#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2202941.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202941_Fobs loop_ _publ_author_name 'Becker, Steffi' 'Lerner, Hans-Wolfram' 'Bolte, Michael' _publ_section_title ; Diammonium tetrathiocyanatocobaltate(II) tetrahydrate ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i156 _journal_page_last i157 _journal_volume 59 _journal_year 2003 _space_group_IT_number 114 _symmetry_space_group_name_Hall 'P -4 2n' _symmetry_space_group_name_H-M 'P -4 21 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.2050 _cell_length_b 12.2050 _cell_length_c 5.3588 _exptl_crystal_F_000 394.00 _reflns_d_resolution_high 0.7770 _[local]_cod_data_source_file wm6002Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa255 in P-42(1)c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 2 0 1312.16 1692.08 25.04 o 1 3 0 773.49 851.83 13.72 o 2 3 0 3155.37 3423.01 50.24 o 3 3 0 255.82 794.79 15.88 o 0 4 0 761.32 494.63 15.51 o 1 4 0 3327.05 3477.52 35.24 o 2 4 0 9718.13 11210.41 132.54 o 3 4 0 155.79 357.46 9.23 o 4 4 0 1189.24 993.52 28.66 o 1 5 0 29.39 1.61 7.75 o 2 5 0 26.22 46.98 9.11 o 3 5 0 424.23 256.08 8.19 o 4 5 0 76.65 79.97 7.22 o 5 5 0 1265.97 1494.11 15.19 o 0 6 0 44.98 34.44 10.25 o 1 6 0 10.04 5.66 7.18 o 2 6 0 3042.01 3194.86 45.27 o 3 6 0 281.57 150.09 8.14 o 4 6 0 1689.10 1486.71 23.55 o 5 6 0 15.28 16.34 6.58 o 6 6 0 1083.22 891.91 21.77 o 1 7 0 722.03 675.90 7.53 o 2 7 0 756.66 737.61 12.78 o 3 7 0 725.15 674.94 8.31 o 4 7 0 198.41 311.93 6.93 o 5 7 0 16.61 14.26 6.11 o 6 7 0 376.82 378.14 6.64 o 7 7 0 103.31 164.28 9.65 o 0 8 0 2906.61 2736.57 84.46 o 1 8 0 68.44 49.08 6.37 o 2 8 0 171.55 137.15 6.27 o 3 8 0 221.28 208.82 6.33 o 4 8 0 1224.87 1235.67 19.87 o 5 8 0 357.14 439.95 9.58 o 6 8 0 8.80 9.95 5.36 o 7 8 0 14.54 14.29 5.76 o 8 8 0 342.51 289.24 7.80 o 1 9 0 14.45 22.94 6.26 o 2 9 0 204.03 243.04 7.12 o 3 9 0 728.95 824.34 13.38 o 4 9 0 83.11 66.51 6.32 o 5 9 0 208.04 218.62 5.84 o 6 9 0 278.78 314.41 5.91 o 7 9 0 168.59 221.58 5.85 o 8 9 0 9.59 9.54 5.02 o 9 9 0 4.66 7.32 6.50 o 0 10 0 277.56 296.85 9.14 o 1 10 0 20.28 29.09 5.91 o 2 10 0 48.01 27.95 6.09 o 3 10 0 0.77 2.63 5.24 o 4 10 0 880.48 877.44 17.66 o 5 10 0 61.80 