#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/31/2203139.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203139_Fobs loop_ _publ_author_name 'van Albada, Gerard A.' 'Mohamadou, Aminou' 'Mutikainen, Ilpo' 'Turpeinen, Urho' 'Reedijk, Jan' _publ_section_title ; Diazidobis(2,2'-biimidazoline)nickel(II) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m237 _journal_page_last m238 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 97.637 _cell_angle_beta 103.327 _cell_angle_gamma 111.756 _cell_length_a 7.2960 _cell_length_b 7.9420 _cell_length_c 8.2080 _exptl_crystal_F_000 218.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file ac6079Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BIZNI2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 61.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 316.28 290.47 7.41 o 2 0 0 1125.93 1067.05 16.35 o 3 0 0 1348.16 1346.08 18.47 o 4 0 0 12.60 7.41 0.60 o 5 0 0 215.52 201.20 5.08 o 6 0 0 0.90 0.71 1.69 o 7 0 0 390.57 391.33 12.58 o 8 0 0 68.22 64.17 4.73 o -8 1 0 39.35 40.71 3.23 o -7 1 0 303.15 298.24 7.82 o -6 1 0 472.29 477.29 11.35 o -5 1 0 143.94 148.89 3.50 o -4 1 0 333.23 320.31 5.39 o -3 1 0 3.34 9.65 0.48 o -2 1 0 1454.07 1426.75 21.79 o -1 1 0 55.60 57.24 2.82 o 1 1 0 1100.95 1082.62 16.36 o 2 1 0 268.10 269.17 4.33 o 3 1 0 1075.15 1075.90 17.93 o 4 1 0 55.93 49.13 1.43 o 5 1 0 398.74 385.31 9.26 o 6 1 0 40.53 40.67 2.40 o 7 1 0 135.66 132.58 5.13 o -8 2 0 166.89 175.20 5.59 o -7 2 0 13.55 15.85 2.15 o -6 2 0 298.05 318.90 7.90 o -5 2 0 264.42 258.28 6.52 o -4 2 0 1309.17 1343.74 22.71 o -3 2 0 165.80 141.06 2.51 o -2 2 0 552.81 540.66 8.43 o -1 2 0 1790.48 1785.49 27.30 o 0 2 0 85.69 102.70 1.89 o 1 2 0 6.88 3.54 0.41 o 2 2 0 63.47 75.36 1.54 o 3 2 0 226.02 227.14 4.35 o 4 2 0 179.82 183.29 4.88 o 5 2 0 27.11 28.67 1.86 o 6 2 0 130.65 132.05 4.45 o 7 2 0 95.89 101.50 5.17 o -9 3 0 71.70 70.11 5.09 o -8 3 0 453.08 452.29 11.32 o -7 3 0 1.02 2.03 1.78 o -6 3 0 143.15 155.51 3.84 o -5 3 0 513.04 509.27 9.09 o -4 3 0 14.16 19.74 1.30 o -3 3 0 1043.69 1057.34 16.37 o -2 3 0 1101.35 1132.74 17.45 o -1 3 0 33.08 38.11 0.93 o 0 3 0 4.55 2.14 0.50 o 1 3 0 25.93 30.44 1.09 o 2 3 0 241.40 232.81 4.32 o 3 3 0 67.49 61.98 2.59 o 4 3 0 150.52 134.81 3.43 o 5 3 0 445.02 443.92 10.79 o 6 3 0 21.01 20.68 2.66 o -9 4 0 247.89 266.93 9.65 o -8 4 0 446.20 459.08 11.40 o -7 4 0 33.94 35.62 2.22 o -6 4 0 120.20 122.60 3.34 o -5 4 0 602.80 599.54 13.16 o -4 4 0 213.31 186.19 4.79 o -3 4 0 269.71 259.26 4.41 o -2 4 0 1221.43 1293.04 24.27 o -1 4 0 339.28 332.35 5.86 o 0 4 0 55.33 43.98 1.60 o 1 4 0 24.45 28.84 1.43 o 2 4 0 509.26 514.02 10.25 o 3 4 0 297.34 289.28 6.21 o 4 4 0 2.18 2.89 1.93 o 5 4 0 725.30 700.22 16.47 o 6 4 0 79.66 81.61 5.34 o -9 5 0 96.15 95.89 8.73 o -8 5 0 52.43 52.27 3.12 o -7 5 0 62.20 69.69 2.52 o -6 5 0 199.38 210.23 5.78 o -5 5 0 3.23 1.17 1.11 o -4 5 0 495.25 510.79 11.90 o -3 5 0 380.80 388.06 9.23 o -2 5 0 379.13 374.31 13.04 o -1 5 0 886.04 893.32 30.32 o 0 5 0 176.18 174.46 4.57 o 1 5 0 914.34 903.17 23.49 o 2 5 0 219.06 229.22 5.90 o 3 5 0 181.14 177.23 4.98 o 4 5 0 65.24 64.29 3.04 o 5 5 0 54.23 54.68 3.41 o -9 6 0 2.60 3.63 3.55 o -8 6 0 63.30 59.47 4.46 o -7 6 0 8.92 10.02 2.30 o -6 6 0 277.47 264.98 7.16 o -5 6 0 54.38 59.03 2.77 o -4 6 0 14.81 18.70 1.92 o -3 6 0 348.97 358.30 8.71 o -2 6 0 9.07 16.17 2.88 o -1 6 0 286.53 298.68 7.10 o 0 6 0 60.14 61.00 2.19 o 1 6 0 665.29 667.49 17.93 o 2 6 0 518.22 505.46 11.85 o 3 6 0 125.50 129.20 5.64 o 4 6 0 175.70 174.49 5.75 o -8 7 0 24.59 20.64 2.20 o -7 7 0 54.62 58.57 3.28 o -6 7 0 127.99 118.50 4.20 o -5 7 0 364.24 381.07 9.70 o -4 7 0 98.60 104.66 3.79 o -3 7 0 968.24 940.94 24.65 o -2 7 0 30.76 26.79 2.34 o -1 7 0 9.32 11.86 1.17 o 0 7 0 373.45 360.82 10.51 o 1 7 0 0.83 1.87 2.27 o 2 7 0 100.67 108.56 4.98 o 3 7 0 34.24 35.73 3.66 o -8 8 0 0.87 1.91 3.11 o -7 8 0 82.80 76.08 4.04 o -6 8 0 125.18 125.16 4.67 o -5 8 0 111.91 110.20 4.03 o -4 8 0 111.79 114.65 4.79 o -3 8 0 363.72 368.48 10.87 o -2 8 0 121.65 113.26 4.67 o -1 8 0 37.09 44.43 6.25 o 0 8 0 201.55 198.59 6.99 o 1 8 0 41.67 44.96 3.93 o 2 8 0 29.39 28.53 3.69 o -7 9 0 144.88 128.61 6.61 o -6 9 0 107.56 105.84 5.59 o -5 9 0 104.69 99.66 5.94 