#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:03:19 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180950 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/30/2203050.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203050_Fobs loop_ _publ_author_name 'Yan, Ze-Qun' _publ_section_title ; trans-Diaquabis(pyridine-4-carboxylato)cobalt(II) dihydrate ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m116 _journal_page_last m117 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.396 _cell_angle_beta 105.286 _cell_angle_gamma 108.178 _cell_length_a 6.3367 _cell_length_b 6.8936 _cell_length_c 9.1801 _exptl_crystal_F_000 193.00 _reflns_d_resolution_high 0.8385 _cod_data_source_file cf6313Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 85.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 176.70 187.94 2.89 o 2 0 0 1.69 5.75 0.57 o 3 0 0 151.01 148.23 2.65 o 4 0 0 170.70 177.77 8.82 o 5 0 0 75.46 76.93 3.09 o -7 1 0 66.55 63.33 5.99 o -6 1 0 73.17 75.94 5.59 o -5 1 0 430.18 452.27 20.14 o -4 1 0 245.33 221.93 4.97 o -3 1 0 370.83 335.93 6.78 o -2 1 0 423.11 391.09 16.05 o -1 1 0 446.40 416.71 7.04 o 0 1 0 564.61 605.84 10.94 o 1 1 0 481.12 475.89 10.40 o 2 1 0 12.26 10.87 0.79 o 3 1 0 627.50 584.04 11.08 o 5 1 0 23.87 26.87 3.61 o 6 1 0 117.04 131.35 7.40 o -7 2 0 21.96 21.91 3.02 o -6 2 0 35.47 38.10 3.50 o -5 2 0 173.34 142.89 15.48 o -4 2 0 334.12 327.93 6.87 o -3 2 0 508.11 468.17 7.26 o -2 2 0 849.03 801.01 12.74 o -1 2 0 7359.43 8927.49 158.42 o 0 2 0 1344.53 1194.91 21.62 o 1 2 0 292.01 326.15 6.40 o 2 2 0 890.26 867.79 19.13 o 3 2 0 175.36 191.29 4.45 o 4 2 0 52.93 60.50 4.21 o 5 2 0 12.60 13.09 3.22 o -7 3 0 20.59 19.34 2.74 o -6 3 0 43.72 40.23 2.49 o -5 3 0 14.03 12.32 1.55 o -4 3 0 0.56 1.33 0.84 o -3 3 0 1418.79 1381.75 20.59 o -2 3 0 184.46 170.38 2.92 o -1 3 0 147.11 146.54 3.12 o 0 3 0 104.88 111.11 2.65 o 1 3 0 4.17 6.15 2.38 o 2 3 0 234.78 251.14 22.30 o 3 3 0 185.39 195.97 6.82 o 4 3 0 168.66 158.45 6.60 o 5 3 0 119.01 164.23 8.05 o -7 4 0 13.95 7.25 3.13 o -6 4 0 83.27 86.70 4.77 o -5 4 0 88.53 85.15 4.30 o -4 4 0 71.97 72.12 2.58 o -3 4 0 213.59 199.95 3.58 o -2 4 0 1732.30 1634.09 44.68 o -1 4 0 0.83 4.29 1.89 o 0 4 0 367.31 374.37 20.44 o 1 4 0 62.20 72.14 2.56 o 2 4 0 1.47 2.84 1.97 o 3 4 0 60.53 64.08 3.95 o 4 4 0 17.41 24.37 3.39 