#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/30/2203069.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203069_Fobs loop_ _publ_author_name 'Castillo, Oscar' 'Garc\'ia-Couceiro, Urko' 'Luque, Antonio' 'Garc\'ia-Ter\'an, Juan P.' 'Rom\'an, Pascual' _publ_section_title ; Bis(\m-1,2,4-triazole-\k^2^N^1^:N^2^)bis[diaqua(oxalato-\k^2^O,O')copper(II)] ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m9 _journal_page_last m11 _journal_volume 60 _journal_year 2004 _space_group_IT_number 142 _symmetry_space_group_name_Hall '-I 4bd 2c' _symmetry_space_group_name_H-M 'I 41/a c d :2' _cell_angle_alpha 90.0 _cell_angle_beta 90.0 _cell_angle_gamma 90.0 _cell_length_a 16.596(1) _cell_length_b 16.596(1) _cell_length_c 11.996(2) _exptl_crystal_F_000 2064.00 _reflns_d_resolution_high 0.7108 _[local]_cod_data_source_file hb6006Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tetragonal-i-nuevo in I 41/a c d' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1318.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z' 'x, -y, -z+1/2' '-x+1/2, y, -z' '-y+1/4, -x+1/4, -z+1/4' 'y+3/4, x+1/4, -z+1/4' 'y+1/4, -x+1/4, z+3/4' '-y+1/4, x+3/4, z+1/4' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1, z+1/2' 'x+1/2, -y+1/2, -z+1' '-x+1, y+1/2, -z+1/2' '-y+3/4, -x+3/4, -z+3/4' 'y+5/4, x+3/4, -z+3/4' 'y+3/4, -x+3/4, z+5/4' '-y+3/4, x+5/4, z+3/4' '-x, -y, -z' 'x, y-1/2, -z' '-x, y, z-1/2' 'x-1/2, -y, z' 'y-1/4, x-1/4, z-1/4' '-y-3/4, -x-1/4, z-1/4' '-y-1/4, x-1/4, -z-3/4' 'y-1/4, -x-3/4, -z-1/4' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, y, -z+1/2' '-x+1/2, y+1/2, z' 'x, -y+1/2, z+1/2' 'y+1/4, x+1/4, z+1/4' '-y-1/4, -x+1/4, z+1/4' '-y+1/4, x+1/4, -z-1/4' 'y+1/4, -x-1/4, -z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 4 0 196815.86 225058.23 3506.67 o 2 4 0 12753.81 15213.31 280.37 o 4 4 0 509.37 784.94 153.38 o 0 6 0 245943.56 281594.31 6670.99 o 2 6 0 108729.39 116683.52 1164.80 o 4 6 0 39369.02 35223.06 776.44 o 6 6 0 109950.28 110222.20 2832.06 o 0 8 0 241401.47 284375.00 6784.29 o 2 8 0 1312.50 930.68 152.87 o 4 8 0 14551.46 15424.18 505.94 o 6 8 0 45514.95 45382.02 1033.08 o 8 8 0 35933.13 34679.72 499.50 o 0 10 0 83196.32 89017.99 1908.04 o 2 10 0 5999.17 5810.75 186.90 o 4 10 0 675.52 473.46 168.93 o 6 10 0 14729.40 13013.14 525.55 o 8 10 0 28155.20 28053.10 737.08 o 10 10 0 19813.94 19503.54 858.62 o 0 12 0 131246.83 144958.38 5072.55 o 2 12 0 13391.71 13883.77 402.13 o 4 12 0 5138.79 5342.61 307.41 o 6 12 0 53925.46 56378.40 1343.51 o 8 12 0 19553.32 18632.12 502.17 o 10 12 0 1739.94 1433.43 299.76 o 12 12 0 19212.52 19791.96 954.26 o 0 14 0 16848.09 17957.83 579.17 o 2 14 0 2541.55 2505.70 255.68 o 4 14 0 10229.90 10082.55 348.72 o 6 14 0 4532.71 4383.90 285.74 o 8 14 0 2378.86 2070.76 335.02 o 10 14 0 18.31 252.36 297.52 o 12 14 0 18279.41 18550.02 587.51 o 14 14 0 1015.17 1066.30 769.54 o 0 16 0 38771.61 38289.78 1613.16 o 2 16 0 4456.38 4060.26 299.93 o 4 16 0 2260.74 2133.50 296.15 o 6 16 0 11682.76 11257.52 516.16 o 8 16 0 2381.04 1565.10 423.50 o 10 16 0 161.54 255.73 312.61 o 12 16 0 4854.84 5238.91 579.45 o 14 16 0 1679.44 1404.64 462.40 o 16 16 0 3853.63 3808.29 