#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/30/2203095.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203095_Fobs loop_ _publ_author_name 'Sakai, Ken' 'Ishigami, Eri' _publ_section_title ; Bis{di-\m-isobutyrato-bis[cis-diammineplatinum(II)]} tetraperchlorate ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m65 _journal_page_last m68 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 74.354 _cell_angle_beta 84.621 _cell_angle_gamma 85.052 _cell_length_a 10.1557 _cell_length_b 14.5963 _cell_length_c 15.5209 _exptl_crystal_F_000 1552.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file ob6329Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' iso21 in P-1 2003/11/26 18:18:13 019 KENX' _shelx_refln_list_code 4 _shelx_f_calc_maximum 583.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 35625.54 39037.78 1258.31 o 3 0 0 1858.49 1554.82 84.55 o 4 0 0 22.71 22.12 24.63 o 5 0 0 896.23 932.05 134.31 o 6 0 0 37079.62 40763.19 1593.85 o 7 0 0 221.16 236.10 64.95 o 8 0 0 9067.49 10086.81 1096.42 o 9 0 0 20.21 38.10 129.72 o 10 0 0 15984.83 17855.43 1859.98 o 11 0 0 318.67 401.78 195.05 o 12 0 0 6.21 -61.15 165.12 o 13 0 0 389.39 423.62 249.26 o -13 1 0 4151.47 4944.55 644.90 o -12 1 0 543.63 787.10 262.66 o -11 1 0 458.84 503.50 209.97 o -10 1 0 493.09 591.97 195.71 o -9 1 0 8200.11 10205.69 1531.75 o -8 1 0 399.25 512.04 160.39 o -7 1 0 19072.16 20438.24 1528.51 o -6 1 0 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