#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/29/2202947.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202947_Fobs loop_ _publ_author_name 'Rajagopal, K.' 'Krishnakumar, R. V.' 'Subha Nandhini, M.' 'Natarajan, S.' _publ_section_title ; L-Histidinium hemihydrochloride tartrate tartaric acid dihydrate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o955 _journal_page_last o958 _journal_volume 59 _journal_year 2003 _space_group_IT_number 5 _symmetry_space_group_name_Hall 'C 2y' _symmetry_space_group_name_H-M 'C 1 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.192 _cell_angle_gamma 90.000 _cell_length_a 35.8568 _cell_length_b 7.4806 _cell_length_c 7.6783 _exptl_crystal_F_000 1066.00 _reflns_d_resolution_high 0.8315 _[local]_cod_data_source_file wn6166Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 200.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1735.24 2468.36 37.62 o 4 0 0 48.19 10.36 0.97 o 6 0 0 395.93 419.91 5.07 o 8 0 0 35866.52 32516.04 342.38 o 10 0 0 3233.79 3021.96 16.45 o 12 0 0 509.53 281.98 5.98 o 14 0 0 167.16 70.12 2.28 o 16 0 0 409.07 531.35 9.14 o 18 0 0 1255.74 1470.48 16.36 o 20 0 0 4765.26 5126.86 33.39 o 22 0 0 1609.61 1482.67 18.58 o 24 0 0 220.98 248.62 7.52 o 26 0 0 40.87 78.20 3.97 o 28 0 0 773.31 828.04 16.93 o 30 0 0 1804.66 1957.05 26.81 o 32 0 0 2717.87 2785.02 32.16 o 34 0 0 24.88 32.30 3.48 o 36 0 0 215.34 253.06 7.37 o 38 0 0 166.54 161.66 5.54 o 40 0 0 515.94 532.63 11.98 o 42 0 0 20.54 34.19 3.35 o 1 1 0 6649.70 5516.90 88.28 o 3 1 0 1275.53 519.95 5.45 o 5 1 0 5618.13 5098.25 18.29 o 7 1 0 19244.57 16997.89 227.82 o 9 1 0 12154.62 10918.16 186.44 o 11 1 0 2395.24 2191.10 15.75 o 13 1 0 1779.39 1465.68 13.82 o 15 1 0 1252.06 1283.47 13.83 o 17 1 0 5762.58 5479.91 31.74 o 19 1 0 2837.75 2786.21 23.53 o 21 1 0 1961.84 2168.72 22.53 o 23 1 0 88.30 102.97 3.73 o 25 1 0 643.47 741.96 14.90 o 27 1 0 266.73 285.93 8.76 o 29 1 0 1743.19 1815.90 25.23 o 31 1 0 35.71 22.64 3.11 o 33 1 0 593.96 561.42 14.90 o 35 1 0 295.82 269.19 8.28 o 37 1 0 260.28 212.29 6.36 o 39 1 0 192.61 191.22 5.65 o 41 1 0 4.60 11.72 3.35 o 0 2 0 8106.86 8528.59 27.96 o 2 2 0 37328.50 39788.91 401.59 o 4 2 0 6023.92 5154.38 23.23 o 6 2 0 12201.52 11273.86 37.85 o 8 2 0 5502.61 4921.18 24.38 