751.79 o 0 18 0 43619.70 46336.08 1252.18 o 2 18 0 6050.76 5749.41 427.42 o 4 18 0 8001.80 7705.05 436.06 o 6 18 0 19513.61 21069.13 734.11 o 8 18 0 9877.26 9918.46 661.76 o 10 18 0 11144.94 11996.93 595.23 o 12 18 0 12354.69 12206.25 707.27 o 14 18 0 814.75 604.08 448.10 o 0 20 0 1217.34 2075.64 624.30 o 2 20 0 669.40 477.29 363.83 o 4 20 0 1411.13 1311.55 423.16 o 6 20 0 3459.94 3444.66 462.33 o 8 20 0 399.06 468.88 370.15 o 10 20 0 423.27 251.63 399.09 o 12 20 0 3547.70 4616.40 756.32 o 0 22 0 2353.20 2717.29 670.57 o 2 22 0 768.44 881.85 477.78 o 4 22 0 9.51 211.06 459.26 o 6 22 0 850.26 948.67 511.54 o 1 2 1 27560.79 23488.99 12989.32 o 2 3 1 11553.21 9447.99 135.84 o 1 4 1 4550.41 5496.62 83.16 o 3 4 1 45070.38 47621.10 859.11 o 2 5 1 32863.25 31378.88 513.60 o 4 5 1 3250.44 2682.83 89.82 o 1 6 1 0.03 138.71 47.14 o 3 6 1 3867.33 4874.33 128.05 o 5 6 1 216.07 367.83 63.06 o 2 7 1 46365.94 54752.79 924.20 o 4 7 1 3413.53 3709.41 147.36 o 6 7 1 274.78 358.23 68.44 o 1 8 1 30188.05 31729.87 544.19 o 3 8 1 88346.78 91079.72 1375.35 o 5 8 1 2125.59 1319.70 124.42 o 7 8 1 23639.77 24713.63 260.34 o 2 9 1 79011.77 87870.05 1345.90 o 4 9 1 38124.52 39397.02 575.85 o 6 9 1 362.58 326.45 97.60 o 8 9 1 51235.80 52551.42 843.38 o 1 10 1 15044.90 14384.46 215.20 o 3 10 1 16736.36 15761.94 240.66 o 5 10 1 14014.20 14665.36 323.76 o 7 10 1 14215.09 14284.33 329.23 o 9 10 1 36831.96 36737.86 831.78 o 2 11 1 99.86 199.50 80.56 o 4 11 1 8585.23 9062.23 196.32 o 6 11 1 354.83 217.07 100.61 o 8 11 1 7559.58 7640.51 254.14 o 10 11 1 218.62 290.38 158.35 o 1 12 1 531.75 873.44 100.28 o 3 12 1 811.58 433.52 102.94 o 5 12 1 446.92 548.55 126.07 o 7 12 1 6.01 188.71 128.11 o 9 12 1 558.19 662.18 188.03 o 11 12 1 65.86 239.54 230.79 o 2 13 1 2096.64 1674.26 146.00 o 4 13 1 1878.56 1419.83 143.79 o 6 13 1 54.65 191.32 118.45 o 8 13 1 5946.83 5037.13 248.65 o 10 13 1 1899.46 1490.77 225.39 o 12 13 1 847.56 624.25 244.40 o 1 14 1 7474.87 7875.21 210.09 o 3 14 1 1611.98 1870.16 155.59 o 5 14 1 722.78 684.20 143.83 o 7 14 1 1442.95 1223.57 210.64 o 9 14 1 12424.68 12990.39 332.40 o 11 14 1 763.69 933.35 223.64 o 13 14 1 1764.95 1591.89 258.14 o 2 15 1 18025.98 17831.41 289.37 o 4 15 1 8089.59 7718.16 229.08 o 6 15 1 1467.28 1205.37 180.24 o 8 15 1 25430.23 24397.89 441.34 o 10 15 1 8237.17 8076.52 309.52 o 12 15 1 373.75 380.69 229.79 o 14 15 1 2323.41 2694.02 328.62 o 1 16 1 781.90 754.89 168.95 o 3 16 1 23994.63 24398.57 369.05 o 5 16 1 8086.61 7525.39 249.90 o 7 16 1 11178.57 10312.99 321.86 o 9 16 1 12087.65 12151.40 351.81 o 11 16 1 396.23 397.78 203.84 o 13 16 1 1577.92 1375.09 316.73 o 15 16 1 6321.11 6941.45 426.19 o 2 17 1 3078.89 3244.31 233.26 o 4 17 1 8959.11 8796.88 280.33 o 6 17 1 206.94 282.85 202.01 o 8 17 1 1365.12 1534.09 249.43 o 10 17 1 2043.31 1955.66 255.47 o 12 17 1 159.57 399.57 254.43 o 14 17 1 759.37 901.20 295.85 o 1 18 1 542.64 460.35 180.27 o 3 18 1 473.45 288.80 166.11 o 5 18 1 29.56 120.28 218.94 o 7 18 1 582.62 488.36 207.02 o 9 18 1 11.39 240.53 224.97 o 11 18 1 8.36 57.84 304.55 o 13 18 1 45.86 203.26 367.54 o 2 19 1 3498.32 3134.38 261.05 o 4 19 1 988.37 890.32 235.41 o 6 19 1 