o -4 9 0 178.97 168.29 6.44 o -3 9 0 6.10 3.70 3.71 o -2 9 0 54.62 52.57 3.46 o -1 9 0 165.20 168.81 6.50 o 0 9 0 23.67 21.29 2.77 o -5 10 0 72.26 65.56 4.78 o -4 10 0 10.45 8.06 3.76 o -3 10 0 44.46 37.97 8.08 o -2 10 0 40.65 40.26 4.04 o 2 -10 1 7.13 7.26 3.88 o 3 -10 1 55.89 48.35 4.43 o 4 -10 1 31.84 24.67 4.87 o 5 -10 1 1.79 2.73 3.66 o 0 -9 1 76.81 80.67 4.14 o 1 -9 1 131.44 125.92 6.89 o 2 -9 1 40.42 44.29 3.00 o 3 -9 1 35.54 33.64 3.32 o 4 -9 1 0.92 -1.39 2.63 o 5 -9 1 4.07 3.13 3.07 o 6 -9 1 14.52 15.51 2.48 o 7 -9 1 12.61 9.76 3.28 o -2 -8 1 1.46 0.00 3.39 o -1 -8 1 91.33 95.17 4.54 o 0 -8 1 173.57 162.01 6.09 o 1 -8 1 2.24 3.43 2.37 o 2 -8 1 234.64 245.83 6.40 o 3 -8 1 494.30 458.70 13.07 o 4 -8 1 2.04 1.99 2.43 o 5 -8 1 152.21 144.65 8.84 o 6 -8 1 177.65 170.01 6.75 o 7 -8 1 52.86 53.71 3.83 o 8 -8 1 60.20 51.12 4.96 o -3 -7 1 100.92 100.87 4.45 o -2 -7 1 10.99 9.34 2.53 o -1 -7 1 125.33 132.20 7.48 o 0 -7 1 82.28 82.93 2.84 o 1 -7 1 10.87 13.86 1.46 o 2 -7 1 56.53 59.94 3.22 o 3 -7 1 240.76 247.25 7.53 o 4 -7 1 217.43 229.56 6.37 o 5 -7 1 403.50 410.02 10.23 o 6 -7 1 663.42 633.58 15.13 o 7 -7 1 198.70 220.74 6.66 o 8 -7 1 165.24 153.67 8.41 o -4 -6 1 6.34 1.96 2.52 o -3 -6 1 55.96 53.68 3.41 o -2 -6 1 238.02 241.51 8.00 o -1 -6 1 418.11 430.43 10.01 o 0 -6 1 190.38 196.10 5.05 o 1 -6 1 129.68 130.44 3.68 o 2 -6 1 153.39 154.32 5.13 o 3 -6 1 64.77 75.62 3.96 o 4 -6 1 153.07 160.21 4.64 o 5 -6 1 104.31 112.84 3.94 o 6 -6 1 711.21 711.03 16.63 o 7 -6 1 80.48 89.45 3.83 o 8 -6 1 23.81 26.97 3.16 o -5 -5 1 28.08 27.70 3.47 o -4 -5 1 63.47 62.08 3.07 o -3 -5 1 172.48 179.26 4.89 o -2 -5 1 139.20 149.56 4.06 o -1 -5 1 41.78 41.15 1.81 o 0 -5 1 878.24 920.25 19.09 o 1 -5 1 165.35 153.05 6.29 o 2 -5 1 376.68 435.55 10.23 o 3 -5 1 126.18 111.23 3.32 o 4 -5 1 348.39 374.71 9.98 o 5 -5 1 204.27 210.96 6.68 o 6 -5 1 46.43 54.18 3.18 o 7 -5 1 72.79 71.87 3.87 o 8 -5 1 12.74 15.30 2.50 o -6 -4 1 189.99 186.41 7.46 o -5 -4 1 206.18 203.53 5.83 o -4 -4 1 11.56 10.32 1.76 o -3 -4 1 728.74 755.88 16.60 o -2 -4 1 840.57 814.22 15.27 o -1 -4 1 64.06 62.25 1.79 o 0 -4 1 584.07 584.51 