#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/31/2203161.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203161_Fobs loop_ _publ_author_name 'Huo, Fangjun' 'Yin, Caixia' 'Guo, Wei' 'Xia, Chizhong' _publ_section_title ; 2-[Hydroxy(2-pyridyl)methyl]-2-cyclopenten-1-one: the Baylis--Hillman adduct of 2-pyridinecarboxaldehyde and 2-cyclopenten-1-one ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o204 _journal_page_last o206 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.4270 _cell_length_b 10.2000 _cell_length_c 11.1630 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.7835 _[local]_cod_data_source_file ci6318Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CI6318R C11 H11 N O2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 106.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2404.82 2469.42 32.59 o 4 0 0 3.90 3.35 0.22 o 6 0 0 308.69 329.86 8.65 o 8 0 0 19.78 21.83 1.47 o 10 0 0 49.20 53.19 2.62 o 1 1 0 81.94 65.48 1.00 o 2 1 0 595.75 602.11 6.88 o 3 1 0 7.34 5.06 0.16 o 4 1 0 185.48 189.56 1.95 o 5 1 0 77.09 74.96 0.94 o 6 1 0 116.83 108.44 1.65 o 7 1 0 18.17 17.55 0.68 o 8 1 0 81.21 83.23 2.20 o 9 1 0 0.70 0.82 0.43 o 10 1 0 0.91 1.02 0.51 o 0 2 0 712.27 739.27 16.26 o 1 2 0 411.03 395.55 4.05 o 2 2 0 1378.83 1387.40 13.99 o 3 2 0 1.26 1.27 0.11 o 4 2 0 2.31 1.97 0.24 o 5 2 0 2.97 4.09 0.20 o 6 2 0 3.40 2.13 0.25 o 7 2 0 21.73 24.80 1.31 o 8 2 0 5.43 3.99 0.47 o 9 2 0 36.31 38.14 1.47 o 10 2 0 2.06 1.47 0.54 o 1 3 0 943.67 916.92 9.26 o 2 3 0 71.19 62.54 0.93 o 3 3 0 9.84 11.61 0.25 o 4 3 0 85.72 89.88 1.04 o 6 3 0 26.19 25.04 1.34 o 7 3 0 34.93 37.58 0.89 o 8 3 0 131.19 126.72 2.40 o 9 3 0 8.76 9.38 1.31 o 10 3 0 1.71 1.64 0.79 o 0 4 0 2506.52 2527.47 54.76 o 1 4 0 189.42 202.47 2.22 o 2 4 0 76.75 79.63 1.01 o 3 4 0 423.46 457.37 5.46 o 4 4 0 23.46 23.72 0.50 o 5 4 0 61.99 69.77 1.09 o 6 4 0 6.72 8.45 0.49 o 7 4 0 1.92 1.47 0.30 o 8 4 0 16.80 17.64 0.99 o 9 4 0 5.75 5.96 0.72 o 10 4 0 0.09 0.60 0.78 o 1 5 0 1428.59 1578.73 15.89 o 2 5 0 45.83 57.31 0.80 o 3 5 0 166.86 179.04 2.18 o 4 5 0 4.31 4.02 0.24 o 5 5 0 149.41 147.47 2.11 o 6 5 0 13.73 13.73 0.67 o 7 5 0 8.28 5.59 0.55 o 8 5 0 51.39 54.46 1.77 o 9 5 0 30.43 35.33 1.47 o 0 6 0 49.57 50.05 1.81 o 1 6 0 30.57 36.01 0.60 o 2 6 0 25.17 20.48 0.44 o 3 6 0 175.54 188.15 2.51 o 4 6 0 0.02 0.12 0.19 o 5 6 0 0.16 0.40 0.57 o 6 6 0 1.05 0.98 0.39 o 7 6 0 