#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/28/2202846.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202846_Fobs loop_ _publ_author_name 'Butcher, Ray J.' 'Bottaro, Jeffrey C.' 'Gilardi, R.' _publ_section_title ; Ammonium 1,3,4,6-tetranitro-2,5-diazapentalene ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1149 _journal_page_last o1150 _journal_volume 59 _journal_year 2003 _space_group_IT_number 12 _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.294 _cell_angle_gamma 90.000 _cell_length_a 12.1938 _cell_length_b 9.8825 _cell_length_c 5.2130 _exptl_crystal_F_000 328.00 _reflns_d_resolution_high 0.8390 _[local]_cod_data_source_file om6155Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bott43st in C2/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 68.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1219.39 1190.67 43.14 o 4 0 0 2950.43 3004.55 49.76 o 6 0 0 31.82 32.55 5.41 o 8 0 0 434.90 395.56 7.44 o 10 0 0 218.08 221.45 6.77 o 12 0 0 39.77 30.69 2.83 o 1 1 0 698.73 727.41 5.67 o 3 1 0 203.78 193.83 3.07 o 5 1 0 461.48 448.00 7.72 o 7 1 0 120.31 116.49 5.48 o 9 1 0 322.93 296.62 6.91 o 11 1 0 9.89 12.91 1.62 o 13 1 0 26.35 25.28 2.16 o 2 2 0 33.47 37.02 1.80 o 4 2 0 271.74 255.96 5.36 o 6 2 0 78.98 79.20 3.63 o 8 2 0 231.15 225.65 7.50 o 10 2 0 33.88 34.36 2.18 o 12 2 0 8.62 9.03 1.27 o 1 3 0 791.54 880.42 13.89 o 3 3 0 1173.96 1243.69 11.77 o 5 3 0 189.26 188.82 5.41 o 7 3 0 0.51 0.24 1.01 o 9 3 0 1.29 2.64 1.07 o 11 3 0 150.30 146.77 5.12 o 0 4 0 2978.31 2952.43 56.61 o 2 4 0 3657.79 3720.71 71.59 o 4 4 0 1227.27 1268.64 15.98 o 6 4 0 978.51 1042.80 22.06 o 8 4 0 112.72 118.69 3.02 o 10 4 0 151.72 169.76 6.57 o 12 4 0 65.75 63.36 4.60 o 1 5 0 402.82 465.42 6.78 o 3 5 0 467.19 512.52 28.36 o 5 5 0 55.04 66.72 4.00 o 7 5 0 201.81 218.30 8.04 o 9 5 0 125.19 129.51 3.68 o 11 5 0 62.86 67.48 5.12 o 0 6 0 184.73 178.34 7.60 o 2 6 0 133.55 100.24 4.38 o 4 6 0 19.06 19.44 1.29 o 6 6 0 45.57 41.48 2.05 o 8 6 0 20.02 22.02 1.92 o 10 6 0 286.45 300.85 9.16 o 1 7 0 793.95 757.74 19.18 o 3 7 0 0.46 -0.05 0.68 o 5 7 0 67.49 69.58 2.52 o 7 