o -6 5 0 68.29 65.11 4.38 o -5 5 0 13.54 7.98 2.49 o -4 5 0 178.66 172.10 4.36 o -3 5 0 3.90 4.28 2.12 o -2 5 0 122.43 111.44 3.07 o -1 5 0 138.14 135.85 5.39 o 0 5 0 48.57 48.72 2.30 o 1 5 0 171.86 180.79 12.15 o 2 5 0 102.08 100.01 3.51 o 3 5 0 72.12 92.02 5.80 o -6 6 0 54.38 52.54 4.77 o -5 6 0 45.73 42.35 4.51 o -4 6 0 118.96 119.85 6.67 o -3 6 0 281.93 298.96 6.80 o -2 6 0 21.47 16.44 3.09 o -1 6 0 25.76 20.73 3.00 o 0 6 0 33.38 34.56 3.18 o 1 6 0 54.13 57.87 4.73 o 2 6 0 65.52 66.00 5.46 o -4 7 0 19.41 20.60 3.73 o -3 7 0 75.03 72.14 4.60 o -2 7 0 13.74 15.40 3.18 o -1 7 0 3.92 0.64 2.79 o 0 7 0 51.18 46.30 4.42 o 1 7 0 31.73 24.17 4.46 o -3 8 0 0.58 0.34 3.35 o -2 8 0 32.12 31.68 4.89 o 1 -8 1 25.78 14.46 3.82 o 2 -8 1 1.05 4.55 3.30 o -1 -7 1 37.74 38.00 4.77 o 0 -7 1 0.90 -2.70 2.70 o 1 -7 1 2.77 4.89 2.70 o 2 -7 1 12.45 13.39 2.83 o 3 -7 1 50.80 54.25 4.42 o 4 -7 1 120.58 112.58 14.40 o 5 -7 1 15.50 14.46 4.29 o -2 -6 1 64.58 59.00 4.86 o -1 -6 1 101.70 107.84 5.64 o 0 -6 1 64.07 58.80 4.04 o 1 -6 1 15.57 16.39 2.92 o 2 -6 1 473.95 469.79 9.75 o 3 -6 1 95.11 102.67 3.17 o 4 -6 1 26.82 31.41 7.40 o 5 -6 1 32.07 35.50 3.86 o 6 -6 1 71.30 58.02 4.81 o -3 -5 1 20.34 22.79 3.09 o -2 -5 1 92.86 97.57 6.73 o -1 -5 1 0.38 1.36 1.01 o 0 -5 1 54.75 51.88 3.22 o 1 -5 1 206.88 212.26 7.14 o 2 -5 1 197.47 190.99 8.74 o 3 -5 1 60.81 71.55 2.67 o 4 -5 1 1.63 3.93 1.33 o 5 -5 1 44.54 50.00 3.87 o 6 -5 1 135.36 130.45 6.20 o -4 -4 1 32.95 39.75 3.56 o -3 -4 1 150.19 147.58 4.11 o -2 -4 1 36.64 35.74 1.91 o -1 -4 1 43.05 47.40 1.87 o 0 -4 1 91.06 90.70 2.42 o 1 -4 1 3534.56 3508.05 62.74 o 2 -4 1 216.85 209.07 6.03 o 3 -4 1 1.53 6.18 2.49 o 4 -4 1 56.22 60.26 2.20 o 5 -4 1 73.95 75.64 4.39 o 6 -4 1 13.48 17.03 3.09 o 7 -4 1 25.84 31.33 3.69 o -5 -3 1 42.92 55.52 4.68 o -4 -3 1 97.71 121.18 5.64 o -3 -3 1 140.85 144.41 3.78 o -2 -3 1 101.12 94.92 2.67 o -1 -3 1 138.48 147.19 4.71 o 0 -3 1 347.83 347.18 11.30 o 1 -3 1 298.89 260.79 5.87 o 2 -3 1 331.38 324.44 7.98 o 3 -3 1 450.52 400.72 6.36 o 4 -3 1 266.59 248.09 5.43 o 5 -3 1 167.60 166.00 4.43 o 6 -3 1 48.97 43.68 2.94 o 7 -3 1 61.84 63.16 5.11 o -6 -2 1 26.37 21.50 4.03 o -5 -2 1 17.40 19.44 3.52 o -4 -2 1 190.00 187.97 6.96 o -3 -2 1 237.13 226.55 5.01 o -2 -2 1 965.82 881.84 34.43 o -1 -2 1 734.34 708.60 15.19 o 0 -2 1 3815.54 4130.99 