#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:02:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180947 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/27/2202777.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202777_Fobs loop_ _publ_author_name 'Sakai, Ken' 'Osada, Manabu' 'Yokoyama, Yoshimi' 'Tomita, Yasushi' 'Tsubomura, Taro' _publ_section_title ; (2,2'-Bipyridine)bis(N-methyl-4,4'-bipyridinium)platinum(II) tetraperchlorate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m512 _journal_page_last m514 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.835 _cell_angle_gamma 90.000 _cell_length_a 10.0690 _cell_length_b 35.1115 _cell_length_c 11.7298 _exptl_crystal_F_000 2152.00 _reflns_d_resolution_high 0.7498 _cod_data_source_file ob6254Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' osada7 in P2(1)/n 2003/06/09 16:50:45 050 KENX' _shelx_refln_list_code 4 _shelx_f_calc_maximum 539.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6583.14 5955.06 79.33 o 4 0 0 514.66 688.32 54.95 o 6 0 0 31785.42 35270.08 562.35 o 8 0 0 10955.11 12095.79 399.25 o 10 0 0 5206.68 5603.12 327.87 o 12 0 0 128.58 117.39 131.64 o 2 1 0 8263.38 10127.62 490.81 o 3 1 0 106309.81 129909.00 7110.27 o 4 1 0 859.57 942.05 43.92 o 5 1 0 38894.19 37261.50 2308.37 o 6 1 0 486.94 611.62 90.82 o 7 1 0 4768.88 4978.37 173.46 o 8 1 0 295.00 353.26 73.28 o 9 1 0 2839.16 2501.23 157.92 o 10 1 0 26.78 115.34 76.07 o 11 1 0 2437.45 2328.76 184.59 o 12 1 0 441.60 395.58 171.31 o 1 2 0 36291.41 30765.64 292.85 o 2 2 0 8865.47 10017.88 750.05 o 3 2 0 632.21 502.69 69.22 o 4 2 0 8100.56 8019.01 1030.66 o 5 2 0 11502.59 11369.39 559.35 o 6 2 0 23214.85 23039.35 1139.74 o 7 2 0 5717.67 5402.88 278.00 o 8 2 0 6274.54 6820.89 385.24 o 9 2 0 1332.92 1367.80 126.34 o 10 2 0 1472.12 1625.99 142.93 o 11 2 0 13.97 42.13 75.55 o 12 2 0 46.50 23.56 131.74 o 1 3 0 144.58 215.44 11.09 o 2 3 0 15298.76 18786.18 498.41 o 3 3 0 4550.66 4426.79 269.72 o 4 3 0 32637.71 35011.98 2350.04 o 5 3 0 2664.63 2627.92 290.79 o 6 3 0 5128.53 5586.20 203.28 o 7 3 0 923.35 978.61 92.18 o 8 3 0 226.83 308.52 75.43 o 9 3 0 375.82 273.53 78.23 o 10 3 0 3487.87 3008.93 203.51 o 11 3 0 261.92 319.70 105.76 o 12 3 0 1813.75 1797.15 180.34 o 0 4 0 114.24 63.15 13.59 o 1 4 0 76235.81 86730.32 1890.21 o 2 4 0 122270.33 146523.92 3730.37 o 3 4 0 23274.91 26715.73 908.90 o 4 4 0 3065.12 3009.95 253.23 o 5 4 0 1987.83 