#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/28/2202885.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202885_Fobs loop_ _publ_author_name 'Lynch, Daniel E.' 'McClenaghan, Ian' _publ_section_title ; 2-Chloro-3-(3-dimethylaminopropylamino)-1,4-naphthoquinone ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1427 _journal_page_last o1428 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.623 _cell_angle_gamma 90.000 _cell_length_a 8.0693 _cell_length_b 13.0017 _cell_length_c 13.9310 _exptl_crystal_F_000 616.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file su6003Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 2-Chloro-3-(3-dimethylaminopropylamino)-1,4-naphthoquinone _shelx_refln_list_code 4 _shelx_f_calc_maximum 151.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1299.87 1222.60 55.19 o 2 0 0 275.76 258.78 19.62 o 3 0 0 34.40 6.60 15.65 o 4 0 0 543.21 338.45 137.95 o 5 0 0 37.25 33.89 14.99 o 6 0 0 132.48 100.73 25.21 o 7 0 0 245.14 305.67 120.18 o 8 0 0 1.44 79.47 193.55 o 1 1 0 13.24 14.20 5.42 o 2 1 0 20926.51 19551.58 1058.43 o 3 1 0 2746.96 2832.24 62.25 o 4 1 0 1.77 9.73 6.88 o 5 1 0 23.60 4.41 16.87 o 6 1 0 94.00 36.58 31.12 o 7 1 0 10.98 28.10 32.66 o 8 1 0 82.02 230.53 221.88 o 0 2 0 1105.63 1138.70 53.50 o 1 2 0 2045.20 2063.01 71.08 o 2 2 0 11592.63 11783.42 1339.40 o 3 2 0 438.30 425.55 25.43 o 4 2 0 227.92 315.96 35.80 o 5 2 0 26.22 9.60 29.75 o 6 2 0 5.24 -23.76 32.01 o 7 2 0 54.00 85.83 35.89 o 8 2 0 0.30 19.35 39.83 o 1 3 0 1033.43 1019.81 41.12 o 2 3 0 3581.79 3661.16 113.09 o 3 3 0 112.70 89.61 20.17 o 4 3 0 4793.03 4999.38 191.01 o 5 3 0 1340.66 1499.05 121.52 o 6 3 0 139.68 177.71 41.75 o 7 3 0 15.89 -45.07 51.30 o 8 3 0 17.42 -28.06 99.10 o 9 3 0 1.47 -33.83 67.67 o 0 4 0 4701.23 4495.47 359.57 o 1 4 0 274.54 264.28 44.18 o 2 4 0 1185.37 1163.29 51.90 o 3 4 0 53.34 36.50 21.58 o 4 4 0 79.04 74.88 28.26 o 5 4 0 12.55 48.49 37.47 o 6 4 0 362.44 345.07 57.05 o 7 4 0 333.57 400.89 74.39 o 8 4 0 34.65 -118.43 78.95 o 1 5 0 16.41 -3.39 24.23 o 2 5 0 650.03 610.19 46.73 o 3 5 0 89.74 95.56 30.55 o 4 5 0 10.09 -22.49 25.78 o 5 5 0 11.49 -28.84 32.49 o 6 5 0 152.00 155.80 53.83 o 7 5 0 1.67 -6.22 61.93 o 8 5 0 21.39 -126.79 169.16 o 0 6 0 2258.09 2314.34 128.81 o 1 6 0 143.74 93.80 34.99 o 2 