o 10 2 0 267.80 249.34 6.04 o 12 2 0 9780.98 8889.88 37.78 o 14 2 0 23.52 15.53 1.93 o 16 2 0 2130.59 1845.46 18.46 o 18 2 0 3912.28 3636.90 27.93 o 20 2 0 893.70 955.27 15.25 o 22 2 0 488.65 514.56 12.08 o 24 2 0 1337.28 1392.53 20.51 o 26 2 0 2257.59 2430.19 28.61 o 28 2 0 24.53 28.84 3.44 o 30 2 0 257.17 234.03 7.09 o 32 2 0 243.33 259.02 7.46 o 34 2 0 995.65 980.57 18.88 o 36 2 0 1023.99 1076.27 18.89 o 38 2 0 1247.31 1261.31 19.02 o 40 2 0 123.76 115.27 4.68 o 1 3 0 2564.19 1984.36 16.20 o 3 3 0 8724.94 8095.27 34.53 o 5 3 0 93.27 134.76 4.11 o 7 3 0 1921.38 2109.90 18.48 o 9 3 0 1698.70 1423.01 15.65 o 11 3 0 638.56 639.42 11.08 o 13 3 0 2799.99 3012.16 24.47 o 15 3 0 255.52 325.41 8.86 o 17 3 0 1828.28 1944.13 21.91 o 19 3 0 2280.22 2472.84 26.15 o 21 3 0 83.25 70.39 3.77 o 23 3 0 60.22 68.32 3.94 o 25 3 0 1001.40 894.83 18.04 o 27 3 0 239.98 236.07 6.49 o 29 3 0 207.45 192.15 6.23 o 31 3 0 973.83 975.89 19.26 o 33 3 0 324.27 327.92 9.63 o 35 3 0 109.25 145.17 5.58 o 37 3 0 72.35 58.48 3.96 o 39 3 0 93.25 88.48 4.23 o 0 4 0 110.42 104.56 3.34 o 2 4 0 1878.16 1814.37 18.85 o 4 4 0 963.30 918.58 13.72 o 6 4 0 742.41 657.03 12.29 o 8 4 0 334.46 298.11 7.78 o 10 4 0 2332.11 2165.80 23.22 o 12 4 0 912.78 873.74 14.99 o 14 4 0 670.21 745.16 14.56 o 16 4 0 97.23 111.44 4.60 o 18 4 0 524.41 507.21 13.23 o 20 4 0 572.82 508.38 13.56 o 22 4 0 236.60 238.81 7.17 o 24 4 0 720.27 741.44 16.76 o 26 4 0 195.96 208.52 6.50 o 28 4 0 192.33 193.82 6.26 o 30 4 0 576.30 562.98 14.59 o 32 4 0 75.52 77.76 4.68 o 34 4 0 272.67 272.55 8.33 o 36 4 0 351.98 369.06 9.70 o 38 4 0 478.19 486.47 9.65 o 1 5 0 356.39 404.68 10.98 o 3 5 0 1121.69 1176.16 18.35 o 5 5 0 709.37 778.67 15.27 o 7 5 0 313.87 354.19 9.50 o 9 5 0 830.15 723.86 15.47 o 11 5 0 391.68 356.33 10.05 o 13 5 0 770.55 768.59 16.69 o 15 5 0 1012.65 880.76 18.30 o 17 5 0 776.73 787.49 17.28 o 19 5 0 2076.15 1954.40 27.44 o 21 5 0 149.65 136.19 5.88 o 23 5 0 82.33 80.79 4.65 o 25 5 0 56.83 59.82 4.11 o 27 5 0 543.45 533.97 14.21 o 29 5 0 326.38 320.61 9.52 o 31 5 0 138.65 154.58 5.42 o 33 5 0 35.24 26.84 3.11 o 35 5 0 53.06 49.19 3.44 o 0 6 0 1113.87 1152.41 20.02 o 2 6 0 1338.68 1470.24 23.17 o 4 6 0 337.41 354.19 10.79 o 6 6 0 187.39 181.68 6.25 o 8 6 0 1735.10 1665.65 25.28 o 10 