1.96 1.19 0.40 o 8 6 0 1.63 0.82 0.83 o 9 6 0 0.34 0.70 0.54 o 1 7 0 36.61 34.97 1.01 o 2 7 0 17.57 17.32 0.51 o 3 7 0 4.77 4.08 0.30 o 4 7 0 20.64 18.32 0.70 o 5 7 0 21.34 23.68 0.84 o 6 7 0 82.01 82.64 1.79 o 7 7 0 0.02 -0.22 0.33 o 8 7 0 0.93 1.32 0.55 o 9 7 0 1.78 1.43 0.60 o 0 8 0 98.97 98.43 3.19 o 1 8 0 41.47 35.02 0.80 o 2 8 0 600.88 572.76 7.89 o 3 8 0 32.79 31.72 0.96 o 4 8 0 291.04 279.33 4.26 o 5 8 0 17.85 17.33 0.74 o 6 8 0 6.89 7.70 0.62 o 7 8 0 0.06 0.24 0.38 o 8 8 0 12.93 15.61 1.05 o 1 9 0 50.93 55.20 1.51 o 2 9 0 154.28 151.13 2.71 o 3 9 0 54.64 47.82 1.24 o 4 9 0 4.89 6.38 0.54 o 5 9 0 3.48 4.47 0.79 o 6 9 0 3.61 4.53 0.69 o 7 9 0 5.57 5.57 0.78 o 0 10 0 37.81 37.47 1.94 o 1 10 0 6.93 7.20 0.54 o 2 10 0 16.09 14.79 0.74 o 3 10 0 9.05 6.47 0.59 o 4 10 0 35.90 32.77 1.38 o 5 10 0 4.09 4.09 0.69 o 6 10 0 6.73 7.77 0.87 o 1 11 0 0.75 -0.11 0.31 o 2 11 0 8.24 7.89 0.62 o 3 11 0 0.03 -0.24 0.34 o 4 11 0 0.12 0.41 0.51 o 5 11 0 0.67 0.72 0.59 o 0 12 0 21.82 24.14 1.76 o 1 12 0 0.00 -0.41 0.44 o 2 12 0 1.63 2.36 0.49 o 3 12 0 1.54 1.91 0.48 o 4 12 0 0.46 0.95 0.61 o 1 0 1 222.87 248.07 2.95 o 2 0 1 2843.77 2786.06 28.34 o 3 0 1 66.15 66.98 0.84 o 4 0 1 21.28 19.57 0.42 o 5 0 1 15.11 16.82 0.37 o 6 0 1 107.20 115.24 2.56 o 7 0 1 62.54 60.01 1.33 o 8 0 1 17.36 16.21 0.90 o 9 0 1 7.76 7.52 0.72 o 10 0 1 0.02 -0.42 0.42 o 0 1 1 1652.73 1608.84 25.17 o 1 1 1 1432.41 1391.57 12.86 o 2 1 1 2069.70 2047.28 17.48 o 3 1 1 452.50 487.25 3.57 o 4 1 1 199.24 207.50 1.74 o 5 1 1 449.49 492.85 3.37 o 6 1 1 35.00 34.50 0.50 o 7 1 1 34.68 34.83 0.63 o 8 1 1 6.68 6.74 0.46 o 9 1 1 0.96 0.72 0.31 o 10 1 1 6.69 6.75 0.54 o 0 2 1 1792.31 1782.54 22.71 o 1 2 1 493.81 459.01 3.50 o 2 2 1 105.55 113.38 1.10 o 3 2 1 290.21 297.66 2.37 o 4 2 1 102.86 113.27 0.92 o 5 2 1 123.22 129.62 1.14 o 6 2 1 94.20 94.04 0.99 o 7 2 1 7.88 7.65 0.33 o 8 2 1 131.44 135.13 1.95 o 9 2 1 22.50 22.04 0.79 o 10 2 1 8.23 8.75 0.59 o 0 3 1 976.53 967.85 10.90 o 1 3 1 124.16 131.39 1.10 o 2 3 1 677.71 706.17 5.73 o 3 3 1 801.22 852.77 6.96 o 4 3 1 173.43 177.71 1.46 o 5 3 1 282.67 270.11 2.43 o 6 3 1 6.91 5.31 0.45 o 7 3 1 13.54 12.32 0.44 o 8 3 1 81.06 85.31 1.38 o 9 3 1 4.83 4.96 0.45 o 10 3 1 27.63 26.47 1.35 o 0 4 1 310.53 354.17 4.14 o 1 4 1 1149.02 1223.03 8.72 o 2 4 1 34.01 36.75 0.39 o 3 4 1 693.16 731.01 5.99 o 4 4 1 6.89 5.10 0.18 o 5 4 1 9.71 7.12 0.25 o 6 4 1 52.21 48.22 