6 0 1275.44 1260.67 72.63 o 3 6 0 22.36 -5.23 28.92 o 4 6 0 39.05 -3.77 27.34 o 5 6 0 201.52 165.78 85.63 o 6 6 0 21.20 38.45 37.34 o 7 6 0 78.62 79.19 72.18 o 8 6 0 223.07 228.10 155.69 o 1 7 0 324.71 357.23 53.83 o 2 7 0 561.72 581.33 59.20 o 3 7 0 40.10 85.50 43.36 o 4 7 0 348.08 293.76 48.53 o 5 7 0 144.98 179.00 40.87 o 6 7 0 566.51 637.45 89.81 o 7 7 0 132.45 23.84 77.58 o 8 7 0 0.07 312.01 148.41 o 0 8 0 67.14 148.92 78.83 o 1 8 0 147.46 152.19 44.86 o 2 8 0 453.37 418.91 60.43 o 3 8 0 204.82 185.05 49.78 o 4 8 0 1293.51 1338.43 123.76 o 5 8 0 486.94 444.45 60.70 o 6 8 0 14.84 -21.20 43.93 o 7 8 0 4.26 97.64 108.65 o 1 9 0 9.30 -69.76 47.80 o 2 9 0 1402.75 1523.04 115.43 o 3 9 0 47.01 80.42 48.91 o 4 9 0 70.80 78.36 48.78 o 5 9 0 246.08 299.26 86.76 o 6 9 0 0.74 -57.92 50.26 o 7 9 0 42.43 140.05 198.28 o 0 10 0 1660.11 1673.04 183.58 o 1 10 0 12.47 -52.25 53.67 o 2 10 0 1687.23 1704.80 130.18 o 3 10 0 437.02 373.36 81.78 o 4 10 0 44.93 -23.52 58.10 o 5 10 0 65.13 30.13 51.30 o 6 10 0 101.64 114.24 133.36 o 7 10 0 1.65 222.67 198.28 o 1 11 0 1.70 -9.22 58.54 o 2 11 0 38.06 -99.25 89.38 o 3 11 0 51.96 5.25 71.64 o 4 11 0 101.92 127.94 68.21 o 5 11 0 8.45 13.64 76.04 o 6 11 0 51.31 501.98 206.14 o 0 12 0 852.68 874.62 169.49 o 1 12 0 2.83 -43.42 73.00 o 2 12 0 45.24 -74.93 108.62 o 3 12 0 115.86 59.05 117.59 o 4 12 0 12.62 -88.40 77.55 o 5 12 0 0.19 192.31 131.51 o 1 13 0 26.78 162.94 88.46 o 2 13 0 152.97 147.24 114.56 o 3 13 0 35.36 108.86 114.92 o 4 13 0 108.58 -143.77 281.28 o 5 13 0 16.03 -114.87 197.49 o 0 14 0 0.04 -103.37 143.26 o 1 14 0 14.55 93.36 132.00 o 2 14 0 122.02 175.54 127.26 o 3 14 0 34.17 150.34 172.07 o 1 15 0 11.96 54.47 131.14 o 2 15 0 1.90 133.60 144.55 o -8 1 1 0.11 105.36 167.98 o -7 1 1 23.80 22.68 43.50 o -6 1 1 62.28 18.28 24.66 o -5 1 1 143.95 142.86 35.17 o -4 1 1 135.52 95.34 22.77 o -3 1 1 2035.20 2157.23 63.31 o -2 1 1 22916.48 22076.81 504.80 o -1 1 1 66.76 80.18 21.10 o 0 1 1 7684.02 7767.73 199.32 o 1 1 1 456.52 423.57 18.84 o 2 1 1 5679.87 5435.08 104.57 o 3 1 1 267.42 256.25 18.29 o 4 1 1 131.93 94.30 28.61 o 5 1 1 103.32 112.43 19.10 o 6 1 1 459.56 489.38 30.59 o 7 1 1 140.98 153.63 42.93 o 8 1 1 23.25 24.81 87.08 o -8 2 1 46.46 20.38 34.47 o -7 2 1 18.62 -9.41 44.40 o -6 2 1 1.70 -4.95 30.12 o -5 