#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203153.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203153_Fobs loop_ _publ_author_name 'Clegg, William' 'Golding, Bernard T.' 'Harrington, Ross W.' 'Scott, Richard' _publ_section_title ; 1-{2-[4-(2,4-Dinitrophenyl)piperazin-1-yl]ethyl}-4-aza-1-azoniabicyclo[2.2.2]octane chloride ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o291 _journal_page_last o293 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.629 _cell_angle_gamma 90.000 _cell_length_a 6.9664 _cell_length_b 24.3886 _cell_length_c 11.7131 _exptl_crystal_F_000 904.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file bt64033sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' btg64 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 210.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11924.99 11628.03 192.57 o 4 0 0 1511.34 1379.26 28.59 o 6 0 0 3516.05 3509.62 116.65 o 8 0 0 131.04 95.09 64.96 o 2 1 0 8.59 9.40 3.42 o 3 1 0 697.98 598.46 10.48 o 4 1 0 860.23 882.37 25.55 o 5 1 0 5.45 7.02 13.58 o 6 1 0 206.51 202.49 27.79 o 7 1 0 939.97 897.52 39.52 o 8 1 0 122.36 166.93 52.57 o 2 2 0 4460.81 4542.02 71.88 o 3 2 0 1586.89 1746.58 45.61 o 4 2 0 1933.75 1905.47 32.93 o 5 2 0 442.72 451.15 14.55 o 6 2 0 314.03 285.65 25.72 o 7 2 0 112.80 88.48 35.90 o 8 2 0 35.79 91.57 41.96 o 2 3 0 573.61 533.09 8.57 o 3 3 0 356.51 368.85 10.88 o 4 3 0 437.87 475.03 13.21 o 5 3 0 300.26 306.23 12.27 o 6 3 0 67.52 81.56 14.84 o 7 3 0 73.71 81.09 30.11 o 8 3 0 17.01 74.85 50.40 o 2 4 0 1074.28 1098.57 16.57 o 3 4 0 63.81 64.48 5.74 o 4 4 0 25.04 31.25 11.67 o 5 4 0 325.98 356.13 13.89 o 6 4 0 1461.71 1497.22 34.31 o 7 4 0 45.81 91.65 21.15 o 8 4 0 0.06 8.57 43.87 o 1 5 0 889.10 879.31 15.52 o 2 5 0 709.63 662.07 9.75 o 3 5 0 1799.04 1705.70 22.41 o 4 5 0 611.57 670.80 17.23 o 5 5 0 12.95 12.40 13.24 o 6 5 0 1155.88 1120.77 35.10 o 7 5 0 377.78 393.17 31.80 o 8 5 0 0.03 0.97 50.10 o 0 6 0 2940.35 2028.70 93.33 o 1 6 0 7262.90 6993.20 56.99 o 2 6 0 256.66 250.72 6.72 o 3 6 0 4256.77 4384.10 51.37 o 4 6 0 561.71 568.13 16.87 o 5 6 0 165.55 176.50 14.80 o 6 6 0 1124.71 1069.85 34.36 o 7 6 0 163.08 161.51 24.85 o 8 6 0 58.49 93.51 56.88 o 1 7 0 5126.57 4979.30 40.53 o 2 7 0 3.67 -5.14 