236.87 255.41 206.77 o 8 19 1 4661.23 3954.06 342.04 o 10 19 1 4265.27 4490.47 362.96 o 12 19 1 67.11 184.01 297.60 o 1 20 1 2367.99 2396.41 282.42 o 3 20 1 3024.99 3339.96 333.96 o 5 20 1 238.64 166.20 273.65 o 7 20 1 152.84 296.83 279.71 o 9 20 1 6061.33 6847.28 476.72 o 11 20 1 690.60 1117.42 351.82 o 2 21 1 3350.16 3244.17 318.97 o 4 21 1 3970.16 3335.59 390.55 o 6 21 1 63.40 214.53 248.90 o 8 21 1 1023.88 931.61 378.43 o 10 21 1 2899.10 2951.52 400.78 o 1 22 1 852.34 809.17 301.60 o 3 22 1 1889.79 1272.10 367.08 o 5 22 1 476.89 419.82 317.55 o 7 22 1 177.08 326.85 313.68 o 2 23 1 304.02 292.11 323.70 o 1 1 2 201271.97 225405.63 1031.56 o 0 2 2 513.84 597.70 64.34 o 1 3 2 15739.02 17004.31 154.47 o 3 3 2 2454.07 2729.54 114.21 o 0 4 2 424.01 718.84 84.39 o 2 4 2 56.66 104.50 46.88 o 1 5 2 32594.77 31031.51 272.28 o 3 5 2 18272.58 20265.71 255.17 o 5 5 2 20333.16 31106.79 842.25 o 0 6 2 197.06 257.89 78.24 o 2 6 2 4.32 124.58 55.59 o 4 6 2 4.50 155.50 64.27 o 1 7 2 44014.14 42324.45 534.24 o 3 7 2 95.68 307.82 73.77 o 5 7 2 36704.04 32237.46 502.01 o 7 7 2 18053.03 17098.53 351.77 o 0 8 2 155.29 156.49 76.89 o 2 8 2 76.42 183.27 50.69 o 4 8 2 113.91 165.20 75.32 o 6 8 2 240.01 265.87 83.83 o 1 9 2 200.20 317.80 55.93 o 3 9 2 844.30 964.24 82.12 o 5 9 2 477.93 655.58 97.78 o 7 9 2 620.39 591.13 106.37 o 9 9 2 12.09 211.52 200.69 o 0 10 2 112.59 147.15 92.29 o 2 10 2 0.58 102.22 70.01 o 4 10 2 0.48 130.27 69.31 o 6 10 2 21.64 103.70 92.25 o 8 10 2 96.80 148.56 107.03 o 1 11 2 24134.76 23349.17 263.63 o 3 11 2 4085.13 4243.41 152.86 o 5 11 2 17822.39 17671.74 297.66 o 7 11 2 23981.66 23932.13 316.14 o 9 11 2 443.41 538.19 210.24 o 11 11 2 6341.79 6929.13 393.19 o 0 12 2 231.44 292.16 136.62 o 2 12 2 8.13 155.86 87.58 o 4 12 2 0.00 90.04 97.20 o 6 12 2 2.52 136.66 113.69 o 8 12 2 92.17 158.92 146.94 o 10 12 2 0.09 200.02 163.06 o 1 13 2 23959.51 24656.74 328.53 o 3 13 2 15971.67 15876.64 286.76 o 5 13 2 262.43 236.30 119.94 o 7 13 2 6740.50 6361.42 215.41 o 9 13 2 2298.63 2012.03 223.97 o 11 13 2 4691.51 4969.16 364.06 o 13 13 2 9061.78 9106.09 512.10 o 0 14 2 106.84 191.52 157.28 o 2 14 2 8.74 150.04 107.55 o 4 14 2 47.41 155.55 132.75 o 6 14 2 72.53 131.43 138.41 o 8 14 2 3.60 211.33 164.54 o 10 14 2 70.79 177.16 167.97 o 12 14 2 28.35 162.76 194.21 o 1 15 2 6449.90 6426.28 231.97 o 3 15 2 1307.86 1122.75 162.58 o 5 15 2 986.41 706.21 151.47 o 7 15 2 3295.28 3023.40 241.95 o 9 15 2 115.94 165.60 167.70 o 11 15 2 6.58 187.68 211.54 o 13 15 2 22.07 245.76 222.63 o 15 15 2 1.68 258.70 388.46 o 0 16 2 172.42 218.85 217.03 o 2 16 2 1.62 150.43 154.88 o 4 16 2 10.02 145.01 145.18 o 6 16 2 72.50 151.61 158.80 o 8 16 2 34.06 147.15 187.88 o 10 16 2 20.34 188.92 219.12 o 12 16 2 13.71 186.90 255.63 o 14 16 2 16.82 252.58 257.66 o 1 17 2 24624.56 24291.59 394.59 o 3 17 2 147.74 175.67 149.33 o 5 17 2 12111.23 12607.91 359.62 o 7 17 2 15897.61 15852.27 427.39 o 9 17 2 1297.79 1496.45 247.56 o 11 17 2 7781.57 8347.19 363.12 o 13 17 2 3802.25 3625.45 437.56 o 15 17 2 241.49 394.88 348.83 o 0 18 2 33.67 231.64 237.97 o 2 18 2 1.30 214.53 176.23 o 4 18 2 0.00 103.69 196.58 o 6 18 2 5.01 276.38 232.72 o 8 18 2 