6 0 5.74 -4.81 4.81 o 12 6 0 917.83 991.10 20.26 o 14 6 0 174.53 169.37 6.38 o 16 6 0 171.48 180.90 6.42 o 18 6 0 678.29 631.83 16.15 o 20 6 0 19.12 18.39 5.19 o 22 6 0 19.30 17.93 3.86 o 24 6 0 1020.90 1026.95 18.89 o 26 6 0 13.16 3.03 3.70 o 28 6 0 436.80 400.26 10.65 o 30 6 0 329.29 300.92 8.76 o 32 6 0 74.86 55.41 3.45 o 1 7 0 269.02 307.97 9.33 o 3 7 0 188.31 236.53 7.55 o 5 7 0 366.05 364.89 10.43 o 7 7 0 345.92 332.46 10.20 o 9 7 0 823.49 802.91 18.23 o 11 7 0 406.57 386.54 11.54 o 13 7 0 454.25 385.19 11.25 o 15 7 0 75.22 101.70 5.49 o 17 7 0 297.21 292.31 8.39 o 19 7 0 68.98 76.68 4.77 o 21 7 0 254.85 236.83 7.14 o 23 7 0 43.84 40.00 3.36 o 25 7 0 154.68 152.65 5.05 o 27 7 0 46.19 34.53 3.12 o 0 8 0 236.47 281.01 8.23 o 2 8 0 208.72 175.56 6.68 o 4 8 0 118.92 103.28 5.81 o 6 8 0 116.39 110.32 5.73 o 8 8 0 327.10 313.87 9.43 o 10 8 0 129.37 120.14 5.53 o 12 8 0 8.23 8.89 4.34 o 14 8 0 140.28 145.59 5.26 o 16 8 0 86.59 88.85 4.75 o 18 8 0 25.15 25.38 3.36 o -42 0 1 0.84 4.25 2.86 o -40 0 1 32.54 33.72 3.32 o -38 0 1 762.42 767.07 15.54 o -36 0 1 1687.86 1661.48 24.13 o -34 0 1 29.06 31.69 3.37 o -32 0 1 119.05 155.70 5.61 o -30 0 1 1261.17 1170.73 20.66 o -28 0 1 1540.78 1483.91 22.25 o -26 0 1 1.63 13.76 2.73 o -24 0 1 37.83 105.81 4.20 o -22 0 1 479.73 397.62 10.08 o -20 0 1 1323.77 1652.25 18.46 o -18 0 1 114.63 193.92 5.69 o -16 0 1 91.68 162.10 4.86 o -14 0 1 11825.86 12541.90 44.05 o -12 0 1 44.15 83.63 2.62 o -10 0 1 6348.12 6257.13 25.63 o -8 0 1 47.29 24.72 1.49 o -6 0 1 30423.76 29721.76 296.37 o -4 0 1 3034.31 2995.47 12.76 o -2 0 1 22.83 108.02 2.55 o 0 0 1 153.72 241.85 5.42 o 2 0 1 31.04 46.03 1.48 o 4 0 1 1009.50 778.39 6.22 o 6 0 1 70.29 70.84 2.29 o 8 0 1 3187.49 2964.06 15.55 o 10 0 1 4628.92 4601.42 21.52 o 12 0 1 561.31 834.87 9.90 o 14 0 1 7721.21 8371.68 36.13 o 16 0 1 190.49 149.79 4.84 o 18 0 1 1441.29 1370.50 16.33 o 20 0 1 610.57 706.82 12.36 o 22 0 1 400.16 463.60 10.88 o 24 0 1 3115.92 3170.60 29.77 o 26 0 1 6758.55 7185.06 48.20 o 28 0 1 692.09 705.28 15.98 o 30 0 1 1.73 6.90 3.86 o 32 0 1 215.64 191.04 6.03 o 34 0 1 60.49 72.78 4.18 o 36 0 1 24.83 38.29 3.79 o 38 0 1 631.79 592.62 13.31 o 40 0 1 223.64 251.46 7.13 o 42 0 1 108.55 77.59 3.96 o -41 1 1 195.51 204.13 6.23 o -39 1 1 65.99 