5.49 o 3 7 0 9158.42 9544.14 96.87 o 4 7 0 45.42 31.73 8.20 o 5 7 0 201.54 184.47 16.21 o 6 7 0 277.93 271.06 24.84 o 7 7 0 20.56 33.07 39.43 o 0 8 0 2208.66 2230.19 28.74 o 1 8 0 80.65 76.65 6.62 o 2 8 0 310.08 257.07 7.14 o 3 8 0 66.53 70.74 7.30 o 4 8 0 828.88 815.27 15.55 o 5 8 0 0.08 7.80 15.96 o 6 8 0 5.00 6.27 24.69 o 7 8 0 835.57 826.62 37.25 o 1 9 0 261.96 245.87 8.64 o 2 9 0 537.63 586.49 10.04 o 3 9 0 319.11 313.02 8.68 o 4 9 0 185.14 174.23 10.19 o 5 9 0 321.49 330.86 20.05 o 6 9 0 95.58 113.15 25.64 o 7 9 0 7.26 -8.34 26.17 o 0 10 0 1354.54 1345.92 21.41 o 1 10 0 494.57 472.42 8.34 o 2 10 0 59.33 47.84 6.46 o 3 10 0 52.06 51.46 7.09 o 4 10 0 1438.27 1411.96 22.85 o 5 10 0 6.76 18.64 8.75 o 6 10 0 34.23 24.40 23.96 o 7 10 0 85.50 33.87 39.77 o 1 11 0 2994.05 3010.88 27.37 o 2 11 0 30.45 21.72 7.48 o 3 11 0 67.89 88.70 8.11 o 4 11 0 9.53 -1.10 10.06 o 5 11 0 564.67 515.64 20.07 o 6 11 0 696.07 649.86 35.04 o 7 11 0 317.22 327.80 49.33 o 0 12 0 2815.68 3164.17 52.19 o 1 12 0 8.05 2.05 6.79 o 2 12 0 970.76 935.58 14.02 o 3 12 0 266.71 266.96 10.51 o 4 12 0 434.19 423.73 12.74 o 5 12 0 112.39 128.71 14.26 o 6 12 0 98.23 107.23 34.86 o 7 12 0 120.75 124.02 33.69 o 1 13 0 3661.57 3644.80 32.98 o 2 13 0 252.11 262.85 9.99 o 3 13 0 2909.98 2917.64 36.03 o 4 13 0 220.60 229.60 13.26 o 5 13 0 394.65 414.76 21.31 o 6 13 0 23.17 25.30 31.01 o 7 13 0 82.48 135.86 36.37 o 0 14 0 338.59 387.32 13.91 o 1 14 0 495.25 561.23 11.11 o 2 14 0 43.22 68.85 10.93 o 3 14 0 2094.67 2041.06 29.87 o 4 14 0 522.06 494.05 16.16 o 5 14 0 267.51 247.14 21.07 o 6 14 0 143.25 145.32 21.96 o 7 14 0 410.31 452.65 51.14 o 1 15 0 227.65 201.54 10.52 o 2 15 0 1.63 11.35 12.80 o 3 15 0 18.96 24.26 12.14 o 4 15 0 1249.10 1226.88 24.41 o 5 15 0 7.64 7.39 23.06 o 6 15 0 37.81 66.34 26.29 o 7 15 0 566.76 575.17 53.36 o 0 16 0 694.74 658.69 20.27 o 1 16 0 1075.91 1095.15 18.59 o 2 16 0 0.87 16.44 12.21 o 3 16 0 46.29 55.38 14.70 o 4 16 0 20.16 34.09 14.05 o 5 16 0 0.33 13.11 21.63 o 6 16 0 36.20 57.33 24.15 o 1 17 0 82.10 110.73 11.84 o 2 17 0 19.13 22.01 13.18 o 3 17 0 1597.63 1545.66 28.23 o 4 17 0 0.34 19.10 20.63 o 5 17 0 384.32 351.22 26.83 o 6 17 0 1.08 65.12 44.97 o 0 18 0 1090.37 1072.27 29.70 o 1 18 0 598.93 583.66 15.64 o 2 18 0 