26.96 214.92 254.48 o 10 18 2 1.97 297.80 236.93 o 12 18 2 0.47 213.64 291.91 o 14 18 2 22.47 297.88 328.86 o 1 19 2 2776.31 2451.94 286.06 o 3 19 2 43.63 173.23 177.67 o 5 19 2 4819.14 4687.13 436.03 o 7 19 2 1134.71 1130.42 290.27 o 9 19 2 101.60 247.39 243.89 o 11 19 2 6962.65 6591.87 457.76 o 13 19 2 1329.83 1667.70 408.07 o 0 20 2 0.02 210.33 355.94 o 2 20 2 0.16 287.61 222.63 o 4 20 2 0.00 158.78 253.06 o 6 20 2 4.85 212.24 344.05 o 8 20 2 0.88 119.52 272.12 o 10 20 2 1.54 241.36 318.86 o 1 21 2 314.33 220.90 240.10 o 3 21 2 246.24 420.66 306.71 o 5 21 2 6.09 171.34 285.79 o 7 21 2 3.25 298.43 294.72 o 9 21 2 27.90 217.20 313.23 o 0 22 2 95.12 176.07 405.48 o 2 22 2 6.39 162.51 347.19 o 4 22 2 10.98 244.98 375.22 o 6 22 2 52.23 392.38 330.66 o 1 23 2 4885.93 5415.28 575.23 o 1 2 3 9740.08 9519.60 111.18 o 2 3 3 1083.90 1954.26 70.54 o 1 4 3 148.85 175.32 40.66 o 3 4 3 7797.92 7192.50 101.05 o 2 5 3 13082.93 11114.61 117.21 o 4 5 3 65.76 112.22 53.24 o 1 6 3 354.82 356.56 59.69 o 3 6 3 346.67 560.16 71.64 o 5 6 3 13.46 152.55 69.87 o 2 7 3 21067.75 23803.22 180.76 o 4 7 3 954.78 1118.99 81.95 o 6 7 3 8.87 122.83 66.20 o 1 8 3 16425.27 17565.16 233.31 o 3 8 3 40965.77 43356.04 673.59 o 5 8 3 209.24 143.71 67.30 o 7 8 3 13816.78 14684.84 202.55 o 2 9 3 41290.82 44252.12 578.62 o 4 9 3 15564.96 15591.92 225.56 o 6 9 3 1470.35 1381.08 122.24 o 8 9 3 31306.40 32310.71 424.85 o 1 10 3 8302.13 7536.78 127.33 o 3 10 3 4024.71 3348.31 116.74 o 5 10 3 6584.47 6729.20 158.63 o 7 10 3 8810.96 8730.92 213.58 o 9 10 3 21336.30 20392.23 323.50 o 2 11 3 1882.96 1760.05 97.69 o 4 11 3 2372.69 2776.21 152.82 o 6 11 3 115.24 212.82 130.37 o 8 11 3 2706.26 2943.57 187.91 o 10 11 3 1503.21 1270.94 187.75 o 1 12 3 1110.37 1442.55 123.40 o 3 12 3 180.61 162.31 106.30 o 5 12 3 215.33 220.88 108.82 o 7 12 3 6.57 135.01 122.48 o 9 12 3 1199.75 1320.76 187.14 o 11 12 3 21.29 176.46 165.23 o 2 13 3 657.51 557.62 136.48 o 4 13 3 793.97 719.83 136.56 o 6 13 3 288.60 176.88 128.09 o 8 13 3 3961.98 3423.37 250.49 o 10 13 3 1020.61 844.39 181.98 o 12 13 3 601.15 523.90 191.55 o 1 14 3 6128.39 6554.71 217.14 o 3 14 3 616.25 733.18 137.87 o 5 14 3 473.99 370.04 144.37 o 7 14 3 1365.68 1272.41 186.09 o 9 14 3 9938.23 10244.73 316.50 o 11 14 3 162.16 308.14 178.31 o 13 14 3 1560.94 1491.61 257.61 o 2 15 3 9652.38 9417.48 251.29 o 4 15 3 3801.23 3527.59 216.20 o 6 15 3 443.93 359.18 165.91 o 8 15 3 16678.73 16556.97 392.90 o 10 15 3 4492.27 4244.37 281.93 o 12 15 3 597.81 597.46 228.20 o 14 15 3 1846.06 2160.46 364.59 o 1 16 3 147.50 166.61 159.25 o 3 16 3 12664.28 12675.42 346.94 o 5 16 3 4597.96 4009.34 229.01 o 7 16 3 7550.58 7119.71 340.17 o 9 16 3 6525.44 6329.45 320.07 o 11 16 3 37.63 266.07 218.76 o 13 16 3 899.21 859.37 265.96 o 15 16 3 3641.75 3722.76 491.76 o 2 17 3 1773.66 1642.68 209.84 o 4 17 3 5456.21 5296.94 294.01 o 6 17 3 153.71 163.31 208.67 o 8 17 3 692.35 739.85 243.10 o 10 17 3 1074.08 1056.63 279.24 o 12 17 3 238.45 319.94 241.67 o 14 17 3 448.08 528.97 330.74 o 1 18 3 173.82 196.97 167.18 o 3 18 3 171.24 177.21 205.18 o 5 18 3 108.01 190.64 213.55 o 7 18 3 574.38 581.69 220.26 o 9 18 3 112.06 284.83 