#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:02:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180947 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/27/2202763.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202763_Fobs loop_ _publ_author_name 'Zhang, Xiu-Lian' 'Ren, Chun-Xia' 'Chen, Xiao-Ming' 'Ng, Seik Weng' _publ_section_title ; Aqua{1-[(2-oxidophenyl)iminomethyl]naphthalen-2-olato}pyridinecopper(II) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1176 _journal_page_last m1177 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.803 _cell_angle_gamma 90.000 _cell_length_a 16.9472 _cell_length_b 5.5645 _cell_length_c 19.4623 _exptl_crystal_F_000 868.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file na6270Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 274.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 15937.67 18569.87 378.75 o 4 0 0 47322.34 53269.26 249.56 o 6 0 0 738.70 621.29 35.14 o 8 0 0 1245.80 1291.04 36.44 o 10 0 0 1124.09 1245.40 39.78 o 12 0 0 1713.10 1880.90 52.38 o 14 0 0 167.24 125.71 22.47 o 16 0 0 44.40 47.21 21.09 o 18 0 0 672.04 678.66 65.06 o 20 0 0 109.83 121.10 44.64 o 1 1 0 12203.42 13137.47 64.17 o 2 1 0 808.24 1064.27 31.33 o 3 1 0 470.94 535.46 10.77 o 4 1 0 803.59 842.31 13.62 o 5 1 0 12008.76 12270.58 89.37 o 6 1 0 2039.06 2209.01 28.47 o 7 1 0 9037.23 9404.57 156.35 o 8 1 0 627.21 681.27 19.75 o 9 1 0 2.61 0.99 7.75 o 10 1 0 41.00 25.00 9.47 o 11 1 0 2686.42 2793.75 60.93 o 12 1 0 580.92 569.26 23.39 o 13 1 0 1190.43 1250.18 32.94 o 14 1 0 15.98 17.66 14.32 o 15 1 0 146.02 128.68 20.16 o 16 1 0 16.65 7.51 15.07 o 17 1 0 123.80 141.53 22.66 o 18 1 0 1.01 7.42 17.54 o 19 1 0 353.89 383.51 39.92 o 20 1 0 1.17 -17.57 21.16 o 21 1 0 2.97 -22.32 34.19 o 0 2 0 1556.35 1356.84 44.17 o 1 2 0 429.64 400.63 16.03 o 2 2 0 3103.48 3158.66 52.16 o 3 2 0 410.64 410.29 23.18 o 4 2 0 148.42 119.78 11.71 o 5 2 0 759.57 833.54 16.59 o 6 2 0 13301.67 14199.69 113.80 o 7 2 0 2761.32 3153.30 36.06 o 8 2 0 8281.67 8438.96 205.30 o 9 2 0 1380.06 1466.85 48.12 o 10 2 0 37.18 38.99 13.49 o 11 2 0 30.57 29.88 13.62 o 12 2 0 2310.75 2119.31 78.41 o 13 2 0 0.09 -3.82 13.12 o 14 2 0 168.76 160.06 21.12 o 15 2 0 19.07 34.06 16.80 o 16 2 0 377.43 366.24 29.65 o 17 2 0 22.48 22.55 17.51 o 18 2 0 450.42 526.52 45.32 o 19 2 0 35.92 51.21 27.51 o 20 2 0 96.65 100.68 33.74 o 21 2 0 21.88 -0.71 28.03 o 1 3 0 5993.55 