#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:02:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180947 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/27/2202766.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202766_Fobs loop_ _publ_author_name 'Lee, Clare' 'Harrison, William T. A.' _publ_section_title ; Piperidinium dihydrogenarsenate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m959 _journal_page_last m960 _journal_volume 59 _journal_year 2003 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.676 _cell_angle_gamma 90.000 _cell_length_a 8.6593 _cell_length_b 6.3233 _cell_length_c 8.9090 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.6612 _cod_data_source_file ng6000Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cl17 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 82.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -9 0 41.31 41.75 2.30 o 2 -9 0 33.73 37.65 3.39 o 3 -9 0 5.12 6.88 2.67 o 4 -9 0 41.55 48.23 3.80 o 0 -8 0 204.03 222.90 5.68 o 1 -8 0 34.51 33.07 2.01 o 2 -8 0 63.65 66.55 2.53 o 3 -8 0 86.38 86.85 2.74 o 4 -8 0 1.75 1.33 2.07 o 5 -8 0 76.49 81.25 3.00 o 6 -8 0 30.66 34.90 2.38 o 1 -7 0 176.52 173.41 4.53 o 2 -7 0 169.49 165.58 6.46 o 3 -7 0 21.50 21.84 1.74 o 4 -7 0 170.05 169.50 3.44 o 5 -7 0 19.09 18.09 1.91 o 6 -7 0 30.71 30.03 2.15 o 7 -7 0 72.92 75.08 3.45 o 8 -7 0 5.43 6.07 1.96 o 0 -6 0 554.90 583.03 7.60 o 1 -6 0 142.75 144.22 2.68 o 2 -6 0 127.88 126.85 2.57 o 3 -6 0 304.47 315.26 10.05 o 4 -6 0 1.62 1.62 1.33 o 5 -6 0 264.10 272.09 5.11 o 6 -6 0 156.21 161.65 3.38 o 7 -6 0 7.14 8.79 1.84 o 8 -6 0 91.84 92.57 3.08 o 9 -6 0 11.21 9.11 2.81 o 1 -5 0 366.18 375.32 7.47 o 2 -5 0 479.17 481.22 8.66 o 3 -5 0 70.40 66.01 1.86 o 4 -5 0 483.95 497.83 4.95 o 5 -5 0 27.28 26.41 1.61 o 6 -5 0 95.79 89.27 2.54 o 7 -5 0 194.68 200.86 3.90 o 8 -5 0 9.68 9.20 2.38 o 9 -5 0 84.25 89.42 4.50 o 10 -5 0 32.21 31.78 3.35 o 0 -4 0 1882.74 1900.54 13.83 o 1 -4 0 354.41 357.65 3.71 o 2 -4 0 517.90 497.48 8.49 o 3 -4 0 573.33 576.96 4.66 o 4 -4 0 124.26 123.84 5.49 o 5 -4 0 670.26 661.54 16.94 o 6 -4 0 178.41 183.58 3.80 o 7 -4 0 45.89 