7 0 27.13 28.72 1.90 o 9 7 0 5.68 5.90 1.16 o 0 8 0 1426.84 1396.64 45.37 o 2 8 0 238.74 242.35 4.53 o 4 8 0 660.19 669.42 13.42 o 6 8 0 9.63 7.64 1.24 o 8 8 0 39.04 44.26 1.95 o 1 9 0 784.44 858.33 28.20 o 3 9 0 11.99 13.71 1.34 o 5 9 0 417.92 411.40 5.71 o 7 9 0 153.61 150.88 4.17 o 0 10 0 59.09 58.15 3.62 o 2 10 0 1.55 0.96 0.93 o 4 10 0 5.97 3.12 0.85 o 6 10 0 2.50 1.54 0.71 o 1 11 0 10.88 8.52 1.19 o 3 11 0 53.33 55.02 2.06 o -14 0 1 230.50 233.56 7.70 o -12 0 1 5.82 4.88 1.86 o -10 0 1 92.76 97.82 6.61 o -8 0 1 816.44 855.63 34.91 o -6 0 1 1982.35 1984.22 70.27 o -4 0 1 1905.48 1916.47 32.48 o -2 0 1 3631.08 3357.64 110.48 o 0 0 1 1709.92 1630.75 118.11 o 4 0 1 846.04 892.40 46.19 o 6 0 1 534.31 473.34 19.48 o 8 0 1 11.76 16.16 3.35 o 10 0 1 0.04 -1.23 1.69 o 12 0 1 45.40 48.56 4.07 o -13 1 1 6.30 4.76 1.06 o -11 1 1 62.21 60.84 2.74 o -9 1 1 52.93 60.67 2.18 o -7 1 1 370.02 344.98 12.23 o -5 1 1 1390.44 1443.05 25.60 o -3 1 1 668.74 631.47 13.64 o -1 1 1 2.48 2.00 0.53 o 3 1 1 5.23 11.60 0.88 o 5 1 1 62.57 67.04 3.34 o 7 1 1 16.44 16.71 1.52 o 9 1 1 0.25 1.71 1.48 o 11 1 1 65.41 66.36 3.70 o -12 2 1 262.65 268.42 6.82 o -10 2 1 75.01 73.57 3.90 o -8 2 1 1.33 1.61 0.97 o -6 2 1 959.17 1055.31 37.12 o -4 2 1 163.00 171.93 3.51 o 0 2 1 2.15 1.15 0.44 o 2 2 1 3015.83 2874.39 81.24 o 4 2 1 476.28 466.52 24.54 o 6 2 1 17.57 14.24 2.27 o 8 2 1 34.77 38.33 2.54 o 10 2 1 71.10 73.58 4.04 o 12 2 1 37.75 39.45 3.50 o -13 3 1 11.14 11.38 1.49 o -11 3 1 6.82 7.65 1.30 o -9 3 1 203.38 197.47 4.32 o -7 3 1 135.56 124.96 5.05 o -5 3 1 0.15 5.25 1.28 o -3 3 1 1280.42 1320.71 32.39 o -1 3 1 0.01 1.35 0.53 o 1 3 1 1832.13 1930.01 45.54 o 3 3 1 162.96 153.42 4.59 o 5 3 1 219.08 199.65 6.24 o 7 3 1 44.05 49.58 2.11 o 9 3 1 1.30 1.91 1.19 o 11 3 1 0.09 0.67 1.52 o -12 4 1 577.25 626.78 8.64 o -10 4 1 208.62 213.55 8.71 o -8 4 1 684.79 666.61 17.07 o -6 4 1 421.18 448.83 9.31 o -4 4 1 1326.27 1392.43 45.83 o -2 4 1 928.89 968.54 21.23 o 0 4 1 1791.56 2019.23 17.53 o 2 4 1 640.68 632.84 11.16 o 4 4 1 985.11 948.22 14.69 o 6 4 1 386.15 399.51 7.84 o 8 4 1 142.12 149.08 3.87 o 10 4 1 