9.82 o 1 -4 1 219.17 209.16 3.87 o 2 -4 1 1158.73 1234.02 21.72 o 3 -4 1 1.09 0.94 0.76 o 4 -4 1 178.08 189.35 4.97 o 5 -4 1 603.94 588.96 13.66 o 6 -4 1 76.70 71.74 4.09 o 7 -4 1 25.11 18.56 1.68 o 8 -4 1 85.93 95.75 5.62 o -7 -3 1 38.01 34.76 4.02 o -6 -3 1 31.34 28.81 2.85 o -5 -3 1 235.59 254.69 6.69 o -4 -3 1 480.34 446.48 12.51 o -3 -3 1 693.18 696.99 13.11 o -2 -3 1 974.69 921.48 14.14 o -1 -3 1 213.31 214.16 3.52 o 0 -3 1 794.72 786.38 12.99 o 1 -3 1 524.62 544.86 8.54 o 2 -3 1 1741.25 1754.35 32.51 o 3 -3 1 650.60 645.62 10.80 o 4 -3 1 804.97 776.05 13.58 o 5 -3 1 351.52 364.98 8.81 o 6 -3 1 14.57 11.46 1.36 o 7 -3 1 55.18 61.37 2.78 o 8 -3 1 50.48 51.73 3.28 o -7 -2 1 123.37 121.10 5.64 o -6 -2 1 72.99 73.69 3.04 o -5 -2 1 287.85 266.69 9.82 o -4 -2 1 833.99 845.54 18.69 o -3 -2 1 712.97 697.90 10.20 o -2 -2 1 626.21 617.34 10.24 o -1 -2 1 164.24 177.24 2.87 o 0 -2 1 132.34 140.96 2.74 o 1 -2 1 98.70 101.85 1.79 o 2 -2 1 85.60 82.08 1.61 o 3 -2 1 814.09 835.53 14.44 o 4 -2 1 861.26 864.17 14.95 o 5 -2 1 788.55 768.79 24.53 o 6 -2 1 112.26 114.83 3.84 o 7 -2 1 198.20 213.42 6.18 o 8 -2 1 201.21 208.97 6.31 o -8 -1 1 139.52 124.95 5.75 o -7 -1 1 2.77 4.49 2.58 o -6 -1 1 61.73 68.19 2.68 o -5 -1 1 85.90 67.86 2.22 o -4 -1 1 643.84 643.56 9.66 o -3 -1 1 214.24 201.99 2.96 o -2 -1 1 3.25 3.70 0.34 o -1 -1 1 750.63 691.99 9.77 o 0 -1 1 904.64 873.23 46.73 o 1 -1 1 852.89 848.32 13.00 o 2 -1 1 230.22 230.61 3.81 o 3 -1 1 717.63 697.37 10.98 o 4 -1 1 54.56 63.20 1.88 o 5 -1 1 278.52 296.91 7.45 o 6 -1 1 153.10 159.01 4.78 o 7 -1 1 466.05 454.05 11.13 o 8 -1 1 159.65 180.41 6.07 o -8 0 1 207.83 198.73 8.62 o -7 0 1 86.63 93.51 3.51 o -6 0 1 259.82 257.71 8.04 o -5 0 1 5.13 6.83 1.31 o -4 0 1 178.03 160.55 2.50 o -3 0 1 2.91 3.31 0.53 o -2 0 1 1700.22 1719.53 23.12 o -1 0 1 1309.29 1053.71 33.55 o 1 0 1 1074.38 1004.07 13.66 o 2 0 1 951.92 929.87 13.42 o 3 0 1 680.89 693.11 12.22 o 4 0 1 67.43 50.56 1.85 o 5 0 1 37.66 43.64 2.29 o 6 0 1 25.45 25.78 2.29 o 7 0 1 304.36 295.66 8.05 o 8 0 1 45.43 45.32 4.31 o -8 1 1 93.60 105.41 4.74 o -7 1 1 142.21 142.15 5.62 o -6 1 1 