#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/30/2203080.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203080_Fobs loop_ _publ_author_name 'Ferguson, George' 'O'Leary, Brian J.' 'Spalding, Trevor R.' _publ_section_title ; Bis(triphenylsilyl)phenylarsenite, PhAs(OSiPh~3~)~2~ ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m118 _journal_page_last m120 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.124 _cell_angle_gamma 90.000 _cell_length_a 9.8563 _cell_length_b 11.3662 _cell_length_c 32.8677 _exptl_crystal_F_000 1456.00 _reflns_d_resolution_high 0.7844 _[local]_cod_data_source_file lh6153Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TRS95-32' _shelx_refln_list_code 4 _shelx_f_calc_maximum 278.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 773.20 696.76 35.17 o 4 0 0 15838.38 15235.00 151.38 o 6 0 0 27.06 119.78 126.92 o 8 0 0 3879.89 3538.86 127.94 o 10 0 0 84.53 44.34 214.58 o 12 0 0 39.06 80.53 248.23 o 1 1 0 3209.42 3299.30 28.54 o 2 1 0 13189.34 14076.45 100.41 o 3 1 0 78.13 75.95 24.47 o 4 1 0 2598.91 2708.05 49.95 o 5 1 0 2035.39 2020.97 49.95 o 6 1 0 1355.82 1232.97 50.46 o 7 1 0 1039.26 1056.61 55.56 o 8 1 0 2151.53 2147.38 73.91 o 9 1 0 162.01 38.74 118.25 o 10 1 0 17.44 78.49 140.68 o 11 1 0 108.41 140.68 162.60 o 12 1 0 12.18 107.04 79.51 o 0 2 0 8502.06 7636.36 75.95 o 1 2 0 15379.29 17387.47 120.80 o 2 2 0 3200.71 3734.59 44.85 o 3 2 0 773.16 890.96 31.09 o 4 2 0 721.06 684.53 33.13 o 5 2 0 37.12 20.39 87.16 o 6 2 0 1932.82 1778.86 57.09 o 7 2 0 42.19 91.24 101.43 o 8 2 0 357.50 487.79 50.46 o 9 2 0 4.40 39.25 121.31 o 10 2 0 569.92 577.49 77.47 o 11 2 0 2.92 51.48 151.38 o 12 2 0 131.32 81.04 182.98 o 1 3 0 50.88 28.54 62.69 o 2 3 0 11464.60 11047.29 80.53 o 3 3 0 5159.09 5367.67 62.18 o 4 3 0 1651.34 1651.44 44.85 o 5 3 0 837.29 906.25 39.76 o 6 3 0 547.89 456.18 43.83 o 7 3 0 2420.13 2479.19 74.42 o 8 3 0 1795.14 1728.91 71.36 o 9 3 0 25.08 101.43 112.13 o 10 3 0 237.33 301.74 72.89 o 11 3 0 403.97 391.45 86.65 o 12 3 0 42.25 201.84 164.12 o 0 4 0 20986.24 20915.63 213.57 o 1 4 0 19.33 14.27 60.65 o 2 4 0 253.85 296.65 24.47 o 3 4 0 10.49 17.33 65.24 o 4 4 0 724.35 597.88 36.19 o 5 4 0 1770.11 1555.61 53.52 o 6 4 0 183.18 28.03 112.64 o 7 4 0 60.82 32.11 118.25 o 8 4 0 746.88 609.60 56.58 