2276.11 97.05 o 6 4 0 2546.54 2964.98 103.17 o 7 4 0 22246.30 23323.54 666.74 o 8 4 0 968.91 883.68 99.08 o 9 4 0 8404.36 9178.48 322.52 o 10 4 0 0.82 1.45 70.84 o 11 4 0 1698.63 1710.93 170.19 o 12 4 0 13.46 87.50 93.59 o 1 5 0 727.87 1632.30 66.50 o 2 5 0 9898.83 11253.53 339.75 o 3 5 0 1777.69 2154.95 70.36 o 4 5 0 41490.36 46382.48 1526.32 o 5 5 0 3825.63 4100.74 239.78 o 6 5 0 21943.00 26230.83 855.01 o 7 5 0 189.88 283.02 54.19 o 8 5 0 435.97 551.72 72.74 o 9 5 0 258.79 327.22 70.46 o 10 5 0 2090.11 1931.07 164.96 o 11 5 0 1345.02 1508.40 158.67 o 12 5 0 3235.12 3111.24 227.74 o 0 6 0 8208.52 9364.29 138.75 o 1 6 0 27750.20 32069.77 813.08 o 2 6 0 409.48 372.32 18.42 o 3 6 0 12914.14 13714.51 480.02 o 4 6 0 82.76 26.89 16.05 o 5 6 0 171.99 228.18 23.15 o 6 6 0 2763.28 2679.68 188.01 o 7 6 0 12839.11 13719.67 326.85 o 8 6 0 7424.40 7695.29 231.34 o 9 6 0 6842.09 7173.75 265.73 o 10 6 0 1186.49 1336.81 146.28 o 11 6 0 1228.40 1240.41 152.18 o 12 6 0 26.82 34.73 93.03 o 13 6 0 144.51 202.87 150.94 o 1 7 0 565.91 372.45 21.45 o 2 7 0 631.68 558.54 21.20 o 3 7 0 4706.52 6205.21 184.65 o 4 7 0 20104.19 20172.29 655.95 o 5 7 0 17831.47 18972.50 720.40 o 6 7 0 1773.41 1594.82 95.32 o 7 7 0 1394.97 1736.77 97.30 o 8 7 0 416.64 503.74 72.31 o 9 7 0 69.60 151.98 77.06 o 10 7 0 823.03 733.26 162.45 o 11 7 0 3339.67 2987.29 209.60 o 12 7 0 352.36 376.65 169.10 o 0 8 0 15749.48 16081.52 1218.42 o 1 8 0 5311.42 5453.98 167.67 o 2 8 0 44972.80 44885.55 747.02 o 3 8 0 12818.07 13831.11 424.82 o 4 8 0 465.87 314.71 25.74 o 5 8 0 70.41 71.35 20.60 o 6 8 0 5795.65 6170.53 265.99 o 7 8 0 151.28 146.74 48.15 o 8 8 0 15972.05 16118.35 365.65 o 9 8 0 153.98 207.76 85.71 o 10 8 0 1436.44 1639.21 160.37 o 11 8 0 4.28 13.48 82.70 o 12 8 0 0.84 17.71 89.26 o 1 9 0 50486.25 57037.60 1125.57 o 2 9 0 861.17 781.25 78.73 o 3 9 0 20421.98 21522.37 605.68 o 4 9 0 9799.89 10010.56 322.97 o 5 9 0 31937.35 34482.59 937.81 o 6 9 0 7438.90 7764.84 163.73 o 7 9 0 563.23 655.06 69.07 o 8 9 0 183.67 328.94 86.15 o 9 9 0 101.49 131.96 79.42 o 10 9 0 1202.81 1111.84 180.54 o 11 9 0 3125.15 3006.19 295.83 o 12 9 0 203.76 105.06 97.74 o 0 10 0 56063.68 56404.25 4545.80 o 1 10 0 34946.38 37660.66 468.52 o 2 10 0 21905.05 24630.54 399.72 o 3 10 0 1902.33 2120.00 72.79 o 4 10 0 184.67 291.12 25.02 o 5 10 0 2298.85 2363.98 98.06 o 6 10 0 10057.28 9747.51 358.37 o 7 10 0 11852.14 11439.66 292.06 o 8 10 0 5612.40 5940.72 