50.71 5.53 o 6 10 0 81.00 87.48 5.14 o 7 10 0 119.44 123.11 4.77 o 8 10 0 73.74 71.69 5.04 o 9 10 0 0.00 3.26 4.43 o 10 10 0 3.58 5.81 6.66 o 1 11 0 111.53 150.64 6.40 o 2 11 0 114.93 113.97 6.18 o 3 11 0 98.52 137.18 6.19 o 4 11 0 0.02 -0.83 5.61 o 5 11 0 56.19 57.79 5.00 o 6 11 0 52.99 54.43 5.44 o 7 11 0 6.20 13.73 4.90 o 8 11 0 44.10 33.12 4.70 o 9 11 0 2.91 7.25 4.63 o 10 11 0 22.99 13.88 4.65 o 11 11 0 55.72 67.28 6.29 o 0 12 0 23.20 33.75 7.32 o 1 12 0 3.46 6.88 5.52 o 2 12 0 220.18 195.64 5.88 o 3 12 0 115.86 120.65 6.06 o 4 12 0 7.61 7.97 5.84 o 5 12 0 10.24 9.11 4.72 o 6 12 0 43.28 33.39 5.08 o 7 12 0 16.19 21.16 4.70 o 8 12 0 18.25 17.26 4.52 o 9 12 0 35.00 30.53 4.66 o 10 12 0 35.35 22.81 6.41 o 1 13 0 19.13 15.69 5.75 o 2 13 0 129.30 117.58 5.90 o 3 13 0 1.61 3.06 5.52 o 4 13 0 3.34 3.85 5.23 o 5 13 0 76.29 108.25 4.92 o 6 13 0 3.49 4.41 4.56 o 7 13 0 34.77 37.80 4.86 o 8 13 0 33.79 31.76 4.73 o 0 14 0 0.41 -2.07 8.47 o 1 14 0 7.10 6.55 6.61 o 2 14 0 36.46 31.83 5.60 o 3 14 0 0.06 4.18 5.71 o 4 14 0 19.30 11.81 4.76 o 5 14 0 3.24 9.84 4.99 o 6 14 0 97.96 91.73 5.23 o 7 14 0 2.67 1.52 10.10 o 1 15 0 11.70 23.76 5.93 o 2 15 0 4.62 5.83 5.62 o 3 15 0 20.69 14.41 4.98 o 4 15 0 12.88 7.47 5.14 o 0 1 1 336.98 520.72 21.32 o -1 2 1 4185.39 3004.55 57.74 o 0 2 1 137.28 116.80 12.48 o 1 2 1 4193.21 3043.95 67.07 o -2 3 1 5070.66 5118.77 88.84 o -1 3 1 7886.63 9777.37 97.64 o 0 3 1 4062.96 4562.97 54.46 o 1 3 1 7836.19 9386.56 76.92 o 2 3 1 5376.78 5752.38 77.19 o -3 4 1 599.48 328.92 7.73 o -2 4 1 93.77 290.29 8.48 o -1 4 1 928.23 1044.35 11.79 o 0 4 1 5425.70 5606.49 68.11 o 1 4 1 966.20 1092.67 17.85 o 2 4 1 100.09 287.45 10.57 o 3 4 1 663.85 385.77 12.01 o -4 5 1 3029.03 3150.77 52.85 o -3 5 1 62.86 44.24 6.95 o -2 5 1 364.30 419.91 7.83 o -1 5 1 775.95 775.05 10.54 o 0 5 1 719.92 227.40 8.38 o 1 5 1 780.82 809.12 10.21 o 2 5 1 322.78 379.15 9.01 o 3 5 1 66.48 46.02 10.22 o 4 5 1 2926.47 3175.70 42.11 o -5 6 1 123.42 98.93 5.52 o -4 6 1 816.49 875.67 17.32 o -3 6 1 359.55 270.48 6.79 o -2 6 1 534.66 655.24 7.43 o -1 6 1 2057.84 2150.62 50.32 o 0 6 1 357.00 326.70 8.81 o 1 6 1 2171.81 2320.65 22.06 o 2 6 1 524.26 666.51 18.15 o 3 6 1 309.84 224.82 8.30 o 4 6 1 799.44 956.22 29.07 o 