#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/31/2203148.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2203148_Fobs
loop_
_publ_author_name
'Cati, Dilovan S.'
'Stoeckli-Evans, Helen'
_publ_section_title
;
 A macrocyclic binuclear copper(II) complex of the ligand
 <i>N,N</i>'-bis(pyridin-2-ylmethyl)pyrazine-2,3-dicarboxamide
;
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m177
_journal_page_last               m179
_journal_volume                  60
_journal_year                    2004
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                90.953
_cell_angle_beta                 100.442
_cell_angle_gamma                116.190
_cell_length_a                   8.9507
_cell_length_b                   10.0094
_cell_length_c                   13.9732
_exptl_crystal_F_000             578.00
_reflns_d_resolution_high        0.8135
_[local]_cod_data_source_file    bt6391Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '  DCII-CUSO4   CATI-13   IPDS -120DEGC'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            178.88
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 6135.68 5615.84 187.40 o
2 0 0 290.76 280.29 60.44 o
3 0 0 5636.51 5759.64 145.67 o
4 0 0 700.14 652.79 43.63 o
5 0 0 79.46 74.35 38.63 o
6 0 0 40.12 47.59 38.98 o
7 0 0 2221.33 2212.17 73.32 o
8 0 0 330.15 321.33 65.45 o
9 0 0 124.02 119.16 94.68 o
-9 1 0 638.99 681.03 81.85 o
-8 1 0 677.08 678.49 57.23 o
-7 1 0 83.07 65.76 40.06 o
-6 1 0 74.55 59.78 43.92 o
-5 1 0 2720.73 2742.82 61.16 o
-4 1 0 91.47 58.15 32.54 o
-3 1 0 60.93 52.86 37.18 o
-2 1 0 1958.35 2189.43 71.87 o
-1 1 0 5841.23 5513.70 127.95 o
0 1 0 501.92 488.11 59.73 o
3 1 0 594.14 434.66 64.38 o
4 1 0 148.83 126.45 46.50 o
5 1 0 44.84 40.53 54.00 o
6 1 0 263.59 285.26 67.60 o
-10 2 0 8.14 -12.03 85.31 o
-9 2 0 47.26 51.84 63.62 o
-8 2 0 2484.01 2576.97 68.29 o
-7 2 0 36.31 21.72 40.41 o
-6 2 0 468.15 473.96 43.62 o
-5 2 0 974.29 1076.61 42.90 o
-4 2 0 1631.91 1639.07 46.08 o
-3 2 0 2.21 5.79 36.46 o
-2 2 0 13624.65 15143.17 241.27 o
-1 2 0 400.02 397.14 39.34 o
0 2 0 1298.12 1306.89 70.81 o
-10 3 0 492.29 459.61 67.53 o
-9 3 0 409.07 383.76 54.95 o
-8 3 0 289.85 300.09 52.54 o
-7 3 0 9.30 24.11 38.94 o
-6 3 0 1948.67 1896.92 47.40 o
-5 3 0 384.99 380.70 34.31 o
-4 3 0 7671.79 7826.98 79.36 o
-3 3 0 6997.05 7278.74 142.13 o
