#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202733.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202733_Fobs loop_ _publ_author_name 'Liddle, Stephen T.' 'Clegg, William' _publ_section_title ; (18-Crown-6)-bis(tetrahydrofuran)potassium iodide ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1184 _journal_page_last m1186 _journal_volume 59 _journal_year 2003 _space_group_IT_number 92 _symmetry_space_group_name_Hall 'P 4abw 2nw' _symmetry_space_group_name_H-M 'P 41 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.2645 _cell_length_b 12.2645 _cell_length_c 34.3720 _exptl_crystal_F_000 2368.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file lh6144Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' STL41 in P4(1)2(1)2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 538.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+1/4' 'y+1/2, -x+1/2, z+3/4' '-x+1/2, y+1/2, -z+1/4' 'x+1/2, -y+1/2, -z+3/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 1324.10 1340.55 30.23 o 0 2 0 186883.98 202716.38 5488.87 o 1 2 0 1918.33 2203.05 41.25 o 2 2 0 5130.09 5388.41 180.33 o 1 3 0 131058.46 138347.17 1838.83 o 2 3 0 512.66 595.00 32.30 o 3 3 0 24048.41 24958.92 220.49 o 0 4 0 159508.98 163042.38 1500.83 o 1 4 0 32.84 27.72 23.18 o 2 4 0 153733.25 160033.48 1287.67 o 3 4 0 6858.01 7156.37 124.40 o 4 4 0 112615.66 113436.49 1891.81 o 1 5 0 26859.72 28751.41 563.70 o 2 5 0 1219.94 1465.95 81.01 o 3 5 0 203.95 352.58 44.84 o 4 5 0 69.61 29.70 38.56 o 5 5 0 20.74 35.97 49.73 o 0 6 0 15663.63 14855.55 173.32 o 1 6 0 1.50 -9.61 33.45 o 2 6 0 55627.70 56025.23 631.35 o 3 6 0 11938.60 12292.12 159.45 o 4 6 0 49272.73 49746.59 1186.14 o 5 6 0 9590.82 9674.80 153.88 o 6 6 0 28710.00 30444.60 319.68 o 1 7 0 1106.27 1185.10 75.94 o 2 7 0 1515.22 1774.55 75.38 o 3 7 0 423.57 642.30 54.79 o 4 7 0 1560.32 1547.52 72.63 o 5 7 0 1548.20 1621.70 75.99 o 6 7 0 2781.64 2776.11 92.30 o 7 7 0 134.78 181.48 76.03 o 0 8 0 31289.23 32616.45 314.34 o 1 8 0 699.11 731.55 48.15 o 2 8 0 19046.30 19504.25 170.37 o 3 8 0 212.49 462.00 55.78 o 4 8 0 3223.74 3159.78 97.84 o 5 8 0 3224.01 3231.27 103.73 o 6 8 0 4537.49 4636.57 114.41 o 7 8 0 1341.79 1475.13 87.47 o 8 8 0 11410.60 11361.47 263.61 o 1 9 0 3066.40 3379.42 95.28 o 2 9 0 2395.23 2458.09 99.96 o 3 9 0 122.91 231.20 53.68 o 4 9 0 3240.70 3264.15 104.59 o 5 9 0 1382.56 1543.02 91.40 o 6 9 0 485.20 451.58 78.24 o 7 9 0 42.17 59.74 68.59 o 8 9 0 1644.21 1985.95 149.76 o 9 9 0 