23.59 28.32 14.15 o 3 18 0 46.53 34.25 15.55 o 4 18 0 1397.55 1390.57 36.98 o 5 18 0 116.32 135.24 29.43 o 6 18 0 21.74 53.77 28.50 o 1 19 0 13.48 31.22 17.65 o 2 19 0 397.10 431.93 21.99 o 3 19 0 2271.68 2184.36 40.85 o 4 19 0 11.30 4.51 23.73 o 5 19 0 38.70 96.38 28.27 o 6 19 0 226.66 264.53 43.51 o 0 20 0 425.74 368.83 22.63 o 1 20 0 392.79 400.20 18.68 o 2 20 0 1090.04 1057.91 26.84 o 3 20 0 49.26 40.76 25.24 o 4 20 0 62.99 66.48 25.28 o 5 20 0 274.34 232.61 29.49 o 1 21 0 457.52 439.59 19.04 o 2 21 0 120.46 140.00 22.21 o 3 21 0 50.23 67.08 25.17 o 4 21 0 63.14 46.21 29.81 o 5 21 0 153.08 191.37 37.08 o 0 22 0 178.46 161.58 22.17 o 1 22 0 144.68 154.77 19.64 o 2 22 0 52.83 30.83 20.55 o 3 22 0 36.20 44.06 25.31 o 4 22 0 9.43 13.64 28.85 o 5 22 0 154.41 194.80 40.64 o 1 23 0 279.02 283.87 20.03 o 2 23 0 2.18 37.40 21.41 o 3 23 0 823.18 804.33 33.80 o 4 23 0 312.69 412.03 48.33 o 5 23 0 0.32 34.48 36.48 o 0 24 0 457.76 458.84 30.90 o 1 24 0 224.18 224.23 20.58 o 2 24 0 209.77 214.17 27.06 o 3 24 0 61.66 51.22 31.53 o 4 24 0 105.85 60.63 32.99 o 1 25 0 559.48 548.99 25.13 o 2 25 0 1.46 -10.89 26.65 o 3 25 0 351.78 352.89 36.58 o 4 25 0 105.54 111.80 35.27 o 0 26 0 210.20 219.44 33.12 o 1 26 0 163.60 152.67 23.19 o 2 26 0 27.77 -0.17 27.65 o 3 26 0 2.85 83.18 36.27 o 1 27 0 281.19 378.17 36.81 o 2 27 0 557.62 570.93 36.01 o 0 28 0 162.88 144.16 42.63 o 1 28 0 0.63 -23.03 26.36 o 2 28 0 1.36 -6.26 39.57 o -7 0 1 1724.45 1713.55 64.27 o -5 0 1 2151.01 2117.13 44.09 o -3 0 1 2278.37 2379.85 43.97 o 3 0 1 995.48 1046.72 67.13 o 5 0 1 1633.01 1675.98 109.24 o 7 0 1 134.41 239.87 53.70 o -8 1 1 105.85 74.90 51.73 o -7 1 1 50.19 30.02 28.31 o -6 1 1 11.04 21.95 11.68 o -5 1 1 493.34 509.29 13.49 o -4 1 1 258.96 269.79 8.14 o -3 1 1 2306.13 2476.73 41.47 o -2 1 1 6153.41 5891.98 106.19 o 2 1 1 145.09 142.32 12.27 o 3 1 1 172.51 218.33 7.58 o 4 1 1 195.19 210.81 19.54 o 5 1 1 2.06 -1.81 21.37 o 6 1 1 748.96 710.01 37.10 o 7 1 1 96.10 130.88 30.87 o 8 1 1 26.51 48.66 32.98 o -8 2 1 62.54 52.58 42.75 o -7 2 1 11.56 10.84 18.01 o -6 2 1 755.49 716.31 25.66 o -5 2 1 322.43 337.14 9.58 o -4 2 1 1305.11 1335.08 19.55 o -3 2 1 1100.36 1066.33 15.21 o -2 2 1 599.28 594.00 8.95 o 2 2 1 4923.51 4866.07 82.39 o 3 2 1 1088.50 