-2 3 0 271.22 301.11 42.20 o
-1 3 0 13.55 32.31 41.13 o
0 3 0 4277.32 4674.04 91.55 o
1 3 0 5553.97 5759.54 119.45 o
-10 4 0 562.23 598.20 66.74 o
-9 4 0 67.85 57.66 42.09 o
-8 4 0 10.55 12.28 41.27 o
-7 4 0 3797.91 3802.56 61.80 o
-6 4 0 56.38 58.62 38.61 o
-5 4 0 163.55 170.12 32.17 o
-4 4 0 1685.11 2049.38 110.27 o
-3 4 0 985.37 925.44 34.90 o
-2 4 0 1116.50 1101.53 40.57 o
-1 4 0 5171.90 5254.19 74.39 o
0 4 0 298.82 424.34 39.34 o
1 4 0 76.46 68.99 35.23 o
2 4 0 6399.52 6514.75 156.29 o
-10 5 0 0.43 4.66 50.67 o
-9 5 0 9.26 -5.77 42.01 o
-8 5 0 61.47 10.82 41.49 o
-7 5 0 528.17 549.47 42.45 o
-6 5 0 336.94 406.33 35.23 o
-5 5 0 1390.40 1328.73 37.19 o
-4 5 0 1008.05 906.34 37.91 o
-3 5 0 135.83 170.00 27.32 o
-2 5 0 37.09 40.78 25.97 o
-1 5 0 302.30 312.73 35.40 o
0 5 0 1080.31 1112.90 45.78 o
1 5 0 875.48 934.57 49.22 o
2 5 0 676.99 692.82 66.88 o
-10 6 0 214.81 163.51 51.76 o
-9 6 0 1693.10 1707.08 58.86 o
-8 6 0 2.92 -21.03 35.27 o
-7 6 0 10.49 14.50 27.15 o
-6 6 0 3849.08 3947.46 58.54 o
-5 6 0 254.84 228.25 32.56 o
-4 6 0 742.21 805.79 29.68 o
-3 6 0 3367.35 3370.86 52.88 o
-2 6 0 2676.53 2627.48 49.22 o
-1 6 0 82.46 68.79 31.47 o
0 6 0 117.79 149.29 40.06 o
1 6 0 25.39 19.19 47.57 o
2 6 0 17.83 22.72 47.57 o
-10 7 0 41.68 20.07 44.60 o
-9 7 0 728.33 673.64 60.29 o
-8 7 0 533.51 580.14 52.80 o
-7 7 0 1204.87 1106.65 40.03 o
-6 7 0 116.69 174.64 33.54 o
-5 7 0 563.34 576.86 41.81 o
-4 7 0 14.76 -11.11 32.30 o
-3 7 0 1.67 6.16 31.63 o
-2 7 0 1302.69 1353.68 43.51 o
-1 7 0 1175.25 1158.53 42.78 o
0 7 0 50.57 61.24 39.70 o
1 7 0 280.18 277.48 46.63 o
2 7 0 61.91 45.98 64.34 o
-10 8 0 661.60 600.24 77.41 o
-9 8 0 100.47 72.20 61.32 o
-8 8 0 868.17 874.04 41.01 o
-7 8 0 273.87 327.31 49.94 o
-6 8 0 784.79 708.27 36.63 o
-5 8 0 322.49 338.45 40.75 o
-4 8 0 1229.64 1199.92 45.00 o
-3 8 0 1447.73 1493.13 42.78 o
-2 8 0 94.09 93.78 40.04 o
-1 8 0 58.55 43.63 40.41 o
0 8 0 4.48 8.13 39.70 o
1 8 0 753.49 743.84 62.35 o
2 8 0 405.74 385.20 72.73 o
-10 9 0 0.54 -4.30 61.98 o
-9 9 0 1.52 -9.15 49.32 o
-8 9 0 916.93 983.99 51.20 o
-7 9 0 584.31 596.61 44.24 o
-6 9 0 854.27 854.09 38.94 o
-5 9 0 0.96 -14.15 39.65 o
-4 9 0 61.86 45.51 41.05 o
-3 9 0 445.37 454.68 50.77 o
-2 9 0 17.53 -3.29 50.40 o
-1 9 0 1597.52 1706.33 53.23 o
0 9 0 1414.69 1370.94 61.52 o
1 9 0 114.06 83.31 62.59 o
