#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202863.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202863_Fobs loop_ _publ_author_name 'Li, Xiao-Fang' 'Feng, Ya-Qing' 'Gao, Bo' 'Chen, Hong-Liang' _publ_section_title ; 1-Methyl-spiro[2.3']oxindole-spiro[3.2'']5'',6''-dihydroimidazo[2'',1''-b]thiazol-3''-one-4-(2-benzo[1,3]dioxol-5-yl)pyrrolidine ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1467 _journal_page_last o1468 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 85.690 _cell_angle_beta 72.206 _cell_angle_gamma 79.169 _cell_length_a 8.7412 _cell_length_b 9.2554 _cell_length_c 14.0970 _exptl_crystal_F_000 468.00 _reflns_d_resolution_high 0.7973 _[local]_cod_data_source_file om6173Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 030823G in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 111.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2126.55 2016.00 44.34 o 2 0 0 112.85 110.10 1.50 o 3 0 0 11.54 10.19 0.39 o 4 0 0 199.27 208.93 2.16 o 5 0 0 10.13 5.78 0.49 o 6 0 0 85.44 88.90 1.75 o 7 0 0 23.55 25.29 1.24 o 8 0 0 96.60 100.74 2.32 o 9 0 0 42.73 46.84 2.07 o 10 0 0 30.91 31.93 1.98 o -10 1 0 5.06 5.49 1.27 o -9 1 0 36.75 38.78 2.07 o -8 1 0 22.99 18.05 1.17 o -7 1 0 4.33 4.09 0.73 o -6 1 0 428.56 407.08 4.60 o -5 1 0 383.90 371.95 3.83 o -4 1 0 502.40 563.52 5.07 o -3 1 0 5.94 13.61 0.60 o -2 1 0 716.08 726.67 6.91 o -1 1 0 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