#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/28/2202808.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202808_Fobs loop_ _publ_author_name 'Ren, XiaoMing' 'Xie, Jingli' 'Meng, Qingjin' _publ_section_title ; 1-(4-Fluorobenzyl)pyridinium bis(maleonitriledithiolato)platinate(III) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m855 _journal_page_last m858 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.710 _cell_angle_beta 99.010 _cell_angle_gamma 108.390 _cell_length_a 13.6310 _cell_length_b 14.2970 _cell_length_c 18.5570 _exptl_crystal_F_000 1902.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file ob6290Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 20416Am in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 537.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 130661.45 114896.48 3634.03 o 3 0 0 55206.52 50284.12 973.81 o 4 0 0 97791.41 92827.38 1069.51 o 5 0 0 31460.74 31237.38 2321.67 o 6 0 0 41850.59 41293.63 1397.31 o 7 0 0 1568.65 1646.94 188.07 o 8 0 0 36251.48 41545.13 4163.61 o 9 0 0 194.09 238.86 186.20 o 10 0 0 2107.88 1773.54 577.91 o 11 0 0 3697.23 2832.89 1407.63 o 12 0 0 1284.40 1556.91 325.80 o 13 0 0 802.20 1181.97 383.62 o 14 0 0 820.68 1214.67 472.95 o -15 1 0 8371.64 13484.98 991.35 o -14 1 0 24.60 0.00 392.39 o -13 1 0 428.33 638.17 204.82 o -12 1 0 6707.22 7933.03 391.81 o -11 1 0 7687.32 7668.15 321.58 o -10 1 0 9379.84 9704.75 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