1176.91 25.34 o 4 2 1 905.67 956.86 29.47 o 5 2 1 1630.44 1708.10 59.16 o 6 2 1 16.05 23.83 22.77 o 7 2 1 434.16 501.78 35.25 o 8 2 1 53.64 63.91 37.57 o -8 3 1 65.53 73.52 43.57 o -7 3 1 318.87 283.89 37.14 o -6 3 1 117.26 163.81 23.35 o -5 3 1 38.72 44.32 7.31 o -4 3 1 3170.22 3288.16 41.53 o -3 3 1 2844.43 2844.10 33.82 o -2 3 1 71.92 78.36 7.15 o 2 3 1 252.26 233.59 8.33 o 3 3 1 4697.12 4600.44 60.12 o 4 3 1 10.89 3.71 8.89 o 5 3 1 630.54 639.43 17.50 o 6 3 1 1613.41 1614.54 44.80 o 7 3 1 545.01 594.18 35.90 o 8 3 1 1325.33 1416.36 63.29 o -8 4 1 19.19 20.94 45.99 o -7 4 1 23.82 95.72 28.59 o -6 4 1 511.44 537.90 20.44 o -5 4 1 0.77 -5.92 7.65 o -4 4 1 4.45 2.91 6.67 o -3 4 1 196.95 191.04 6.37 o -2 4 1 7681.22 7220.74 73.05 o 1 4 1 283.30 216.16 11.81 o 2 4 1 691.41 663.29 10.41 o 3 4 1 1677.70 1748.21 27.25 o 4 4 1 3663.51 3630.14 57.60 o 5 4 1 403.20 421.97 15.00 o 6 4 1 4650.80 4785.65 104.92 o 7 4 1 545.85 524.86 35.84 o 8 4 1 300.61 352.72 42.06 o -8 5 1 185.20 262.45 57.96 o -7 5 1 33.48 33.96 21.76 o -6 5 1 94.50 117.76 19.77 o -5 5 1 766.36 742.90 16.20 o -4 5 1 33.76 17.82 6.62 o -3 5 1 2796.17 2882.50 33.47 o -2 5 1 8.28 22.46 5.51 o -1 5 1 1001.89 992.71 11.16 o 1 5 1 2877.17 2742.25 29.29 o 2 5 1 771.93 785.70 11.39 o 3 5 1 1361.07 1362.44 23.26 o 4 5 1 129.64 106.44 9.99 o 5 5 1 1514.83 1506.09 34.45 o 6 5 1 6.33 19.64 17.57 o 7 5 1 99.12 77.96 29.89 o -8 6 1 6.62 63.13 54.11 o -7 6 1 777.25 735.85 33.48 o -6 6 1 48.35 60.47 18.41 o -5 6 1 151.34 151.85 11.52 o -4 6 1 1340.63 1267.65 19.62 o -3 6 1 1373.34 1362.87 18.07 o -2 6 1 2704.12 2749.46 28.65 o -1 6 1 479.67 460.98 7.04 o 0 6 1 431.97 334.86 7.01 o 1 6 1 93.61 130.78 5.58 o 2 6 1 6250.90 6025.41 57.80 o 3 6 1 1569.81 1619.61 20.51 o 4 6 1 49.59 51.32 11.42 o 5 6 1 40.51 34.38 12.81 o 6 6 1 1.53 -15.37 19.86 o 7 6 1 4.23 6.85 22.55 o -8 7 1 1032.25 1125.25 73.93 o -7 7 1 41.36 46.15 28.63 o -6 7 1 2553.40 2447.40 52.58 o -5 7 1 536.04 473.35 12.71 o -4 7 1 2097.44 2143.28 27.74 o -3 7 1 424.67 461.43 9.94 o -2 7 1 1832.02 1797.29 19.98 o -1 7 1 3476.04 3345.50 29.27 o 0 7 1 2305.81 2256.95 20.04 o 1 7 1 1588.53 1565.27 16.36 o 2 7 1 1171.35 1174.00 16.34 o 3 7 1 5.48 22.75 7.19 o 4 7 1 0.16 14.65 12.47 o 5 7 1 363.46 360.01 16.06 o 