87.97 85.81 5.37 o -11 5 1 218.33 234.27 5.41 o -9 5 1 33.30 35.08 2.27 o -7 5 1 148.55 157.23 3.51 o -5 5 1 929.50 971.69 13.98 o -3 5 1 72.17 79.53 3.58 o -1 5 1 1189.76 1238.52 19.95 o 1 5 1 7.84 3.06 1.18 o 3 5 1 376.13 423.26 9.12 o 5 5 1 352.11 334.51 10.41 o 7 5 1 1.85 0.73 1.05 o 9 5 1 22.67 19.81 2.07 o -12 6 1 44.20 46.39 3.96 o -10 6 1 298.50 311.02 7.43 o -8 6 1 301.41 304.94 6.05 o -6 6 1 38.24 35.26 1.96 o -4 6 1 1051.14 1033.57 23.56 o -2 6 1 206.43 185.16 13.40 o 0 6 1 6.16 7.09 1.65 o 2 6 1 468.85 438.12 13.39 o 4 6 1 332.30 323.20 9.71 o 6 6 1 0.06 -0.32 0.93 o 8 6 1 3.08 4.15 1.22 o -11 7 1 1.72 0.81 0.71 o -9 7 1 125.93 121.63 4.72 o -7 7 1 0.24 0.16 1.01 o -5 7 1 197.59 187.63 4.43 o -3 7 1 38.33 35.75 1.78 o -1 7 1 22.72 17.24 1.82 o 1 7 1 176.35 177.98 3.93 o 3 7 1 574.19 596.85 10.41 o 5 7 1 50.95 47.10 2.27 o 7 7 1 4.53 4.38 1.24 o 9 7 1 0.22 -0.06 0.91 o -10 8 1 3.94 4.09 0.85 o -8 8 1 121.67 112.03 4.32 o -6 8 1 48.01 42.01 2.15 o -4 8 1 49.17 43.95 2.16 o -2 8 1 456.17 451.82 7.57 o 0 8 1 44.67 47.05 2.13 o 2 8 1 647.19 680.93 16.15 o 4 8 1 92.92 90.42 3.59 o 6 8 1 395.23 411.00 5.60 o 8 8 1 34.76 31.14 1.72 o -9 9 1 1.70 1.27 0.67 o -7 9 1 67.87 81.67 4.11 o -5 9 1 216.05 223.54 4.58 o -3 9 1 754.90 729.00 8.52 o -1 9 1 136.17 128.74 3.80 o 1 9 1 1048.44 1137.86 40.52 o 3 9 1 329.19 334.59 5.21 o 5 9 1 29.76 28.22 1.73 o 7 9 1 82.35 75.15 2.47 o -6 10 1 22.94 22.69 1.44 o -4 10 1 50.99 52.25 2.30 o -2 10 1 75.85 79.91 3.26 o 0 10 1 1.22 1.31 1.14 o 2 10 1 82.66 77.52 2.83 o 4 10 1 8.40 8.03 1.04 o -5 11 1 19.90 21.26 2.45 o -3 11 1 8.23 7.18 1.15 o -1 11 1 33.03 35.71 4.37 o 1 11 1 5.77 5.32 1.16 o 3 11 1 15.50 12.74 1.71 o -14 0 2 99.96 91.16 5.60 o -12 0 2 383.31 343.62 8.53 o -10 0 2 6.20 5.46 1.48 o -8 0 2 644.62 720.11 23.87 o -6 0 2 614.01 639.37 12.75 o -4 0 2 447.52 470.51 9.94 o -2 0 2 3252.87 3154.03 211.10 o 0 0 2 4681.19 4667.11 419.31 o 2 0 2 2042.36 2247.83 35.35 o 4 0 2 4207.19 4469.74 150.04 o 6 0 2 86.11 76.71 4.18 o 8 0 2 37.58 27.65 2.99 o 10 0 2 21.37 21.62 3.36 o -13 1 2 66.79 65.08 2.65 o -11 1 2 2.23 0.62 0.89 o -9 1 2 