o 9 4 0 709.54 679.43 62.18 o 10 4 0 3.46 113.15 108.57 o 11 4 0 18.42 54.03 77.98 o 12 4 0 29.46 213.06 150.87 o 1 5 0 301.73 286.96 25.49 o 2 5 0 4917.00 5232.60 67.28 o 3 5 0 91.38 179.92 27.01 o 4 5 0 1019.90 923.58 42.81 o 5 5 0 26.41 37.21 97.86 o 6 5 0 2824.07 2853.31 73.40 o 7 5 0 162.54 84.10 144.25 o 8 5 0 192.27 39.25 130.99 o 9 5 0 109.38 44.34 154.95 o 10 5 0 467.42 478.61 56.58 o 11 5 0 2.81 56.07 170.24 o 0 6 0 75.38 25.49 95.82 o 1 6 0 3361.94 3370.66 58.62 o 2 6 0 93.69 136.60 35.17 o 3 6 0 474.35 416.94 37.21 o 4 6 0 93.95 88.69 96.84 o 5 6 0 2188.24 2298.76 66.77 o 6 6 0 15.39 33.13 95.31 o 7 6 0 14.90 136.60 105.00 o 8 6 0 25.20 41.80 61.16 o 9 6 0 444.70 350.17 59.64 o 10 6 0 12.36 145.77 153.93 o 11 6 0 5.78 58.62 145.77 o 1 7 0 365.25 358.83 44.85 o 2 7 0 1530.54 1416.97 50.46 o 3 7 0 29.51 90.22 45.36 o 4 7 0 162.88 188.08 48.42 o 5 7 0 1223.85 1147.34 56.58 o 6 7 0 372.50 295.63 61.16 o 7 7 0 25.37 40.27 123.35 o 8 7 0 128.94 91.75 134.05 o 9 7 0 0.57 49.44 142.72 o 10 7 0 154.07 55.05 176.36 o 11 7 0 17.45 83.59 187.06 o 0 8 0 158.76 127.43 50.97 o 1 8 0 1049.23 1022.97 48.93 o 2 8 0 84.80 29.05 110.61 o 3 8 0 1708.90 1685.08 62.69 o 4 8 0 13.17 34.66 107.04 o 5 8 0 221.00 247.72 59.64 o 6 8 0 323.03 227.33 50.46 o 7 8 0 167.04 43.32 128.95 o 8 8 0 6.50 47.91 145.77 o 9 8 0 59.00 53.01 149.34 o 10 8 0 26.20 74.42 77.47 o 1 9 0 700.64 688.10 49.44 o 2 9 0 2526.01 2221.28 71.36 o 3 9 0 604.97 478.61 62.69 o 4 9 0 413.20 231.91 67.79 o 5 9 0 121.33 152.40 64.22 o 6 9 0 690.97 621.84 82.57 o 7 9 0 232.37 461.28 69.83 o 8 9 0 5.76 63.20 63.20 o 9 9 0 22.80 57.60 161.58 o 0 10 0 2568.05 2386.94 106.02 o 1 10 0 43.89 136.60 54.03 o 2 10 0 40.83 114.68 54.03 o 3 10 0 287.80 248.23 51.48 o 4 10 0 947.88 921.03 61.67 o 5 10 0 160.02 77.98 136.09 o 6 10 0 6.81 47.91 124.88 o 7 10 0 49.54 57.60 70.85 o 8 10 0 104.73 56.07 151.89 o 9 10 0 51.43 60.65 149.85 o 1 11 0 776.12 781.37 57.60 o 2 11 0 45.76 159.54 107.04 o 3 11 0 168.32 44.34 155.46 o 4 11 0 22.16 46.38 112.13 o 5 11 0 167.33 267.59 49.44 o 6 11 0 1.93 52.50 65.75 o 7 11 0 116.35 56.07 151.38 o 8 11 0 46.59 60.65 177.89 o 0 12 0 45.04 206.43 147.81 o 1 12 0 12.94 115.70 54.03 o 2 12 0 0.08 47.91 136.09 o 3 12 0 135.21 237.52 67.28 o 4 12 0 75.78 51.48 128.95 o 5 12 0 3.70 