73.50 o 1 -2 1 370.28 248.26 8.29 o 2 -2 1 2.68 6.86 1.00 o 3 -2 1 568.10 495.50 8.38 o 4 -2 1 174.73 178.18 4.29 o 5 -2 1 73.12 72.13 3.68 o 6 -2 1 51.78 46.10 2.90 o -6 -1 1 30.55 30.95 4.55 o -5 -1 1 2.44 2.36 2.53 o -4 -1 1 36.41 37.67 2.83 o -3 -1 1 23.02 32.42 2.10 o -2 -1 1 1633.04 1605.39 29.00 o -1 -1 1 719.90 667.04 13.24 o 0 -1 1 709.10 676.21 12.17 o 1 -1 1 507.92 573.13 14.80 o 2 -1 1 216.28 206.46 4.15 o 3 -1 1 62.23 66.65 3.70 o 4 -1 1 465.88 493.72 10.00 o 5 -1 1 443.21 428.96 9.23 o 6 -1 1 146.22 151.62 4.95 o -6 0 1 25.87 30.69 3.99 o -5 0 1 305.40 305.30 7.22 o -4 0 1 267.23 260.82 5.86 o -3 0 1 245.58 247.71 4.16 o -2 0 1 93.88 91.54 3.07 o -1 0 1 5170.11 4098.80 103.16 o 0 0 1 341.62 313.87 8.15 o 1 0 1 223.92 220.62 3.42 o 2 0 1 96.06 94.38 2.01 o 3 0 1 0.76 3.48 0.95 o 4 0 1 127.06 132.14 4.46 o 5 0 1 64.57 64.96 3.11 o 6 0 1 50.30 55.92 3.56 o -7 1 1 5.97 7.80 4.70 o -6 1 1 29.91 27.18 2.58 o -5 1 1 320.86 307.50 6.97 o -4 1 1 3.92 4.68 1.30 o -3 1 1 407.71 401.56 8.19 o -2 1 1 0.95 4.60 0.48 o -1 1 1 654.23 686.22 17.82 o 0 1 1 751.61 875.03 15.87 o 1 1 1 466.73 480.84 7.32 o 2 1 1 669.88 653.66 9.97 o 3 1 1 957.30 934.34 17.64 o 4 1 1 334.63 348.39 17.05 o 5 1 1 4.07 4.07 2.32 o 6 1 1 1.93 -2.40 2.57 o -7 2 1 9.36 13.75 2.75 o -6 2 1 238.21 211.02 5.52 o -5 2 1 178.82 194.64 6.95 o -4 2 1 270.77 232.12 7.21 o -3 2 1 761.67 669.64 10.22 o -2 2 1 2283.05 2212.25 32.42 o -1 2 1 196.95 144.93 3.48 o 0 2 1 547.82 406.59 11.79 o 1 2 1 125.79 133.37 7.57 o 2 2 1 331.68 276.43 14.33 o 3 2 1 365.00 407.64 12.37 o 5 2 1 25.77 21.46 3.18 o -7 3 1 27.10 21.40 6.72 o -6 3 1 50.41 43.91 4.12 o -5 3 1 17.94 14.72 2.15 o -4 3 1 423.86 408.59 6.67 o -3 3 1 513.96 477.84 7.53 o -2 3 1 706.13 664.14 12.67 o -1 3 1 282.50 259.24 4.79 o 0 3 1 162.84 172.74 3.90 o 1 3 1 370.23 374.65 7.59 o 2 3 1 335.83 337.17 7.10 o 3 3 1 220.60 233.81 8.04 o 4 3 1 3.93 6.52 2.62 o -7 4 1 145.31 143.73 6.85 o -6 4 1 40.71 40.20 3.31 o -5 4 1 49.96 44.60 2.08 o -4 4 1 138.41 140.13 2.94 o -3 4 1 178.76 186.02 9.46 o -2 4 1 2.54 4.73 1.76 o -1 4 1 99.15 102.60 2.70 o 0 4 1 402.38 406.92 8.23 o 1 4 1 80.87 85.53 2.81 o 2 4 1 32.44 29.54 2.09 o 3 4 1 2.16 0.04 2.23 o 4 4 1 44.85 52.30 4.77 o -7 5 1 43.91 30.96 3.65 o -6 5 1 34.21 29.88 3.35 o -5 5 1 257.63 271.26 11.77 o -4 5 1 28.85 28.38 1.94 o -3 5 1 17.13 16.13 1.53 o -2 5 1 136.41 136.05 3.52 o -1 5 1 198.37 190.31 4.46 o 0 5 1 253.80 257.69 9.09 o 1 5 1 136.72 135.22 11.68 o 2 5 1 109.78 112.89 3.96 o 3 5 1 6.64 1.50 3.09 o -6 6 1 39.31 50.54 4.08 o -5 6 1 72.79 78.61 9.80 o -4 6 1 58.94 58.66 3.61 o -3 6 1 9.50 11.15 2.32 o -2 6 1 24.24 23.99 3.00 o -1 6 1 28.57 30.35 3.43 o 1 6 1 54.30 45.92 4.38 o -5 7 1 5.93 1.50 2.27 o -4 7 1 57.83 58.30 4.25 o -3 7 1 122.23 145.99 6.80 o -2 7 1 24.41 29.92 3.69 o -1 7 1 26.60 24.81 3.82 o 0 7 1 20.74 20.98 4.21 o 1 -8 2 4.92 8.36 3.39 o 2 -8 2 129.18 134.01 7.02 o 3 -8 2 17.33 22.31 4.08 o -1 -7 2 0.22 5.83 3.13 o 0 -7 2 31.16 27.39 3.82 o 1 -7 2 16.67 15.32 3.18 o 2 -7 2 68.49 70.53 4.43 o 3 -7 2 21.92 24.65 2.14 o 4 -7 2 71.28 74.91 3.52 o 5 -7 2 37.15 49.42 5.80 o -2 -6 2 39.13 38.47 3.91 o -1 -6 2 49.69 42.18 3.48 o 0 -6 2 93.63 91.95 4.78 o 1 -6 2 165.27 176.17 6.95 o 2 -6 2 5.93 10.30 2.36 o 3 -6 2 10.55 13.52 1.68 o 4 -6 2 13.17 15.28 2.51 o 5 -6 2 70.88 77.11 5.20 o 6 -6 2 41.96 32.89 4.42 o -4 -5 2 0.31 3.04 3.09 o -3 -5 2 13.01 14.00 1.94 o -2 -5 2 4.11 3.30 2.17 o -1 -5 2 131.99 126.26 5.22 o 0 -5 2 146.02 153.27 5.95 o 1 -5 2 432.93 424.28 12.50 o 2 -5 2 96.08 98.27 4.09 o 3 -5 2 115.85 125.26 3.52 o 4 -5 2 9.31 14.77 2.96 o 5 -5 2 46.11 41.79 3.87 o 6 -5 2 245.58 289.25 11.23 o -4 -4 2 187.70 211.87 8.41 o -3 -4 2 89.92 77.49 2.87 o -2 -4 2 15.29 17.87 1.56 o -1 -4 2 71.22 82.68 2.75 o 0 -4 2 307.06 323.78 6.46 o 1 -4 2 343.68 338.67 10.00 o 2 -4 2 49.59 51.68 2.58 o 3 -4 2 7.82 11.56 1.29 o 6 -4 2 29.77 28.46 3.82 o -5 -3 2 5.78 5.45 3.09 o -4 -3 2 144.01 143.15 5.86 o -3 -3 2 49.02 48.41 2.18 o -2 -3 2 132.02 142.61 3.55 o -1 -3 2 258.84 262.14 7.95 o 0 -3 2 709.30 681.30 12.61 o 1 -3 2 69.31 77.17 3.10 o 2 -3 2 570.56 525.52 8.07 o 3 -3 2 361.74 371.58 7.21 o 4 -3 2 432.75 412.23 8.42 o 5 -3 2 424.36 487.88 10.39 o 6 -3 2 10.12 9.22 2.45 o -6 -2 2 7.84 13.08 4.03 o -5 -2 2 244.25 230.98 8.60 o -3 -2 2 77.81 72.93 2.45 o -2 -2 2 933.25 860.71 17.02 o -1 -2 2 637.14 606.97 11.32 o 0 -2 2 4.26 10.14 0.57 o 1 -2 2 862.12 747.63 13.60 o 2 -2 2 8.45 9.98 1.09 o 3 -2 2 826.25 838.39 16.75 o 4 -2 2 304.59 308.59 6.77 o 5 -2 2 94.48 98.73 3.31 o 6 -2 2 92.64 84.62 4.15 o -6 -1 2 17.61 18.49 4.03 o -5 -1 2 54.52 41.04 3.09 o -4 -1 2 0.64 3.00 1.63 o -3 -1 2 380.16 363.19 