669.94 650.17 13.82 o -5 1 1 645.76 658.39 11.48 o -4 1 1 224.45 199.41 3.41 o -3 1 1 1.80 1.93 0.43 o -2 1 1 117.70 100.12 1.59 o -1 1 1 1252.20 1316.50 18.62 o 0 1 1 198.14 206.76 3.84 o 1 1 1 2203.56 2144.57 34.89 o 2 1 1 1163.22 1173.74 18.08 o 3 1 1 698.05 727.04 13.92 o 4 1 1 124.20 125.26 3.77 o 5 1 1 58.02 56.97 2.62 o 6 1 1 272.61 278.85 7.39 o 7 1 1 90.22 93.01 4.17 o -9 2 1 14.38 20.03 4.64 o -8 2 1 59.06 64.42 4.14 o -7 2 1 6.26 7.54 1.48 o -6 2 1 411.67 408.97 9.25 o -5 2 1 530.63 543.63 9.62 o -4 2 1 306.14 297.66 4.59 o -3 2 1 1670.56 1709.78 26.15 o -2 2 1 1261.75 1269.03 19.42 o -1 2 1 3147.98 3182.98 48.41 o 0 2 1 2374.24 2297.79 40.71 o 1 2 1 1940.56 1864.50 33.05 o 2 2 1 529.40 528.04 8.99 o 3 2 1 407.84 382.12 7.04 o 4 2 1 220.97 229.98 6.02 o 5 2 1 60.64 61.30 2.85 o 6 2 1 92.86 101.68 3.72 o 7 2 1 33.48 35.87 4.11 o -9 3 1 119.84 131.96 6.51 o -8 3 1 96.31 113.79 5.03 o -7 3 1 2.35 5.09 1.64 o -6 3 1 759.88 746.67 13.16 o -5 3 1 113.51 114.06 2.68 o -4 3 1 1.86 5.85 0.66 o -3 3 1 1453.10 1524.17 23.47 o -2 3 1 745.42 735.80 11.48 o -1 3 1 2063.28 2100.60 38.75 o 0 3 1 16.39 34.46 1.14 o 1 3 1 649.23 616.16 10.33 o 2 3 1 579.78 594.71 11.70 o 3 3 1 16.74 20.66 1.11 o 4 3 1 410.07 391.34 9.61 o 5 3 1 394.91 385.79 9.77 o 6 3 1 52.58 54.82 3.14 o -9 4 1 70.09 70.35 4.71 o -8 4 1 180.70 178.80 11.17 o -7 4 1 95.22 105.41 3.13 o -6 4 1 93.07 92.91 2.99 o -5 4 1 228.30 239.13 5.30 o -4 4 1 107.23 97.32 2.71 o -3 4 1 897.96 947.06 14.81 o -2 4 1 529.47 529.06 8.48 o -1 4 1 1208.29 1254.56 23.37 o 0 4 1 1.07 3.02 0.88 o 1 4 1 1.22 -0.67 1.28 o 2 4 1 67.13 58.61 1.86 o 3 4 1 122.87 110.22 3.04 o 4 4 1 155.21 151.91 4.73 o 5 4 1 88.97 88.35 3.67 o -9 5 1 120.26 124.07 13.80 o -8 5 1 124.62 121.49 6.27 o -7 5 1 570.72 569.02 11.84 o -6 5 1 9.23 9.43 2.44 o -5 5 1 50.09 54.65 2.26 o -4 5 1 26.59 33.69 1.66 o -3 5 1 290.59 287.68 8.66 o -2 5 1 307.85 310.40 7.49 o -1 5 1 58.98 54.64 2.15 o 0 5 1 352.31 349.81 9.77 o 1 5 1 134.96 130.30 4.61 o 2 5 1 82.54 85.02 3.08 o 3 5 1 3.20 2.81 1.75 o 4 5 1 118.92 112.69 4.75 o 5 5 1 29.01 29.31 3.50 o -9 6 1 245.06 240.25 21.34 