1.60 2.13 0.84 o -7 1 2 430.85 454.67 9.99 o -5 1 2 169.31 168.72 5.08 o -3 1 2 309.29 341.37 13.46 o -1 1 2 146.69 152.20 3.24 o 1 1 2 0.41 0.60 0.59 o 3 1 2 1137.60 1086.80 14.39 o 5 1 2 85.71 96.04 3.47 o 7 1 2 91.75 93.17 3.34 o 9 1 2 1.90 1.76 1.08 o -14 2 2 46.53 37.21 2.06 o -12 2 2 2.11 1.25 0.91 o -10 2 2 874.64 903.38 20.06 o -8 2 2 605.58 565.99 13.30 o -6 2 2 3.88 1.81 1.07 o -4 2 2 2315.73 2462.78 23.12 o -2 2 2 448.16 472.29 12.00 o 0 2 2 2766.60 2731.19 65.85 o 2 2 2 175.20 195.73 4.80 o 4 2 2 698.20 656.02 27.78 o 6 2 2 90.82 89.95 3.15 o 8 2 2 0.69 0.29 1.00 o 10 2 2 3.63 2.47 1.24 o -13 3 2 116.47 122.70 3.85 o -11 3 2 65.69 67.99 2.49 o -9 3 2 2.58 4.21 1.18 o -7 3 2 0.12 0.60 1.46 o -5 3 2 130.34 110.72 4.20 o -3 3 2 325.46 250.17 4.41 o -1 3 2 254.24 259.00 4.64 o 1 3 2 204.69 200.86 5.40 o 3 3 2 122.87 119.36 5.81 o 5 3 2 66.50 62.60 2.14 o 7 3 2 2.38 2.08 1.15 o 9 3 2 41.58 47.65 2.53 o -12 4 2 4.79 5.13 1.11 o -10 4 2 1274.60 1313.91 14.05 o -8 4 2 221.69 203.05 6.46 o -6 4 2 390.32 358.22 14.17 o -4 4 2 1689.08 1755.41 52.21 o -2 4 2 672.84 656.56 14.34 o 0 4 2 1298.69 1255.87 22.71 o 2 4 2 2.14 1.79 1.44 o 4 4 2 33.13 26.38 1.75 o 6 4 2 219.04 244.47 7.54 o 8 4 2 24.26 24.93 2.18 o -13 5 2 46.96 51.91 2.85 o -11 5 2 219.34 233.77 11.58 o -9 5 2 785.13 810.00 16.64 o -7 5 2 11.57 13.29 1.44 o -5 5 2 152.11 168.79 5.20 o -3 5 2 389.97 450.38 10.56 o -1 5 2 24.27 14.01 2.12 o 1 5 2 611.64 626.93 33.33 o 3 5 2 0.12 0.14 0.92 o 5 5 2 36.65 37.76 2.40 o 7 5 2 147.69 143.16 6.45 o 9 5 2 3.88 2.66 1.80 o -12 6 2 0.38 0.73 0.83 o -10 6 2 314.44 339.50 5.76 o -8 6 2 472.33 460.73 10.14 o -6 6 2 291.51 275.46 6.01 o -4 6 2 3.34 2.29 1.09 o -2 6 2 1393.72 1304.54 30.95 o 0 6 2 5.85 6.56 1.02 o 2 6 2 21.48 20.75 1.52 o 4 6 2 365.19 388.62 6.52 o 6 6 2 39.89 47.00 2.50 o 8 6 2 6.64 5.15 1.51 o -11 7 2 20.98 18.72 1.41 o -9 7 2 83.34 83.82 3.05 o -7 7 2 84.74 85.39 3.16 o -5 7 2 0.20 0.56 1.20 o -3 7 2 25.21 22.90 1.87 o -1 7 2 29.97 26.20 2.26 o 1 7 2 13.75 15.74 1.63 o 3 7 2 78.94 79.19 2.82 o 5 7 2 92.06 99.60 3.40 o 7 7 2 63.98 71.83 5.00 o -10 8 2 112.39 