44.38 1.97 o 8 -4 0 138.23 147.82 4.83 o 9 -4 0 6.60 4.38 2.56 o 10 -4 0 46.75 54.82 3.93 o 1 -3 0 1980.86 1931.81 45.56 o 2 -3 0 445.73 431.21 5.15 o 3 -3 0 173.83 176.00 2.31 o 4 -3 0 739.14 740.89 6.45 o 5 -3 0 135.51 140.15 3.00 o 6 -3 0 406.69 410.19 6.61 o 7 -3 0 370.09 363.41 6.30 o 8 -3 0 4.25 2.82 2.17 o 9 -3 0 106.50 106.19 4.12 o 10 -3 0 57.44 56.05 3.59 o 11 -3 0 6.92 9.08 2.99 o 0 -2 0 3090.40 3169.36 19.45 o 1 -2 0 845.45 864.48 6.13 o 2 -2 0 357.64 363.45 6.71 o 3 -2 0 1092.22 1100.25 8.24 o 4 -2 0 12.56 16.38 1.00 o 5 -2 0 1147.68 1127.91 7.01 o 6 -2 0 784.30 765.37 8.35 o 7 -2 0 25.46 23.24 2.25 o 8 -2 0 352.60 342.85 6.26 o 9 -2 0 34.21 33.41 2.98 o 10 -2 0 96.61 97.68 4.43 o 11 -2 0 102.36 89.66 4.39 o 1 -1 0 1170.13 1243.30 22.82 o 2 -1 0 2449.45 2449.78 25.61 o 3 -1 0 792.80 848.76 3.88 o 4 -1 0 1410.39 1482.25 9.38 o 5 -1 0 864.07 874.26 9.82 o 6 -1 0 269.39 273.14 3.08 o 7 -1 0 773.02 774.80 10.51 o 8 -1 0 32.85 32.17 1.83 o 9 -1 0 176.71 164.86 4.78 o 10 -1 0 107.95 105.99 4.46 o 11 -1 0 5.97 7.74 2.76 o 12 -1 0 71.43 72.51 4.40 o 1 0 0 524.61 558.66 4.26 o 2 0 0 6804.01 6699.29 38.79 o 3 0 0 1045.67 987.55 19.28 o 4 0 0 9.09 7.06 0.58 o 5 0 0 2636.93 2749.84 35.88 o 6 0 0 1049.35 1131.65 20.01 o 7 0 0 326.47 341.97 3.18 o 8 0 0 161.90 165.43 2.43 o 9 0 0 2.94 3.04 2.22 o 10 0 0 22.05 24.56 2.72 o 11 0 0 113.78 122.65 4.90 o 12 0 0 3.09 -0.58 2.90 o 1 1 0 1176.92 1216.70 10.03 o 2 1 0 2698.88 2600.17 17.36 o 3 1 0 938.06 1010.62 7.69 o 4 1 0 1530.17 1558.17 6.52 o 5 1 0 747.19 801.72 5.65 o 6 1 0 270.20 264.06 2.54 o 7 1 0 715.44 719.03 4.82 o 8 1 0 32.23 30.61 1.45 o 9 1 0 187.97 189.36 2.86 o 10 1 0 94.01 94.23 2.83 o 11 1 0 7.12 6.09 2.76 o 12 1 0 61.53 58.46 3.90 o 1 2 0 783.16 813.87 4.30 o 2 2 0 225.81 237.09 1.83 o 3 2 0 894.85 938.65 7.77 o 4 2 0 13.89 15.98 1.43 o 5 2 0 1117.82 1101.89 9.63 o 6 2 0 780.16 767.72 6.84 o 7 2 0 28.17 25.87 1.27 o 8 2 0 344.86 324.76 6.69 o 9 2 0 33.61 37.05 1.72 o 10 2 0 98.11 102.42 2.55 o 11 2 0 106.90 103.36 3.31 o 1 3 0 1755.24 1810.86 22.24 o 2 3 0 487.64 453.67 4.91 o 3 3 0 164.32 158.71 3.11 o 4 3 0 744.61 726.81 7.32 o 