1433.92 1646.33 254.29 o 0 10 0 5070.10 4737.50 191.72 o 1 10 0 1978.54 2079.06 124.42 o 2 10 0 5305.90 4866.40 161.65 o 3 10 0 488.42 526.88 93.89 o 4 10 0 1491.65 1630.31 110.23 o 5 10 0 4850.55 5193.67 147.58 o 6 10 0 1819.40 1954.55 112.07 o 7 10 0 67.40 51.12 67.04 o 8 10 0 4296.35 4345.49 190.77 o 9 10 0 23.61 -82.99 102.35 o 10 10 0 1566.36 1742.47 252.41 o 1 11 0 920.49 981.34 126.23 o 2 11 0 124.01 2.51 93.88 o 3 11 0 916.31 964.42 125.42 o 4 11 0 30.60 -41.67 69.56 o 5 11 0 290.42 287.47 92.70 o 6 11 0 8.96 35.70 78.11 o 7 11 0 107.80 118.60 94.82 o 8 11 0 335.99 422.33 126.70 o 9 11 0 23.72 99.87 130.83 o 0 12 0 736.48 923.46 176.17 o 1 12 0 708.95 717.73 119.72 o 2 12 0 68.55 -97.16 82.20 o 3 12 0 272.22 412.00 136.12 o 4 12 0 501.14 403.39 113.27 o 5 12 0 367.13 567.58 120.25 o 6 12 0 1260.92 1422.05 145.04 o 7 12 0 4.49 73.54 143.55 o 8 12 0 882.95 1290.03 220.77 o 1 13 0 2125.59 1958.09 159.25 o 2 13 0 70.38 16.13 94.01 o 3 13 0 1691.92 1737.57 161.28 o 4 13 0 110.28 58.78 99.09 o 5 13 0 1914.33 1935.78 158.16 o 6 13 0 0.63 3.05 97.12 o 0 14 0 2.71 -28.07 138.31 o 1 14 0 23.03 52.70 103.25 o 2 14 0 1.63 25.75 93.83 o 3 14 0 1.12 23.58 93.28 o 4 14 0 187.41 211.87 114.01 o 0 1 1 903.18 868.74 32.03 o 1 1 1 176.92 220.23 11.50 o -1 2 1 917.21 1024.72 37.30 o 0 2 1 437.70 470.82 22.57 o 1 2 1 702.12 760.66 32.47 o 2 2 1 1242.18 1312.56 38.86 o -2 3 1 9963.54 10710.26 124.97 o -1 3 1 485.31 685.98 34.22 o 0 3 1 38189.25 40221.38 269.91 o 1 3 1 427.73 635.13 37.12 o 2 3 1 10168.80 11249.70 94.59 o 3 3 1 561.61 851.03 38.48 o -3 4 1 15433.38 16638.58 143.86 o -2 4 1 2860.94 3277.50 192.05 o -1 4 1 29168.31 31482.14 445.03 o 0 4 1 4374.68 4271.41 58.17 o 1 4 1 29309.04 30556.83 317.47 o 2 4 1 2972.58 3102.69 63.76 o 3 4 1 14699.14 15780.87 164.81 o 4 4 1 987.79 1011.12 53.12 o -4 5 1 19785.40 20311.33 289.36 o -3 5 1 319.53 268.75 44.59 o -2 5 1 16773.77 17403.89 333.30 o -1 5 1 3982.07 4008.49 76.98 o 0 5 1 18387.90 18728.38 202.39 o 1 5 1 4058.61 4047.65 81.56 o 2 5 1 17736.47 18069.92 219.22 o 3 5 1 360.77 332.40 45.80 o 4 5 1 20821.02 21417.39 222.51 o 5 5 1 202.90 361.38 44.26 o -5 6 1 10524.81 10115.93 133.35 o -4 6 1 199.09 435.00 49.45 o -3 6 1 13343.36 13526.23 187.26 o -2 6 1 937.54 1294.58 63.38 o -1 6 1 18108.55 18067.32 286.85 o 0 6 1 537.87 703.08 43.85 o 1 6 1 17318.09 16968.38 178.56 o 2 6 1 828.28 1146.62 63.88 o 3 6 1 12272.65 12258.00 236.71 o 4 6 1 191.70 386.42 48.09 o 5 6 1 10125.61 10324.95 