11.63 o -2 -1 2 2022.11 2066.81 37.29 o -1 -1 2 1422.99 1394.06 25.16 o 0 -1 2 269.65 325.70 6.14 o 1 -1 2 1438.35 1614.83 28.97 o 2 -1 2 252.63 250.76 5.89 o 3 -1 2 204.65 198.17 4.44 o 4 -1 2 495.90 478.69 9.76 o 5 -1 2 7.90 6.96 1.44 o 6 -1 2 68.29 65.56 3.25 o -7 0 2 50.72 67.95 6.01 o -6 0 2 251.74 226.63 8.30 o -5 0 2 39.60 48.84 3.48 o -4 0 2 142.81 136.90 7.00 o -3 0 2 278.51 299.21 8.90 o 0 0 2 77.03 103.54 3.12 o 1 0 2 1276.07 1133.69 20.51 o 2 0 2 887.15 960.97 36.30 o 3 0 2 49.62 52.45 2.79 o 4 0 2 86.36 91.32 4.05 o 5 0 2 120.38 123.91 4.11 o 6 0 2 26.73 16.80 2.18 o -7 1 2 0.70 5.32 3.26 o -6 1 2 105.28 97.33 3.85 o -5 1 2 271.19 247.57 5.85 o -4 1 2 730.29 726.13 14.12 o -3 1 2 532.58 523.54 10.19 o -2 1 2 1.89 2.41 0.69 o -1 1 2 691.16 727.12 13.40 o 0 1 2 1815.30 1802.02 26.34 o 1 1 2 318.77 326.19 5.14 o 2 1 2 543.10 545.46 8.50 o 3 1 2 709.35 741.08 14.36 o 4 1 2 83.53 81.70 3.85 o 5 1 2 24.21 27.00 3.65 o -7 2 2 75.61 65.80 3.75 o -6 2 2 22.92 17.69 2.09 o -5 2 2 131.83 117.45 3.58 o -4 2 2 145.74 164.90 4.64 o -3 2 2 72.10 77.04 1.91 o -2 2 2 827.33 761.84 11.50 o -1 2 2 2.99 3.19 0.37 o 0 2 2 6.36 7.29 0.80 o 1 2 2 531.18 542.70 10.43 o 2 2 2 324.14 319.71 9.27 o 3 2 2 326.36 314.53 9.99 o 4 2 2 91.91 104.02 5.25 o 5 2 2 24.92 25.02 4.03 o -7 3 2 118.67 125.68 9.83 o -6 3 2 63.46 59.27 2.79 o -5 3 2 30.80 32.20 2.06 o -4 3 2 162.39 149.18 4.77 o -3 3 2 403.76 394.84 8.22 o -2 3 2 1650.79 1575.28 23.34 o -1 3 2 348.74 316.91 5.85 o 0 3 2 32.94 37.09 1.57 o 1 3 2 239.67 243.98 5.46 o 2 3 2 201.83 209.32 5.00 o 4 3 2 93.77 110.92 5.98 o -7 4 2 33.94 30.52 3.69 o -6 4 2 34.02 35.12 4.31 o -5 4 2 8.81 14.16 1.31 o -4 4 2 38.11 29.67 2.71 o -3 4 2 165.65 157.92 4.33 o -2 4 2 7.21 7.98 2.03 o -1 4 2 281.09 323.55 6.91 o 0 4 2 877.94 914.62 17.37 o 1 4 2 80.47 83.24 2.96 o 2 4 2 35.20 29.51 2.14 o 3 4 2 16.83 18.58 3.82 o -7 5 2 23.27 10.13 3.52 o -6 5 2 51.76 42.79 3.57 o -5 5 2 160.45 165.48 6.40 o -4 5 2 81.08 82.06 5.81 o -3 5 2 146.43 146.05 5.61 o -2 5 2 8.68 7.90 1.27 o -1 5 2 98.39 96.84 2.98 o 0 5 2 201.55 226.29 9.18 o 1 5 2 67.72 72.83 3.48 o 2 5 2 32.92 43.32 4.46 o -5 6 2 86.41 114.65 5.89 o -4 6 2 72.89 67.20 3.74 o -3 6 2 19.82 21.33 2.88 o -2 6 2 72.86 78.51 4.43 o -1 6 2 130.50 135.99 6.55 o 0 6 2 1.00 -0.73 2.87 o 1 6 2 45.96 43.72 4.38 o -5 7 2 16.70 