105.83 4.19 o -8 8 2 0.36 0.25 0.90 o -6 8 2 16.38 10.10 1.77 o -4 8 2 0.08 1.27 1.21 o -2 8 2 94.19 88.26 3.65 o 0 8 2 462.72 458.45 7.66 o 2 8 2 71.43 78.44 3.07 o 4 8 2 147.84 168.26 3.99 o 6 8 2 48.13 46.60 2.09 o -9 9 2 1.28 2.35 0.91 o -7 9 2 89.98 78.18 3.20 o -5 9 2 104.96 117.78 4.93 o -3 9 2 402.27 385.72 8.51 o -1 9 2 437.07 407.74 13.33 o 1 9 2 162.02 157.34 4.03 o 3 9 2 395.54 429.75 11.13 o 5 9 2 134.67 132.05 3.27 o -6 10 2 1.75 3.03 1.21 o -4 10 2 58.31 62.52 3.24 o -2 10 2 76.88 73.38 3.65 o 0 10 2 76.61 76.49 2.65 o 2 10 2 19.90 20.31 1.52 o -3 11 2 0.03 0.80 1.23 o -1 11 2 10.16 6.58 1.31 o -14 0 3 173.45 168.98 8.07 o -12 0 3 545.35 510.23 12.61 o -10 0 3 337.40 294.92 9.45 o -8 0 3 0.04 -0.08 1.15 o -6 0 3 2665.93 2594.45 187.18 o -4 0 3 152.27 136.64 6.90 o -2 0 3 62.72 63.41 4.76 o 0 0 3 487.34 451.56 11.90 o 2 0 3 1460.78 1498.52 34.94 o 4 0 3 690.46 742.30 39.94 o 6 0 3 653.89 664.02 22.16 o 8 0 3 0.04 1.44 1.22 o -13 1 3 12.64 13.09 1.32 o -11 1 3 62.54 57.83 2.21 o -9 1 3 74.81 66.56 2.80 o -7 1 3 132.41 115.56 2.78 o -5 1 3 133.90 141.15 6.64 o -3 1 3 387.90 394.24 19.26 o -1 1 3 10.38 12.04 1.76 o 1 1 3 31.91 26.38 2.44 o 3 1 3 105.37 123.37 3.13 o 5 1 3 166.24 161.13 4.34 o 7 1 3 50.06 47.55 2.46 o 9 1 3 9.91 7.06 1.35 o -14 2 3 1.88 1.01 1.03 o -12 2 3 32.99 27.33 1.76 o -10 2 3 2.23 1.08 0.88 o -8 2 3 683.19 667.71 14.47 o -6 2 3 360.04 349.67 10.08 o -4 2 3 29.93 28.15 2.21 o -2 2 3 282.93 309.56 7.39 o 0 2 3 0.01 0.64 1.17 o 2 2 3 443.53 439.85 5.84 o 4 2 3 55.25 52.42 2.82 o 6 2 3 28.42 25.79 2.06 o 8 2 3 0.45 0.88 0.83 o -13 3 3 0.74 0.58 0.80 o -11 3 3 61.21 67.52 3.15 o -9 3 3 335.25 339.38 4.65 o -7 3 3 0.01 0.22 0.83 o -5 3 3 20.46 20.45 2.28 o -3 3 3 161.59 146.32 4.76 o -1 3 3 267.17 232.11 6.98 o 1 3 3 89.53 88.19 2.36 o 3 3 3 11.70 12.67 1.44 o 5 3 3 7.15 8.91 1.35 o 7 3 3 6.27 5.38 1.16 o -12 4 3 457.51 500.63 19.78 o -10 4 3 105.07 95.01 3.19 o -8 4 3 2377.24 2367.86 29.23 o -6 4 3 1.29 2.06 1.13 o -4 4 3 36.71 38.10 2.49 o -2 4 3 761.17 753.50 12.66 o 0 4 3 299.11 282.89 5.53 o 2 4 3 642.11 681.13 16.87 o 4 4 3 16.73 19.02 