0.70 o 7 4 1 97.87 94.90 1.35 o 8 4 1 9.39 9.45 0.55 o 9 4 1 38.87 45.94 1.17 o 10 4 1 12.06 13.21 1.04 o 1 5 1 54.88 59.10 0.58 o 2 5 1 4.19 4.19 0.20 o 3 5 1 229.40 228.34 2.21 o 4 5 1 56.86 54.17 0.65 o 5 5 1 78.86 78.32 1.02 o 6 5 1 178.91 171.67 2.26 o 7 5 1 67.39 63.93 1.07 o 8 5 1 45.67 45.89 1.14 o 9 5 1 1.53 1.47 0.39 o 0 6 1 4.12 2.07 0.19 o 1 6 1 37.45 36.76 0.47 o 2 6 1 195.91 196.97 1.70 o 3 6 1 66.01 60.47 1.06 o 4 6 1 64.55 59.42 0.83 o 5 6 1 29.10 28.21 0.58 o 6 6 1 185.62 181.71 3.11 o 7 6 1 4.73 4.85 0.36 o 8 6 1 10.71 11.17 0.56 o 9 6 1 0.50 0.14 0.33 o 0 7 1 395.99 338.21 7.60 o 1 7 1 12.56 12.66 0.32 o 2 7 1 18.26 17.37 0.41 o 3 7 1 42.10 39.36 0.59 o 4 7 1 113.78 106.90 1.29 o 5 7 1 90.74 84.84 1.14 o 6 7 1 22.74 22.57 0.61 o 7 7 1 27.67 26.22 0.69 o 8 7 1 4.83 6.06 0.47 o 9 7 1 9.19 9.68 0.64 o 0 8 1 0.81 0.70 0.20 o 1 8 1 120.11 116.51 1.33 o 2 8 1 90.33 84.21 1.19 o 3 8 1 40.45 39.65 0.77 o 4 8 1 1.06 1.16 0.43 o 5 8 1 22.45 20.45 0.58 o 6 8 1 17.74 18.04 0.57 o 7 8 1 35.92 37.73 0.86 o 8 8 1 11.61 11.27 0.60 o 0 9 1 134.93 119.42 2.16 o 1 9 1 65.04 61.66 0.99 o 2 9 1 158.20 149.90 1.85 o 3 9 1 8.81 6.99 0.49 o 4 9 1 5.74 6.24 0.48 o 5 9 1 6.43 5.61 0.49 o 6 9 1 3.17 2.68 0.44 o 7 9 1 5.08 4.91 0.55 o 0 10 1 1.49 0.59 0.30 o 1 10 1 5.93 5.16 0.35 o 2 10 1 14.62 12.81 0.49 o 3 10 1 0.98 0.92 0.26 o 4 10 1 6.21 7.13 0.55 o 5 10 1 4.10 4.22 0.49 o 6 10 1 11.24 13.60 0.74 o 0 11 1 16.80 14.92 0.95 o 1 11 1 0.00 -0.06 0.24 o 2 11 1 4.85 5.60 0.39 o 3 11 1 0.81 1.11 0.32 o 4 11 1 5.22 5.86 0.55 o 5 11 1 9.54 11.70 0.71 o 0 12 1 0.19 0.40 0.53 o 1 12 1 8.50 10.25 0.65 o 2 12 1 2.75 4.65 0.45 o 3 12 1 3.91 5.35 0.48 o 4 12 1 3.41 4.39 0.60 o 0 0 2 3585.57 3422.00 75.52 o 1 0 2 6036.56 5444.54 70.13 o 2 0 2 4203.40 4069.06 46.20 o 3 0 2 39.80 40.10 0.56 o 4 0 2 139.85 137.90 1.60 o 5 0 2 135.11 138.60 1.92 o 6 0 2 56.66 61.39 0.97 o 7 0 2 176.85 176.92 2.53 o 8 0 2 27.40 27.40 1.15 o 9 0 2 3.15 3.58 0.57 o 10 0 2 0.64 1.38 0.55 o 0 1 2 608.46 604.78 7.80 o 1 1 2 3662.26 3496.00 36.03 o 2 1 2 3425.96 3455.02 29.32 o 3 1 2 260.56 260.52 2.09 o 4 1 2 291.55 332.60 2.68 o 5 1 2 116.21 117.05 1.05 o 6 1 2 5.61 6.68 0.25 o 7 1 2 79.79 79.02 1.15 o 8 1 2 29.21 28.51 0.99 o 9 1 2 10.78 11.28 0.60 o 10 1 2 2.27 2.30 0.41 o 0 2 2 938.69 976.72 15.66 o 1 2 2 168.89 172.86 1.58 o 2 2 2 873.14 900.68 7.23 o 3 2 2 719.63 757.85 5.77 o 4 2 2 