6156.03 64.62 o 2 3 0 89.81 88.26 11.96 o 3 3 0 164.79 199.54 15.79 o 4 3 0 45.28 29.19 10.58 o 5 3 0 1099.90 995.26 28.42 o 6 3 0 329.48 301.25 15.12 o 7 3 0 3788.32 3436.50 105.91 o 8 3 0 164.29 134.44 17.68 o 9 3 0 70.25 58.68 14.90 o 10 3 0 145.96 183.16 20.58 o 11 3 0 2210.36 2266.10 54.08 o 12 3 0 149.14 148.29 20.80 o 13 3 0 775.06 829.61 40.76 o 14 3 0 25.21 13.08 16.43 o 15 3 0 33.03 32.90 18.34 o 16 3 0 0.20 16.54 21.90 o 17 3 0 275.17 265.63 38.09 o 18 3 0 5.73 3.45 24.74 o 19 3 0 264.84 303.53 43.48 o 0 4 0 4692.91 4905.87 80.75 o 1 4 0 124.49 120.37 13.82 o 2 4 0 231.66 211.32 18.47 o 3 4 0 6.31 9.65 11.08 o 4 4 0 466.83 462.35 24.54 o 5 4 0 39.10 47.79 17.44 o 6 4 0 308.09 298.85 29.37 o 7 4 0 310.16 279.04 30.36 o 8 4 0 80.17 73.83 21.30 o 9 4 0 6.47 -17.41 16.62 o 10 4 0 567.01 518.18 40.37 o 11 4 0 61.08 85.59 25.08 o 12 4 0 632.54 651.93 47.11 o 13 4 0 111.15 102.67 28.04 o 14 4 0 279.04 328.67 39.46 o 15 4 0 1.04 10.71 23.39 o 16 4 0 17.20 15.91 24.85 o 17 4 0 18.87 8.90 25.75 o 1 5 0 1544.07 1530.09 38.44 o 2 5 0 0.75 -1.14 13.21 o 3 5 0 122.35 133.93 37.04 o 4 5 0 20.69 5.26 16.89 o 5 5 0 858.49 940.04 48.66 o 6 5 0 74.17 66.91 22.99 o 7 5 0 245.53 331.77 56.04 o 8 5 0 113.66 118.75 27.87 o 9 5 0 38.83 53.72 22.78 o 10 5 0 33.28 45.74 23.14 o 11 5 0 275.13 326.93 39.92 o 12 5 0 109.78 112.19 30.63 o 13 5 0 357.15 337.67 43.03 o 14 5 0 0.61 -5.55 24.19 o 15 5 0 15.87 22.30 26.76 o 0 6 0 123.02 94.03 36.09 o 1 6 0 72.35 75.04 35.14 o 2 6 0 15.37 16.15 30.87 o 3 6 0 165.66 205.97 27.14 o 4 6 0 31.52 58.12 20.74 o 5 6 0 1.03 -1.21 18.01 o 6 6 0 430.61 472.77 45.16 o 7 6 0 94.77 96.22 28.80 o 8 6 0 191.18 189.59 34.39 o 9 6 0 24.80 18.57 23.84 o 10 6 0 92.39 88.89 30.33 o 11 6 0 12.25 5.01 26.58 o 1 7 0 94.78 86.60 28.70 o 2 7 0 96.51 118.24 31.33 o 3 7 0 14.89 36.57 37.99 o 4 7 0 38.54 6.17 36.09 o 5 7 0 1.84 15.67 37.52 o -21 0 1 245.86 310.12 56.99 o -19 0 1 223.79 297.77 51.29 o -17 0 1 432.89 388.96 51.29 o -15 0 1 1581.78 1632.72 72.90 o -13 0 1 11.64 4.55 14.67 o -11 0 1 1063.52 1031.15 39.29 o -9 0 1 2160.72 2235.50 47.85 o -7 0 1 1288.09 1124.82 31.06 o -5 0 1 258.97 202.09 15.45 o -3 0 1 10695.22 11534.97 92.37 o -1 0 1 9448.25 4.96 3.85 o 1 0 1 4890.61 5595.48 60.79 o 3 0 1 9270.69 10514.14 103.53 o 5 0 1 629.72 643.80 22.72 o 7 0 1 620.85 647.97 39.89 o 9 0 1 3285.97 3387.83 104.24 o 11 0 1 1519.12 1603.65 46.98 o 13 0 1 6.34 18.28 15.48 o 