5 3 0 126.62 127.31 3.33 o 6 3 0 385.05 388.25 5.93 o 7 3 0 383.10 376.05 3.56 o 8 3 0 5.57 4.66 1.18 o 9 3 0 125.12 120.12 2.44 o 10 3 0 59.91 60.67 2.17 o 0 4 0 1868.52 1818.27 12.87 o 1 4 0 382.98 388.11 3.32 o 2 4 0 517.22 512.37 11.11 o 3 4 0 655.86 627.62 5.17 o 4 4 0 123.90 119.52 3.38 o 5 4 0 690.56 618.06 7.52 o 6 4 0 167.84 166.81 4.31 o 7 4 0 38.29 35.09 2.83 o 8 4 0 144.74 145.74 2.61 o 9 4 0 9.58 10.52 1.34 o 10 4 0 52.25 52.15 2.09 o 1 5 0 406.47 394.72 3.73 o 2 5 0 507.31 495.85 5.33 o 3 5 0 81.45 76.79 1.83 o 4 5 0 505.97 488.82 8.25 o 5 5 0 22.90 20.68 2.46 o 6 5 0 92.62 85.17 3.60 o 7 5 0 186.30 190.13 5.17 o 8 5 0 9.39 10.99 1.45 o 9 5 0 78.84 82.56 2.36 o 10 5 0 31.34 32.59 1.96 o 0 6 0 580.19 570.17 7.16 o 1 6 0 147.40 147.88 2.68 o 2 6 0 127.60 128.96 2.59 o 3 6 0 308.48 313.74 11.46 o 4 6 0 2.03 2.38 1.39 o 5 6 0 269.38 273.62 5.95 o 6 6 0 162.78 173.82 5.18 o 7 6 0 5.42 4.50 2.84 o 8 6 0 90.60 89.58 4.35 o 9 6 0 11.31 11.60 1.61 o 1 7 0 166.54 168.15 3.11 o 2 7 0 169.70 170.05 5.61 o 3 7 0 18.64 20.20 1.82 o 4 7 0 168.41 169.74 5.10 o 5 7 0 22.09 19.73 3.02 o 6 7 0 28.14 26.81 3.28 o 7 7 0 75.59 82.95 4.67 o 8 7 0 5.14 5.67 2.93 o 0 8 0 205.44 208.76 5.30 o 1 8 0 33.00 29.74 2.14 o 2 8 0 60.42 60.30 2.48 o 3 8 0 77.06 78.33 4.08 o 4 8 0 2.00 2.04 2.94 o 5 8 0 77.33 79.51 4.41 o 6 8 0 31.59 37.78 3.80 o 1 9 0 41.95 38.61 2.42 o 2 9 0 33.34 34.12 3.76 o 3 9 0 6.77 7.64 3.15 o 4 9 0 41.30 41.92 3.98 o -4 -9 1 30.99 31.58 3.27 o -3 -9 1 0.99 0.24 2.54 o -2 -9 1 59.91 57.96 3.76 o -1 -9 1 38.98 36.87 3.22 o 0 -9 1 10.42 9.21 2.61 o 1 -9 1 52.28 53.93 3.62 o 2 -9 1 5.16 5.76 2.70 o 3 -9 1 22.54 23.44 3.41 o -6 -8 1 44.89 47.16 2.54 o -5 -8 1 53.78 56.21 2.66 o -4 -8 1 12.16 12.55 1.76 o -3 -8 1 123.63 126.29 3.17 o -2 -8 1 6.45 6.17 2.01 o -1 -8 1 102.55 101.68 2.82 o 0 -8 1 135.35 136.01 3.18 o 1 -8 1 1.06 -1.16 1.40 o 2 -8 1 105.89 107.42 4.42 o 3 -8 1 31.57 33.19 3.20 o 4 -8 1 28.80 28.00 3.28 o 5 -8 1 63.13 64.24 3.84 o 6 -8 1 11.37 13.89 2.93 o -8 -7 1 25.42 26.53 2.38 o -7 -7 1 92.37 95.36 3.24 o -6 -7 1 6.79 7.94 2.16 o -5 -7 1 48.44 50.17 3.47 o -4 -7 1 126.37 122.07 