5 6 1 122.89 95.49 9.37 o -6 7 1 865.57 846.95 26.60 o -5 7 1 266.90 217.35 6.53 o -4 7 1 259.77 247.07 5.66 o -3 7 1 472.78 442.09 5.93 o -2 7 1 469.35 450.01 6.23 o -1 7 1 498.08 656.57 10.56 o 0 7 1 1991.01 2132.33 23.65 o 1 7 1 494.74 649.49 13.49 o 2 7 1 557.18 530.04 6.75 o 3 7 1 467.05 445.88 9.32 o 4 7 1 271.95 265.01 6.84 o 5 7 1 267.56 223.82 7.10 o 6 7 1 810.21 852.81 18.54 o -7 8 1 244.68 269.16 8.12 o -6 8 1 39.95 33.98 4.74 o -5 8 1 428.22 425.29 10.85 o -4 8 1 237.31 212.21 6.31 o -3 8 1 1138.65 1166.00 23.44 o -2 8 1 191.06 172.62 6.05 o -1 8 1 195.96 175.43 6.20 o 0 8 1 70.89 69.12 7.48 o 1 8 1 235.24 208.49 7.32 o 2 8 1 185.28 170.11 6.79 o 3 8 1 1128.70 1156.36 15.71 o 4 8 1 238.52 228.70 7.54 o 5 8 1 435.05 458.85 10.01 o 6 8 1 40.59 38.32 7.25 o 7 8 1 222.70 255.83 8.56 o -8 9 1 46.60 39.71 4.30 o -7 9 1 11.65 17.70 4.80 o -6 9 1 228.45 213.24 5.33 o -5 9 1 11.98 12.55 4.96 o -4 9 1 106.72 107.22 5.35 o -3 9 1 22.34 19.78 5.30 o -2 9 1 654.81 640.30 16.06 o -1 9 1 58.35 53.45 6.07 o 0 9 1 261.73 292.06 6.41 o 1 9 1 55.39 62.70 7.38 o 2 9 1 626.45 664.15 15.16 o 3 9 1 23.08 24.17 6.29 o 4 9 1 112.24 118.11 7.74 o 5 9 1 12.08 13.44 7.37 o 6 9 1 234.02 234.25 6.86 o 7 9 1 11.79 11.22 5.57 o 8 9 1 61.55 63.88 5.92 o -9 10 1 167.88 167.99 5.16 o -8 10 1 54.09 47.78 4.70 o -7 10 1 79.64 71.31 4.64 o -6 10 1 66.77 69.03 5.05 o -5 10 1 23.65 28.88 4.97 o -4 10 1 124.85 125.71 5.36 o -3 10 1 65.24 71.66 5.73 o -2 10 1 14.32 14.70 5.78 o -1 10 1 578.26 553.99 6.20 o 0 10 1 397.41 386.75 8.00 o 1 10 1 560.88 568.74 8.82 o 2 10 1 14.08 15.89 6.67 o 3 10 1 84.10 86.60 5.73 o 4 10 1 125.06 132.14 6.72 o 5 10 1 26.92 33.61 6.80 o 6 10 1 64.83 84.65 6.68 o 7 10 1 85.23 79.09 6.02 o 8 10 1 53.30 51.23 5.68 o 9 10 1 167.82 189.32 6.07 o -10 11 1 8.25 10.54 4.54 o -9 11 1 0.25 2.47 4.51 o -8 11 1 59.49 60.08 4.27 o -7 11 1 41.56 50.22 4.73 o -6 11 1 160.32 168.91 4.71 o -5 11 1 67.99 75.61 5.03 o -4 11 1 69.87 66.22 5.32 o -3 11 1 14.31 10.16 5.80 o -2 11 1 191.17 201.94 7.29 o -1 11 1 72.90 80.03 5.19 o 0 11 1 0.64 2.95 5.79 o 1 11 1 73.96 77.95 5.48 o 2 11 1 200.47 228.60 6.24 o 3 11 1 14.46 11.23 5.25 o 4 11 1 82.57 82.24 5.19 o 5 11 1 67.64 74.76 5.80 o 6 11 1 158.32 195.25 6.87 o 