14.80 3.13 o -4 7 2 97.90 95.79 5.20 o -3 7 2 20.73 27.38 3.52 o -2 7 2 35.21 39.80 4.16 o -1 7 2 18.72 16.35 3.60 o 1 -8 3 27.36 38.37 4.42 o 2 -8 3 14.12 18.92 3.82 o 3 -8 3 14.65 11.87 2.15 o -1 -7 3 41.51 39.68 4.12 o 0 -7 3 33.94 36.06 3.82 o 1 -7 3 59.07 75.80 4.94 o 2 -7 3 4.36 1.84 2.10 o 3 -7 3 27.72 27.72 2.40 o 4 -7 3 51.72 68.45 6.57 o 5 -7 3 24.40 23.39 4.12 o -3 -6 3 5.22 5.36 3.65 o -2 -6 3 1.44 -0.73 2.14 o 0 -6 3 78.49 71.09 4.13 o 1 -6 3 12.40 10.00 2.70 o 2 -6 3 1.48 0.30 1.50 o 3 -6 3 1.65 3.08 1.53 o 4 -6 3 157.64 155.11 6.38 o 5 -6 3 79.41 89.55 6.36 o -3 -5 3 14.61 15.79 3.18 o -2 -5 3 105.96 83.68 4.39 o -1 -5 3 160.86 157.64 6.47 o 0 -5 3 179.67 190.62 6.91 o 1 -5 3 96.74 101.58 4.91 o 2 -5 3 223.52 250.52 8.18 o 3 -5 3 71.14 68.06 2.50 o 4 -5 3 2.38 -0.86 2.62 o 5 -5 3 219.30 218.36 8.46 o 6 -5 3 2.12 2.53 3.47 o -5 -4 3 60.67 60.83 5.07 o -4 -4 3 24.83 27.30 3.56 o -3 -4 3 28.47 23.73 5.39 o -2 -4 3 115.54 109.57 3.23 o -1 -4 3 13.29 12.24 1.41 o 0 -4 3 35.03 39.22 2.21 o 1 -4 3 264.49 319.22 9.86 o 2 -4 3 157.77 161.17 5.44 o 3 -4 3 594.43 605.41 16.09 o 4 -4 3 100.35 95.44 4.56 o 5 -4 3 48.91 48.50 3.91 o 6 -4 3 48.19 38.83 4.08 o -5 -3 3 50.99 54.68 5.03 o -4 -3 3 236.43 226.74 7.96 o -3 -3 3 326.29 325.92 9.39 o -2 -3 3 184.76 176.06 5.95 o -1 -3 3 88.83 88.44 3.38 o 0 -3 3 253.49 240.31 5.25 o 1 -3 3 321.00 332.42 20.09 o 2 -3 3 78.59 72.44 3.28 o 3 -3 3 156.75 150.56 6.79 o 4 -3 3 826.53 858.30 16.51 o 5 -3 3 43.93 46.17 4.04 o 6 -3 3 12.68 6.95 2.70 o -6 -2 3 53.45 61.47 5.54 o -5 -2 3 22.97 16.44 2.62 o -4 -2 3 18.55 23.87 5.30 o -3 -2 3 87.50 82.22 2.38 o -2 -2 3 48.46 47.80 1.70 o -1 -2 3 1134.54 1049.04 28.49 o 0 -2 3 261.73 299.78 5.87 o 1 -2 3 70.61 56.38 1.52 o 2 -2 3 1317.77 1297.85 19.30 o 3 -2 3 393.77 383.20 6.18 o 4 -2 3 296.72 294.52 6.56 o 5 -2 3 105.26 106.68 3.67 o 6 -2 3 35.06 33.31 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151.56 164.80 6.04 o 0 -2 7 830.62 896.39 24.15 o 1 -2 7 129.75 115.29 4.70 o 2 -2 7 13.25 17.32 1.58 o 3 -2 7 135.79 124.18 8.23 o -6 -1 7 33.95 30.52 4.38 o -5 -1 7 90.83 97.20 4.20 o -4 -1 7 92.82 113.81 5.81 o -3 -1 7 1.45 -1.76 2.06 o -2 -1 7 147.08 158.61 6.00 o -1 -1 7 480.58 505.08 14.61 o 0 -1 7 3.85 6.01 2.27 o 1 -1 7 198.31 215.16 5.28 o 2 -1 7 9.06 13.99 2.40 o 3 -1 7 108.03 89.29 4.69 o -6 