15 0 1 1332.93 1309.95 58.65 o 17 0 1 651.90 685.78 61.74 o 19 0 1 17.27 40.37 34.19 o 21 0 1 64.53 104.01 44.17 o -21 1 1 16.23 19.95 37.52 o -20 1 1 209.69 243.63 52.24 o -19 1 1 2.45 2.38 17.66 o -18 1 1 31.22 16.82 17.35 o -17 1 1 123.28 145.26 22.84 o -16 1 1 250.63 313.63 26.91 o -15 1 1 15.49 18.17 14.99 o -14 1 1 1122.52 1125.91 44.41 o -13 1 1 0.99 3.06 10.35 o -12 1 1 29.44 28.20 11.05 o -11 1 1 137.17 131.78 13.78 o -10 1 1 750.06 641.80 21.67 o -9 1 1 120.21 145.47 12.41 o -8 1 1 2030.54 1992.36 30.97 o -7 1 1 111.94 136.56 10.79 o -6 1 1 41.40 46.82 8.34 o -5 1 1 8206.76 9095.64 67.20 o -4 1 1 28060.95 30578.23 320.07 o -3 1 1 11706.57 14136.61 157.88 o -2 1 1 12913.95 14020.90 74.03 o -1 1 1 369.43 421.29 15.95 o 0 1 1 622.58 652.31 14.70 o 1 1 1 2440.68 2783.75 26.12 o 2 1 1 12398.20 14165.54 158.28 o 3 1 1 25587.48 29082.37 367.90 o 4 1 1 75158.63 80209.88 583.28 o 5 1 1 17180.81 20450.48 124.96 o 6 1 1 683.69 704.86 20.63 o 7 1 1 1984.59 2102.08 51.93 o 8 1 1 8523.45 9142.01 185.83 o 9 1 1 0.15 0.67 7.86 o 10 1 1 1894.62 1862.57 61.56 o 11 1 1 823.95 776.41 24.86 o 12 1 1 166.20 161.94 15.70 o 13 1 1 5.01 15.82 13.33 o 14 1 1 810.19 851.92 35.64 o 15 1 1 3.59 -10.75 12.79 o 16 1 1 787.53 829.66 38.46 o 17 1 1 1.13 -11.97 15.30 o 18 1 1 5.47 -14.70 16.39 o 19 1 1 10.98 12.58 20.97 o 20 1 1 198.52 206.59 34.92 o 21 1 1 21.78 7.63 26.81 o -21 2 1 75.34 120.39 36.34 o -20 2 1 58.91 68.96 30.54 o -19 2 1 10.48 7.83 23.84 o -18 2 1 0.08 15.48 22.49 o -17 2 1 1.77 -1.23 20.41 o -16 2 1 65.55 76.57 19.70 o -15 2 1 896.71 909.93 38.81 o -14 2 1 38.03 32.03 15.51 o -13 2 1 419.62 402.62 27.04 o -12 2 1 3.99 6.02 12.59 o -11 2 1 1275.82 1164.78 36.43 o -10 2 1 71.89 69.15 11.78 o -9 2 1 2275.66 2332.85 36.89 o -8 2 1 104.82 87.23 9.16 o -7 2 1 5816.60 6575.32 62.27 o -6 2 1 526.28 492.73 14.47 o -5 2 1 118.00 112.36 8.78 o -4 2 1 580.87 579.22 18.99 o -3 2 1 12707.47 13267.52 85.49 o -2 2 1 119.78 133.71 14.20 o -1 2 1 135.81 85.81 10.59 o 0 2 1 7.74 9.72 7.92 o 1 2 1 61.89 72.88 11.36 o 2 2 1 23.28 30.22 7.50 o 3 2 1 8581.22 8687.29 113.42 o 4 2 1 130.88 133.58 10.22 o 5 2 1 6436.93 6682.19 40.89 o 6 2 1 1267.58 1310.05 27.05 o 7 2 1 4541.84 4969.80 58.68 o 8 2 1 819.36 823.17 22.07 o 9 2 1 5396.38 5660.08 72.49 o 10 2 1 0.40 2.26 11.51 o 11 2 1 1643.07 1452.82 41.39 o 12 2 1 316.85 316.46 24.89 o 13 2 1 95.68 87.81 18.32 o 14 2 1 49.64 37.06 16.33 o 15 2 1 