66.39 81.22 0.83 o 5 2 2 96.70 104.08 1.03 o 6 2 2 117.74 113.85 1.40 o 7 2 2 97.75 93.57 1.89 o 8 2 2 33.62 34.77 0.83 o 9 2 2 15.98 16.06 0.69 o 10 2 2 12.01 12.95 0.68 o 0 3 2 539.53 534.78 7.00 o 1 3 2 1163.73 1189.64 10.02 o 2 3 2 181.75 160.47 1.42 o 3 3 2 53.40 58.14 0.60 o 4 3 2 141.19 146.45 1.30 o 5 3 2 1.76 1.67 0.14 o 6 3 2 6.94 7.60 0.28 o 7 3 2 64.83 62.91 1.02 o 8 3 2 13.08 12.87 0.49 o 9 3 2 0.93 0.81 0.33 o 10 3 2 0.34 -0.02 0.44 o 0 4 2 5.53 8.15 0.90 o 1 4 2 306.66 297.63 2.52 o 2 4 2 119.25 128.24 1.20 o 3 4 2 306.11 318.23 2.58 o 4 4 2 24.61 27.03 0.41 o 5 4 2 79.15 75.78 0.84 o 6 4 2 7.31 7.33 0.27 o 7 4 2 21.85 18.30 0.61 o 8 4 2 33.54 35.88 1.01 o 9 4 2 7.88 7.66 0.64 o 10 4 2 6.57 7.44 0.86 o 0 5 2 223.38 241.53 3.07 o 1 5 2 434.25 439.20 3.66 o 2 5 2 363.41 402.11 3.19 o 3 5 2 115.17 120.36 1.42 o 4 5 2 36.14 38.93 0.63 o 5 5 2 36.95 41.82 0.68 o 6 5 2 20.28 19.28 0.50 o 7 5 2 2.12 3.21 0.40 o 8 5 2 34.55 34.26 0.88 o 9 5 2 2.27 2.12 0.41 o 0 6 2 37.71 47.43 0.86 o 1 6 2 252.45 252.41 2.23 o 2 6 2 37.54 36.37 0.48 o 3 6 2 12.57 11.57 0.31 o 4 6 2 9.30 7.63 0.31 o 5 6 2 120.17 111.44 1.48 o 6 6 2 41.36 40.72 0.81 o 7 6 2 19.42 17.79 0.64 o 8 6 2 20.80 19.71 0.71 o 9 6 2 1.14 0.90 0.37 o 0 7 2 162.67 156.07 2.16 o 1 7 2 257.30 251.35 2.27 o 2 7 2 195.50 184.70 2.53 o 3 7 2 46.90 46.51 0.71 o 4 7 2 51.80 48.79 0.78 o 5 7 2 9.82 8.89 0.41 o 6 7 2 18.81 19.61 0.58 o 7 7 2 0.57 0.19 0.28 o 8 7 2 1.69 2.07 0.37 o 0 8 2 62.78 54.79 1.04 o 1 8 2 13.84 14.52 0.52 o 2 8 2 64.73 60.29 1.38 o 3 8 2 93.39 90.76 1.80 o 4 8 2 33.14 31.49 0.70 o 5 8 2 50.36 52.10 0.96 o 6 8 2 6.99 6.90 0.41 o 7 8 2 4.04 3.61 0.36 o 8 8 2 1.17 1.85 0.38 o 0 9 2 132.16 113.45 1.88 o 1 9 2 21.52 21.19 0.58 o 2 9 2 16.00 15.04 0.51 o 3 9 2 180.48 184.25 2.20 o 4 9 2 30.42 32.70 0.87 o 5 9 2 22.00 20.76 0.72 o 6 9 2 36.54 38.85 1.11 o 7 9 2 1.07 1.24 0.35 o 0 10 2 28.04 26.36 1.79 o 1 10 2 6.01 5.65 0.51 o 2 10 2 21.76 20.62 0.61 o 3 10 2 6.33 6.59 0.44 o 4 10 2 16.15 15.73 0.65 o 5 10 2 5.54 5.48 0.53 o 6 10 2 12.90 14.64 0.76 o 0 11 2 0.39 0.12 0.45 o 1 11 2 14.61 13.94 0.59 o 2 11 2 5.27 7.87 0.44 o 3 11 2 2.16 2.88 0.38 o 4 11 2 5.10 6.36 0.50 o 5 11 2 3.99 5.13 0.56 o 0 12 2 8.92 9.33 0.87 o 1 12 2 1.85 2.61 0.45 o 2 12 2 4.72 5.88 0.51 o 3 12 2 12.05 15.27 0.80 o 1 0 3 11340.38 10171.87 130.26 o 2 0 3 1286.26 1314.18 16.83 o 3 0 3 1487.92 1588.70 17.85 