7 11 1 41.19 53.03 5.59 o 8 11 1 58.95 59.37 5.86 o 9 11 1 0.16 2.29 5.15 o 10 11 1 11.13 12.42 4.91 o -9 12 1 18.27 22.79 4.80 o -8 12 1 2.64 6.44 4.33 o -7 12 1 8.94 12.84 4.60 o -6 12 1 7.67 6.56 4.85 o -5 12 1 285.49 271.14 6.18 o -4 12 1 0.55 -0.21 5.13 o -3 12 1 95.36 106.89 5.45 o -2 12 1 6.03 12.32 5.41 o -1 12 1 38.17 45.10 5.55 o 0 12 1 34.70 37.18 5.70 o 1 12 1 26.48 30.88 5.27 o 2 12 1 6.16 8.18 5.94 o 3 12 1 103.38 112.80 6.13 o 4 12 1 0.56 2.77 6.30 o 5 12 1 285.15 297.02 6.67 o 6 12 1 8.01 8.14 5.13 o 7 12 1 14.77 21.47 5.25 o 8 12 1 2.73 7.37 4.64 o 9 12 1 17.74 20.53 5.08 o -8 13 1 52.01 32.35 4.72 o -7 13 1 1.02 2.27 4.09 o -6 13 1 10.58 12.02 4.95 o -5 13 1 7.08 5.89 4.84 o -4 13 1 48.50 50.73 5.28 o -3 13 1 3.99 7.32 5.12 o -2 13 1 71.28 62.51 5.12 o -1 13 1 5.75 5.36 4.99 o 0 13 1 51.14 47.80 5.47 o 1 13 1 5.81 6.06 5.57 o 2 13 1 64.63 58.17 5.28 o 3 13 1 4.17 9.78 5.58 o 4 13 1 46.79 54.18 6.34 o 5 13 1 6.65 7.76 5.99 o 6 13 1 16.03 16.69 5.42 o 7 13 1 1.01 3.93 4.96 o 8 13 1 51.46 33.98 5.41 o -6 14 1 3.86 -4.27 4.99 o -5 14 1 0.59 5.40 4.88 o -4 14 1 19.62 20.00 4.75 o -3 14 1 23.45 31.31 5.14 o -2 14 1 4.61 6.53 4.95 o -1 14 1 65.87 69.80 5.31 o 0 14 1 3.03 6.89 5.33 o 1 14 1 64.12 64.08 5.09 o 2 14 1 4.57 3.05 5.95 o 3 14 1 20.50 25.86 5.64 o 4 14 1 18.85 13.83 5.74 o 5 14 1 1.56 1.22 5.76 o 6 14 1 3.71 0.84 5.29 o -3 15 1 10.84 9.20 4.92 o -2 15 1 3.12 2.25 5.30 o -1 15 1 2.39 0.54 4.88 o 0 15 1 24.60 25.96 5.01 o 1 15 1 2.39 2.47 5.35 o 2 15 1 2.67 2.73 5.54 o 3 15 1 11.01 10.08 5.65 o 0 0 2 3967.56 6282.40 55.65 o -1 1 2 1645.26 1618.20 29.48 o 0 1 2 1083.09 1154.88 17.53 o 1 1 2 1929.00 1885.04 31.67 o -2 2 2 1582.43 1549.47 64.59 o -1 2 2 898.92 1284.96 12.85 o 0 2 2 294.04 156.95 9.76 o 1 2 2 927.57 1282.80 9.53 o 2 2 2 1529.80 1498.94 14.33 o -3 3 2 2429.24 2234.78 15.27 o -2 3 2 270.07 279.17 8.74 o -1 3 2 1877.08 2059.06 21.50 o 0 3 2 488.44 424.31 9.51 o 1 3 2 1886.57 2099.44 10.30 o 2 3 2 273.89 267.45 8.50 o 3 3 2 2205.28 1939.97 18.76 o -4 4 2 1077.69 978.14 25.91 o -3 4 2 75.12 86.24 6.59 o -2 4 2 3210.43 3378.01 38.08 o -1 4 2 486.45 477.89 9.96 o 0 4 2 1266.22 1025.63 14.26 o 1 4 2 491.30 469.93 7.65 o 2 4 2 3229.27 3498.82 45.00 o 3 4 2 73.88 