o -8 6 1 151.37 157.66 9.73 o -7 6 1 376.87 353.66 7.96 o -6 6 1 221.19 231.61 6.42 o -5 6 1 118.54 125.58 3.96 o -4 6 1 472.50 489.24 11.62 o -3 6 1 86.72 90.02 3.63 o -2 6 1 5.20 7.19 1.82 o -1 6 1 60.35 56.66 2.87 o 0 6 1 112.70 117.43 4.23 o 1 6 1 23.39 23.44 2.43 o 2 6 1 310.26 299.85 7.75 o 3 6 1 243.20 244.59 6.79 o 4 6 1 120.26 109.81 4.76 o -8 7 1 5.49 6.05 2.73 o -7 7 1 63.32 62.48 3.38 o -6 7 1 121.63 122.61 4.27 o -5 7 1 11.45 10.45 1.60 o -4 7 1 883.74 908.51 20.78 o -3 7 1 389.26 403.45 11.55 o -2 7 1 1.60 -0.45 1.92 o -1 7 1 207.90 208.52 6.85 o 0 7 1 140.34 149.09 9.09 o 1 7 1 42.93 49.15 3.47 o 2 7 1 93.24 91.20 9.77 o 3 7 1 140.45 139.28 6.15 o -8 8 1 1.76 7.75 3.15 o -7 8 1 2.79 7.15 3.39 o -6 8 1 11.57 9.59 2.41 o -5 8 1 45.75 44.73 2.86 o -4 8 1 122.36 123.28 5.02 o -3 8 1 69.22 76.37 7.98 o -2 8 1 169.16 168.05 5.86 o -1 8 1 79.62 69.81 3.52 o 0 8 1 82.41 84.07 4.35 o 1 8 1 122.61 121.01 12.12 o -7 9 1 22.11 21.70 4.41 o -6 9 1 37.45 32.60 2.79 o -5 9 1 116.76 100.73 6.85 o -4 9 1 139.19 135.02 8.36 o -3 9 1 8.15 3.96 2.04 o -2 9 1 145.80 149.72 5.75 o -1 9 1 40.05 34.46 4.29 o 0 9 1 66.91 65.96 4.55 o -4 10 1 61.85 62.54 8.34 o 2 -10 2 25.41 25.25 3.12 o 3 -10 2 192.75 163.41 7.01 o 4 -10 2 80.22 70.20 4.86 o 5 -10 2 42.57 42.79 3.67 o -1 -9 2 112.80 108.76 5.53 o 0 -9 2 27.26 33.12 3.66 o 1 -9 2 133.79 128.63 5.52 o 2 -9 2 403.13 377.16 11.43 o 3 -9 2 63.82 64.02 4.04 o 4 -9 2 33.91 26.29 3.22 o 5 -9 2 21.88 12.58 4.87 o 6 -9 2 13.85 11.35 3.56 o -2 -8 2 5.19 3.67 3.01 o -1 -8 2 156.52 164.24 6.13 o 0 -8 2 15.71 18.37 2.88 o 1 -8 2 2.65 1.96 1.72 o 2 -8 2 692.84 668.14 18.16 o 3 -8 2 26.90 25.79 3.85 o 4 -8 2 95.38 100.42 4.44 o 5 -8 2 20.96 16.06 1.94 o 6 -8 2 21.94 25.64 2.61 o 7 -8 2 66.82 73.31 4.14 o -3 -7 2 167.72 164.79 8.93 o -2 -7 2 226.96 231.24 7.35 o -1 -7 2 14.31 18.01 2.68 o 0 -7 2 204.41 204.01 5.53 o 1 -7 2 1.73 1.90 1.25 o 2 -7 2 148.39 150.04 5.22 o 3 -7 2 0.84 2.61 2.07 o 4 -7 2 0.84 2.46 1.82 o 5 -7 2 239.22 222.39 6.27 o 6 -7 2 42.01 41.26 2.56 o 7 -7 2 161.58 163.55 5.28 o 8 -7 2 27.31 26.96 3.50 o -5 -6 2 17.27 21.01 4.04 o -4 -6 2 33.90 39.82 4.62 o -3 -6 2 35.75 37.05 2.56 o -2 -6 2 275.01 277.40 6.84 o -1 -6 2 175.20 181.03 4.82 o 0 -6 2 557.77 590.69 18.97 o 1 -6 2 177.12 186.27 5.87 o 2 -6 2 135.14 127.62 4.56 o 3 -6 2 206.26 216.46 5.84 o 4 -6 2 8.31 6.92 1.42 o 5 -6 2 367.57 376.25 9.45 o 6 -6 2 254.10 256.20 7.06 o 7 -6 2 170.05 165.14 5.63 o 8 -6 2 123.13 114.58 10.24 o -5 -5 2 22.92 23.70 2.76 o -4 -5 2 28.27 31.96 3.97 o -3 -5 2 181.36 184.34 5.96 o -2 -5 2 3.11 3.23 0.88 o -1 -5 2 225.41 213.09 4.55 o 0 -5 2 370.76 386.67 7.59 o 1 -5 2 848.68 896.46 18.81 o 2 -5 2 115.52 111.32 3.02 o 3 -5 2 64.45 57.45 2.26 o 4 -5 2 864.35 880.95 19.95 o 5 -5 2 377.70 373.89 9.20 o 6 -5 2 189.30 187.82 5.37 o 7 -5 2 590.54 624.85 14.80 o 8 -5 2 165.00 165.09 5.61 o -6 -4 2 135.04 133.34 5.78 o -5 -4 2 11.37 12.26 2.48 o -4 -4 2 1.02 0.88 1.10 o -3 -4 2 176.56 169.78 6.53 o -2 -4 2 91.68 96.22 2.90 o -1 -4 2 204.77 198.10 4.12 o 0 -4 2 292.54 306.08 5.00 o 1 -4 2 636.98 631.10 12.38 o 2 -4 2 466.93 459.84 7.44 o 3 -4 2 4.93 2.82 0.93 o 4 -4 2 818.32 835.17 18.87 o 5 -4 2 354.89 362.34 8.78 o 6 -4 2 2.56 1.28 1.46 o 7 -4 2 341.28 355.79 9.23 o 8 -4 2 12.65 11.30 2.44 o -7 -3 2 39.99 45.55 3.82 o -6 -3 2 0.65 0.66 2.43 o -5 -3 2 38.03 43.70 2.12 o -4 -3 2 162.71 151.94 3.58 o -3 -3 2 73.28 72.45 1.93 o -2 -3 2 290.32 283.19 4.58 o -1 -3 2 43.34 42.54 1.12 o 0 -3 2 769.49 757.38 13.67 o 1 -3 2 168.62 159.63 2.79 o 2 -3 2 44.35 35.84 1.29 o 3 -3 2 1737.12 1682.30 30.87 o 4 -3 2 480.63 474.77 11.09 o 5 -3 2 364.66 372.13 9.12 o 6 -3 2 1.09 0.86 0.84 o 7 -3 2 32.07 38.85 2.68 o 8 -3 2 4.97 4.27 2.54 o -7 -2 2 1.10 1.43 2.72 o -6 -2 2 169.91 164.51 6.01 o -5 -2 2 66.25 69.11 3.37 o -4 -2 2 1206.66 1181.51 23.76 o -3 -2 2 911.15 922.73 14.06 o -2 -2 2 1093.88 1091.66 15.46 o -1 -2 2 2536.03 2638.02 50.90 o 0 -2 2 208.95 269.32 4.29 o 1 -2 2 333.05 327.94 5.26 o 2 -2 2 1.71 6.90 0.83 o 3 -2 2 425.18 435.92 7.08 o 4 -2 2 303.12 298.79 7.32 o 5 -2 2 317.97 323.18 8.03 o 6 -2 2 155.01 165.31 5.01 o 7 -2 2 0.79 0.31 3.21 o 8 -2 2 117.97 119.28 4.79 o -8 -1 2 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