210.57 o 6 6 1 2125.23 2165.20 76.60 o -6 7 1 4211.41 4517.21 105.74 o -5 7 1 90.87 120.02 45.41 o -4 7 1 5581.44 6161.39 110.88 o -3 7 1 1251.90 1230.15 64.29 o -2 7 1 9144.64 9283.85 182.55 o -1 7 1 344.63 318.27 40.37 o 0 7 1 16116.68 15976.90 150.28 o 1 7 1 417.94 375.54 36.96 o 2 7 1 9356.12 9547.26 131.36 o 3 7 1 1252.75 1325.68 70.02 o 4 7 1 5440.45 5757.16 114.90 o 5 7 1 128.77 170.76 47.17 o 6 7 1 3960.54 4203.27 104.27 o 7 7 1 1824.78 1744.23 89.80 o -7 8 1 2264.02 2701.87 108.78 o -6 8 1 1167.66 1205.34 78.43 o -5 8 1 5442.76 5492.45 118.98 o -4 8 1 425.09 599.84 63.38 o -3 8 1 17491.85 17448.60 273.29 o -2 8 1 819.13 974.56 63.33 o -1 8 1 28321.68 28003.37 209.91 o 0 8 1 2281.09 2428.99 68.41 o 1 8 1 28162.00 27419.52 340.54 o 2 8 1 805.36 1032.24 66.71 o 3 8 1 18590.43 18534.30 225.69 o 4 8 1 508.33 601.48 62.39 o 5 8 1 5446.33 5376.78 124.57 o 6 8 1 1061.92 1125.47 82.05 o 7 8 1 2118.82 2392.93 103.81 o 8 8 1 314.96 469.23 84.77 o -8 9 1 2570.74 2750.29 126.79 o -7 9 1 4293.42 4118.73 131.42 o -6 9 1 3277.86 3371.19 128.38 o -5 9 1 2052.80 2034.41 108.13 o -4 9 1 4892.89 4972.81 134.39 o -3 9 1 999.20 1254.21 77.32 o -2 9 1 4304.88 3928.60 115.86 o -1 9 1 659.11 788.35 64.81 o 0 9 1 6060.08 5524.11 110.03 o 1 9 1 720.60 720.50 63.13 o 2 9 1 4137.56 3761.58 94.24 o 3 9 1 903.09 1178.55 78.11 o 4 9 1 4631.48 4581.76 116.18 o 5 9 1 2227.76 2177.23 99.07 o 6 9 1 3479.07 3553.98 117.31 o 7 9 1 4155.59 3965.70 136.99 o 8 9 1 2830.62 2933.20 156.81 o 9 9 1 3131.99 3074.75 170.10 o -9 10 1 1509.74 1623.15 175.22 o -8 10 1 1500.57 1544.88 143.21 o -7 10 1 1590.89 1923.62 113.37 o -6 10 1 2386.74 2668.38 123.02 o -5 10 1 4608.02 4516.22 148.03 o -4 10 1 2075.35 2038.16 127.96 o -3 10 1 12659.90 12311.07 239.81 o -2 10 1 815.94 762.53 102.43 o -1 10 1 14452.12 14427.44 219.25 o 0 10 1 83.30 -44.41 60.62 o 1 10 1 13809.62 13158.62 239.40 o 2 10 1 734.67 734.19 101.57 o 3 10 1 12973.07 12612.28 198.40 o 4 10 1 2088.02 1972.86 106.20 o 5 10 1 4308.04 4303.87 137.81 o 6 10 1 2196.17 2236.41 117.68 o 7 10 1 1614.10 1923.64 115.28 o 8 10 1 1655.30 1641.80 142.77 o 9 10 1 1444.68 1570.42 151.96 o 10 10 1 1220.09 1313.30 159.49 o -9 11 1 1770.36 2083.95 213.70 o -8 11 1 354.31 578.62 143.31 o -7 11 1 1668.01 1694.62 135.32 o -6 11 1 1467.97 1520.20 131.79 o -5 11 1 1643.72 1453.63 144.61 o -4 11 1 576.80 667.55 119.16 o -3 11 1 107.99 -27.51 96.71 o -2 11 1 2834.64 2577.38 164.46 o -1 11 1 648.08 751.02 124.32 o 0 11 1 7933.72 