2 1 1046.04 1059.98 66.14 o -4 2 1 5132.81 5311.66 145.79 o -3 2 1 40.56 36.07 22.40 o -2 2 1 14652.16 13763.92 3869.22 o -1 2 1 1917.94 1847.08 59.63 o 0 2 1 2085.33 2037.34 52.44 o 1 2 1 2864.81 2884.15 108.37 o 2 2 1 452.95 451.50 28.71 o 3 2 1 1393.30 1421.79 73.37 o 4 2 1 227.25 166.42 32.13 o 5 2 1 1.64 -12.48 15.37 o 6 2 1 3.03 69.73 40.07 o 7 2 1 1.67 -15.01 40.03 o 8 2 1 56.32 76.84 40.57 o -9 3 1 13.84 -17.31 60.58 o -8 3 1 0.30 -4.03 48.41 o -7 3 1 26.03 11.94 46.33 o -6 3 1 2.09 -29.70 34.15 o -5 3 1 452.79 555.66 54.10 o -4 3 1 3661.99 3921.13 143.43 o -3 3 1 185.02 161.64 31.82 o -2 3 1 105.75 118.16 19.99 o -1 3 1 972.77 959.51 38.63 o 0 3 1 4.28 -14.66 17.68 o 1 3 1 2005.39 2042.08 60.31 o 2 3 1 9.35 -6.04 16.93 o 3 3 1 1179.72 1267.04 47.18 o 4 3 1 433.18 324.44 77.98 o 5 3 1 177.70 196.03 26.33 o 6 3 1 385.49 334.93 60.95 o 7 3 1 5.55 65.72 52.95 o 8 3 1 3.96 4.30 77.72 o -9 4 1 24.61 -25.18 84.19 o -8 4 1 27.42 -8.56 56.52 o -7 4 1 318.55 351.67 69.43 o -6 4 1 502.91 515.90 68.28 o -5 4 1 5.62 35.39 47.58 o -4 4 1 1581.08 1808.45 65.35 o -3 4 1 275.80 304.30 27.25 o -2 4 1 111.05 134.35 25.49 o -1 4 1 379.00 403.82 28.62 o 0 4 1 15.10 -3.60 23.35 o 1 4 1 623.29 648.15 34.22 o 2 4 1 4.94 -3.23 21.15 o 3 4 1 5.87 6.56 22.73 o 4 4 1 22.25 21.21 36.36 o 5 4 1 50.26 57.86 25.95 o 6 4 1 158.54 115.54 61.32 o 7 4 1 0.01 105.49 66.24 o 8 4 1 21.98 -52.24 63.79 o -8 5 1 346.57 242.81 112.32 o -7 5 1 215.85 318.37 82.79 o -6 5 1 347.41 233.22 64.04 o -5 5 1 1.32 -2.39 27.09 o -4 5 1 209.47 173.38 32.93 o -3 5 1 4.19 -10.57 25.88 o -2 5 1 561.65 509.63 41.24 o -1 5 1 36.45 36.07 24.82 o 0 5 1 210.31 141.32 29.60 o 1 5 1 0.09 10.21 26.61 o 2 5 1 104.77 105.44 27.95 o 3 5 1 6.35 -5.85 34.07 o 4 5 1 782.52 871.46 72.58 o 5 5 1 23.09 -6.71 33.98 o 6 5 1 2.18 -17.70 16.89 o 7 5 1 14.74 54.33 75.61 o 8 5 1 0.35 85.53 88.91 o -8 6 1 7.13 257.55 138.68 o -7 6 1 36.52 -12.64 59.92 o -6 6 1 230.94 323.93 70.93 o -5 6 1 6.14 -23.97 34.73 o -4 6 1 130.16 107.45 30.45 o -3 6 1 99.62 95.09 32.63 o -2 6 1 83.90 68.99 32.43 o -1 6 1 78.67 69.29 40.54 o 0 6 1 3540.60 3565.08 140.24 o 1 6 1 28.26 20.21 40.09 o 2 6 1 330.13 284.99 40.66 o 3 6 1 76.17 62.83 30.57 o 4 6 1 26.39 26.90 29.00 o 5 6 1 2.25 36.38 34.84 o 6 6 1 58.71 96.13 42.13 o 7 6 1 198.39 