54.03 142.21 o 6 12 0 72.25 57.60 70.85 o 7 12 0 7.79 61.16 153.42 o 1 13 0 3.96 52.50 138.13 o 2 13 0 0.83 54.03 129.97 o 3 13 0 39.72 55.05 134.05 o 4 13 0 12.03 64.22 118.76 o 5 13 0 14.87 59.64 122.84 o 0 14 0 135.36 58.11 233.44 o 1 14 0 19.42 92.26 130.48 o 2 14 0 0.12 86.14 122.84 o 3 14 0 12.41 60.65 149.85 o -11 0 1 4.19 50.46 184.51 o -9 0 1 1550.28 1621.87 107.04 o -7 0 1 78.44 61.16 153.93 o -5 0 1 7886.94 7568.06 123.86 o -3 0 1 3364.88 4236.65 74.42 o -1 0 1 75213.15 79625.18 473.00 o 1 0 1 6311.73 7550.22 73.40 o 3 0 1 73.66 16.82 110.61 o 5 0 1 23.17 176.87 41.29 o 7 0 1 581.98 487.79 68.81 o 9 0 1 487.21 507.66 83.08 o 11 0 1 34.32 50.46 234.46 o -12 1 1 154.54 215.09 82.06 o -11 1 1 127.18 70.85 218.66 o -10 1 1 390.86 188.08 217.13 o -9 1 1 8.75 38.74 178.40 o -8 1 1 1815.61 1611.68 99.90 o -7 1 1 1372.17 1355.81 83.08 o -6 1 1 3131.39 3174.94 98.37 o -5 1 1 1827.77 1971.53 72.89 o -4 1 1 1494.20 1755.41 59.64 o -3 1 1 828.87 929.19 44.34 o -2 1 1 45468.21 49495.15 440.38 o -1 1 1 4911.09 6056.28 59.64 o 1 1 1 8796.18 10457.05 103.98 o 2 1 1 22259.17 23415.72 237.52 o 3 1 1 2447.43 2263.08 57.60 o 4 1 1 74.99 99.39 36.19 o 5 1 1 754.94 838.97 54.54 o 6 1 1 5160.22 5260.64 122.84 o 7 1 1 152.01 41.29 146.28 o 8 1 1 39.81 144.76 186.55 o 9 1 1 36.43 38.74 192.16 o 10 1 1 660.89 574.94 93.79 o 11 1 1 115.56 50.97 199.80 o 12 1 1 51.26 120.80 286.96 o -12 2 1 96.86 125.39 96.33 o -11 2 1 65.93 51.48 173.30 o -10 2 1 92.46 45.36 233.44 o -9 2 1 197.43 39.25 173.81 o -8 2 1 825.16 603.49 79.00 o -7 2 1 237.52 186.04 178.91 o -6 2 1 730.37 820.11 64.22 o -5 2 1 1819.34 2114.75 73.40 o -4 2 1 10793.44 11428.54 136.09 o -3 2 1 1431.63 1678.96 53.52 o -2 2 1 12508.26 13669.71 140.68 o -1 2 1 2756.66 3374.74 49.44 o 0 2 1 88.00 12.23 65.75 o 1 2 1 5358.23 4897.22 57.60 o 2 2 1 2382.29 2913.46 58.11 o 3 2 1 15091.23 16252.37 161.58 o 4 2 1 147.69 255.36 39.25 o 5 2 1 1992.58 2095.39 73.91 o 6 2 1 285.01 179.92 52.50 o 7 2 1 1854.54 1778.35 91.75 o 8 2 1 419.97 399.61 72.38 o 9 2 1 265.81 252.81 200.82 o 10 2 1 51.61 45.36 228.86 o 11 2 1 277.76 476.57 86.14 o 12 2 1 119.32 144.25 90.73 o -12 3 1 113.55 59.13 270.14 o -11 3 1 60.11 52.50 214.07 o -10 3 1 18.56 130.99 130.99 o -9 3 1 142.20 200.82 143.74 o -8 3 1 92.36 150.36 173.30 o -7 3 1 