5135.19 377.18 o 3 1 30 1380.81 1215.82 259.64 o 4 1 30 8007.16 9682.32 655.40 o 5 1 30 51.37 -318.85 212.57 o 6 1 30 6653.44 5752.78 596.66 o 7 1 30 661.51 27.56 301.67 o 0 2 30 2449.96 3696.34 427.52 o 1 2 30 692.38 660.11 235.22 o 2 2 30 1793.73 2136.74 285.53 o 3 2 30 1868.63 2167.99 286.99 o 4 2 30 487.77 731.68 257.16 o 5 2 30 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6 31 218.36 431.74 286.74 o 2 6 31 85.85 439.90 282.26 o 3 6 31 732.84 688.48 289.40 o 4 6 31 1.67 -212.60 267.12 o 1 7 31 1372.45 1476.05 334.93 o 2 7 31 2.18 -434.66 289.77 o 0 0 32 11399.85 13177.26 1293.89 o 1 0 32 529.35 41.13 383.96 o 2 0 32 7571.01 8206.79 755.41 o 3 0 32 3086.96 2938.98 587.36 o 4 0 32 1484.01 1607.64 473.83 o 5 0 32 4902.24 5697.54 674.13 o 1 1 32 5145.11 4879.55 432.97 o 2 1 32 1641.28 1358.76 319.29 o 3 1 32 1955.32 1877.64 338.58 o 4 1 32 4610.57 4804.99 446.20 o 5 1 32 24.08 464.82 275.67 o 0 2 32 4006.15 5529.76 640.96 o 1 2 32 534.15 505.29 277.74 o 2 2 32 3491.64 3605.90 418.90 o 3 2 32 1140.93 878.03 279.20 o 4 2 32 1634.25 1574.89 379.66 o 5 2 32 1842.87 1687.30 360.59 o 1 3 32 156.09 232.87 240.46 o 2 3 32 214.08 202.47 243.18 o 3 3 32 0.39 304.38 284.63 o 4 3 32 30.11 196.20 298.67 o 0 4 32 746.58 1175.89 365.55 o 1 4 32 9.27 165.79 242.51 o 2 4 32 414.19 283.70 296.05 o 3 4 32 305.23 367.27 292.55 o 4 4 32 6.78 5.12 297.47 o 1 5 32 3483.35 3297.44 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