2.24 o 6 4 3 9.57 9.62 1.64 o 8 4 3 62.15 61.74 4.10 o -11 5 3 21.00 25.74 2.05 o -9 5 3 207.93 207.57 5.86 o -7 5 3 1240.33 1171.59 12.64 o -5 5 3 0.49 1.45 1.55 o -3 5 3 362.19 370.93 13.84 o -1 5 3 34.61 36.04 1.87 o 1 5 3 2.23 3.15 1.29 o 3 5 3 69.15 69.65 2.96 o 5 5 3 14.68 13.54 1.92 o 7 5 3 5.36 3.78 1.10 o -12 6 3 13.92 13.99 2.51 o -10 6 3 0.82 1.30 1.09 o -8 6 3 267.99 290.38 10.58 o -6 6 3 130.23 122.94 3.62 o -4 6 3 79.58 78.62 4.37 o -2 6 3 5.58 6.10 1.52 o 0 6 3 215.66 213.14 4.72 o 2 6 3 13.72 12.16 1.65 o 4 6 3 48.23 50.54 2.51 o 6 6 3 89.08 85.28 3.07 o -11 7 3 40.96 47.55 2.56 o -9 7 3 0.08 -0.17 0.98 o -7 7 3 224.91 210.06 10.04 o -5 7 3 179.37 172.14 7.25 o -3 7 3 22.78 22.98 2.27 o -1 7 3 19.50 16.31 2.61 o 1 7 3 5.68 7.47 1.45 o 3 7 3 3.88 3.85 1.22 o 5 7 3 46.96 42.12 2.77 o -10 8 3 13.34 11.68 2.50 o -8 8 3 257.15 282.65 5.54 o -6 8 3 36.50 31.80 2.95 o -4 8 3 17.12 19.64 2.15 o -2 8 3 3.85 3.13 1.68 o 0 8 3 35.68 34.70 2.53 o 2 8 3 274.25 294.39 6.85 o 4 8 3 76.59 83.84 2.51 o -7 9 3 1.64 3.46 1.25 o -5 9 3 93.42 82.84 5.19 o -3 9 3 3.90 5.63 1.68 o -1 9 3 323.96 317.88 7.28 o 1 9 3 236.62 219.63 9.00 o 3 9 3 18.03 15.68 2.36 o -2 10 3 0.56 1.30 1.12 o 0 10 3 8.95 5.43 1.25 o -12 0 4 420.59 442.09 16.47 o -10 0 4 659.03 626.82 18.69 o -8 0 4 319.45 268.59 23.37 o -6 0 4 28.80 29.14 2.27 o -4 0 4 1476.50 1533.99 51.85 o -2 0 4 211.60 210.44 11.19 o 0 0 4 10.93 14.06 2.30 o 2 0 4 72.77 77.25 3.56 o 4 0 4 123.28 125.42 5.25 o 6 0 4 137.80 119.07 4.26 o -13 1 4 5.18 3.86 0.96 o -11 1 4 30.59 29.75 2.13 o -9 1 4 29.31 26.48 2.13 o -7 1 4 48.20 51.81 2.29 o -5 1 4 0.08 -0.22 0.67 o -3 1 4 0.25 -0.16 0.67 o -1 1 4 80.08 76.06 2.87 o 1 1 4 3.96 2.38 0.94 o 3 1 4 3.65 2.36 1.10 o 5 1 4 83.07 81.16 2.85 o -12 2 4 1.88 1.48 0.97 o -10 2 4 84.05 77.39 3.35 o -8 2 4 146.10 151.84 3.67 o -6 2 4 130.99 141.98 3.44 o -4 2 4 167.70 153.03 7.46 o -2 2 4 13.10 12.88 1.37 o 0 2 4 9.38 9.82 1.53 o 2 2 4 16.00 14.90 1.53 o 4 2 4 108.44 107.27 3.01 o 6 2 4 1.57 0.91 0.74 o -13 3 4 22.11 20.31 1.98 o -11 3 4 8.67 7.93 1.54 o -9 3 4 0.58 0.33 0.91 o -7 3 4 137.97 149.58 