720.66 722.08 36.88 o 16 2 1 1.00 -1.32 15.34 o 17 2 1 5.89 4.97 16.75 o 18 2 1 31.89 -1.19 17.91 o 19 2 1 1.25 8.43 24.17 o 20 2 1 16.54 20.03 27.67 o -20 3 1 124.03 118.73 49.87 o -19 3 1 33.23 34.49 29.01 o -18 3 1 1.82 -12.17 24.46 o -17 3 1 37.54 -3.00 22.99 o -16 3 1 413.64 434.71 46.07 o -15 3 1 143.36 154.14 30.63 o -14 3 1 642.37 590.41 44.32 o -13 3 1 33.81 35.94 15.91 o -12 3 1 18.20 20.49 14.33 o -11 3 1 7.10 4.74 13.20 o -10 3 1 1189.57 1145.21 52.23 o -9 3 1 3.95 2.06 10.73 o -8 3 1 1510.76 1308.67 107.81 o -7 3 1 14.96 3.45 8.20 o -6 3 1 5.36 1.39 7.71 o -5 3 1 381.13 331.58 16.19 o -4 3 1 1816.79 1692.35 36.90 o -3 3 1 33.76 28.38 10.57 o -2 3 1 3831.80 3692.73 60.08 o -1 3 1 17.53 28.59 10.04 o 0 3 1 406.35 405.59 19.69 o 1 3 1 78.66 79.02 11.30 o 2 3 1 3571.04 3682.88 46.06 o 3 3 1 125.28 134.93 15.35 o 4 3 1 3453.86 3552.40 58.54 o 5 3 1 1337.35 1290.59 30.69 o 6 3 1 8.96 -2.73 8.76 o 7 3 1 605.72 609.77 35.14 o 8 3 1 859.74 831.46 32.13 o 9 3 1 34.25 25.88 13.50 o 10 3 1 761.15 806.74 35.06 o 11 3 1 2873.81 2810.51 61.02 o 12 3 1 85.99 74.52 18.70 o 13 3 1 253.50 235.17 25.31 o 14 3 1 258.58 321.32 29.43 o 15 3 1 0.26 -7.28 15.53 o 16 3 1 570.59 599.68 37.65 o 17 3 1 32.82 39.35 24.05 o 18 3 1 27.96 35.26 26.66 o 19 3 1 32.74 39.00 29.12 o -17 4 1 93.99 70.01 29.53 o -16 4 1 16.63 42.75 26.43 o -15 4 1 487.50 425.44 81.45 o -14 4 1 0.21 4.27 21.32 o -13 4 1 262.65 262.80 36.19 o -12 4 1 67.65 89.99 25.68 o -11 4 1 67.02 64.09 22.28 o -10 4 1 65.47 34.98 21.42 o -9 4 1 1161.75 1019.21 48.66 o -8 4 1 0.25 1.93 15.18 o -7 4 1 408.78 355.32 32.57 o -6 4 1 117.22 125.70 23.16 o -5 4 1 478.88 463.78 25.31 o -4 4 1 304.08 318.35 21.82 o -3 4 1 2787.77 2582.19 49.68 o -2 4 1 36.14 30.50 14.39 o -1 4 1 1456.62 1472.57 37.16 o 0 4 1 373.06 383.53 19.47 o 1 4 1 470.85 474.98 19.03 o 2 4 1 16.81 22.50 11.92 o 3 4 1 3062.49 3045.78 51.92 o 4 4 1 101.18 88.86 26.36 o 5 4 1 853.37 865.68 43.32 o 6 4 1 7.44 17.76 16.16 o 7 4 1 310.45 376.24 35.14 o 8 4 1 1.10 0.44 15.21 o 9 4 1 450.20 493.19 38.89 o 10 4 1 15.31 7.52 18.48 o 11 4 1 187.00 169.90 29.46 o 12 4 1 19.43 18.85 21.34 o 13 4 1 6.99 -1.40 20.30 o 14 4 1 121.31 68.68 27.03 o 15 4 1 921.81 1029.48 78.60 o 16 4 1 16.11 30.22 24.84 o 17 4 1 314.21 289.94 43.30 o -15 5 1 80.85 120.63 33.46 o -14 5 1 490.23 470.53 47.87 o -13 5 1 8.77 6.83 21.56 o -12 5 1 36.40 26.47 23.51 o -11 5 1 50.45 76.24 27.78 o -10 