48.24 3.59 o -37 1 1 215.08 249.19 7.53 o -35 1 1 240.45 282.58 8.25 o -33 1 1 63.15 68.89 4.29 o -31 1 1 995.89 985.61 18.92 o -29 1 1 2354.94 2270.64 28.32 o -27 1 1 1438.39 1647.95 23.44 o -25 1 1 499.13 568.19 13.35 o -23 1 1 336.23 317.85 9.49 o -21 1 1 1005.13 1099.53 15.92 o -19 1 1 435.98 474.53 10.12 o -17 1 1 1054.98 1057.58 13.85 o -15 1 1 4259.68 4104.07 25.40 o -13 1 1 3810.21 3433.17 21.57 o -11 1 1 189.35 141.87 4.06 o -9 1 1 1615.21 1831.14 13.10 o -7 1 1 18728.27 17145.63 230.97 o -5 1 1 9167.87 7752.99 134.04 o -3 1 1 8970.73 8568.38 130.80 o -1 1 1 1049.17 983.07 7.43 o 1 1 1 1013.81 982.89 7.42 o 3 1 1 10374.06 10468.79 146.48 o 5 1 1 6289.97 6392.28 22.73 o 7 1 1 767.41 956.27 8.95 o 9 1 1 1196.81 1301.72 11.48 o 11 1 1 63.52 60.29 2.22 o 13 1 1 600.06 677.52 9.63 o 15 1 1 1844.24 1687.47 16.50 o 17 1 1 2132.81 2020.24 19.32 o 19 1 1 7619.79 7187.47 40.30 o 21 1 1 274.84 285.64 7.38 o 23 1 1 2783.45 2875.13 28.29 o 25 1 1 579.68 562.28 13.29 o 27 1 1 239.27 182.92 5.72 o 29 1 1 881.22 957.82 18.22 o 31 1 1 724.91 608.71 15.52 o 33 1 1 165.37 168.28 5.84 o 35 1 1 54.03 35.49 3.73 o 37 1 1 907.72 919.20 17.03 o 39 1 1 154.02 166.71 5.28 o 41 1 1 137.15 106.98 4.51 o -40 2 1 375.12 347.79 9.17 o -38 2 1 270.34 237.93 6.94 o -36 2 1 17.99 13.61 3.22 o -34 2 1 71.23 66.54 4.44 o -32 2 1 485.08 536.01 14.54 o -30 2 1 90.02 100.21 5.05 o -28 2 1 1039.95 1087.38 19.89 o -26 2 1 2009.58 1956.19 25.63 o -24 2 1 1150.42 1097.18 18.63 o -22 2 1 508.65 478.17 11.65 o -20 2 1 199.27 168.97 5.14 o -18 2 1 44.73 46.35 2.69 o -16 2 1 69.86 57.97 2.69 o -14 2 1 1244.07 1082.57 13.59 o -12 2 1 15991.10 15892.67 54.52 o -10 2 1 9422.46 9643.94 37.94 o -8 2 1 16561.03 16716.49 263.08 o -6 2 1 21213.02 21865.58 296.02 o -4 2 1 11626.20 10436.74 34.67 o -2 2 1 2115.61 2027.28 13.25 o 0 2 1 24629.94 29452.73 554.01 o 2 2 1 2954.54 2357.34 15.13 o 4 2 1 6737.50 6170.32 25.45 o 6 2 1 1781.63 1216.15 11.64 o 8 2 1 7570.15 7575.73 31.98 o 10 2 1 3588.00 3975.26 24.03 o 12 2 1 3701.00 3976.97 24.88 o 14 2 1 32.14 34.28 2.31 o 16 2 1 4227.42 3517.18 26.73 o 18 2 1 2079.61 2128.60 21.70 o 20 2 1 4553.01 4777.74 35.00 o 22 2 1 351.65 382.68 10.95 o 24 2 1 326.49 362.20 9.61 o 26 2 1 523.80 495.16 13.07 o 28 2 1 608.89 590.45 14.94 o 30 