249.74 o 11 18 3 38.78 177.33 283.87 o 13 18 3 23.74 153.79 290.29 o 2 19 3 2810.14 2544.47 254.99 o 4 19 3 1001.42 955.91 287.28 o 6 19 3 47.25 165.43 267.29 o 8 19 3 4376.19 3850.95 370.18 o 10 19 3 3831.17 3916.36 432.21 o 12 19 3 144.12 397.57 342.97 o 1 20 3 2038.74 1880.14 290.93 o 3 20 3 2000.06 2192.14 365.45 o 5 20 3 107.03 318.96 265.10 o 7 20 3 82.50 145.87 290.95 o 9 20 3 5066.25 5540.85 493.91 o 11 20 3 313.62 387.71 401.82 o 2 21 3 1936.55 1874.56 330.59 o 4 21 3 2237.41 1900.19 491.53 o 6 21 3 136.22 289.49 328.80 o 8 21 3 463.73 436.44 302.19 o 1 22 3 428.22 431.39 376.75 o 3 22 3 931.08 504.66 508.14 o 5 22 3 244.54 292.60 389.89 o 0 0 4 1738731.13 1437178.00 38687.86 o 0 2 4 3490.25 3015.84 141.67 o 2 2 4 45699.68 47438.70 357.80 o 1 3 4 911.15 1197.86 80.14 o 0 4 4 85441.97 91349.69 2222.99 o 2 4 4 5294.34 5289.70 133.58 o 4 4 4 143.88 262.44 91.75 o 1 5 4 94.31 134.01 47.73 o 3 5 4 789.03 765.24 68.70 o 0 6 4 105238.05 108204.66 875.56 o 2 6 4 50478.80 52967.66 460.51 o 4 6 4 19286.88 17868.68 199.83 o 6 6 4 49942.96 49421.29 558.93 o 1 7 4 1.19 87.57 52.44 o 3 7 4 288.74 286.69 70.86 o 5 7 4 88.54 121.34 71.72 o 0 8 4 119016.30 132732.17 1158.64 o 2 8 4 215.95 210.20 63.78 o 4 8 4 7101.79 7082.22 141.67 o 6 8 4 21544.47 21524.28 327.93 o 8 8 4 18628.79 19287.08 338.78 o 1 9 4 402.29 393.39 77.17 o 3 9 4 2.41 82.98 66.71 o 5 9 4 484.66 306.45 94.75 o 7 9 4 35.19 122.07 82.65 o 0 10 4 46568.51 48427.78 965.24 o 2 10 4 3675.00 3619.25 109.49 o 4 10 4 365.24 306.77 90.56 o 6 10 4 8730.48 8057.32 195.25 o 8 10 4 17314.18 16903.52 260.78 o 10 10 4 13753.47 13296.16 404.20 o 1 11 4 200.91 203.54 79.67 o 3 11 4 242.49 235.98 104.20 o 5 11 4 348.28 256.64 110.89 o 7 11 4 141.91 143.57 117.45 o 9 11 4 31.38 141.15 129.46 o 0 12 4 75603.96 79762.98 585.13 o 2 12 4 6712.38 6844.46 171.40 o 4 12 4 2690.86 2781.18 171.56 o 6 12 4 30219.24 32977.03 606.20 o 8 12 4 10493.92 10614.94 254.48 o 10 12 4 967.70 1147.90 192.62 o 12 12 4 11339.46 12362.68 470.47 o 1 13 4 13.67 124.55 116.58 o 3 13 4 65.23 186.08 120.68 o 5 13 4 1.30 145.54 122.30 o 7 13 4 14.76 184.74 136.70 o 9 13 4 115.91 212.86 172.60 o 11 13 4 36.85 151.24 180.00 o 0 14 4 8218.95 7597.49 361.27 o 2 14 4 957.87 1056.22 186.77 o 4 14 4 6097.34 5980.68 219.72 o 6 14 4 1511.99 1507.10 199.41 o 8 14 4 1086.16 1181.98 221.14 o 10 14 4 25.58 82.95 162.62 o 12 14 4 11368.17 11411.38 415.33 o 14 14 4 494.01 520.54 392.04 o 1 15 4 82.75 190.04 143.43 o 3 15 4 4.38 196.30 145.27 o 5 15 4 43.84 111.17 188.50 o 7 15 4 6.53 53.05 85.50 o 9 15 4 59.35 106.80 191.01 o 11 15 4 8.29 125.09 241.48 o 13 15 4 34.23 231.03 251.42 o 0 16 4 28779.22 29190.17 654.38 o 2 16 4 3167.73 2967.94 225.08 o 4 16 4 1756.51 1538.16 205.75 o 6 16 4 8593.58 8367.94 352.61 o 8 16 4 1552.36 1199.07 227.20 o 10 16 4 139.99 209.80 265.87 o 12 16 4 3771.93 3972.65 426.35 o 14 16 4 1110.64 1143.39 407.33 o 16 16 4 3378.92 3505.26 655.01 o 1 17 4 133.83 273.22 167.72 o 3 17 4 109.89 158.41 185.91 o 5 17 4 338.18 340.18 199.31 o 7 17 4 55.47 135.80 212.55 o 9 17 4 23.32 185.27 249.11 o 11 17 4 16.34 267.48 263.29 o 13 17 4 74.87 143.42 328.23 o 15 17 4 0.13 342.31 377.17 