195.09 102.75 o 8 6 1 3.34 163.37 190.41 o -8 7 1 1.77 8.04 108.72 o -7 7 1 340.04 238.30 89.85 o -6 7 1 366.26 325.72 66.39 o -5 7 1 111.66 124.71 35.16 o -4 7 1 198.03 223.77 55.31 o -3 7 1 106.70 206.06 42.59 o -2 7 1 317.63 364.27 50.93 o -1 7 1 214.85 299.78 49.82 o 0 7 1 86.71 109.13 41.21 o 1 7 1 2.89 -20.63 36.03 o 2 7 1 1294.57 1280.58 74.54 o 3 7 1 68.08 99.88 48.11 o 4 7 1 9.43 18.74 43.66 o 5 7 1 167.07 138.80 38.92 o 6 7 1 134.63 155.46 49.46 o 7 7 1 41.51 -18.87 95.73 o 8 7 1 1.99 -332.82 227.39 o -8 8 1 2.29 -149.40 99.60 o -7 8 1 68.48 0.69 100.09 o -6 8 1 28.06 16.57 38.36 o -5 8 1 142.73 202.89 45.65 o -4 8 1 1268.74 1434.03 118.87 o -3 8 1 49.54 21.20 45.43 o -2 8 1 407.12 429.53 87.22 o -1 8 1 34.00 12.53 41.18 o 0 8 1 156.39 150.45 45.91 o 1 8 1 25.70 44.94 60.76 o 2 8 1 432.50 439.81 56.01 o 3 8 1 53.32 85.97 42.01 o 4 8 1 64.82 87.20 46.15 o 5 8 1 98.46 66.99 41.61 o 6 8 1 6.74 62.19 58.14 o 7 8 1 5.27 19.84 106.22 o -7 9 1 11.24 37.64 48.80 o -6 9 1 19.08 -1.68 50.50 o -5 9 1 36.19 43.06 45.05 o -4 9 1 164.44 64.81 60.96 o -3 9 1 2.97 95.34 76.43 o -2 9 1 231.96 241.28 64.51 o -1 9 1 71.82 68.69 52.04 o 0 9 1 120.18 109.56 50.55 o 1 9 1 1.59 -30.45 52.75 o 2 9 1 1775.96 1921.57 128.79 o 3 9 1 345.20 330.93 70.53 o 4 9 1 991.41 1090.09 157.97 o 5 9 1 168.50 59.85 52.35 o 6 9 1 43.55 192.09 67.95 o 7 9 1 0.58 58.22 184.11 o -7 10 1 1.16 65.31 171.52 o -6 10 1 11.08 45.49 136.12 o -5 10 1 2.51 -76.50 51.00 o -4 10 1 10.84 -54.97 60.69 o -3 10 1 80.64 63.93 55.91 o -2 10 1 283.07 279.17 64.91 o -1 10 1 197.56 164.38 63.10 o 0 10 1 770.79 757.45 91.35 o 1 10 1 46.49 -1.95 55.87 o 2 10 1 216.71 145.74 63.12 o 3 10 1 343.61 327.29 79.42 o 4 10 1 5.39 29.42 58.42 o 5 10 1 131.11 95.16 96.07 o 6 10 1 35.29 83.24 91.89 o -6 11 1 12.35 -68.07 106.41 o -5 11 1 3.66 -97.61 82.24 o -4 11 1 0.81 -52.41 68.03 o -3 11 1 16.27 -78.30 78.26 o -2 11 1 55.20 -70.66 65.29 o -1 11 1 372.24 268.84 81.19 o 0 11 1 1762.30 1838.22 143.05 o 1 11 1 1052.85 1000.64 96.56 o 2 11 1 6.24 -26.54 63.93 o 3 11 1 6.23 105.75 88.58 o 4 11 1 123.49 55.45 69.84 o 5 11 1 6.61 16.01 112.51 o 6 11 1 57.06 74.75 191.19 o -5 12 1 2.09 -30.44 218.34 o -4 12 1 0.82 39.98 92.95 o -3 12 1 155.25 87.79 93.12 o -2 12 1 1084.11 1096.50 135.75 o -1 12 1 149.19 162.70 77.43 