6 7 1 325.26 276.99 26.86 o 7 7 1 276.90 293.77 26.49 o -7 8 1 28.58 19.78 26.61 o -6 8 1 486.00 453.75 25.75 o -5 8 1 72.63 69.89 10.34 o -4 8 1 340.32 353.02 12.54 o -3 8 1 839.54 821.46 13.07 o -2 8 1 1668.16 1577.23 17.46 o -1 8 1 550.19 507.12 7.98 o 0 8 1 8983.50 8910.01 70.48 o 1 8 1 612.37 625.21 9.50 o 2 8 1 1278.40 1429.90 16.51 o 3 8 1 923.28 970.56 15.03 o 4 8 1 63.78 83.60 14.64 o 5 8 1 832.82 855.93 24.02 o 6 8 1 85.26 91.39 22.76 o 7 8 1 28.77 -15.56 24.28 o -7 9 1 186.75 175.14 36.18 o -6 9 1 1503.93 1395.99 40.82 o -5 9 1 370.94 353.85 15.59 o -4 9 1 0.01 3.10 8.70 o -3 9 1 43.88 32.78 7.42 o -2 9 1 272.99 313.06 8.21 o -1 9 1 34.71 -0.84 5.27 o 0 9 1 2155.52 2232.26 21.34 o 1 9 1 3734.55 3628.50 32.84 o 2 9 1 24.97 21.41 6.67 o 3 9 1 1829.43 1897.73 24.71 o 4 9 1 246.43 269.00 12.04 o 5 9 1 1542.20 1535.12 35.59 o 6 9 1 566.71 556.92 45.16 o 7 9 1 278.02 336.48 37.95 o -7 10 1 378.97 327.70 35.00 o -6 10 1 230.29 184.96 25.63 o -5 10 1 381.48 370.26 14.52 o -4 10 1 78.54 77.04 9.73 o -3 10 1 68.28 73.57 9.76 o -2 10 1 408.21 395.88 9.30 o -1 10 1 114.63 136.73 6.98 o 0 10 1 751.98 806.18 10.83 o 1 10 1 614.15 640.81 10.16 o 2 10 1 2078.47 2100.12 22.37 o 3 10 1 113.20 141.11 7.96 o 4 10 1 42.20 24.88 18.09 o 5 10 1 155.32 182.37 18.43 o 6 10 1 1.61 11.76 22.73 o 7 10 1 289.23 280.00 31.88 o -7 11 1 13.95 32.50 31.77 o -6 11 1 111.35 136.19 20.69 o -5 11 1 105.25 110.80 11.32 o -4 11 1 14.70 -6.50 9.71 o -3 11 1 463.55 411.16 10.86 o -2 11 1 53.96 64.21 8.41 o -1 11 1 4117.37 4158.28 36.15 o 0 11 1 599.39 609.24 10.00 o 1 11 1 1554.27 1545.09 17.08 o 2 11 1 528.33 569.91 10.75 o 3 11 1 2220.66 2113.66 25.39 o 4 11 1 607.13 610.02 14.11 o 5 11 1 758.60 789.24 30.75 o 6 11 1 0.04 -41.84 27.90 o 7 11 1 38.27 97.62 33.32 o -7 12 1 137.19 179.98 44.72 o -6 12 1 21.80 6.53 40.47 o -5 12 1 7.72 17.10 12.81 o -4 12 1 1271.04 1225.16 20.12 o -3 12 1 109.22 127.15 10.29 o -2 12 1 6.76 6.14 7.79 o -1 12 1 169.07 162.72 7.48 o 0 12 1 443.67 504.80 9.72 o 1 12 1 63.12 56.29 7.98 o 2 12 1 554.04 524.14 11.58 o 3 12 1 6.33 15.05 9.19 o 4 12 1 0.55 15.01 9.71 o 5 12 1 6.56 -1.51 10.57 o 6 12 1 25.88 -5.29 26.96 o 7 12 1 13.96 23.89 31.39 o -7 13 1 2.32 -24.81 46.27 o -6 13 1 7.95 43.10 23.08 o -5 13 1 