o 0 18 4 27528.72 28002.71 664.34 o 2 18 4 3846.01 4072.99 290.43 o 4 18 4 5431.61 5226.35 439.02 o 6 18 4 12260.05 13304.34 469.50 o 8 18 4 6169.19 5894.49 434.71 o 10 18 4 8260.80 8970.34 504.31 o 12 18 4 8182.71 9248.16 565.05 o 1 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5 3315.25 2598.04 113.46 o 7 8 5 15549.87 15096.82 204.31 o 2 9 5 52795.11 56737.93 360.85 o 4 9 5 30285.04 31351.60 411.60 o 6 9 5 93.17 146.14 90.24 o 8 9 5 37048.62 37429.18 559.70 o 1 10 5 9358.32 8850.38 150.33 o 3 10 5 17004.07 16612.16 196.03 o 5 10 5 11790.52 11644.46 200.80 o 7 10 5 9587.64 9486.87 198.30 o 9 10 5 25995.01 26985.23 511.22 o 2 11 5 946.84 857.51 115.66 o 4 11 5 10085.98 10493.43 204.90 o 6 11 5 245.71 208.29 119.10 o 8 11 5 9804.78 9639.85 240.12 o 10 11 5 95.59 215.74 160.80 o 1 12 5 155.66 236.09 100.58 o 3 12 5 251.29 249.05 107.98 o 5 12 5 204.52 213.31 119.49 o 7 12 5 31.68 217.06 146.38 o 9 12 5 314.13 404.32 184.71 o 11 12 5 9.09 160.78 165.92 o 2 13 5 1448.10 1203.41 153.97 o 4 13 5 983.96 808.26 153.57 o 6 13 5 3.58 238.79 168.13 o 8 13 5 3905.17 3443.20 238.00 o 10 13 5 1136.35 1077.68 237.50 o 12 13 5 489.33 408.42 227.90 o 1 14 5 5131.04 5238.38 233.06 o 3 14 5 2449.16 2661.02 240.76 o 5 14 5 773.85 729.79 209.00 o 7 14 5 1019.44 978.35 209.13 o 9 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704.98 755.55 138.68 o 6 7 9 0.81 140.34 122.00 o 1 8 9 5044.23 4718.19 183.65 o 3 8 9 20740.49 20377.37 288.92 o 5 8 9 665.66 648.20 143.74 o 7 8 9 4500.45 4184.05 200.84 o 2 9 9 12125.04 12601.03 358.34 o 4 9 9 7549.80 8036.08 264.68 o 6 9 9 138.00 138.10 116.52 o 8 9 9 11192.47 11786.93 280.06 o 1 10 9 1752.00 1463.11 162.32 o 3 10 9 3953.98 4058.73 206.05 o 5 10 9 3403.77 2914.34 193.19 o 7 10 9 3006.70 2716.49 197.20 o 9 10 9 6842.94 7174.33 266.88 o 2 11 9 557.30 486.83 161.64 o 4 11 9 3497.22 2904.75 219.51 o 6 11 9 67.51 178.79 146.75 o 8 11 9 4815.42 4620.33 240.60 o 10 11 9 30.19 159.91 213.56 o 1 12 9 51.83 111.27 148.66 o 3 12 9 2.43 136.37 144.56 o 5 12 9 14.88 127.92 160.77 o 7 12 9 149.71 202.59 174.99 o 9 12 9 295.15 424.91 210.75 o 11 12 9 11.77 135.53 268.57 o 2 13 9 355.73 411.79 209.19 o 4 13 9 137.53 100.60 240.89 o 6 13 9 4.89 253.18 194.51 o 8 13 9 1394.39 1303.72 250.01 o 10 13 9 257.23 248.76 239.12 o 12 13 9 113.41 345.15 244.91 o 1 14 9 1721.37 1780.13 364.61 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0 12 10 282.17 383.07 246.57 o 2 12 10 145.48 275.57 177.10 o 4 12 10 0.84 167.14 164.02 o 6 12 10 14.04 177.11 135.13 o 8 12 10 60.20 118.31 190.23 o 10 12 10 22.54 226.38 239.27 o 1 13 10 10122.46 10229.23 387.21 o 3 13 10 2402.05 2005.02 319.16 o 5 13 10 655.17 630.86 214.22 o 7 13 10 3912.82 4268.28 336.24 o 9 13 10 1042.70 960.26 282.16 o 11 13 10 1894.42 2135.03 429.94 o 13 13 10 5032.94 5115.28 593.27 o 0 14 10 65.97 182.70 331.17 o 2 14 10 4.02 253.11 235.61 o 4 14 10 44.36 241.40 292.99 o 6 14 10 54.62 267.28 382.21 o 8 14 10 7.32 207.72 261.34 o 10 14 10 106.27 161.80 443.84 o 12 14 10 16.83 265.13 361.52 o 1 15 10 914.26 902.20 319.22 o 3 15 10 204.28 348.58 263.62 o 5 15 10 376.11 395.68 289.40 o 7 15 10 317.69 273.97 372.12 o 9 15 10 