#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/27/2202776.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202776_Fobs loop_ _publ_author_name 'Sakai, Ken' 'Ishigami, Eri' 'Yokokawa, Kazuo' 'Kajiwara, Takashi' 'Ito, Tasuku' _publ_section_title ; Di-\m-pivalato-bis[cis-diammineplatinum(II)] sulfate monohydrate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m443 _journal_page_last m445 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.850 _cell_angle_beta 88.835 _cell_angle_gamma 75.852 _cell_length_a 6.7043 _cell_length_b 10.6717 _cell_length_c 16.1002 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.7674 _[local]_cod_data_source_file ob6253Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sakai43 in P-1 2003/05/23 11:17:58 019 KENX' _shelx_refln_list_code 4 _shelx_f_calc_maximum 298.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8342.39 10089.18 208.35 o 2 0 0 10711.56 13046.11 301.30 o 3 0 0 9106.70 10571.10 341.64 o 4 0 0 32.50 -57.09 124.77 o 5 0 0 20516.23 20620.67 531.54 o 6 0 0 4563.66 4750.27 407.53 o 7 0 0 87.12 81.60 291.71 o 8 0 0 4057.03 3449.18 615.53 o -8 1 0 8544.55 7643.82 664.43 o -7 1 0 1846.52 1948.77 375.72 o -6 1 0 4528.23 4751.96 442.59 o -5 1 0 55.23 28.73 178.68 o -4 1 0 2.03 -124.93 149.30 o -3 1 0 39541.84 43304.59 694.55 o -2 1 0 24341.05 26435.21 448.35 o -1 1 0 2025.86 2009.50 124.94 o 0 1 0 12164.59 11567.66 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