415.21 384.89 22.89 o -4 13 1 1248.29 1217.23 29.11 o -3 13 1 2021.02 1990.47 28.21 o -2 13 1 39.98 42.67 8.32 o -1 13 1 2051.32 2185.81 22.73 o 0 13 1 187.03 187.40 7.71 o 1 13 1 1679.41 1695.52 18.43 o 2 13 1 149.50 176.92 9.65 o 3 13 1 1.91 -0.47 10.04 o 4 13 1 160.92 178.29 14.36 o 5 13 1 109.10 87.06 15.64 o 6 13 1 1.56 48.23 42.82 o 7 13 1 333.03 348.49 36.55 o -7 14 1 12.12 87.69 45.63 o -6 14 1 346.64 338.74 33.72 o -5 14 1 79.86 80.55 19.75 o -4 14 1 1051.34 1005.35 22.37 o -3 14 1 269.41 258.87 13.07 o -2 14 1 2557.83 2467.39 29.19 o -1 14 1 867.17 974.29 14.74 o 0 14 1 3212.45 3266.47 30.61 o 1 14 1 339.99 335.10 10.48 o 2 14 1 779.91 780.78 16.23 o 3 14 1 504.85 532.35 15.39 o 4 14 1 768.23 775.60 19.92 o 5 14 1 155.14 142.98 20.01 o 6 14 1 842.47 866.81 43.17 o 7 14 1 83.42 149.66 52.63 o -7 15 1 164.90 203.23 52.18 o -6 15 1 0.56 45.67 35.48 o -5 15 1 186.73 241.82 27.26 o -4 15 1 1065.88 1000.27 24.86 o -3 15 1 80.00 90.96 14.49 o -2 15 1 221.99 223.32 13.02 o -1 15 1 299.08 309.67 10.93 o 0 15 1 532.50 519.51 12.16 o 1 15 1 85.11 97.41 9.26 o 2 15 1 176.81 184.66 11.46 o 3 15 1 1.52 4.52 13.58 o 4 15 1 0.45 18.28 12.81 o 5 15 1 16.16 4.89 25.91 o 6 15 1 163.10 272.13 95.97 o -6 16 1 31.53 47.50 30.70 o -5 16 1 468.71 448.68 26.42 o -4 16 1 2586.01 2545.04 46.66 o -3 16 1 120.49 126.96 13.63 o -2 16 1 1098.67 1094.21 20.26 o -1 16 1 83.96 90.00 10.29 o 0 16 1 113.79 81.04 9.83 o 1 16 1 152.77 169.99 10.48 o 2 16 1 644.88 625.38 18.13 o 3 16 1 447.84 444.15 16.96 o 4 16 1 282.61 290.49 18.95 o 5 16 1 75.41 72.72 28.78 o 6 16 1 18.10 130.76 45.14 o -6 17 1 136.11 144.70 28.30 o -5 17 1 27.59 24.38 23.95 o -4 17 1 2165.96 2129.94 45.47 o -3 17 1 55.57 93.02 15.67 o -2 17 1 685.87 680.46 17.26 o -1 17 1 1869.14 1907.64 26.10 o 0 17 1 55.08 56.70 18.27 o 1 17 1 290.30 299.65 12.67 o 2 17 1 705.08 700.16 19.71 o 3 17 1 561.44 580.95 18.52 o 4 17 1 5.67 17.16 18.05 o 5 17 1 878.79 839.03 31.98 o 6 17 1 85.90 37.03 38.63 o -6 18 1 446.97 419.63 41.64 o -5 18 1 656.68 733.14 32.63 o -4 18 1 42.86 48.94 21.03 o -3 18 1 26.42 0.46 15.47 o -2 18 1 469.67 478.65 16.67 o -1 18 1 1671.71 1732.54 27.85 o 0 18 1 1276.27 1221.43 21.10 o 1 18 1 1867.50 1950.21 26.98 o 2 18 1 24.30 34.38 13.85 o 3 18 1 833.62 851.30 