19.05 324.75 354.29 o 11 15 10 72.45 303.53 276.07 o 0 16 10 83.94 271.86 349.49 o 2 16 10 49.93 290.66 247.25 o 4 16 10 0.02 223.46 307.49 o 6 16 10 22.41 213.01 314.63 o 8 16 10 6.17 306.25 369.14 o 1 17 10 6397.14 6877.00 502.10 o 3 17 10 2.38 231.26 348.63 o 5 17 10 3376.75 3613.07 467.79 o 7 17 10 4182.61 4764.58 640.96 o 0 18 10 29.24 359.76 427.42 o 2 18 10 4.32 329.00 301.81 o 4 18 10 0.25 305.27 319.47 o 1 2 11 1502.76 1278.16 275.46 o 2 3 11 261.63 408.81 192.50 o 1 4 11 114.92 183.40 189.07 o 3 4 11 2843.21 2710.87 212.72 o 2 5 11 2385.77 2259.85 201.29 o 4 5 11 388.65 420.19 155.48 o 1 6 11 112.97 236.59 140.55 o 3 6 11 127.94 257.11 146.38 o 5 6 11 73.81 179.08 154.74 o 2 7 11 1401.78 1413.59 182.84 o 4 7 11 269.35 368.95 148.71 o 6 7 11 243.93 221.79 161.30 o 1 8 11 1631.85 1554.96 227.84 o 3 8 11 5969.85 5784.40 249.36 o 5 8 11 113.13 220.03 147.85 o 7 8 11 997.96 936.94 198.39 o 2 9 11 4870.41 4758.74 257.03 o 4 9 11 2489.54 2399.89 221.41 o 6 9 11 477.39 500.43 178.65 o 8 9 11 4561.37 4746.37 271.42 o 1 10 11 1096.72 1116.16 225.90 o 3 10 11 997.01 872.95 182.24 o 5 10 11 1668.92 1548.79 219.67 o 7 10 11 1379.08 1468.67 231.73 o 9 10 11 3518.63 3585.24 298.76 o 2 11 11 11.65 181.61 188.60 o 4 11 11 609.51 457.38 178.49 o 6 11 11 7.68 256.28 177.31 o 8 11 11 742.84 819.00 238.75 o 10 11 11 113.82 314.00 247.45 o 1 12 11 135.89 189.36 211.98 o 3 12 11 1.93 202.75 199.74 o 5 12 11 63.27 179.15 192.57 o 7 12 11 15.28 225.33 211.87 o 9 12 11 190.04 253.30 283.98 o 11 12 11 0.23 135.05 336.83 o 2 13 11 12.81 226.86 239.00 o 4 13 11 5.67 213.06 252.30 o 6 13 11 164.22 256.81 221.34 o 8 13 11 321.94 406.87 245.96 o 10 13 11 47.01 325.04 330.74 o 12 13 11 127.99 387.89 334.85 o 1 14 11 1411.48 1309.14 299.46 o 3 14 11 444.60 567.85 337.86 o 5 14 11 488.39 595.85 339.26 o 7 14 11 458.74 489.23 295.30 o 9 14 11 2486.68 2426.65 539.74 o 2 15 11 1155.65 1015.94 337.12 o 4 15 11 674.75 690.50 359.44 o 6 15 11 1.40 127.95 321.80 o 8 15 11 2339.51 2432.90 611.18 o 1 16 11 6.48 256.83 295.20 o 3 16 11 1909.00 2217.53 439.05 o 5 16 11 887.33 973.13 422.29 o 7 16 11 917.80 766.12 398.19 o 2 17 11 702.39 671.66 331.79 o 4 17 11 1462.90 1232.73 458.20 o 0 0 12 39419.73 43314.27 1812.72 o 0 2 12 25.75 165.78 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215.20 o 9 11 12 22.29 238.33 256.96 o 0 12 12 3936.51 4174.31 518.13 o 2 12 12 134.01 150.71 258.41 o 4 12 12 36.87 212.38 229.87 o 6 12 12 1157.70 1474.91 289.17 o 8 12 12 269.29 450.21 259.21 o 10 12 12 9.84 258.90 385.49 o 1 13 12 0.00 222.88 253.76 o 3 13 12 13.28 208.75 395.30 o 5 13 12 30.01 207.74 328.80 o 7 13 12 12.26 206.24 264.90 o 9 13 12 12.05 215.09 453.78 o 0 14 12 89.19 139.60 403.47 o 2 14 12 19.39 206.84 327.59 o 4 14 12 315.14 228.13 330.46 o 6 14 12 126.04 289.29 358.84 o 8 14 12 6.70 253.23 368.59 o 1 15 12 5.33 284.59 375.16 o 3 15 12 4.02 275.67 311.69 o 5 15 12 27.43 388.92 403.26 o 0 16 12 3932.00 4311.91 809.66 o 2 16 12 329.71 562.37 596.08 o 1 2 13 139.74 306.14 271.30 o 2 3 13 296.30 596.10 229.19 o 1 4 13 14.72 385.46 318.10 o 3 4 13 774.55 866.71 225.88 o 2 5 13 328.68 392.14 230.21 o 4 5 13 25.99 185.06 190.15 