2 1 430.19 377.56 10.61 o 32 2 1 102.03 114.33 5.24 o 34 2 1 772.83 719.84 16.15 o 36 2 1 1431.28 1379.89 20.93 o 38 2 1 426.60 425.96 10.99 o 40 2 1 216.87 186.87 5.41 o -39 3 1 24.49 38.37 3.21 o -37 3 1 215.67 218.41 6.65 o -35 3 1 208.23 219.96 6.47 o -33 3 1 423.54 479.09 13.44 o -31 3 1 25.06 21.11 3.50 o -29 3 1 389.10 375.50 10.84 o -27 3 1 877.81 775.40 17.54 o -25 3 1 2613.17 2526.12 29.93 o -23 3 1 92.44 104.77 4.60 o -21 3 1 496.08 550.72 13.46 o -19 3 1 3291.45 3584.52 31.70 o -17 3 1 1782.05 1761.32 20.84 o -15 3 1 163.48 160.33 4.83 o -13 3 1 562.59 579.08 11.19 o -11 3 1 4605.98 4084.63 28.02 o -9 3 1 3233.23 3241.96 23.93 o -7 3 1 2983.85 3133.20 21.94 o -5 3 1 529.69 563.77 9.10 o -3 3 1 7567.36 6813.03 31.31 o -1 3 1 1921.54 1833.26 15.45 o 1 3 1 111.43 211.83 6.15 o 3 3 1 8638.52 8799.35 37.25 o 5 3 1 2977.84 2964.42 22.12 o 7 3 1 3065.78 2952.00 22.06 o 9 3 1 6152.76 5914.58 33.07 o 11 3 1 5380.97 5118.56 32.56 o 13 3 1 480.44 489.56 10.28 o 15 3 1 277.10 226.41 6.77 o 17 3 1 1099.86 967.27 15.80 o 19 3 1 83.56 63.27 3.68 o 21 3 1 53.92 83.11 4.22 o 23 3 1 209.92 201.36 6.19 o 25 3 1 219.69 188.81 5.99 o 27 3 1 125.16 147.17 5.29 o 29 3 1 253.33 236.32 7.76 o 31 3 1 727.25 734.82 16.31 o 33 3 1 874.17 869.36 17.36 o 35 3 1 61.52 65.32 4.18 o 37 3 1 418.77 401.81 10.40 o 39 3 1 219.04 206.80 5.69 o -38 4 1 49.08 54.88 3.43 o -36 4 1 196.57 175.58 5.24 o -34 4 1 124.18 128.95 4.95 o -32 4 1 795.74 825.20 16.90 o -30 4 1 201.52 210.51 6.73 o -28 4 1 298.82 291.80 8.62 o -26 4 1 754.84 725.05 17.31 o -24 4 1 2954.26 2900.26 33.62 o -22 4 1 77.52 66.88 4.23 o -20 4 1 428.89 443.13 12.93 o -18 4 1 1082.69 1067.57 18.82 o -16 4 1 2718.54 2773.41 29.22 o -14 4 1 747.50 806.17 15.15 o -12 4 1 254.30 187.68 5.42 o -10 4 1 2686.97 2793.32 25.70 o -8 4 1 2199.44 2149.70 21.83 o -6 4 1 603.46 505.75 10.77 o -4 4 1 1884.74 1931.20 19.44 o -2 4 1 2793.92 2806.21 23.61 o 0 4 1 1916.50 1996.89 82.23 o 2 4 1 4855.17 5043.14 33.15 o 4 4 1 863.01 841.54 13.92 o 6 4 1 533.66 449.04 10.72 o 8 4 1 220.64 213.28 6.77 o 10 4 1 2456.68 2122.63 23.00 o 12 4 1 2967.53 2846.85 27.46 o 14 4 1 779.71 815.44 15.64 o 16 4 1 3724.89 3447.51 32.79 o 18 4 1 734.94 707.70 15.65 o 20 4 1 127.64 128.16 5.09 o 22 4 1 874.45 891.99 18.40 o 24 