85.18 7.95 o 4 4 2 1183.47 1100.76 20.27 o -5 5 2 1223.12 1221.74 24.28 o -4 5 2 430.65 394.45 8.04 o -3 5 2 1935.29 1862.69 27.21 o -2 5 2 1118.51 1102.75 12.01 o -1 5 2 687.83 579.45 7.12 o 0 5 2 49.28 44.09 7.45 o 1 5 2 727.18 622.83 7.94 o 2 5 2 1134.14 1116.52 18.49 o 3 5 2 2080.56 2052.81 19.53 o 4 5 2 431.50 395.45 7.26 o 5 5 2 1200.24 1175.93 62.55 o -6 6 2 312.79 288.62 7.34 o -5 6 2 161.14 176.46 5.41 o -4 6 2 456.65 459.82 6.30 o -3 6 2 805.30 810.16 11.14 o -2 6 2 990.60 1017.86 19.80 o -1 6 2 578.85 590.44 7.84 o 0 6 2 1009.45 1011.12 7.70 o 1 6 2 583.15 605.57 12.65 o 2 6 2 970.88 1042.08 14.40 o 3 6 2 790.56 856.71 9.25 o 4 6 2 442.72 431.77 14.15 o 5 6 2 163.49 177.18 8.94 o 6 6 2 282.26 299.39 16.76 o -7 7 2 725.32 791.17 17.54 o -6 7 2 61.77 72.24 5.02 o -5 7 2 270.16 257.43 5.53 o -4 7 2 2.96 5.93 5.77 o -3 7 2 190.07 155.50 5.59 o -2 7 2 133.23 136.75 6.02 o -1 7 2 1591.67 1522.73 19.87 o 0 7 2 18.82 46.82 6.37 o 1 7 2 1470.45 1423.17 28.74 o 2 7 2 131.36 130.98 6.47 o 3 7 2 175.04 145.50 7.17 o 4 7 2 2.97 5.45 7.89 o 5 7 2 208.81 215.70 11.66 o 6 7 2 62.69 80.36 10.17 o 7 7 2 766.85 994.29 17.96 o -8 8 2 114.13 132.48 6.93 o -7 8 2 0.17 -0.07 4.51 o -6 8 2 214.06 200.19 4.64 o -5 8 2 265.78 278.37 5.08 o -4 8 2 346.86 373.00 5.18 o -3 8 2 1.27 2.19 5.31 o -2 8 2 97.79 102.87 6.42 o -1 8 2 267.59 260.81 6.38 o 0 8 2 419.50 463.43 7.56 o 1 8 2 268.05 262.45 6.29 o 2 8 2 111.39 112.57 6.00 o 3 8 2 1.64 3.99 5.88 o 4 8 2 333.30 363.60 21.23 o 5 8 2 267.75 298.48 9.52 o 6 8 2 218.51 225.72 30.93 o 7 8 2 0.22 5.99 10.12 o 8 8 2 105.58 136.56 11.43 o -9 9 2 50.82 54.84 6.50 o -8 9 2 25.81 28.94 4.24 o -7 9 2 182.99 170.40 5.15 o -6 9 2 120.97 110.18 4.43 o -5 9 2 80.51 74.85 4.64 o -4 9 2 132.64 133.77 5.29 o -3 9 2 388.03 400.40 7.65 o -2 9 2 201.80 210.84 6.55 o -1 9 2 135.76 123.65 5.60 o 0 9 2 110.16 103.48 5.57 o 1 9 2 171.61 162.09 6.01 o 2 9 2 200.21 214.06 7.41 o 3 9 2 428.24 449.80 17.95 o 4 9 2 133.07 133.57 6.12 o 5 9 2 67.35 64.87 6.55 o 6 9 2 127.09 125.51 7.78 o 7 9 2 174.84 175.89 7.94 o 8 9 2 26.09 26.11 7.38 o 9 9 2 49.37 52.70 9.15 o -10 10 2 36.51 27.15 6.29 o -9 10 2 3.63 3.51 4.29 o -8 10 2 126.55 116.76 4.42 o -7 10 2 4.06 5.95 4.37 o -6 10 2 94.77 98.97 