2.93 o -3 -7 1 3.31 4.38 2.01 o -2 -7 1 322.68 309.71 6.01 o -1 -7 1 100.28 102.10 2.61 o 0 -7 1 48.32 46.68 2.21 o 1 -7 1 185.52 183.29 3.24 o 2 -7 1 46.32 45.77 1.95 o 3 -7 1 136.35 139.53 3.00 o 4 -7 1 194.45 196.90 3.68 o 5 -7 1 8.44 8.59 1.72 o 6 -7 1 67.38 70.74 2.74 o 7 -7 1 32.88 32.39 3.49 o -9 -6 1 56.73 60.33 2.96 o -8 -6 1 49.68 53.75 3.88 o -7 -6 1 18.96 18.21 1.91 o -6 -6 1 132.90 137.66 3.19 o -5 -6 1 91.23 93.55 2.60 o -4 -6 1 36.25 34.98 1.75 o -3 -6 1 266.23 265.63 10.19 o -2 -6 1 18.62 18.05 1.49 o -1 -6 1 219.81 218.36 5.23 o 0 -6 1 334.12 325.73 9.94 o 1 -6 1 49.94 48.36 1.78 o 2 -6 1 218.90 209.88 3.18 o 3 -6 1 219.26 213.92 3.31 o 4 -6 1 46.00 43.83 1.99 o 5 -6 1 284.16 290.94 4.30 o 6 -6 1 76.11 77.39 2.70 o 7 -6 1 41.10 40.68 2.30 o 8 -6 1 88.98 88.97 4.64 o -10 -5 1 55.68 51.46 3.97 o -9 -5 1 46.82 48.35 3.70 o -8 -5 1 44.80 46.89 2.39 o -7 -5 1 353.19 348.11 5.46 o -6 -5 1 76.07 71.96 3.36 o -5 -5 1 239.95 233.37 3.55 o -4 -5 1 439.85 434.64 4.54 o -3 -5 1 19.08 17.00 1.56 o -2 -5 1 903.25 900.63 9.05 o -1 -5 1 441.49 448.22 14.52 o 0 -5 1 141.91 146.13 4.66 o 1 -5 1 608.53 622.62 10.58 o 2 -5 1 28.34 27.00 1.33 o 3 -5 1 342.90 347.68 3.95 o 4 -5 1 307.67 315.54 3.96 o 5 -5 1 2.35 1.54 1.38 o 6 -5 1 159.18 166.11 3.30 o 7 -5 1 63.27 60.13 2.35 o 8 -5 1 12.81 13.18 2.59 o 9 -5 1 64.57 62.73 4.02 o -11 -4 1 43.27 45.63 3.88 o -10 -4 1 18.23 20.44 3.17 o -9 -4 1 55.13 55.68 3.64 o -8 -4 1 201.34 212.59 3.90 o -7 -4 1 16.35 15.87 1.57 o -6 -4 1 353.53 373.02 11.14 o -5 -4 1 593.00 596.68 5.24 o -4 -4 1 21.11 19.29 1.24 o -3 -4 1 1271.72 1299.23 20.95 o -2 -4 1 286.31 283.87 14.96 o -1 -4 1 995.28 1021.22 9.80 o 0 -4 1 1331.25 1331.13 10.05 o 1 -4 1 134.35 133.57 2.05 o 2 -4 1 661.31 689.84 5.08 o 3 -4 1 459.34 469.08 4.20 o 4 -4 1 292.83 288.87 5.37 o 5 -4 1 569.86 589.03 8.48 o 6 -4 1 36.40 37.16 1.80 o 7 -4 1 53.89 54.16 3.11 o 8 -4 1 96.25 103.39 4.32 o 9 -4 1 1.12 1.43 2.49 o 10 -4 1 70.76 74.06 4.44 o -11 -3 1 0.57 0.28 2.65 o -10 -3 1 151.27 160.97 5.38 o -9 -3 1 62.16 68.33 3.68 o -8 -3 1 133.46 134.86 4.33 o -7 -3 1 533.29 528.85 29.95 o -6 -3 1 232.04 235.41 