138.88 192.67 59.64 o -6 3 1 183.74 25.99 140.68 o -5 3 1 7.65 21.92 125.39 o -4 3 1 766.47 897.08 50.97 o -3 3 1 2412.69 2555.14 64.73 o -2 3 1 1084.96 1235.52 46.38 o -1 3 1 1673.89 1407.29 44.85 o 0 3 1 503.41 453.64 33.64 o 1 3 1 3517.45 3563.84 62.69 o 2 3 1 22650.08 22892.77 235.99 o 3 3 1 604.02 637.64 42.81 o 4 3 1 2.60 74.42 105.51 o 5 3 1 2117.71 2167.25 75.95 o 6 3 1 1899.55 1907.82 84.10 o 7 3 1 952.79 1020.93 77.98 o 8 3 1 178.83 35.68 197.76 o 9 3 1 194.60 229.88 226.31 o 10 3 1 75.53 46.38 207.45 o 11 3 1 150.65 258.93 185.02 o 12 3 1 14.88 89.20 92.77 o -12 4 1 2.31 60.65 249.24 o -11 4 1 14.91 54.03 201.33 o -10 4 1 432.92 99.39 250.77 o -9 4 1 195.41 200.82 74.93 o -8 4 1 2.57 37.21 149.34 o -7 4 1 59.99 133.54 144.25 o -6 4 1 484.54 474.53 57.09 o -5 4 1 1071.61 942.95 66.77 o -4 4 1 5802.16 6014.49 111.12 o -3 4 1 4.34 102.96 82.06 o -2 4 1 109.79 70.85 29.56 o -1 4 1 5877.74 5791.75 84.10 o 0 4 1 3375.63 3164.74 64.22 o 1 4 1 15.20 13.76 82.06 o 2 4 1 105.74 155.97 32.11 o 3 4 1 1347.79 1295.66 53.52 o 4 4 1 6046.66 6260.67 112.13 o 5 4 1 1.88 48.93 122.84 o 6 4 1 224.97 251.79 53.52 o 7 4 1 2612.57 2151.96 103.98 o 8 4 1 820.33 256.89 256.89 o 9 4 1 1.93 42.31 146.79 o 10 4 1 7.21 47.91 224.27 o 11 4 1 16.52 54.03 83.08 o 12 4 1 52.94 60.65 295.12 o -11 5 1 103.31 136.09 90.22 o -10 5 1 56.80 171.77 202.86 o -9 5 1 73.86 44.34 166.16 o -8 5 1 65.30 161.07 66.26 o -7 5 1 767.16 687.59 79.00 o -6 5 1 84.12 40.78 168.20 o -5 5 1 1.07 39.76 46.89 o -4 5 1 188.04 268.10 44.34 o -3 5 1 4507.12 4972.66 99.90 o -2 5 1 1759.32 1834.42 61.67 o -1 5 1 1.82 16.82 81.55 o 0 5 1 498.37 486.77 39.76 o 1 5 1 3109.78 3118.87 71.36 o 2 5 1 108.65 18.35 108.06 o 3 5 1 3124.34 3263.62 82.06 o 4 5 1 110.55 203.88 43.32 o 5 5 1 4562.18 4638.29 117.74 o 6 5 1 234.60 310.92 56.07 o 7 5 1 29.89 34.66 124.37 o 8 5 1 11.66 215.60 166.16 o 9 5 1 190.75 44.34 212.04 o 10 5 1 0.56 49.95 201.33 o 11 5 1 27.66 56.07 81.04 o -11 6 1 17.57 160.56 188.59 o -10 6 1 319.55 179.42 212.55 o -9 6 1 17.50 46.89 190.12 o -8 6 1 292.99 171.26 221.21 o -7 6 1 149.21 37.21 184.00 o -6 6 1 546.07 284.41 194.71 o -5 6 1 3.52 29.05 143.74 o -4 6 1 2543.59 2397.13 89.71 o -3 6 1 536.20 91.75 167.18 o -2 6 1 6245.18 6468.12 114.17 o -1 6 1 39.77 57.09 34.66 o 0 6 1 2206.67 