7290.59 230.42 o 1 11 1 629.25 597.80 111.71 o 2 11 1 3146.45 2884.54 166.01 o 3 11 1 96.26 -49.62 74.31 o 4 11 1 556.33 716.86 101.52 o 5 11 1 1802.39 1673.58 128.44 o 6 11 1 1544.28 1524.14 125.36 o 7 11 1 1628.32 1737.22 153.48 o 8 11 1 349.52 733.84 125.90 o 9 11 1 1856.05 2105.82 173.12 o -8 12 1 2102.60 2116.52 263.94 o -7 12 1 1652.23 1916.58 191.92 o -6 12 1 1368.72 1655.62 145.33 o -5 12 1 5131.24 5179.74 215.80 o -4 12 1 902.32 1072.98 143.58 o -3 12 1 6834.31 6130.07 226.64 o -2 12 1 319.18 311.47 105.32 o -1 12 1 2799.63 2670.60 163.37 o 0 12 1 1110.69 1038.16 131.22 o 1 12 1 2444.52 2415.02 161.71 o 2 12 1 330.29 333.16 111.29 o 3 12 1 6912.42 6160.09 225.06 o 4 12 1 958.68 1206.17 140.34 o 5 12 1 4983.81 4761.57 205.38 o 6 12 1 1355.79 1651.43 154.05 o 7 12 1 1654.14 1988.94 269.79 o 8 12 1 2047.32 2226.39 238.55 o -6 13 1 287.97 264.80 109.00 o -5 13 1 3158.95 2975.39 180.95 o -4 13 1 186.65 124.46 108.58 o -3 13 1 2146.42 2133.80 163.36 o -2 13 1 886.05 946.14 129.94 o -1 13 1 1392.55 1711.76 154.42 o 0 13 1 1501.62 1588.99 160.02 o 1 13 1 1276.78 1578.55 160.12 o 2 13 1 922.66 873.40 133.71 o 3 13 1 2112.81 2165.25 155.34 o 4 13 1 161.94 205.40 102.40 o 5 13 1 3169.86 2830.34 176.16 o 6 13 1 267.19 230.76 104.10 o -4 14 1 616.86 251.50 115.35 o -3 14 1 3154.04 3279.31 188.40 o -2 14 1 315.39 411.65 114.73 o -1 14 1 3863.71 3818.48 198.50 o 0 14 1 430.59 245.69 108.38 o 1 14 1 3831.39 3786.64 204.93 o 2 14 1 365.88 401.01 119.24 o 3 14 1 3208.97 3324.41 187.77 o 4 14 1 577.54 497.23 119.64 o -1 2 2 85.84 86.32 16.07 o 0 2 2 893.39 970.46 35.53 o 1 2 2 110.08 125.24 21.51 o 2 2 2 431.56 633.82 30.62 o -2 3 2 1406.80 1631.28 43.27 o -1 3 2 7384.94 8062.63 111.23 o 0 3 2 2305.78 2714.99 44.91 o 1 3 2 7057.40 7514.17 132.35 o 2 3 2 1292.66 1532.62 45.57 o 3 3 2 7179.03 8238.47 160.34 o -3 4 2 6986.42 6734.75 85.76 o -2 4 2 8663.90 9726.12 191.59 o -1 4 2 5455.40 5060.36 66.19 o 0 4 2 3746.14 3808.97 53.05 o 1 4 2 5351.98 5134.58 86.06 o 2 4 2 9453.19 10407.69 182.88 o 3 4 2 6628.05 6425.62 97.60 o 4 4 2 10428.30 10164.58 194.66 o -4 5 2 4648.25 4532.16 84.41 o -3 5 2 6577.29 6854.41 119.71 o -2 5 2 3546.49 3993.36 79.50 o -1 5 2 1798.45 1817.24 60.92 o 0 5 2 1992.54 1976.68 53.05 o 1 5 2 1893.12 1833.48 57.99 o 2 5 2 3003.29 3396.48 112.39 o 3 5 2 6723.83 7078.57 130.51 o 4 5 2 4887.31 4899.97 95.00 o 5 5 2 15268.55 15962.18 149.42 o -5 6 2 3417.62 3540.68 89.58 o -4 6 2 15349.08 16132.17 332.08 o -3 6 2 4840.20 