4 1 1970.06 1908.56 26.50 o 26 4 1 180.57 169.03 6.02 o 28 4 1 438.63 424.33 11.25 o 30 4 1 284.88 298.09 9.42 o 32 4 1 606.31 596.30 14.02 o 34 4 1 415.03 416.62 10.87 o 36 4 1 102.08 114.07 4.66 o 38 4 1 46.72 38.81 2.97 o -35 5 1 82.63 85.67 3.91 o -33 5 1 242.65 227.50 6.99 o -31 5 1 164.83 158.74 5.32 o -29 5 1 156.48 156.81 5.80 o -27 5 1 7.37 9.89 4.32 o -25 5 1 292.54 295.52 8.68 o -23 5 1 234.10 220.40 6.88 o -21 5 1 1001.01 960.86 19.54 o -19 5 1 645.88 602.40 15.77 o -17 5 1 173.69 186.64 6.33 o -15 5 1 98.17 89.74 4.77 o -13 5 1 18.09 5.51 4.64 o -11 5 1 512.46 496.39 13.09 o -9 5 1 4121.21 4042.04 35.59 o -7 5 1 1901.80 1817.52 23.52 o -5 5 1 955.94 790.94 15.42 o -3 5 1 135.77 127.27 4.77 o -1 5 1 3103.46 3011.77 28.25 o 1 5 1 3268.14 3293.76 31.98 o 3 5 1 22.49 21.11 6.00 o 5 5 1 464.33 509.35 13.25 o 7 5 1 2371.12 2486.54 28.29 o 9 5 1 1129.88 1128.88 19.36 o 11 5 1 924.88 997.45 18.60 o 13 5 1 1957.26 1907.07 25.90 o 15 5 1 73.62 51.21 4.39 o 17 5 1 85.99 103.23 5.12 o 19 5 1 379.18 368.09 11.00 o 21 5 1 1513.64 1503.58 24.52 o 23 5 1 124.85 137.73 5.60 o 25 5 1 281.94 266.24 8.46 o 27 5 1 200.76 201.72 6.78 o 29 5 1 360.89 363.67 9.63 o 31 5 1 350.52 336.16 8.51 o 33 5 1 200.92 215.20 6.60 o 35 5 1 118.39 88.27 3.84 o -32 6 1 120.62 111.82 4.03 o -30 6 1 85.76 84.54 4.13 o -28 6 1 54.38 51.30 3.71 o -26 6 1 213.11 228.36 6.39 o -24 6 1 1.89 2.78 3.86 o -22 6 1 170.66 170.25 6.22 o -20 6 1 551.02 550.21 14.74 o -18 6 1 108.24 102.57 5.24 o -16 6 1 216.57 186.92 6.34 o -14 6 1 1816.30 1714.38 26.23 o -12 6 1 232.16 254.62 7.83 o -10 6 1 525.70 511.32 14.21 o -8 6 1 72.60 74.66 5.18 o -6 6 1 58.39 85.99 5.05 o -4 6 1 706.02 709.35 16.39 o -2 6 1 384.37 435.39 11.39 o 0 6 1 304.50 357.32 10.96 o 2 6 1 289.97 319.92 9.76 o 4 6 1 106.51 97.93 5.80 o 6 6 1 654.41 613.97 16.60 o 8 6 1 375.22 315.16 9.93 o 10 6 1 198.13 225.18 6.95 o 12 6 1 44.50 45.88 4.80 o 14 6 1 1012.78 1083.15 21.65 o 16 6 1 1347.75 1380.57 23.47 o 18 6 1 1468.63 1487.42 23.85 o 20 6 1 704.47 712.57 16.79 o 22 6 1 236.75 215.20 7.00 o 24 6 1 5.68 2.08 3.46 o 26 6 1 49.59 58.45 4.27 o 28 6 1 122.64 121.19 4.65 o 30 6 1 226.28 196.17 5.54 o -25 7 1 182.05 165.61 5.26 o -23 7 1 77.75 71.88 3.93 o -21 7 1 8.47 7.49 4.17 o -19 7 1 8.42 8.93 4.52 o -17 7 1 50.29 58.98 4.70 o -15 7 1 399.66 374.30 10.83 o -13 7 1 196.41 186.69 6.89 o -11 7 1 19.92 3.90 5.11 o -9 7 1 31.06 28.99 3.96 o -7 7 1 166.64 165.12 6.13 o -5 7 1 1036.34 1061.98 20.55 o -3 7 1 439.50 490.56 14.21 o -1 7 1 89.90 93.11 5.12 o 1 7 1 508.91 515.51 15.50 o 3 7 1 8.99 11.86 6.66 o 5 7 1 303.89 299.32 8.97 o 7 7 1 20.30 27.19 4.97 o 9 7 1 155.46 205.47 7.03 o 11 7 1 505.68 496.19 12.78 o 13 7 1 404.82 380.94 11.46 o 15 7 1 237.42 249.26 7.53 o 17 7 1 317.42 329.19 9.65 o 19 7 1 34.67 54.25 4.31 o 21 7 1 23.96 14.12 4.76 o 23 7 1 159.05 172.97 5.92 o 25 7 1 113.70 108.79 4.55 o -18 8 1 112.64 98.66 4.46 o -16 8 1 389.58 345.66 9.65 o -14 8 1 52.45 47.95 4.24 o -12 8 1 98.97 97.13 4.56 o -10 8 1 152.44 138.30 5.61 o -8 8 1 385.68 357.40 9.55 o -6 8 1 837.86 832.82 16.20 o -4 8 1 352.46 312.04 9.16 o -2 8 1 43.84 45.43 4.13 o 0 8 1 91.71 118.18 6.85 o 2 8 1 69.78 73.49 5.72 o 4 8 1 108.77 111.02 5.89 o 6 8 1 139.83 158.68 6.35 o 8 8 1 7.75 3.90 4.43 o 10 8 1 52.23 68.66 4.74 o 12 8 1 54.14 49.57 4.32 o 14 8 1 60.70 51.80 4.31 o 16 8 1 36.91 32.55 3.73 o 18 8 1 115.85 106.40 4.36 o -42 0 2 173.17 191.28 5.84 o -40 0 2 4.27 11.17 4.00 o -38 0 2 357.36 368.91 11.01 o -36 0 2 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339.59 9.81 o -7 3 8 149.53 136.07 5.09 o -5 3 8 395.00 376.08 10.59 o -3 3 8 933.89 997.25 16.88 o -1 3 8 28.07 25.44 3.16 o 1 3 8 58.36 45.71 3.96 o 3 3 8 287.42 308.95 8.39 o 5 3 8 168.05 155.18 4.92 o 7 3 8 68.59 59.52 3.99 o 9 3 8 14.11 27.19 3.19 o 11 3 8 12.58 12.00 4.01 o 13 3 8 501.27 517.37 9.95 o -10 4 8 467.16 453.54 9.90 o -8 4 8 396.35 395.50 9.51 o -6 4 8 324.99 391.18 9.45 o -4 4 8 26.25 17.13 3.10 o -2 4 8 4.96 11.08 3.53 o 0 4 8 394.38 463.13 17.05 o 2 4 8 15.87 17.41 2.90 o 4 4 8 145.55 146.31 4.95 o 6 4 8 47.27 45.25 3.48 o -10 0 9 173.38 128.81 4.49 o -8 0 9 164.99 151.18 4.86 o -6 0 9 45.72 60.14 3.69 o -4 0 9 204.59 201.09 6.19 o -2 0 9 818.40 816.97 13.32 o 0 0 9 22.05 24.99 2.14 o 2 0 9 18.73 11.31 3.57 o 4 0 9 6.22 15.42 2.99 o 6 0 9 12.58 25.57 3.10 o -9 1 9 358.79 356.18 8.50 o -7 1 9 495.62 473.71 9.82 o -5 1 9 269.15 276.84 7.94 o -3 1 9 289.69 305.09 8.34 o -1 1 9 39.56 57.52 3.72 o 1 1 9 22.62 9.93 2.62 o 3 1 9 21.24 19.10 2.79 o 5 1 9 176.36 170.77 4.99 o