2249.83 68.30 o 1 6 1 123.41 159.54 37.72 o 2 6 1 263.27 56.07 126.41 o 3 6 1 472.74 578.00 52.50 o 4 6 1 4787.81 4728.51 116.72 o 5 6 1 494.45 446.50 65.75 o 6 6 1 315.30 400.12 67.28 o 7 6 1 59.66 37.21 182.98 o 8 6 1 579.96 584.63 74.42 o 9 6 1 25.38 46.89 220.19 o 10 6 1 1.03 108.06 165.14 o 11 6 1 3.32 58.62 261.48 o -11 7 1 128.65 83.59 213.06 o -10 7 1 26.75 112.64 172.28 o -9 7 1 5.99 67.28 190.63 o -8 7 1 0.55 44.34 190.63 o -7 7 1 312.99 396.04 75.44 o -6 7 1 141.62 192.67 58.62 o -5 7 1 20.08 32.62 191.65 o -4 7 1 134.36 210.51 154.44 o -3 7 1 1207.97 1237.56 70.34 o -2 7 1 1.74 25.49 115.19 o -1 7 1 32.58 48.93 41.29 o 0 7 1 7.46 23.96 108.57 o 1 7 1 370.03 342.52 49.95 o 2 7 1 434.87 479.12 55.56 o 3 7 1 635.51 713.58 59.64 o 4 7 1 20.52 114.68 155.46 o 5 7 1 1146.21 1077.00 77.47 o 6 7 1 368.17 262.50 200.82 o 7 7 1 532.01 373.10 83.59 o 8 7 1 47.10 150.87 193.18 o 9 7 1 157.48 203.37 185.53 o 10 7 1 2.87 302.25 214.07 o -10 8 1 87.20 118.76 247.21 o -9 8 1 9.63 53.01 214.07 o -8 8 1 166.97 246.70 72.38 o -7 8 1 15.89 200.82 174.32 o -6 8 1 696.22 600.43 78.49 o -5 8 1 2.99 36.19 181.45 o -4 8 1 326.33 330.29 62.18 o -3 8 1 54.94 109.08 53.01 o -2 8 1 1582.65 1469.47 77.98 o -1 8 1 219.99 215.09 151.89 o 0 8 1 748.09 613.68 59.64 o 1 8 1 131.40 28.54 146.79 o 2 8 1 611.11 695.23 65.75 o 3 8 1 7.87 31.09 182.98 o 4 8 1 499.60 554.05 68.81 o 5 8 1 854.83 740.09 75.44 o 6 8 1 39.13 103.98 151.38 o 7 8 1 38.03 78.49 65.75 o 8 8 1 384.83 192.16 235.48 o 9 8 1 32.29 53.01 193.18 o 10 8 1 11.01 58.62 211.02 o -9 9 1 10.92 56.58 207.96 o -8 9 1 190.40 239.56 190.63 o -7 9 1 664.59 556.09 84.10 o -6 9 1 156.48 110.61 68.30 o -5 9 1 5.40 112.13 60.14 o -4 9 1 1127.93 911.35 84.10 o -3 9 1 1769.55 1657.04 97.35 o -2 9 1 78.60 148.83 181.96 o -1 9 1 100.06 151.38 55.05 o 0 9 1 110.82 184.51 127.94 o 1 9 1 1560.67 1642.77 87.67 o 2 9 1 290.14 325.70 60.65 o 3 9 1 120.40 225.29 162.60 o 4 9 1 4.48 37.21 178.40 o 5 9 1 242.51 175.85 67.79 o 6 9 1 418.20 43.32 223.25 o 7 9 1 4.72 47.40 74.93 o 8 9 1 23.58 103.47 178.91 o 9 9 1 68.41 56.58 246.19 o -9 10 1 134.66 60.65 256.89 o -8 10 1 12.91 56.07 248.73 o -7 10 1 0.19 51.48 221.72 o -6 10 1 3.62 47.91 198.27 o -5 10 1 832.71 755.38 95.82 o -4 10 1 734.47 710.02 90.22 o -3 10 1 46.55 94.29 60.65 o -2 10 1 5.21 38.23 145.27 o -1 10 1 1225.91 1097.39 87.16 o 0 10 1 399.30 366.48 64.22 o 1 10 1 73.28 37.21 181.96 o 2 10 1 155.37 197.25 56.58 o 3 10 1 263.65 337.42 68.81 o 4 10 1 615.38 644.26 83.59 o 5 10 1 24.63 44.34 175.85 o 6 10 1 171.95 219.68 205.41 o 7 10 1 37.70 204.39 144.76 o 8 10 1 18.47 56.07 244.15 o 9 10 1 56.88 62.18 91.24 o -8 11 1 66.64 60.65 239.05 o -7 11 1 47.57 164.63 80.53 o -6 11 1 139.12 206.94 189.10 o -5 11 1 86.44 95.31 226.82 o -4 11 1 205.19 46.38 227.33 o -3 11 1 0.73 44.34 155.97 o -2 11 1 831.31 815.01 88.18 o -1 11 1 59.64 186.04 148.32 o 0 11 1 489.33 537.23 74.42 o 1 11 1 7.88 133.03 170.24 o 2 11 1 349.07 505.11 70.34 o 3 11 1 88.37 44.34 172.79 o 4 11 1 79.92 89.71 213.57 o 5 11 1 76.11 48.93 186.04 o 6 11 1 246.44 186.55 85.12 o 7 11 1 1.22 111.12 192.67 o 8 11 1 3.63 60.65 201.33 o -7 12 1 10.84 61.16 250.26 o -6 12 1 25.13 57.60 213.06 o -5 12 1 33.68 54.03 207.45 o -4 12 1 34.64 51.48 211.53 o -3 12 1 127.71 95.31 182.98 o -2 12 1 27.03 214.58 153.42 o -1 12 1 173.09 46.89 246.19 o 0 12 1 0.10 59.13 167.18 o 1 12 1 40.86 150.36 192.67 o 2 12 1 24.05 245.17 173.30 o 3 12 1 195.45 126.92 228.86 o 4 12 1 0.36 51.48 214.58 o 5 12 1 55.04 54.03 195.73 o 6 12 1 1.60 57.60 208.98 o 7 12 1 154.92 281.36 223.76 o -5 13 1 7.79 59.64 188.59 o -4 13 1 24.17 57.09 76.97 o -3 13 1 0.28 106.02 184.00 o -2 13 1 77.80 205.41 167.69 o -1 13 1 5.18 52.50 210.51 o 0 13 1 19.43 52.50 162.09 o 1 13 1 5.96 62.18 65.75 o 2 13 1 240.17 53.52 246.19 o 3 13 1 50.49 176.87 226.31 o 4 13 1 0.67 57.09 222.74 o 5 13 1 9.89 154.44 180.94 o -3 14 1 0.28 274.22 195.73 o -2 14 1 9.51 75.95 193.69 o -1 14 1 66.94 58.62 219.68 o 0 14 1 60.98 58.11 255.87 o 1 14 1 0.73 58.62 186.55 o 2 14 1 17.55 59.64 269.12 o 3 14 1 59.65 60.65 187.06 o -12 0 2 37.71 57.09 265.55 o -10 0 2 849.04 804.82 99.39 o -8 0 2 1235.18 1138.17 91.24 o -6 0 2 713.24 840.50 61.16 o -4 0 2 4.14 33.13 103.47 o -2 0 2 2644.64 2666.76 50.46 o 2 0 2 53343.89 52471.30 451.60 o 4 0 2 26950.45 29653.97 297.67 o 6 0 2 3192.06 3381.36 101.94 o 8 0 2 3967.16 3832.45 130.48 o 10 0 2 1197.15 902.68 97.35 o 12 0 2 100.95 57.60 202.86 o -12 1 2 96.22 200.31 256.38 o -11 1 2 111.17 86.14 79.51 o -10 1 2 3.17 44.85 180.43 o -9 1 2 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