5 1 585.99 539.92 44.66 o -9 5 1 29.01 37.08 23.51 o -8 5 1 773.17 715.31 46.96 o -7 5 1 0.36 11.25 19.74 o -6 5 1 243.67 233.27 30.56 o -5 5 1 8.28 17.47 19.39 o -4 5 1 645.78 637.97 40.95 o -3 5 1 34.98 20.32 17.80 o -2 5 1 153.69 150.07 37.52 o -1 5 1 12.66 15.00 14.05 o 0 5 1 12.02 29.94 13.07 o 1 5 1 414.19 403.90 27.62 o 2 5 1 68.80 79.85 18.62 o 3 5 1 1144.09 1229.16 43.69 o 4 5 1 64.88 63.10 18.80 o 5 5 1 24.25 7.86 18.03 o 6 5 1 3.49 4.28 17.68 o 7 5 1 253.85 256.40 32.86 o 8 5 1 194.03 187.84 31.04 o 9 5 1 16.93 44.70 23.44 o 10 5 1 403.31 475.12 43.52 o 11 5 1 117.44 145.86 31.03 o 12 5 1 149.18 147.76 33.72 o 13 5 1 3.52 15.41 23.81 o 14 5 1 146.55 184.32 37.53 o 15 5 1 9.39 13.75 29.48 o -11 6 1 27.13 9.57 26.30 o -10 6 1 3.71 7.53 24.52 o -9 6 1 293.68 323.44 40.97 o -8 6 1 30.97 28.64 23.80 o -7 6 1 141.84 141.83 30.66 o -6 6 1 43.70 36.09 22.84 o -5 6 1 222.51 260.73 51.29 o -4 6 1 31.49 38.31 19.83 o -3 6 1 303.50 294.75 29.21 o -2 6 1 2.77 5.22 30.39 o -1 6 1 16.66 3.09 19.81 o 0 6 1 198.28 166.22 39.89 o 1 6 1 6.48 -19.00 26.12 o 2 6 1 67.74 79.51 21.31 o 3 6 1 313.89 354.36 31.22 o 4 6 1 29.06 36.91 19.55 o 5 6 1 478.52 443.17 35.07 o 6 6 1 125.43 145.83 27.11 o 7 6 1 31.65 35.18 21.40 o 8 6 1 0.52 0.47 36.57 o 9 6 1 185.00 255.24 38.27 o 10 6 1 3.28 -0.16 23.50 o 11 6 1 15.30 5.40 26.23 o -5 7 1 309.89 355.71 63.16 o -4 7 1 10.62 34.67 42.27 o -3 7 1 74.70 90.23 44.64 o -2 7 1 229.12 248.38 53.19 o -1 7 1 44.76 47.97 39.89 o 0 7 1 17.75 20.56 25.61 o 1 7 1 21.91 18.58 25.56 o 2 7 1 67.72 132.50 47.02 o 3 7 1 14.01 -6.65 34.19 o 4 7 1 23.81 28.50 38.94 o 5 7 1 153.63 148.17 50.34 o -20 0 2 37.97 41.79 36.57 o -18 0 2 886.46 873.85 70.29 o -16 0 2 134.33 133.45 24.84 o -14 0 2 172.95 149.32 22.77 o -12 0 2 211.51 248.29 37.99 o -10 0 2 2838.23 2883.12 56.39 o -8 0 2 27.50 24.46 11.42 o -6 0 2 2124.06 1839.57 35.18 o -4 0 2 1424.05 1547.82 59.36 o -2 0 2 2643.59 2751.47 48.68 o 0 0 2 51362.68 53106.10 283.67 o 2 0 2 19642.53 21946.41 158.15 o 4 0 2 734.21 735.39 21.84 o 6 0 2 2935.74 2957.24 46.11 o 8 0 2 4174.63 4056.40 61.06 o 10 0 2 956.54 875.83 34.91 o 12 0 2 2337.91 2432.74 58.92 o 14 0 2 504.32 500.74 33.69 o 16 0 2 38.84 26.60 28.97 o 18 0 2 633.69 642.56 65.06 o 20 0 2 195.86 208.96 49.87 o -21 1 2 2.04 32.29 38.47 o -20 1 2 16.37 33.72 37.99 o -19 1 2 179.90 194.18 33.65 o -18 1 2 109.79 115.62 28.38 o -17 1 2 326.66 368.94 29.24 o -16 1 