0 7 32.58 42.03 4.85 o -5 0 7 35.46 45.64 4.77 o -4 0 7 138.82 161.26 6.81 o -3 0 7 108.09 104.45 5.00 o -2 0 7 149.38 146.20 5.65 o -1 0 7 626.32 630.97 17.77 o 0 0 7 8.71 8.37 2.23 o 1 0 7 115.91 105.43 4.74 o 2 0 7 423.48 383.59 12.09 o 3 0 7 102.89 78.81 4.82 o -6 1 7 58.20 68.66 5.84 o -5 1 7 18.40 15.53 3.09 o -4 1 7 47.64 49.79 3.74 o -3 1 7 505.39 543.28 16.05 o -2 1 7 337.85 361.77 11.39 o -1 1 7 115.18 99.08 4.70 o 0 1 7 50.89 40.35 3.18 o 1 1 7 27.69 26.36 3.13 o 2 1 7 205.80 187.11 7.42 o 3 1 7 42.61 20.52 3.69 o -6 2 7 2.31 5.02 3.26 o -5 2 7 40.13 40.15 4.04 o -4 2 7 155.36 163.48 6.99 o -3 2 7 214.81 225.47 8.17 o -2 2 7 460.97 446.70 13.61 o -1 2 7 3.94 4.55 2.40 o 0 2 7 144.30 123.44 5.47 o 1 2 7 160.10 137.51 6.21 o 2 2 7 19.00 17.55 3.22 o -6 3 7 12.33 19.61 3.60 o -5 3 7 36.42 31.00 3.69 o -4 3 7 127.84 134.42 6.50 o -3 3 7 29.33 31.17 3.48 o -2 3 7 22.92 22.19 3.26 o -1 3 7 244.24 257.70 5.48 o 1 3 7 91.27 87.47 5.38 o -6 4 7 73.65 61.46 4.99 o -5 4 7 108.18 87.13 5.12 o -4 4 7 28.16 19.02 3.82 o -3 4 7 89.37 85.37 3.79 o -2 4 7 0.64 3.32 1.85 o -1 4 7 116.94 139.24 4.15 o 0 4 7 100.36 92.14 4.03 o -5 5 7 76.63 64.39 4.90 o -4 5 7 25.77 19.89 2.73 o -3 5 7 0.61 -1.04 2.66 o -2 5 7 72.22 68.86 3.95 o -1 -6 8 38.40 38.13 4.51 o 0 -6 8 19.68 24.25 4.68 o 1 -6 8 189.45 187.47 7.98 o 2 -6 8 31.89 40.65 4.59 o -3 -5 8 24.62 20.00 3.99 o -2 -5 8 1.39 1.46 2.74 o -1 -5 8 17.61 12.44 2.87 o 0 -5 8 208.66 208.42 8.03 o 1 -5 8 1.80 11.37 2.74 o 2 -5 8 62.69 68.62 4.60 o 3 -5 8 25.56 25.15 3.61 o -4 -4 8 17.65 24.03 3.35 o -3 -4 8 24.25 16.65 2.92 o -2 -4 8 134.20 111.13 5.51 o -1 -4 8 51.98 44.77 3.91 o 0 -4 8 246.87 252.23 9.12 o 1 -4 8 0.54 -0.21 1.93 o 2 -4 8 14.97 12.70 3.13 o 3 -4 8 189.22 192.25 7.68 o -5 -3 8 19.47 18.23 3.52 o -4 -3 8 5.66 5.06 1.91 o -3 -3 8 4.43 8.38 2.15 o -2 -3 8 244.58 258.63 8.69 o -1 -3 8 336.14 343.64 20.98 o 0 -3 8 82.11 72.69 5.12 o 1 -3 8 56.15 61.36 4.86 o 2 -3 8 46.91 38.91 3.95 o 3 -3 8 107.76 121.24 5.98 o -5 -2 8 6.91 7.54 2.64 o -4 -2 8 20.35 21.18 2.87 o -3 -2 8 242.69 253.78 6.56 o -2 -2 8 81.71 99.23 4.86 o -1 -2 8 441.20 482.50 14.34 o 0 -2 8 11.70 9.95 2.10 o 1 -2 8 100.29 107.97 3.79 o 2 -2 8 144.11 146.63 5.60 o -5 -1 8 27.78 27.99 4.81 o -4 -1 8 19.48 29.35 3.60 o -2 -1 8 51.27 51.48 3.61 o -1 -1 8 61.34 61.08 3.87 o 0 -1 8 