3.28 o -5 -3 1 459.82 470.37 4.30 o -4 -3 1 872.13 874.97 5.83 o -3 -3 1 170.77 183.39 2.33 o -2 -3 1 1022.90 991.91 34.07 o -1 -3 1 1172.48 1165.05 7.20 o 0 -3 1 116.67 117.00 2.25 o 1 -3 1 1502.97 1492.86 18.35 o 2 -3 1 196.87 199.51 3.29 o 3 -3 1 537.31 540.93 11.38 o 4 -3 1 523.69 512.03 4.39 o 5 -3 1 40.10 36.21 1.47 o 6 -3 1 271.76 275.24 5.34 o 7 -3 1 204.98 206.04 4.98 o 8 -3 1 38.01 35.75 2.76 o 9 -3 1 128.59 136.52 4.92 o 10 -3 1 13.62 13.75 3.08 o 11 -3 1 15.31 16.41 3.20 o -12 -2 1 25.56 22.97 3.11 o -11 -2 1 114.72 113.16 4.91 o -10 -2 1 12.92 13.07 2.59 o -9 -2 1 118.59 116.09 4.19 o -8 -2 1 299.24 286.33 5.64 o -7 -2 1 17.41 18.10 2.05 o -6 -2 1 1027.38 1000.13 13.30 o -5 -2 1 540.83 563.67 4.53 o -4 -2 1 141.95 147.90 1.60 o -3 -2 1 946.68 976.82 4.45 o -2 -2 1 553.56 544.72 2.72 o -1 -2 1 1444.50 1469.48 18.28 o 0 -2 1 3269.82 3195.12 48.01 o 1 -2 1 561.42 622.57 7.32 o 2 -2 1 538.78 543.56 4.85 o 3 -2 1 798.98 855.45 5.75 o 4 -2 1 166.95 180.95 7.45 o 5 -2 1 1705.72 1793.18 14.30 o 6 -2 1 311.13 308.04 5.30 o 7 -2 1 202.35 196.38 4.63 o 8 -2 1 241.16 221.03 5.14 o 9 -2 1 4.48 7.18 2.21 o 10 -2 1 133.94 131.65 5.14 o 11 -2 1 61.95 58.12 3.91 o -12 -1 1 78.69 81.03 4.52 o -11 -1 1 1.35 1.50 2.56 o -10 -1 1 130.29 130.05 4.42 o -9 -1 1 76.08 76.30 3.54 o -8 -1 1 73.75 68.86 3.00 o -7 -1 1 1147.16 1174.39 13.98 o -6 -1 1 241.10 252.38 4.43 o -5 -1 1 1366.20 1391.97 20.26 o -4 -1 1 655.71 663.64 9.72 o -3 -1 1 623.59 687.95 5.74 o -2 -1 1 3670.82 3656.27 12.70 o -1 -1 1 5673.74 5595.96 29.87 o 0 -1 1 2718.33 2464.83 56.70 o 1 -1 1 5365.31 5298.96 22.59 o 2 -1 1 132.32 163.63 2.65 o 3 -1 1 1408.15 1409.81 14.07 o 4 -1 1 1571.39 1602.14 35.46 o 5 -1 1 38.08 38.02 1.43 o 6 -1 1 925.57 942.13 6.53 o 7 -1 1 233.82 234.40 8.36 o 8 -1 1 67.88 67.71 3.71 o 9 -1 1 162.57 158.14 4.76 o 10 -1 1 41.21 36.67 2.92 o 11 -1 1 25.79 26.73 3.36 o -12 0 1 11.35 9.74 2.97 o -11 0 1 107.93 107.77 4.63 o -10 0 1 9.92 8.56 2.13 o -9 0 1 149.53 149.46 3.08 o -8 0 1 144.10 149.88 2.26 o -7 0 1 5.07 6.59 1.51 o -6 0 1 828.34 829.71 8.71 o -5 0 1 987.08 996.79 4.16 o -4 0 1 500.64 495.80 3.44 o -3 0 1 1896.41 