243.48 o 9 10 0 5180.09 5012.10 232.19 o 10 10 0 2256.89 2216.44 179.49 o 11 10 0 374.90 467.47 117.44 o 12 10 0 1.31 9.71 86.70 o 1 11 0 5308.40 6456.66 175.24 o 2 11 0 45696.57 46090.03 950.14 o 3 11 0 6021.87 5615.82 163.63 o 4 11 0 39386.87 41256.30 961.61 o 5 11 0 12148.45 11926.29 366.12 o 6 11 0 13619.59 14472.12 920.58 o 7 11 0 708.70 778.14 100.89 o 8 11 0 45.47 78.57 81.16 o 9 11 0 1144.73 1224.18 135.42 o 10 11 0 2274.13 2223.45 180.94 o 11 11 0 311.12 355.44 113.47 o 12 11 0 2231.07 2310.26 208.11 o 0 12 0 4707.90 5341.99 554.68 o 1 12 0 21259.91 23188.08 383.75 o 2 12 0 2511.43 3683.19 182.90 o 3 12 0 7449.22 7722.66 174.30 o 4 12 0 4683.97 4148.79 155.61 o 5 12 0 8871.41 8821.77 232.81 o 6 12 0 1461.82 1440.05 135.36 o 7 12 0 22329.34 23185.34 1078.23 o 8 12 0 422.96 449.74 94.36 o 9 12 0 8828.15 8777.81 301.96 o 10 12 0 111.98 190.83 96.19 o 11 12 0 253.94 317.05 112.96 o 12 12 0 35.81 110.57 99.60 o 1 13 0 1916.96 1896.71 132.64 o 2 13 0 26126.59 27239.37 335.65 o 3 13 0 6482.28 5393.15 404.88 o 4 13 0 39423.58 42233.07 1069.90 o 5 13 0 132.25 165.66 32.21 o 6 13 0 7425.59 7666.26 180.90 o 7 13 0 109.28 244.55 60.46 o 8 13 0 209.19 229.94 85.10 o 9 13 0 367.60 462.93 134.70 o 10 13 0 1873.05 1903.23 174.67 o 11 13 0 305.59 280.67 111.55 o 12 13 0 1969.02 2151.04 243.85 o 0 14 0 22728.50 26111.33 729.45 o 1 14 0 31272.59 33379.16 589.55 o 2 14 0 11298.73 9306.91 228.39 o 3 14 0 2144.99 1818.10 64.29 o 4 14 0 129.35 146.68 31.55 o 5 14 0 82.92 119.96 32.76 o 6 14 0 6188.93 6391.33 320.85 o 7 14 0 4156.55 3559.14 140.76 o 8 14 0 10125.78 9217.83 293.32 o 9 14 0 4039.47 4235.55 218.70 o 10 14 0 792.30 884.74 132.52 o 11 14 0 313.43 414.38 157.41 o 12 14 0 23.27 60.05 128.33 o 1 15 0 24883.60 23555.18 355.48 o 2 15 0 4229.11 3728.54 117.08 o 3 15 0 45148.07 48985.10 816.44 o 4 15 0 188.88 346.43 42.86 o 5 15 0 28363.71 27613.64 691.18 o 6 15 0 3007.34 3480.63 132.62 o 7 15 0 57.68 101.19 54.92 o 8 15 0 17.03 5.88 63.46 o 9 15 0 650.19 630.95 176.73 o 10 15 0 104.69 165.74 94.93 o 11 15 0 2115.22 1893.21 184.43 o 0 16 0 69734.34 71238.40 3775.33 o 1 16 0 204.62 38.15 50.46 o 2 16 0 12415.17 12807.97 258.60 o 3 16 0 10551.72 10114.55 311.34 o 4 16 0 1680.91 1833.98 70.51 o 5 16 0 227.38 237.16 40.74 o 6 16 0 12041.00 11683.42 538.18 o 7 16 0 143.89 193.94 60.84 o 8 16 0 7569.92 7329.81 267.45 o 9 16 0 16.77 -9.19 74.44 o 10 16 0 4420.41 4207.11 238.67 o 11 16 0 