383.26 378.23 11.69 o 1 -1 8 189.61 160.73 6.30 o 2 -1 8 141.72 139.36 6.03 o 3 -1 8 66.35 62.56 4.64 o -6 0 8 38.50 42.08 4.94 o -5 0 8 103.02 109.12 5.98 o -4 0 8 301.98 367.84 12.69 o -3 0 8 30.18 30.14 3.13 o -2 0 8 272.33 271.67 9.27 o -1 0 8 3.06 -1.67 1.67 o 0 0 8 94.48 93.40 5.16 o 1 0 8 162.11 153.66 6.55 o 2 0 8 67.77 60.38 4.43 o -6 1 8 7.39 1.84 3.82 o -5 1 8 5.98 1.89 2.66 o -4 1 8 178.35 193.59 7.90 o -3 1 8 112.52 95.63 4.99 o -2 1 8 1.44 6.43 3.00 o -1 1 8 221.74 230.26 8.51 o 1 1 8 111.54 100.66 5.25 o 2 1 8 110.93 107.26 5.77 o -6 2 8 17.80 14.50 3.56 o -5 2 8 74.78 81.29 5.85 o -4 2 8 14.89 14.16 3.09 o -3 2 8 250.94 263.25 9.77 o -2 2 8 5.80 2.83 2.53 o -1 2 8 146.08 145.69 6.64 o 0 2 8 100.27 94.39 5.42 o 1 2 8 19.37 15.23 3.26 o -6 3 8 13.10 19.09 3.86 o -5 3 8 111.22 92.13 5.94 o -4 3 8 7.77 0.09 2.79 o -3 3 8 0.63 -2.32 2.32 o -2 3 8 153.14 158.24 7.37 o -1 3 8 137.72 148.88 7.32 o -5 4 8 21.56 17.29 3.69 o -4 4 8 64.66 46.45 4.64 o -3 4 8 0.70 1.84 3.13 o -2 4 8 56.82 52.28 4.85 o -2 -5 9 32.58 27.77 3.69 o -1 -5 9 29.48 21.42 3.22 o 0 -5 9 1.35 2.19 2.19 o 1 -5 9 48.82 51.75 4.25 o -3 -4 9 102.71 80.57 5.51 o -2 -4 9 26.22 25.41 3.86 o -1 -4 9 70.87 62.88 4.51 o 0 -4 9 0.33 -1.07 2.23 o 1 -4 9 14.97 14.24 3.52 o 2 -4 9 33.33 20.61 3.69 o -4 -3 9 1.34 -0.18 5.53 o -3 -3 9 75.91 76.74 3.88 o -2 -3 9 124.13 122.03 6.80 o -1 -3 9 18.83 11.80 3.18 o 0 -3 9 68.08 72.64 5.11 o 1 -3 9 110.76 123.16 6.63 o 2 -3 9 55.05 55.59 4.64 o -5 -2 9 1.83 0.73 2.39 o -4 -2 9 74.70 60.64 6.56 o -3 -2 9 18.80 17.65 2.31 o -2 -2 9 74.95 71.97 4.73 o -1 -2 9 12.28 13.56 3.35 o 0 -2 9 86.16 78.36 4.47 o 1 -2 9 102.91 106.79 5.42 o -5 -1 9 18.57 26.35 4.81 o -4 -1 9 149.48 150.68 7.20 o -3 -1 9 43.19 42.86 3.91 o -2 -1 9 0.43 -0.51 2.36 o -1 -1 9 97.44 90.87 4.95 o 0 -1 9 349.84 361.23 11.67 o 1 -1 9 162.22 154.47 6.98 o 2 -1 9 82.53 64.05 5.33 o -5 0 9 148.05 184.76 8.62 o -4 0 9 38.89 37.57 3.82 o -3 0 9 40.19 48.87 4.77 o -2 0 9 12.36 10.98 2.87 o -1 0 9 46.26 47.42 3.95 o 0 0 9 64.80 66.78 4.86 o 1 0 9 73.70 75.35 5.42 o -5 1 9 76.75 81.97 5.55 o -4 1 9 23.91 26.05 3.86 o -3 1 9 60.90 64.67 4.81 o -2 1 9 241.75 277.21 10.29 o -1 1 9 213.68 224.21 8.76 o 0 1 9 26.50 31.15 3.44 o 1 1 9 25.07 14.16 3.61 o -5 2 9 0.25 7.08 3.30 o 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