1772.78 10.61 o -2 0 1 263.67 262.18 1.81 o -1 0 1 1553.84 1641.95 22.87 o 0 0 1 4511.99 4310.58 87.20 o 1 0 1 803.45 796.59 4.15 o 2 0 1 3964.63 3970.40 18.23 o 3 0 1 427.65 410.77 9.08 o 4 0 1 544.39 634.23 15.02 o 5 0 1 1414.81 1410.46 6.58 o 6 0 1 522.62 504.68 3.73 o 7 0 1 170.24 176.40 2.93 o 8 0 1 357.68 339.08 12.38 o 9 0 1 1.21 1.44 1.44 o 10 0 1 101.51 92.74 4.17 o 11 0 1 73.10 75.05 4.32 o -12 1 1 75.60 75.10 4.46 o -11 1 1 1.68 1.89 1.83 o -10 1 1 115.44 121.73 3.22 o -9 1 1 85.61 86.20 2.06 o -8 1 1 62.98 63.22 1.68 o -7 1 1 1186.22 1168.89 6.21 o -6 1 1 246.89 244.31 2.04 o -5 1 1 1330.55 1374.09 12.86 o -4 1 1 646.24 632.19 3.94 o -3 1 1 616.08 665.74 35.60 o -2 1 1 3645.31 3684.79 20.77 o -1 1 1 5793.01 5679.78 21.58 o 0 1 1 2760.02 2538.02 41.10 o 1 1 1 5029.46 5279.33 31.15 o 2 1 1 116.04 139.44 2.22 o 3 1 1 1293.45 1336.40 10.58 o 4 1 1 1558.36 1604.50 6.85 o 5 1 1 36.10 36.75 1.17 o 6 1 1 897.89 918.07 5.34 o 7 1 1 191.61 197.31 2.60 o 8 1 1 61.17 60.64 1.78 o 9 1 1 148.11 152.47 3.87 o 10 1 1 44.00 45.06 3.35 o 11 1 1 25.53 30.31 3.39 o -12 2 1 22.93 24.79 2.37 o -11 2 1 117.67 125.83 3.66 o -10 2 1 18.48 18.80 1.97 o -9 2 1 130.06 122.35 2.78 o -8 2 1 302.70 294.66 3.17 o -7 2 1 16.54 19.44 1.11 o -6 2 1 972.24 972.98 6.15 o -5 2 1 660.88 637.91 4.30 o -4 2 1 91.77 99.11 1.55 o -3 2 1 1210.88 1149.83 5.77 o -2 2 1 542.56 521.08 3.21 o -1 2 1 1366.42 1336.21 27.03 o 0 2 1 3236.08 3140.55 13.61 o 1 2 1 562.12 621.98 5.32 o 2 2 1 592.77 547.83 5.10 o 3 2 1 788.40 838.42 7.46 o 4 2 1 208.56 212.77 3.71 o 5 2 1 1604.28 1641.98 20.37 o 6 2 1 297.25 290.70 4.26 o 7 2 1 186.27 180.68 2.50 o 8 2 1 243.12 238.54 3.07 o 9 2 1 3.52 2.50 1.38 o 10 2 1 133.82 134.66 3.86 o 11 2 1 56.40 59.83 3.93 o -11 3 1 0.46 1.00 1.84 o -10 3 1 161.89 154.70 3.66 o -9 3 1 68.94 68.36 1.97 o -8 3 1 151.07 144.54 2.41 o -7 3 1 528.03 528.58 7.13 o -6 3 1 219.00 225.94 4.44 o -5 3 1 427.81 429.42 19.03 o -4 3 1 857.04 844.93 24.67 o -3 3 1 171.22 170.17 2.42 o -2 3 1 1010.52 957.33 4.12 o -1 3 1 1056.09 1071.06 18.47 o 0 3 1 66.53 70.92 0.97 o 1 3 1 1322.70 1309.09 9.81 o 3 3 1 513.25 499.93 5.67 o 