2 9 0 85.40 101.65 101.93 o
-9 10 0 60.64 48.81 58.98 o
-8 10 0 11.47 -14.70 96.10 o
-7 10 0 2.41 21.94 59.26 o
-6 10 0 525.25 498.14 38.22 o
-5 10 0 878.98 929.47 46.42 o
-4 10 0 74.37 81.67 41.79 o
-3 10 0 11.27 32.46 41.16 o
-2 10 0 109.99 115.92 37.18 o
-1 10 0 3.23 7.01 63.30 o
0 10 0 88.53 90.57 64.73 o
1 10 0 12.69 35.18 93.30 o
-8 11 0 3.52 44.13 51.37 o
-7 11 0 620.79 579.15 63.56 o
-6 11 0 169.03 146.15 86.49 o
-5 11 0 1696.49 1680.33 62.21 o
-4 11 0 433.92 420.90 53.47 o
-3 11 0 420.10 474.85 63.95 o
-2 11 0 1069.26 1018.03 69.68 o
-1 11 0 24.71 28.84 77.59 o
-6 12 0 551.59 461.30 62.63 o
-5 12 0 580.09 542.86 63.04 o
-4 12 0 167.10 133.08 61.53 o
-3 12 0 127.01 139.40 62.29 o
3 -12 1 421.98 439.93 79.31 o
4 -12 1 19.41 41.96 74.95 o
5 -12 1 208.56 177.14 62.68 o
6 -12 1 34.89 52.41 74.23 o
1 -11 1 545.89 583.16 60.35 o
2 -11 1 46.99 26.66 64.37 o
3 -11 1 88.47 67.55 63.23 o
4 -11 1 162.45 89.25 62.51 o
5 -11 1 42.33 3.84 49.75 o
6 -11 1 769.69 737.50 61.71 o
7 -11 1 127.19 114.87 42.76 o
8 -11 1 182.34 129.15 61.74 o
-1 -10 1 129.31 118.30 72.16 o
0 -10 1 11.26 3.70 69.76 o
1 -10 1 702.66 749.06 67.94 o
2 -10 1 26.99 33.62 51.14 o
3 -10 1 581.51 617.54 44.91 o
4 -10 1 348.24 339.84 51.44 o
5 -10 1 212.22 258.32 50.01 o
6 -10 1 64.47 45.28 35.68 o
7 -10 1 143.24 148.64 55.13 o
8 -10 1 916.24 787.44 53.11 o
9 -10 1 309.78 348.32 62.47 o
-2 -9 1 80.28 105.52 90.12 o
-1 -9 1 171.28 227.23 76.16 o
0 -9 1 817.35 857.16 57.58 o
1 -9 1 88.54 79.33 51.86 o
2 -9 1 559.50 607.38 52.92 o
3 -9 1 35.93 32.34 34.96 o
4 -9 1 2552.93 2651.19 55.30 o
5 -9 1 430.68 456.11 42.75 o
6 -9 1 11.77 22.78 49.62 o
7 -9 1 918.62 970.30 40.30 o
8 -9 1 193.17 213.73 43.06 o
9 -9 1 99.65 98.17 49.32 o
10 -9 1 106.80 156.80 77.90 o
-2 -8 1 0.49 -10.24 66.54 o
-1 -8 1 24.33 26.94 60.75 o
0 -8 1 29.24 9.59 40.04 o
1 -8 1 58.25 31.08 40.04 o
2 -8 1 1552.21 1590.81 44.91 o
3 -8 1 291.56 300.83 40.75 o
4 -8 1 69.26 77.17 27.87 o
5 -8 1 80.02 92.63 38.61 o
6 -8 1 463.03 425.48 30.34 o
7 -8 1 582.18 561.91 42.84 o
8 -8 1 170.68 133.02 42.29 o
9 -8 1 715.97 733.80 53.72 o
10 -8 1 747.49 771.07 65.13 o
-2 -7 1 163.86 171.91 62.59 o
-1 -7 1 132.79 139.72 44.48 o
0 -7 1 31.55 43.46 39.70 o
1 -7 1 10.94 8.64 39.32 o
2 -7 1 1249.24 1246.16 42.74 o
3 -7 1 249.36 260.23 33.77 o
4 -7 1 1358.25 1295.00 40.59 o