o 1 6 13 16.99 202.33 214.91 o 3 6 13 22.17 249.17 191.34 o 5 6 13 5.01 170.87 186.19 o 2 7 13 1261.61 1305.08 264.13 o 4 7 13 90.74 232.56 237.37 o 6 7 13 21.21 217.90 211.58 o 1 8 13 705.39 584.29 266.88 o 3 8 13 3074.21 3009.74 334.98 o 5 8 13 3.97 268.90 236.49 o 7 8 13 784.27 691.56 244.17 o 2 9 13 1261.25 1323.59 305.38 o 4 9 13 825.73 904.43 257.15 o 6 9 13 103.29 177.61 234.82 o 8 9 13 1703.72 1901.60 333.03 o 1 10 13 94.87 232.91 243.87 o 3 10 13 224.40 347.53 234.62 o 5 10 13 438.33 520.68 274.84 o 7 10 13 633.32 556.82 268.22 o 9 10 13 803.93 1013.88 313.20 o 2 11 13 44.13 251.88 301.10 o 4 11 13 492.39 510.69 260.05 o 6 11 13 19.93 312.52 310.34 o 8 11 13 1178.24 1203.95 317.72 o 10 11 13 17.75 209.52 301.59 o 1 12 13 7.50 231.54 270.91 o 3 12 13 18.94 184.05 287.91 o 5 12 13 0.02 55.36 329.47 o 7 12 13 119.11 219.82 328.16 o 2 13 13 61.76 264.88 299.58 o 4 13 13 9.54 277.76 329.49 o 6 13 13 4.61 138.72 349.39 o 1 14 13 299.47 473.58 346.38 o 3 14 13 66.83 333.23 390.36 o 5 14 13 2.92 216.75 424.66 o 1 1 14 6894.53 6741.46 743.23 o 0 2 14 222.00 199.44 321.78 o 1 3 14 70.78 119.03 273.91 o 3 3 14 2.28 193.28 440.36 o 0 4 14 22.60 320.01 472.58 o 2 4 14 115.97 306.06 279.14 o 1 5 14 2830.21 3052.41 381.13 o 3 5 14 1.67 224.12 224.19 o 5 5 14 353.23 661.93 495.87 o 0 6 14 13.72 353.77 435.36 o 2 6 14 11.36 149.17 297.87 o 4 6 14 24.10 178.87 239.79 o 1 7 14 2748.90 3036.37 405.80 o 3 7 14 18.26 146.85 225.41 o 5 7 14 2101.79 2278.94 340.31 o 7 7 14 1231.46 1588.29 449.25 o 0 8 14 3.85 297.86 320.86 o 2 8 14 11.45 226.85 271.73 o 4 8 14 0.22 115.62 274.68 o 6 8 14 27.34 50.97 294.12 o 1 9 14 20.17 160.54 272.11 o 3 9 14 39.58 175.48 284.91 o 5 9 14 77.57 183.66 255.45 o 7 9 14 72.03 238.70 314.43 o 9 9 14 59.95 365.41 630.73 o 0 10 14 55.26 188.12 343.34 o 2 10 14 36.27 177.31 308.49 o 4 10 14 2.44 182.04 262.98 o 6 10 14 59.50 330.66 303.70 o 8 10 14 3.77 293.22 416.11 o 1 11 14 1347.79 1489.75 414.00 o 3 11 14 436.67 310.21 376.61 o 5 11 14 992.04 859.27 383.34 o 7 11 14 1607.85 1802.26 416.99 o 0 12 14 49.93 356.37 465.34 o 2 12 14 98.91 264.38 311.56 o 4 12 14 0.44 227.70 392.94 o 1 13 14 2064.79 2170.81 566.80 o 1 2 15 388.96 370.65 328.56 o 2 3 15 129.63 352.64 360.86 o 1 4 15 24.67 213.25 346.43 o 3 4 15 1049.81 1027.21 331.70 o 2 5 15 704.25 587.64 298.93 o 4 5 15 144.65 288.66 382.23 o 1 6 15 18.60 255.08 299.55 o 3 6 15 27.93 219.65 318.07 o 5 6 15 19.20 199.31 328.81 o 2 7 15 373.93 442.71 385.89 o 4 7 15 107.90 220.76 278.70 o 6 7 15 94.27 313.86 295.73 o 1 8 15 319.18 504.26 355.46 o 3 8 15 1606.96 1577.76 397.48 o 5 8 15 17.28 389.72 314.41 o 7 8 15 195.36 200.30 335.81 o 2 9 15 1210.92 1226.26 359.29 o 4 9 15 743.95 759.45 317.40 o 1 10 15 313.28 480.89 327.69 o 3 10 15 433.10 378.16 390.49 o 0 0 16 7803.09 9508.14 1552.63 o 0 2 16 7.72 196.00 618.63 o 2 2 16 393.94 475.16 690.94 o 1 3 16 31.52 209.66 337.77 o 0 4 16 429.63 262.83 643.97 o 2 4 16 44.76 272.32 406.98 o 4 4 16 11.52 218.70 654.61 o 1 5 16 19.11 319.86 375.92 o 3 5 16 38.18 236.47 447.47 o 0 6 16 393.84 625.10 460.04 o 2 6 16 469.72 545.26 427.96 o 4 6 16 187.98 429.16 386.65 o 1 7 16 3.38 364.42 341.65 o