2 120.66 115.25 20.54 o -15 1 2 47.03 60.23 17.14 o -14 1 2 15.32 15.03 11.78 o -13 1 2 603.16 617.55 25.27 o -12 1 2 721.47 700.19 24.94 o -11 1 2 2773.51 2772.27 48.81 o -10 1 2 427.37 476.52 19.43 o -9 1 2 11.59 4.04 7.66 o -8 1 2 291.90 346.13 15.74 o -7 1 2 3025.76 3055.02 38.39 o -6 1 2 785.74 767.01 17.43 o -5 1 2 366.75 285.46 13.68 o -4 1 2 966.06 816.61 18.02 o -3 1 2 4516.61 5015.46 59.70 o -2 1 2 7677.14 8851.26 54.73 o -1 1 2 92.83 111.47 8.86 o 0 1 2 1761.87 1895.10 20.84 o 1 1 2 7702.17 8869.92 127.64 o 2 1 2 9466.34 10597.49 64.14 o 3 1 2 933.01 1095.94 23.38 o 4 1 2 303.45 267.09 10.27 o 5 1 2 2439.46 2680.75 49.70 o 6 1 2 30.12 25.25 7.65 o 7 1 2 2347.68 2189.48 61.21 o 8 1 2 683.94 756.15 31.88 o 9 1 2 808.50 773.26 28.38 o 10 1 2 228.09 230.02 15.45 o 11 1 2 1068.53 1042.44 31.33 o 12 1 2 102.83 117.83 18.48 o 13 1 2 1516.09 1502.75 43.13 o 14 1 2 0.06 16.08 14.14 o 15 1 2 177.23 202.99 23.13 o 16 1 2 25.74 30.21 16.88 o 17 1 2 27.68 64.84 20.36 o 18 1 2 66.06 75.18 26.36 o 19 1 2 113.75 127.92 52.00 o 20 1 2 35.46 31.47 25.52 o 21 1 2 0.46 1.82 25.50 o -21 2 2 20.59 -1.20 27.02 o -20 2 2 0.59 22.80 26.19 o -19 2 2 16.49 28.77 24.79 o -18 2 2 190.92 210.23 34.51 o -17 2 2 3.50 11.11 21.09 o -16 2 2 713.20 704.70 46.33 o -15 2 2 83.30 80.76 18.64 o -14 2 2 6.87 13.76 13.99 o -13 2 2 213.01 193.89 21.64 o -12 2 2 1940.35 1881.60 46.52 o -11 2 2 79.96 107.10 13.56 o -10 2 2 572.16 494.30 20.99 o -9 2 2 90.13 94.99 9.92 o -8 2 2 311.19 360.00 14.53 o -7 2 2 161.04 140.91 10.26 o -6 2 2 1431.01 1246.22 21.18 o -5 2 2 1973.63 2207.11 34.55 o -4 2 2 1099.58 891.91 20.34 o -3 2 2 1406.16 1558.28 28.81 o -2 2 2 34.95 62.94 11.89 o -1 2 2 286.81 350.31 20.12 o 0 2 2 1348.05 1264.95 37.33 o 1 2 2 0.01 1.20 6.72 o 2 2 2 4024.86 3949.97 90.47 o 3 2 2 700.98 647.25 18.90 o 4 2 2 1.84 8.73 6.56 o 5 2 2 537.28 581.56 15.41 o 6 2 2 11050.38 11887.47 130.52 o 7 2 2 504.59 498.35 16.33 o 8 2 2 10535.16 11611.21 102.37 o 9 2 2 427.43 423.04 25.12 o 10 2 2 74.93 80.98 16.08 o 11 2 2 10.42 4.91 12.12 o 12 2 2 2141.40 2196.07 52.60 o 13 2 2 145.90 127.07 20.28 o 14 2 2 29.54 42.37 16.80 o 15 2 2 274.47 256.07 26.56 o 16 2 2 417.91 379.07 31.35 o 17 2 2 0.77 -10.56 16.79 o 18 2 2 158.66 174.56 26.42 o 19 2 2 9.36 10.51 19.52 o 20 2 2 146.44 107.81 49.39 o -20 3 2 16.88 16.42 30.54 o -19 3 2 51.31 41.33 29.71 o -18 3 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