29.32 43.36 90.61 o 1 17 0 15666.39 17707.25 283.64 o 2 17 0 8951.93 9838.29 323.08 o 3 17 0 30451.47 29526.37 463.27 o 4 17 0 3029.70 2696.18 114.46 o 5 17 0 20645.27 19631.21 576.09 o 6 17 0 2023.38 2250.08 113.48 o 7 17 0 12349.28 12807.48 395.73 o 8 17 0 23.23 20.68 74.54 o 9 17 0 904.59 849.17 196.62 o 10 17 0 270.98 282.87 106.60 o 11 17 0 1964.87 1649.85 173.36 o 0 18 0 15990.79 16897.43 1062.82 o 1 18 0 15127.70 14737.52 273.48 o 2 18 0 7783.55 7144.96 122.40 o 3 18 0 3174.01 3673.11 94.73 o 4 18 0 2850.06 3352.52 96.21 o 5 18 0 2817.20 2756.51 167.61 o 6 18 0 2067.60 1924.33 156.75 o 7 18 0 2602.28 2762.11 222.37 o 8 18 0 5382.37 4985.90 228.90 o 9 18 0 959.56 953.36 133.59 o 10 18 0 1087.35 1236.90 155.20 o 11 18 0 44.02 133.28 102.01 o 1 19 0 2867.81 3522.74 174.60 o 2 19 0 2751.25 2387.56 94.85 o 3 19 0 109.97 184.13 36.21 o 4 19 0 13591.11 13551.39 187.50 o 5 19 0 7512.65 7446.09 155.74 o 6 19 0 2753.61 2302.54 118.62 o 7 19 0 99.47 97.95 54.88 o 8 19 0 66.78 198.32 85.99 o 9 19 0 2.44 74.34 82.25 o 10 19 0 2070.46 1763.62 170.82 o 11 19 0 547.76 533.01 131.32 o 0 20 0 875.41 866.71 150.98 o 1 20 0 30467.27 32058.44 358.15 o 2 20 0 1180.46 1368.99 94.99 o 3 20 0 3213.11 3190.99 93.87 o 4 20 0 158.13 180.24 69.97 o 5 20 0 2613.67 2811.92 99.73 o 6 20 0 143.02 141.46 56.58 o 7 20 0 3797.13 3651.44 152.88 o 8 20 0 2.31 99.40 73.76 o 9 20 0 4021.10 3953.75 223.34 o 10 20 0 8.16 47.92 82.99 o 11 20 0 438.59 495.57 130.69 o 2 21 0 11023.47 10987.13 161.24 o 3 21 0 3588.49 3502.28 230.04 o 4 21 0 36988.39 35548.42 764.98 o 5 21 0 4496.15 4348.51 218.66 o 6 21 0 7977.39 8136.46 288.94 o 7 21 0 833.90 900.52 92.32 o 8 21 0 73.46 172.82 84.19 o 9 21 0 42.78 24.40 83.28 o 10 21 0 1931.55 1769.08 175.73 o 11 21 0 311.13 352.74 122.72 o 0 22 0 3180.78 3182.35 185.13 o 1 22 0 19236.26 19292.50 425.94 o 2 22 0 3709.45 4127.28 250.43 o 3 22 0 6602.41 6503.68 236.52 o 4 22 0 411.48 537.98 82.14 o 5 22 0 3035.66 2848.56 102.87 o 6 22 0 2428.96 2722.59 268.66 o 7 22 0 3835.97 4159.79 166.33 o 8 22 0 1538.59 1317.27 140.47 o 9 22 0 4442.41 3915.97 227.48 o 10 22 0 764.88 711.49 133.50 o 11 22 0 348.27 339.61 175.74 o 1 23 0 127.93 264.39 61.07 o 2 23 0 6239.42 5867.85 222.71 o 3 23 0 19155.86 18551.07 598.21 o 4 23 0 8834.91 8780.68 266.87 o 5 23 0 1121.42 1000.53 73.17 o 6 23 0 1659.39 1600.08 110.14 o 7 23 0 2118.94 2199.42 131.38 o 8 23 0 42.47 84.65 79.91 o 9 23 0 1582.46 1349.94 