o 0 12 1 219.24 169.13 93.24 o 1 12 1 16.42 -75.91 87.24 o 2 12 1 18.84 43.60 93.46 o 3 12 1 85.26 215.37 112.74 o 4 12 1 11.91 49.95 103.94 o 5 12 1 5.77 -115.36 125.47 o -5 13 1 116.83 60.79 101.30 o -4 13 1 3.84 6.50 112.21 o -3 13 1 24.74 136.28 127.88 o -2 13 1 509.20 482.74 136.34 o -1 13 1 59.90 210.97 98.33 o 0 13 1 82.83 188.75 98.81 o 1 13 1 181.76 146.39 104.80 o 2 13 1 0.06 -49.38 155.74 o 3 13 1 22.35 -26.90 96.84 o 4 13 1 22.07 -91.65 102.10 o -4 14 1 123.59 -18.29 138.69 o -3 14 1 150.48 182.70 134.75 o -2 14 1 21.57 56.59 131.26 o -1 14 1 7.29 30.48 119.56 o 0 14 1 9.96 136.34 116.08 o 1 14 1 31.87 63.48 112.51 o 2 14 1 10.65 -128.50 130.98 o 3 14 1 32.62 49.63 267.51 o -2 15 1 38.27 96.44 127.57 o -1 15 1 1.50 -46.99 125.85 o 0 15 1 1.70 -154.31 142.03 o 1 15 1 0.05 -9.19 125.65 o 2 15 1 9.61 -74.33 153.68 o -8 0 2 0.38 -45.22 111.56 o -7 0 2 5.22 -24.00 91.46 o -6 0 2 681.12 675.71 167.98 o -5 0 2 20.27 17.79 12.52 o -4 0 2 481.57 471.30 29.64 o -3 0 2 3952.16 3787.81 141.66 o -2 0 2 3519.66 3170.77 105.77 o -1 0 2 2957.92 2540.37 82.33 o 0 0 2 261.75 246.86 17.39 o 1 0 2 11014.01 10163.13 255.73 o 2 0 2 135.04 138.51 23.85 o 3 0 2 61.72 47.97 25.41 o 4 0 2 1781.41 1991.03 102.89 o 5 0 2 210.68 247.54 38.16 o 6 0 2 530.15 509.36 62.90 o 7 0 2 82.85 63.41 33.00 o 8 0 2 92.50 30.55 83.98 o -8 1 2 34.80 -25.32 97.44 o -7 1 2 8.32 19.62 18.57 o -6 1 2 0.93 -8.44 20.56 o -5 1 2 198.10 178.77 27.81 o -4 1 2 521.56 503.13 34.85 o -3 1 2 1443.15 1515.80 46.05 o -2 1 2 6120.52 5926.73 132.84 o -1 1 2 2036.72 1959.29 63.92 o 0 1 2 8.82 24.70 12.09 o 1 1 2 357.88 349.54 20.09 o 2 1 2 2319.07 2378.58 57.01 o 3 1 2 27.65 37.00 18.16 o 4 1 2 552.75 575.77 53.49 o 5 1 2 9.84 3.20 24.51 o 6 1 2 35.82 41.33 25.66 o 7 1 2 21.89 3.84 23.09 o 8 1 2 31.15 11.99 41.18 o -8 2 2 11.76 29.03 28.78 o -7 2 2 2.11 -65.79 43.86 o -6 2 2 8.79 28.28 31.57 o -5 2 2 308.72 225.25 44.81 o -4 2 2 1143.60 1313.29 68.82 o -3 2 2 12.14 8.29 12.14 o -2 2 2 548.35 557.51 26.47 o -1 2 2 3332.35 3134.17 98.03 o 0 2 2 8.65 -7.92 14.50 o 1 2 2 1005.92 939.10 48.48 o 2 2 2 509.85 550.15 29.39 o 3 2 2 23.59 6.48 17.52 o 4 2 2 388.05 406.05 32.84 o 5 2 2 94.03 77.85 24.28 o 6 2 2 11.98 5.79 18.33 o 7 2 2 61.40 34.65 53.70 o 8 2 2 4.49 53.05 61.76 o -8 3 2 97.46 102.90 