23.64 o 4 18 1 175.50 185.90 22.33 o 5 18 1 0.62 47.07 25.36 o 6 18 1 0.06 -52.28 41.13 o -6 19 1 5.67 -12.00 32.15 o -5 19 1 83.89 68.00 32.28 o -4 19 1 7.32 39.09 20.04 o -3 19 1 99.13 88.30 19.28 o -2 19 1 0.00 -21.13 14.09 o -1 19 1 458.74 440.50 16.88 o 0 19 1 15.68 16.43 11.66 o 1 19 1 486.26 507.44 16.21 o 2 19 1 173.19 191.49 19.90 o 3 19 1 102.70 127.16 23.62 o 4 19 1 1133.65 1097.62 37.70 o 5 19 1 693.10 710.04 33.34 o 6 19 1 12.99 54.01 60.66 o -5 20 1 84.94 66.40 36.93 o -4 20 1 105.25 107.18 26.23 o -3 20 1 2280.06 2334.08 48.37 o -2 20 1 358.99 339.43 20.79 o -1 20 1 909.15 907.04 20.97 o 0 20 1 98.16 120.56 16.39 o 1 20 1 19.74 12.04 12.65 o 2 20 1 955.98 919.33 26.95 o 3 20 1 129.15 98.78 27.05 o 4 20 1 413.58 359.35 29.90 o 5 20 1 0.40 62.36 28.95 o -5 21 1 1267.85 1239.65 43.31 o -4 21 1 175.24 174.60 28.31 o -3 21 1 904.17 902.67 33.46 o -2 21 1 779.14 767.44 27.21 o -1 21 1 246.81 255.14 16.65 o 0 21 1 4.65 20.01 13.88 o 1 21 1 927.71 940.34 23.27 o 2 21 1 585.23 620.24 30.72 o 3 21 1 1872.86 1876.52 44.83 o 4 21 1 469.06 456.37 35.34 o 5 21 1 21.88 -0.84 30.55 o -5 22 1 170.82 200.14 38.94 o -4 22 1 0.29 77.29 30.32 o -3 22 1 93.83 65.88 25.46 o -2 22 1 0.07 32.80 20.98 o -1 22 1 129.41 138.22 21.45 o 0 22 1 258.58 291.61 17.73 o 1 22 1 55.19 58.45 17.33 o 2 22 1 1391.18 1377.69 39.01 o 3 22 1 138.84 156.44 27.32 o 4 22 1 39.18 65.21 36.11 o 5 22 1 0.17 1.23 34.92 o -5 23 1 183.95 217.63 40.93 o -4 23 1 70.11 26.12 30.67 o -3 23 1 70.45 30.26 31.60 o -2 23 1 130.65 112.87 25.84 o -1 23 1 268.85 245.97 19.80 o 0 23 1 114.27 97.94 18.85 o 1 23 1 328.63 352.57 20.01 o 2 23 1 30.06 65.41 30.88 o 3 23 1 68.52 74.90 31.25 o 4 23 1 14.83 -15.72 36.03 o -4 24 1 126.37 191.13 42.39 o -3 24 1 22.43 21.04 38.23 o -2 24 1 24.21 15.35 23.88 o -1 24 1 143.03 120.92 19.25 o 0 24 1 18.62 16.94 18.46 o 1 24 1 11.26 46.19 18.68 o 2 24 1 917.44 952.60 36.88 o 3 24 1 84.57 75.82 35.37 o 4 24 1 317.13 385.97 56.70 o -4 25 1 710.80 735.36 49.62 o -3 25 1 70.77 48.65 29.48 o -2 25 1 466.18 476.51 27.24 o -1 25 1 980.84 969.42 29.01 o 0 25 1 122.28 141.88 21.56 o 1 25 1 1.36 29.03 23.26 o 2 25 1 52.78 23.46 33.37 o 3 25 1 13.94 81.04 33.26 o 4 25 1 13.56 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