5196.88 95.88 o -2 6 2 2565.23 2497.52 76.98 o -1 6 2 11824.26 12121.12 134.38 o 0 6 2 6785.72 6673.32 90.24 o 1 6 2 12950.66 13188.69 125.99 o 2 6 2 2276.56 2223.36 84.73 o 3 6 2 5082.40 5503.62 105.58 o 4 6 2 14106.40 14289.65 160.24 o 5 6 2 3481.44 3619.54 100.32 o 6 6 2 9771.47 10707.78 178.49 o -6 7 2 3872.32 4021.39 103.59 o -5 7 2 13316.49 13562.54 160.70 o -4 7 2 12082.27 12273.00 266.06 o -3 7 2 5648.03 5944.11 126.09 o -2 7 2 9038.45 8976.61 118.51 o -1 7 2 2638.73 2672.20 72.90 o 0 7 2 9542.92 9222.22 103.78 o 1 7 2 2792.53 2800.39 62.66 o 2 7 2 8960.75 8510.68 109.54 o 3 7 2 5265.69 5454.19 108.19 o 4 7 2 12518.12 12385.22 248.92 o 5 7 2 14245.39 14185.87 218.14 o 6 7 2 3858.89 3973.15 109.95 o 7 7 2 9130.64 8831.35 144.61 o -7 8 2 1894.74 1907.13 106.48 o -6 8 2 9459.23 10173.14 212.03 o -5 8 2 1434.57 1471.50 81.41 o -4 8 2 12240.96 12447.78 231.73 o -3 8 2 9437.74 9588.08 152.77 o -2 8 2 4899.05 5297.67 127.46 o -1 8 2 8286.05 8124.36 134.42 o 0 8 2 133.66 189.91 35.63 o 1 8 2 8546.14 8247.28 115.49 o 2 8 2 5111.41 5190.12 99.62 o 3 8 2 8190.78 8271.14 143.10 o 4 8 2 12416.51 12340.91 166.64 o 5 8 2 1567.73 1520.69 85.04 o 6 8 2 9615.27 9975.71 168.56 o 7 8 2 1911.82 1828.02 95.29 o 8 8 2 7738.63 7825.06 191.66 o -8 9 2 1181.55 1301.80 114.25 o -7 9 2 10584.35 10966.12 191.49 o -6 9 2 2911.62 3211.72 118.27 o -5 9 2 8703.51 8894.55 163.02 o -4 9 2 6068.22 5921.77 306.63 o -3 9 2 1553.98 1767.25 95.97 o -2 9 2 6747.44 6251.23 125.31 o -1 9 2 223.73 257.34 55.78 o 0 9 2 6937.05 5929.97 115.67 o 1 9 2 282.31 286.14 51.84 o 2 9 2 6935.87 6363.21 126.11 o 3 9 2 1352.07 1517.59 83.80 o 4 9 2 6290.07 6332.94 134.05 o 5 9 2 9188.13 9437.15 161.64 o 6 9 2 2645.32 2849.43 110.67 o 7 9 2 10185.80 10545.96 179.85 o 8 9 2 1258.46 1289.62 130.89 o 9 9 2 7326.81 7707.17 234.05 o -9 10 2 115.91 83.82 108.23 o -8 10 2 4214.14 4528.28 199.13 o -7 10 2 669.99 859.19 102.52 o -6 10 2 4926.96 4905.00 158.35 o -5 10 2 4598.83 4714.93 170.76 o -4 10 2 3687.50 3519.53 150.89 o -3 10 2 10630.24 10161.13 230.47 o -2 10 2 2823.01 2487.15 124.61 o -1 10 2 10174.54 9384.98 205.13 o 0 10 2 3.81 -43.61 65.11 o 1 10 2 10775.04 10093.25 213.48 o 2 10 2 2606.66 2472.91 119.46 o 3 10 2 10316.35 9622.07 162.32 o 4 10 2 3697.50 3768.44 128.30 o 5 10 2 4887.26 4764.56 141.12 o 6 10 2 4717.46 4765.82 146.40 o 7 10 2 672.03 974.28 102.47 o 8 10 2 4065.03 4226.49 251.13 o 9 10 2 91.66 119.79 98.55 o 10 10 2 3822.40 4461.49 225.57 o -9 11 2 2034.01 