109.83 o -7 3 2 12.64 -49.20 47.02 o -6 3 2 311.08 364.28 52.62 o -5 3 2 0.06 -47.95 31.96 o -4 3 2 1548.45 1634.06 61.99 o -3 3 2 454.09 495.00 34.64 o -2 3 2 294.66 275.37 23.17 o -1 3 2 64.24 49.38 19.02 o 0 3 2 6656.06 6719.89 159.45 o 1 3 2 3435.95 3468.96 102.05 o 2 3 2 5249.03 5612.07 142.39 o 3 3 2 98.09 105.97 21.93 o 4 3 2 287.04 284.28 28.71 o 5 3 2 78.67 23.31 26.43 o 6 3 2 75.22 117.67 41.11 o 7 3 2 60.87 29.00 56.88 o 8 3 2 25.30 -41.18 100.32 o -9 4 2 3.96 111.73 95.20 o -8 4 2 37.92 30.56 61.63 o -7 4 2 298.27 288.03 60.69 o -6 4 2 1607.79 1846.87 121.44 o -5 4 2 22.98 40.05 39.15 o -4 4 2 710.43 750.98 45.30 o -3 4 2 850.30 830.30 39.28 o -2 4 2 5172.93 5444.67 148.79 o -1 4 2 1195.45 1233.00 52.47 o 0 4 2 355.59 331.42 33.23 o 1 4 2 1505.92 1452.71 64.01 o 2 4 2 0.30 18.33 24.42 o 3 4 2 251.64 326.11 35.22 o 4 4 2 223.79 201.09 31.34 o 5 4 2 193.48 140.74 48.59 o 6 4 2 187.90 230.84 39.05 o 7 4 2 0.12 -73.15 68.25 o 8 4 2 35.99 8.92 73.54 o -8 5 2 5.16 8.75 64.22 o -7 5 2 3.84 33.10 67.33 o -6 5 2 96.54 88.00 53.15 o -5 5 2 18.81 32.16 19.12 o -4 5 2 77.52 65.29 29.35 o -3 5 2 1.39 53.09 34.64 o -2 5 2 3574.81 3862.16 130.56 o -1 5 2 1.33 -4.56 27.18 o 0 5 2 11.86 -0.57 37.93 o 1 5 2 0.99 -6.22 26.88 o 2 5 2 2.86 -6.40 26.25 o 3 5 2 25.38 -6.54 25.86 o 4 5 2 121.67 120.04 33.24 o 5 5 2 379.38 427.00 48.73 o 6 5 2 3.51 -2.12 29.67 o 7 5 2 5.98 69.76 74.37 o 8 5 2 13.53 78.72 87.53 o -8 6 2 380.41 238.43 128.82 o -7 6 2 4.90 -27.23 63.62 o -6 6 2 662.31 471.75 103.16 o -5 6 2 177.60 152.41 32.44 o -4 6 2 0.95 -30.35 28.12 o -3 6 2 18.96 43.42 34.15 o -2 6 2 1249.63 1225.84 73.36 o -1 6 2 1585.03 1722.97 76.90 o 0 6 2 3572.48 3956.16 137.28 o 1 6 2 3.42 -48.90 32.60 o 2 6 2 273.38 227.94 49.28 o 3 6 2 230.75 271.70 46.02 o 4 6 2 148.58 122.52 33.98 o 5 6 2 7.40 12.12 32.21 o 6 6 2 11.72 23.16 33.55 o 7 6 2 44.26 73.10 105.78 o 8 6 2 5.79 -142.41 210.08 o -8 7 2 36.56 -47.46 106.00 o -7 7 2 7.58 12.51 86.28 o -6 7 2 47.43 54.13 62.34 o -5 7 2 122.50 226.59 44.19 o -4 7 2 262.31 294.78 58.83 o -3 7 2 119.36 113.48 36.70 o -2 7 2 494.84 440.63 82.11 o -1 7 2 17.53 38.25 36.59 o 0 7 2 3145.97 3579.75 174.32 o 1 7 2 110.24 100.53 40.91 o 2 7 2 3826.99 4175.03 179.89 o 3 7 2 31.25 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