5 -7 1 4497.14 4654.73 166.92 o
6 -7 1 370.27 365.84 34.06 o
7 -7 1 3.64 0.26 38.86 o
8 -7 1 268.25 213.21 51.05 o
9 -7 1 191.06 156.33 44.28 o
10 -7 1 153.54 208.57 66.16 o
-2 -6 1 26.82 14.71 50.51 o
-1 -6 1 443.70 412.80 47.24 o
0 -6 1 47.81 41.83 39.66 o
1 -6 1 859.75 819.91 40.41 o
2 -6 1 3621.65 3699.86 72.33 o
3 -6 1 647.12 850.52 50.58 o
4 -6 1 504.95 479.57 29.64 o
5 -6 1 34.71 3.31 31.23 o
6 -6 1 838.50 886.18 38.13 o
7 -6 1 942.07 941.53 39.03 o
8 -6 1 1616.23 1743.03 50.46 o
9 -6 1 309.94 252.62 43.01 o
10 -6 1 42.75 76.68 62.75 o
-2 -5 1 605.88 584.05 62.94 o
-1 -5 1 6.99 7.19 33.78 o
0 -5 1 183.61 196.95 33.62 o
1 -5 1 562.81 536.94 32.81 o
2 -5 1 2663.32 2779.22 52.16 o
3 -5 1 5821.45 5875.81 196.76 o
4 -5 1 1585.07 1599.76 43.24 o
5 -5 1 4.45 4.86 24.32 o
6 -5 1 2027.08 2059.13 70.81 o
7 -5 1 534.38 532.97 36.46 o
8 -5 1 366.87 353.29 51.77 o
9 -5 1 37.54 -1.83 41.06 o
10 -5 1 177.65 176.30 64.59 o
-2 -4 1 2067.06 2117.39 82.94 o
-1 -4 1 145.96 161.68 40.70 o
0 -4 1 4398.19 4456.42 76.50 o
1 -4 1 1297.72 1461.25 87.51 o
2 -4 1 396.40 383.99 37.20 o
3 -4 1 915.99 935.88 41.13 o
4 -4 1 634.76 604.20 33.52 o
5 -4 1 9.00 28.85 30.34 o
6 -4 1 383.84 386.06 41.42 o
7 -4 1 774.03 762.02 34.69 o
8 -4 1 358.66 369.95 43.75 o
9 -4 1 614.50 610.20 46.60 o
10 -4 1 61.82 46.64 52.89 o
-2 -3 1 5734.59 5645.47 170.96 o
-1 -3 1 2303.14 2704.09 172.48 o
0 -3 1 246.20 298.52 42.92 o
1 -3 1 863.86 930.77 51.14 o
2 -3 1 1175.78 1138.43 49.68 o
3 -3 1 6197.62 6390.88 77.25 o
4 -3 1 1478.29 1564.67 40.37 o
5 -3 1 3006.11 3026.55 71.32 o
6 -3 1 8.79 -1.99 39.27 o
7 -3 1 11.12 -8.17 32.74 o
8 -3 1 1.72 12.13 42.01 o
9 -3 1 681.78 626.04 62.90 o
10 -3 1 243.77 336.09 79.36 o
-2 -2 1 3531.05 3447.20 134.43 o
-1 -2 1 13020.23 14915.31 261.51 o
0 -2 1 7191.51 7793.86 128.04 o
1 -2 1 1054.83 1039.25 53.72 o
2 -2 1 4972.64 4996.21 84.68 o
3 -2 1 120.56 133.78 30.69 o
4 -2 1 927.69 1111.98 44.67 o
5 -2 1 2987.69 2971.68 57.89 o
6 -2 1 31.68 48.04 39.66 o
7 -2 1 398.75 398.05 32.49 o
8 -2 1 76.60 56.46 51.83 o
9 -2 1 196.28 199.30 70.70 o
10 -2 1 28.31 -5.95 78.68 o
-7 -1 1 441.93 459.97 73.94 o
-6 -1 1 2617.21 2665.28 78.46 o
-5 -1 1 618.10 651.18 62.84 o
-4 -1 1 2298.71 2245.88 84.47 o
-3 -1 1 921.94 943.44 54.58 o
-2 -1 1 1659.70 1735.75 73.96 o
-1 -1 1 613.17 606.31 56.46 o
0 -1 1 315.09 332.90 47.20 o