3.55 o -5 3 4 48.70 49.35 3.20 o -3 3 4 3.53 3.27 1.03 o -1 3 4 158.85 164.91 3.64 o 1 3 4 5.21 4.23 1.15 o 3 3 4 38.77 39.87 2.08 o 5 3 4 0.36 -0.14 0.73 o -12 4 4 0.48 0.99 1.18 o -10 4 4 618.18 689.65 11.13 o -8 4 4 72.30 70.40 2.96 o -6 4 4 2097.25 2020.98 73.27 o -4 4 4 0.37 1.06 1.17 o -2 4 4 72.16 74.28 3.46 o 0 4 4 137.77 142.15 4.49 o 2 4 4 24.58 22.69 2.30 o 4 4 4 117.37 108.13 3.62 o -11 5 4 81.51 88.07 3.72 o -9 5 4 0.34 1.97 1.28 o -7 5 4 299.68 308.30 8.35 o -5 5 4 462.32 449.81 29.14 o -3 5 4 23.73 20.40 2.27 o -1 5 4 146.64 146.90 3.90 o 1 5 4 19.26 15.34 1.71 o 3 5 4 39.91 40.40 2.47 o 5 5 4 9.44 8.21 2.02 o -10 6 4 105.77 111.59 4.19 o -8 6 4 43.67 45.94 3.46 o -6 6 4 23.34 35.03 3.30 o -4 6 4 54.44 52.35 3.77 o -2 6 4 9.73 8.85 1.66 o 0 6 4 28.36 27.29 2.33 o 2 6 4 9.97 11.04 1.60 o 4 6 4 1.04 0.30 1.01 o -9 7 4 82.40 94.44 5.64 o -7 7 4 0.82 0.09 1.31 o -5 7 4 68.53 73.72 4.16 o -3 7 4 193.60 207.41 7.23 o -1 7 4 1.56 1.43 1.21 o 1 7 4 9.68 7.70 1.37 o -8 8 4 1.61 0.33 1.43 o -6 8 4 273.32 284.75 10.01 o -4 8 4 16.19 17.09 2.27 o -2 8 4 2.46 1.02 1.77 o 0 8 4 27.04 26.41 2.25 o -3 9 4 22.87 14.77 2.57 o -12 0 5 124.98 117.32 5.79 o -10 0 5 160.34 182.47 11.61 o -8 0 5 275.63 271.93 15.14 o -6 0 5 75.18 79.23 4.35 o -4 0 5 0.35 -0.15 1.35 o -2 0 5 239.01 263.10 7.54 o 0 0 5 110.08 116.82 6.91 o 2 0 5 0.03 0.21 0.99 o -11 1 5 40.06 37.56 1.99 o -9 1 5 63.85 64.37 2.75 o -7 1 5 119.45 122.99 3.03 o -5 1 5 2.15 1.11 0.91 o -3 1 5 16.63 18.78 1.88 o -1 1 5 6.09 4.67 1.24 o 1 1 5 0.12 -0.53 0.83 o 3 1 5 0.14 0.47 0.86 o -12 2 5 14.58 12.06 1.73 o -10 2 5 34.86 37.12 2.06 o -8 2 5 139.58 131.83 3.31 o -6 2 5 207.81 214.36 4.24 o -4 2 5 70.00 72.61 2.62 o -2 2 5 58.28 60.48 2.91 o 0 2 5 14.58 16.54 1.70 o 2 2 5 9.18 9.51 1.22 o -11 3 5 69.11 63.96 2.67 o -9 3 5 3.55 4.89 1.15 o -7 3 5 0.12 0.63 0.95 o -5 3 5 0.69 0.24 0.82 o -3 3 5 17.00 16.82 1.57 o -1 3 5 14.79 15.08 1.59 o 1 3 5 22.33 21.83 1.95 o -10 4 5 40.56 49.93 2.10 o -8 4 5 307.79 335.14 15.84 o -6 4 5 78.44 72.68 3.21 o -4 4 5 619.33 641.79 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