2509.13 227.66 o -8 11 2 268.70 195.56 126.69 o -7 11 2 2641.01 2610.26 170.59 o -6 11 2 776.18 724.17 121.59 o -5 11 2 3284.19 3507.21 182.35 o -4 11 2 1190.72 1339.20 142.23 o -3 11 2 3903.57 4066.05 188.18 o -2 11 2 5732.71 5627.92 210.75 o -1 11 2 1024.99 917.30 123.77 o 0 11 2 6868.14 6397.17 216.59 o 1 11 2 1066.74 1078.02 131.75 o 2 11 2 5667.92 5444.32 175.11 o 3 11 2 3802.65 4050.78 161.27 o 4 11 2 1230.44 1222.97 121.55 o 5 11 2 3317.35 3279.98 150.21 o 6 11 2 756.31 717.62 105.41 o 7 11 2 2643.99 2657.99 166.90 o 8 11 2 279.16 231.29 101.34 o 9 11 2 2138.52 2402.04 161.45 o -8 12 2 2355.52 2741.60 273.06 o -7 12 2 455.54 530.23 119.26 o -6 12 2 3042.71 2903.19 177.11 o -5 12 2 1902.52 1880.72 155.27 o -4 12 2 565.38 818.47 133.17 o -3 12 2 3509.16 3008.73 176.83 o -2 12 2 576.59 555.18 115.03 o -1 12 2 3651.19 2999.75 172.17 o 0 12 2 37.71 19.30 89.19 o 1 12 2 3909.91 3183.09 179.42 o 2 12 2 463.55 232.00 104.17 o 3 12 2 3455.98 3112.51 171.87 o 4 12 2 608.98 777.43 127.83 o 5 12 2 1919.66 1781.03 153.95 o 6 12 2 3043.37 3011.60 177.02 o 7 12 2 421.74 566.76 139.00 o 8 12 2 2387.58 2693.48 206.77 o -6 13 2 979.36 1225.83 154.23 o -5 13 2 817.55 1060.64 145.65 o -4 13 2 1495.80 1604.44 160.89 o -3 13 2 507.76 555.44 121.57 o -2 13 2 5601.53 4969.83 261.07 o -1 13 2 65.41 67.76 99.52 o 0 13 2 4617.86 4186.98 203.18 o 1 13 2 76.96 -8.41 100.65 o 2 13 2 5428.42 5048.32 215.03 o 3 13 2 545.37 462.57 104.92 o 4 13 2 1414.34 1563.91 148.14 o 5 13 2 905.72 1048.85 141.32 o 6 13 2 1077.52 1537.84 242.27 o -4 14 2 975.81 1206.79 153.98 o -3 14 2 2046.52 2006.78 162.64 o -2 14 2 461.48 564.62 120.80 o -1 14 2 2766.37 2738.20 175.69 o 0 14 2 39.95 -44.69 97.77 o 1 14 2 2946.26 2942.68 184.37 o 2 14 2 478.07 439.73 117.06 o 3 14 2 2073.95 1942.23 160.74 o 4 14 2 922.33 1095.40 143.00 o 0 1 3 5964.10 6179.75 130.76 o 1 1 3 4.00 10.66 10.72 o -1 2 3 3309.49 3170.52 139.58 o 0 2 3 65.60 82.77 25.06 o 1 2 3 3938.19 4075.63 53.29 o 2 2 3 8424.42 8644.76 91.02 o -2 3 3 21486.63 22535.24 273.68 o -1 3 3 2626.67 2527.43 49.69 o 0 3 3 129739.90 132829.80 1029.28 o 1 3 3 2572.86 2456.27 62.23 o 2 3 3 20245.01 21113.44 178.69 o 3 3 3 12966.61 12640.84 217.48 o -3 4 3 7750.51 7879.58 193.38 o -2 4 3 299.66 441.46 34.02 o -1 4 3 6917.00 7367.66 88.93 o 0 4 3 241.64 414.57 24.84 o 1 4 3 6631.03 6673.14 107.13 o 2 4 3 229.26 337.63 34.81 o 3 4 3 8085.81 8465.15 108.74 o 4 4 3 1862.51 1878.95 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