#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202806.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202806_Fobs loop_ _publ_author_name 'Yoshikawa, Naokazu' 'Sakamoto, Jun' 'Kanehisa, Nobuko' 'Kai, Yasushi' 'Matsumura-Inoue, Takeko' 'Takashima, Hiroshi' 'Tsukahara, Keiichi' _publ_section_title ; (4,4'-Dimethyl-2,2'-bipyridine)chloro-(2,2':6',2''-terpyridine)-iridium(III) hexafluorophosphate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m830 _journal_page_last m832 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 77.320 _cell_angle_beta 79.481 _cell_angle_gamma 69.137 _cell_length_a 10.9819 _cell_length_b 13.5905 _cell_length_c 14.0636 _exptl_crystal_F_000 904.00 _reflns_d_resolution_high 0.7001 _[local]_cod_data_source_file ob6287Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' irterpy' _shelx_refln_list_code 4 _shelx_f_calc_maximum 335.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2130.75 -2.15 3.72 o 3 0 0 7979.72 7610.52 34.90 o 4 0 0 12552.44 13550.95 86.47 o 5 0 0 3602.46 4026.37 39.55 o 6 0 0 847.36 869.22 26.05 o 7 0 0 4082.29 3872.13 54.21 o 8 0 0 901.11 1024.06 34.18 o 9 0 0 559.37 532.63 56.44 o 10 0 0 330.40 253.12 61.22 o 11 0 0 60.88 105.63 34.01 o 12 0 0 350.07 378.79 71.52 o 13 0 0 358.67 488.93 85.83 o 14 0 0 54.83 -59.84 117.01 o -14 1 0 121.14 62.94 101.13 o -13 1 0 61.52 -40.77 90.83 o -12 1 0 62.00 57.45 60.00 o -11 1 0 599.40 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