1 -1 1 3313.49 3287.88 89.28 o
2 -1 1 9.33 8.91 36.11 o
3 -1 1 7.31 24.74 35.36 o
4 -1 1 1282.95 1205.38 47.53 o
5 -1 1 2.27 -1.15 30.73 o
6 -1 1 3.83 2.08 38.94 o
7 -1 1 2009.80 2033.80 62.51 o
8 -1 1 169.42 182.28 52.54 o
9 -1 1 22.11 16.89 76.84 o
-9 0 1 3.09 8.03 73.16 o
-8 0 1 584.47 643.22 77.26 o
-7 0 1 411.44 390.08 53.29 o
-6 0 1 130.58 105.51 40.75 o
-5 0 1 39.67 43.18 38.22 o
-4 0 1 361.21 298.41 37.55 o
-3 0 1 1710.26 1747.05 63.30 o
-2 0 1 2094.84 2297.23 82.97 o
-1 0 1 5597.93 5357.82 138.77 o
1 0 1 795.12 814.20 60.80 o
2 0 1 2067.34 2141.99 82.82 o
3 0 1 1360.13 1247.44 59.01 o
4 0 1 953.36 940.48 47.86 o
5 0 1 39.36 45.09 34.42 o
6 0 1 2417.66 2427.46 70.13 o
7 0 1 39.95 44.07 60.42 o
8 0 1 9.34 -19.93 66.54 o
9 0 1 49.50 37.03 95.49 o
-10 1 1 32.17 43.25 94.42 o
-9 1 1 77.96 54.46 69.01 o
-8 1 1 131.07 97.10 51.86 o
-7 1 1 1018.08 957.58 49.71 o
-6 1 1 1451.53 1442.72 53.26 o
-5 1 1 1922.20 1916.18 77.90 o
-4 1 1 3554.45 3763.56 90.03 o
-3 1 1 2708.64 2758.03 67.94 o
-2 1 1 610.99 579.70 53.65 o
-1 1 1 7426.28 7272.39 133.67 o
0 1 1 59.00 52.08 32.54 o
1 1 1 1621.15 1532.79 95.82 o
2 1 1 82.89 61.61 49.07 o
3 1 1 447.43 490.15 56.84 o
4 1 1 40.33 42.71 40.18 o
5 1 1 24.34 27.80 54.00 o
6 1 1 2053.44 1986.40 97.64 o
-10 2 1 173.89 136.90 86.93 o
-9 2 1 1328.62 1404.98 62.22 o
-8 2 1 135.30 162.37 51.50 o
-7 2 1 65.90 73.26 32.93 o
-6 2 1 82.24 88.56 39.70 o
-5 2 1 3242.26 3273.83 59.01 o
-4 2 1 1006.68 1033.60 39.84 o
-3 2 1 324.04 284.41 34.27 o
-2 2 1 15402.44 16194.93 148.37 o
-1 2 1 471.52 483.26 39.70 o
0 2 1 1740.37 1791.10 72.96 o
1 2 1 2391.14 2380.71 96.50 o
-10 3 1 33.36 81.71 63.23 o
-9 3 1 596.94 587.71 55.07 o
-8 3 1 17.69 -4.51 50.73 o
-7 3 1 1213.62 1212.86 42.52 o
-6 3 1 1335.96 1352.35 40.04 o
-5 3 1 151.88 95.16 31.11 o
-4 3 1 1429.00 1588.86 43.47 o
-3 3 1 3154.40 3304.83 88.52 o
-2 3 1 77.86 48.48 38.61 o
-1 3 1 89.33 105.38 32.93 o
0 3 1 3304.62 3333.18 77.96 o
1 3 1 9.25 9.99 35.00 o
2 3 1 5.53 8.64 60.44 o
-10 4 1 1026.45 972.73 68.18 o
-9 4 1 2.09 20.86 51.44 o
-8 4 1 692.39 680.15 51.14 o
-7 4 1 2.16 -24.63 38.94 o
-6 4 1 612.78 670.90 42.52 o
-5 4 1 162.85 205.50 34.90 o
-4 4 1 4374.99 4416.45 59.70 o
-3 4 1 3862.76 4178.67 62.22 o
-2 4 1 312.08 381.89 36.48 o
-1 4 1 43.78 37.12 26.92 o
0 4 1 2169.21 2348.98 64.24 o
1 4 1 1305.11 1298.36 57.58 o