153.61 o 10 23 0 422.30 444.28 116.13 o 0 24 0 23162.22 22211.49 303.52 o 1 24 0 1062.93 1050.94 72.01 o 2 24 0 7152.79 6675.35 137.86 o 3 24 0 29.62 13.60 78.14 o 4 24 0 247.14 306.28 49.90 o 5 24 0 36.99 40.60 49.68 o 6 24 0 6597.12 6232.31 341.46 o 7 24 0 0.84 23.58 59.49 o 8 24 0 3260.53 2992.22 190.38 o 9 24 0 13.54 36.58 79.93 o 10 24 0 924.56 934.89 146.09 o 1 25 0 3583.98 3906.71 155.35 o 2 25 0 1099.20 1157.39 126.42 o 3 25 0 16070.59 15998.27 218.96 o 4 25 0 2372.30 2280.46 144.57 o 5 25 0 7124.34 6879.90 192.84 o 6 25 0 2632.30 2242.42 153.81 o 7 25 0 204.02 259.91 76.06 o 8 25 0 70.20 72.77 80.69 o 9 25 0 419.66 343.24 109.54 o 10 25 0 343.62 212.58 139.61 o 0 26 0 16353.02 14993.91 426.60 o 1 26 0 14544.72 13278.19 212.03 o 2 26 0 7054.94 6900.42 146.34 o 3 26 0 1213.39 1466.92 114.18 o 4 26 0 31.45 88.89 44.98 o 5 26 0 772.10 1031.55 94.42 o 6 26 0 1538.76 1657.37 141.03 o 7 26 0 2823.76 2594.23 144.23 o 8 26 0 3006.27 3278.53 204.38 o 9 26 0 1033.49 914.73 139.69 o 10 26 0 1112.52 1215.35 164.32 o 1 27 0 723.80 1513.93 87.45 o 2 27 0 8894.33 9046.72 168.94 o 3 27 0 8312.82 7993.50 343.59 o 4 27 0 11392.96 10530.82 194.26 o 5 27 0 1594.77 1480.52 107.50 o 6 27 0 3048.74 3244.32 200.00 o 7 27 0 1551.66 1614.59 126.50 o 8 27 0 128.40 108.74 86.49 o 9 27 0 81.55 59.28 89.55 o 10 27 0 1067.00 996.98 225.51 o 0 28 0 1457.78 1364.54 167.64 o 1 28 0 12665.29 12202.22 286.99 o 2 28 0 316.89 441.60 84.59 o 3 28 0 2503.37 2559.18 104.40 o 4 28 0 565.16 682.22 67.57 o 5 28 0 1096.65 1119.11 110.69 o 6 28 0 7.25 12.08 57.86 o 7 28 0 3515.36 3408.22 166.43 o 8 28 0 43.89 101.33 86.43 o 9 28 0 2815.34 2566.88 200.05 o 1 29 0 67.51 233.69 76.31 o 2 29 0 5118.89 4796.22 147.41 o 3 29 0 963.44 848.44 98.82 o 4 29 0 4895.88 4739.83 140.72 o 5 29 0 1895.56 1678.96 116.92 o 6 29 0 2059.00 2176.56 134.80 o 7 29 0 23.80 74.64 70.77 o 8 29 0 0.54 -11.26 75.68 o 9 29 0 121.72 130.04 98.42 o 0 30 0 5622.49 5244.90 290.51 o 1 30 0 1122.75 1476.01 127.94 o 2 30 0 3649.35 4218.92 188.78 o 3 30 0 725.90 918.46 76.94 o 4 30 0 220.69 269.66 58.31 o 5 30 0 197.33 282.14 74.42 o 6 30 0 1446.82 1173.80 109.76 o 7 30 0 2246.33 2218.58 144.59 o 8 30 0 1409.19 1194.82 146.24 o 9 30 0 1199.50 1217.11 159.82 o 1 31 0 7103.13 6832.11 233.67 o 2 31 0 1699.50 1966.30 148.97 o 3 31 0 3354.67 3090.49 119.17 o 4 31 0 1330.04 1060.16 84.61 o 5 31 0 8045.90 7656.79 349.12 o 6 31 0 801.52 848.53 103.08 o 7 