4.62 o -5 10 2 61.58 73.63 4.66 o -4 10 2 38.57 44.52 4.84 o -3 10 2 59.11 61.07 5.00 o -2 10 2 161.48 156.38 5.33 o -1 10 2 56.44 66.09 5.44 o 0 10 2 414.33 430.54 9.50 o 1 10 2 58.71 57.75 5.97 o 2 10 2 179.25 183.18 8.81 o 3 10 2 59.98 60.19 6.42 o 4 10 2 29.52 31.65 6.16 o 5 10 2 63.66 81.22 5.80 o 6 10 2 104.49 121.12 7.70 o 7 10 2 4.00 4.84 6.38 o 8 10 2 129.37 127.93 7.13 o 9 10 2 3.45 3.92 6.76 o 10 10 2 36.14 33.06 9.43 o -10 11 2 9.03 13.61 3.86 o -9 11 2 41.30 46.24 4.09 o -8 11 2 0.64 0.65 4.25 o -7 11 2 28.49 30.39 4.19 o -6 11 2 1.27 2.83 4.31 o -5 11 2 103.75 85.45 4.66 o -4 11 2 11.56 15.74 4.95 o -3 11 2 160.43 147.93 4.93 o -2 11 2 42.00 36.85 4.69 o -1 11 2 237.89 226.70 5.67 o 0 11 2 6.12 8.74 5.99 o 1 11 2 250.91 253.67 9.18 o 2 11 2 43.43 40.49 5.97 o 3 11 2 133.58 131.27 6.95 o 4 11 2 11.46 12.02 5.79 o 5 11 2 118.90 108.64 6.19 o 6 11 2 1.23 2.54 5.99 o 7 11 2 32.84 37.46 6.49 o 8 11 2 0.71 7.73 7.54 o 9 11 2 43.84 52.52 5.71 o 10 11 2 9.32 12.85 6.07 o -9 12 2 22.51 26.74 13.09 o -8 12 2 18.15 16.53 4.28 o -7 12 2 0.98 2.84 4.24 o -6 12 2 25.48 23.85 4.17 o -5 12 2 3.91 2.56 4.48 o -4 12 2 53.26 45.09 4.78 o -3 12 2 31.97 33.91 5.08 o -2 12 2 148.31 142.80 5.07 o -1 12 2 13.12 14.60 5.15 o 0 12 2 55.52 78.22 5.24 o 1 12 2 13.20 12.57 5.86 o 2 12 2 150.07 158.92 5.77 o 3 12 2 31.69 33.09 6.62 o 4 12 2 53.05 53.50 6.40 o 5 12 2 3.75 -2.31 6.37 o 6 12 2 25.19 29.19 6.37 o 7 12 2 0.95 3.15 5.91 o 8 12 2 18.67 19.54 6.37 o -7 13 2 19.75 17.14 4.77 o -6 13 2 2.70 3.55 4.81 o -5 13 2 36.92 32.69 4.86 o -4 13 2 6.04 6.08 4.74 o -3 13 2 14.61 23.71 5.02 o -2 13 2 35.43 32.56 4.74 o -1 13 2 99.84 83.85 5.37 o 0 13 2 18.95 17.85 5.29 o 1 13 2 106.00 83.30 4.96 o 2 13 2 35.97 37.48 5.27 o 3 13 2 12.51 23.43 6.57 o 4 13 2 6.33 7.90 7.08 o 5 13 2 35.03 38.13 7.18 o 6 13 2 2.84 3.58 6.05 o 7 13 2 15.94 20.81 6.37 o -5 14 2 7.77 3.90 4.76 o -4 14 2 10.77 10.96 4.96 o -3 14 2 0.82 3.33 4.79 o -2 14 2 32.52 34.26 4.77 o -1 14 2 19.65 12.97 5.12 o 0 14 2 55.98 58.44 5.17 o 1 14 2 18.98 13.61 5.15 o 2 14 2 28.90 28.45 5.62 o 3 14 2 0.73 7.17 6.23 o 4 14 2 9.46 13.00 7.06 o 5 14 2 7.52 7.58 7.25 o -1 15 2 20.10 11.94 10.60 o 0 15 2 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