2 4 1 4810.39 4554.09 107.74 o
-10 5 1 10.37 30.07 50.24 o
-9 5 1 152.39 209.72 51.77 o
-8 5 1 2062.39 2217.21 131.01 o
-7 5 1 20.02 47.66 39.66 o
-6 5 1 1508.20 1556.24 38.94 o
-5 5 1 4699.81 4560.02 55.41 o
-4 5 1 431.45 417.19 26.82 o
-3 5 1 2113.66 2192.06 43.27 o
-2 5 1 16.73 4.18 25.07 o
-1 5 1 2940.43 2832.90 92.56 o
0 5 1 749.53 707.77 41.13 o
1 5 1 2023.30 2148.14 66.10 o
2 5 1 406.88 362.22 61.16 o
-10 6 1 458.81 473.17 64.80 o
-9 6 1 733.26 651.09 54.31 o
-8 6 1 422.98 434.65 51.44 o
-7 6 1 396.80 402.40 40.70 o
-6 6 1 203.44 201.17 31.81 o
-5 6 1 1191.41 1225.51 66.77 o
-4 6 1 95.27 99.80 30.73 o
-3 6 1 1080.65 1067.11 39.32 o
-2 6 1 64.46 45.31 30.73 o
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0 6 1 116.75 145.27 40.41 o
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2 6 1 1553.89 1494.78 76.06 o
-10 7 1 541.02 505.07 64.91 o
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-7 7 1 885.29 970.39 58.67 o
-6 7 1 117.01 118.36 31.56 o
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-1 7 1 407.97 413.99 36.70 o
0 7 1 840.81 819.94 47.20 o
1 7 1 96.88 76.38 49.36 o
2 7 1 22.30 17.23 69.74 o
-10 8 1 2.24 -11.13 65.09 o
-9 8 1 59.92 91.53 51.04 o
-8 8 1 415.06 368.32 42.26 o
-7 8 1 1021.80 1017.30 41.01 o
-6 8 1 5.52 -17.89 31.04 o
-5 8 1 1053.95 1046.98 43.24 o
-4 8 1 2056.02 2120.25 45.94 o
-3 8 1 41.08 46.41 38.61 o
-2 8 1 0.03 32.26 38.98 o
-1 8 1 67.83 43.50 40.06 o
0 8 1 990.63 1071.66 57.93 o
1 8 1 196.21 214.48 62.59 o
2 8 1 497.88 475.70 82.23 o
-10 9 1 137.55 102.38 119.37 o
-9 9 1 60.29 70.80 43.17 o
-8 9 1 273.72 214.79 43.33 o
-7 9 1 81.95 45.19 43.50 o
-6 9 1 30.41 69.17 48.19 o
-5 9 1 827.86 858.41 52.88 o
-4 9 1 642.27 591.89 43.59 o
-3 9 1 107.91 114.89 41.27 o
-2 9 1 398.02 413.23 52.20 o
-1 9 1 771.78 767.32 55.43 o
0 9 1 17.45 42.03 50.77 o
1 9 1 48.41 51.59 76.54 o
2 9 1 55.00 70.25 82.49 o
-9 10 1 143.76 96.14 73.51 o
-8 10 1 469.18 492.12 62.44 o
-7 10 1 91.35 114.13 60.37 o
-6 10 1 1083.97 1004.64 42.13 o
-5 10 1 169.70 167.25 50.77 o
-4 10 1 101.14 88.48 50.40 o
-3 10 1 82.05 70.17 50.40 o
-2 10 1 67.83 46.04 51.44 o
-1 10 1 612.16 599.91 66.16 o
0 10 1 356.99 342.00 67.24 o
1 10 1 303.65 355.59 78.68 o
-8 11 1 13.98 -73.19 73.19 o
-7 11 1 40.88 10.31 43.95 o
-6 11 1 165.56 159.75 50.76 o
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