31 0 71.28 79.11 71.27 o 8 31 0 163.47 133.44 94.12 o 9 31 0 222.87 89.30 103.98 o 0 32 0 3092.06 3186.80 246.79 o 1 32 0 29.24 192.47 81.13 o 2 32 0 8585.06 8868.61 272.81 o 3 32 0 81.45 206.87 54.55 o 4 32 0 52.24 38.60 51.09 o 5 32 0 37.68 128.97 67.41 o 6 32 0 1065.98 1131.45 112.26 o 7 32 0 1.54 -10.84 65.62 o 8 32 0 4312.34 3675.25 227.57 o 9 32 0 193.27 211.39 166.46 o 1 33 0 788.08 1028.52 144.56 o 2 33 0 1236.11 1703.45 145.66 o 3 33 0 6138.39 5508.38 229.69 o 4 33 0 25.34 33.37 51.25 o 5 33 0 5452.58 5393.08 237.16 o 6 33 0 15.23 30.58 65.27 o 7 33 0 348.13 424.98 94.73 o 8 33 0 13.41 98.51 92.30 o 0 34 0 5511.25 4352.68 293.85 o 1 34 0 386.92 542.35 105.64 o 2 34 0 3460.24 3497.39 192.34 o 3 34 0 316.02 391.99 145.58 o 4 34 0 110.47 81.31 71.10 o 5 34 0 350.95 304.57 79.22 o 6 34 0 1277.47 1434.06 127.89 o 7 34 0 687.51 646.18 102.26 o 8 34 0 1804.61 1646.56 172.21 o 1 35 0 1189.82 1600.75 149.64 o 2 35 0 2382.50 2204.60 165.28 o 3 35 0 705.89 548.88 112.53 o 4 35 0 3656.70 3531.98 167.68 o 5 35 0 1587.61 1666.16 129.04 o 6 35 0 1735.30 1481.27 129.51 o 7 35 0 288.46 325.26 93.43 o 8 35 0 29.36 27.19 95.64 o 0 36 0 71.80 194.41 132.95 o 1 36 0 5184.27 5003.73 230.05 o 2 36 0 599.40 677.74 117.87 o 3 36 0 505.48 707.62 120.09 o 4 36 0 53.22 153.34 77.75 o 5 36 0 649.08 779.74 138.70 o 6 36 0 9.31 51.19 68.84 o 7 36 0 1933.11 2113.36 166.66 o 8 36 0 44.71 216.38 142.67 o 1 37 0 319.26 400.58 111.77 o 2 37 0 2887.82 2980.97 190.64 o 3 37 0 237.95 287.98 107.46 o 4 37 0 4492.26 4776.14 235.78 o 5 37 0 156.45 170.86 107.14 o 6 37 0 1930.40 2100.25 151.39 o 7 37 0 11.66 19.04 73.33 o 0 38 0 1360.65 1713.72 228.41 o 1 38 0 3351.99 3086.69 198.62 o 2 38 0 986.73 910.76 132.50 o 3 38 0 922.67 982.47 143.69 o 4 38 0 2.47 183.78 163.06 o 5 38 0 302.45 395.92 125.57 o 6 38 0 698.54 815.10 172.64 o 7 38 0 728.67 834.01 122.19 o 1 39 0 308.22 307.47 108.56 o 2 39 0 249.17 270.81 109.06 o 3 39 0 3234.63 3291.62 211.85 o 4 39 0 952.33 1079.67 219.64 o 5 39 0 1238.02 1117.54 160.84 o 6 39 0 670.04 800.00 152.36 o 0 40 0 4036.89 3607.56 309.86 o 1 40 0 141.66 126.60 102.09 o 2 40 0 472.63 554.67 124.82 o 3 40 0 70.57 204.14 105.99 o 4 40 0 11.24 -54.50 129.68 o 5 40 0 78.45 63.54 102.17 o 6 40 0 1211.28 1279.82 178.25 o 1 41 0 272.58 211.58 111.01 o 2 41 0 343.75 505.95 125.00 o 3 41 0 1753.41 1982.23 180.62 o 4 41 0 330.61 367.39 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