4 3 1 558.39 539.20 6.47 o 5 3 1 39.18 43.80 2.46 o 6 3 1 250.96 246.25 2.76 o 7 3 1 209.00 200.95 2.67 o 8 3 1 35.46 35.38 1.54 o 9 3 1 146.42 149.41 2.77 o 10 3 1 12.90 14.26 1.69 o 11 3 1 19.82 18.79 2.07 o -11 4 1 40.51 41.24 2.59 o -10 4 1 18.91 19.14 1.65 o -9 4 1 54.22 54.16 2.06 o -8 4 1 204.11 207.09 5.24 o -7 4 1 18.55 20.56 2.38 o -6 4 1 353.70 360.38 5.95 o -5 4 1 559.02 570.65 7.19 o -4 4 1 5.46 3.74 1.28 o -3 4 1 1281.28 1270.97 16.51 o -2 4 1 275.19 275.60 2.73 o -1 4 1 1035.54 1028.17 6.02 o 0 4 1 1263.36 1291.41 6.57 o 1 4 1 132.81 131.51 1.77 o 2 4 1 607.59 629.57 6.88 o 3 4 1 501.86 478.33 5.94 o 4 4 1 296.93 300.51 5.22 o 5 4 1 592.41 604.72 7.93 o 6 4 1 36.81 37.23 2.71 o 7 4 1 46.68 46.79 1.66 o 8 4 1 103.83 101.37 2.76 o 9 4 1 1.71 2.83 1.32 o 10 4 1 76.32 81.88 3.08 o -10 5 1 53.41 54.00 2.18 o -9 5 1 43.31 39.91 1.89 o -8 5 1 42.97 48.53 3.40 o -7 5 1 338.51 347.02 6.69 o -6 5 1 83.22 80.25 3.54 o -5 5 1 240.84 231.88 5.01 o -4 5 1 469.21 460.33 22.12 o -3 5 1 19.86 17.67 1.31 o -2 5 1 948.43 934.84 24.91 o -1 5 1 457.77 439.93 11.71 o 0 5 1 159.42 158.56 5.76 o 1 5 1 688.27 698.32 12.58 o 2 5 1 16.15 19.32 1.41 o 3 5 1 393.81 393.55 17.09 o 4 5 1 312.02 302.20 5.55 o 5 5 1 1.91 3.61 2.26 o 6 5 1 165.49 164.96 4.76 o 7 5 1 58.90 59.32 1.89 o 8 5 1 14.60 14.19 1.48 o 9 5 1 62.41 61.73 2.17 o -9 6 1 53.85 59.28 3.96 o -8 6 1 51.90 55.38 3.96 o -7 6 1 19.26 19.80 3.17 o -6 6 1 132.77 128.05 4.35 o -5 6 1 91.15 87.99 3.73 o -4 6 1 33.52 38.26 3.05 o -3 6 1 294.13 288.56 5.22 o -2 6 1 9.18 8.26 1.38 o -1 6 1 256.85 240.91 3.25 o 0 6 1 312.68 307.26 3.69 o 1 6 1 48.64 48.96 1.95 o 2 6 1 218.24 214.65 3.27 o 3 6 1 223.47 219.96 3.75 o 4 6 1 54.54 50.42 1.99 o 5 6 1 281.48 281.25 6.15 o 6 6 1 72.40 68.81 3.71 o 7 6 1 33.28 33.50 3.26 o 8 6 1 89.15 89.51 2.43 o -8 7 1 26.19 23.65 3.66 o -7 7 1 90.54 98.81 4.80 o -6 7 1 5.03 3.77 2.82 o -5 7 1 49.89 55.37 3.68 o -4 7 1 108.60 111.04 4.36 o -3 7 1 3.47 2.05 2.50 o -2 7 1 299.87 294.65 3.96 o -1 7 1 103.18 100.45 3.48 o 0 7 1 41.53 41.29 1.99 o 1 7 1 180.33 177.05 4.20 o 2 7 1 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