o 4 0 3 0.29 0.62 0.18 o 5 0 3 18.62 21.25 0.83 o 6 0 3 37.30 39.06 0.89 o 7 0 3 28.84 22.60 1.32 o 8 0 3 87.03 79.09 2.14 o 9 0 3 0.08 -0.01 0.37 o 10 0 3 0.22 0.39 0.48 o 0 1 3 1728.07 1714.01 21.81 o 1 1 3 599.56 603.30 6.05 o 2 1 3 237.11 236.96 2.15 o 3 1 3 279.40 288.51 2.47 o 4 1 3 280.16 318.59 2.74 o 5 1 3 17.43 16.35 0.32 o 6 1 3 1.92 1.59 0.16 o 7 1 3 73.71 68.36 0.99 o 8 1 3 8.38 7.78 0.63 o 9 1 3 2.64 3.12 0.41 o 10 1 3 4.60 6.72 0.60 o 0 2 3 16.32 15.38 0.43 o 1 2 3 252.76 280.97 2.70 o 2 2 3 385.85 415.54 3.65 o 3 2 3 194.82 204.01 1.82 o 4 2 3 269.05 285.30 2.67 o 5 2 3 13.25 13.59 0.32 o 6 2 3 162.16 152.74 2.18 o 7 2 3 20.19 18.66 0.45 o 8 2 3 25.31 26.37 0.72 o 9 2 3 15.38 14.55 0.67 o 10 2 3 0.26 0.11 0.33 o 0 3 3 1045.32 1086.38 16.90 o 1 3 3 481.69 491.30 4.28 o 2 3 3 210.68 221.13 1.92 o 3 3 3 278.62 287.27 2.32 o 4 3 3 72.85 74.83 0.86 o 5 3 3 57.75 56.94 1.01 o 6 3 3 134.19 136.96 1.56 o 7 3 3 73.48 69.08 1.01 o 8 3 3 4.96 4.02 0.37 o 9 3 3 21.97 22.79 0.82 o 10 3 3 25.08 28.29 1.13 o 0 4 3 152.44 158.84 2.90 o 1 4 3 352.53 348.87 3.13 o 2 4 3 404.23 396.74 3.54 o 3 4 3 88.41 87.36 1.09 o 4 4 3 78.20 72.51 0.84 o 5 4 3 27.66 25.98 0.47 o 6 4 3 37.05 36.03 0.80 o 7 4 3 30.16 29.41 0.91 o 8 4 3 16.05 15.03 0.54 o 9 4 3 14.89 15.80 0.83 o 0 5 3 57.58 52.45 1.31 o 1 5 3 272.18 286.59 2.66 o 2 5 3 239.52 247.90 2.20 o 3 5 3 53.50 54.68 0.69 o 4 5 3 218.01 213.43 2.17 o 5 5 3 19.86 16.71 0.49 o 6 5 3 56.38 58.52 0.90 o 7 5 3 50.33 48.87 1.02 o 8 5 3 21.17 23.33 0.75 o 9 5 3 14.10 16.03 0.75 o 0 6 3 17.21 20.13 0.54 o 1 6 3 185.57 202.36 1.86 o 2 6 3 15.28 14.20 0.40 o 3 6 3 54.30 53.08 0.78 o 4 6 3 241.36 232.59 2.38 o 5 6 3 39.69 37.58 0.73 o 6 6 3 27.87 27.39 0.75 o 7 6 3 11.62 11.26 0.54 o 8 6 3 16.75 17.86 0.68 o 9 6 3 1.22 2.41 0.46 o 0 7 3 91.74 86.77 1.40 o 1 7 3 29.08 24.97 0.50 o 2 7 3 190.08 184.50 2.08 o 3 7 3 49.49 48.11 0.83 o 4 7 3 13.68 13.09 0.42 o 5 7 3 109.29 107.50 1.37 o 6 7 3 10.81 11.47 0.47 o 7 7 3 10.17 10.20 0.53 o 8 7 3 6.57 6.64 0.49 o 0 8 3 66.06 63.24 1.18 o 1 8 3 213.06 214.28 2.38 o 2 8 3 58.68 56.80 1.04 o 3 8 3 4.89 5.79 0.45 o 4 8 3 35.75 33.18 0.73 o 5 8 3 65.69 59.48 1.05 o 6 8 3 14.92 16.12 0.63 o 7 8 3 1.14 1.20 0.33 o 8 8 3 3.17 3.74 0.44 o 0 9 3 61.73 62.46 1.43 o 1 9 3 51.85 51.08 0.91 o 2 9 3 1.96 1.55 0.26 o 3 9 3 23.48 22.75 0.78 o 4 9 3 32.23 30.82 0.84 o 5 9 3 9.11 9.25 0.53 o 6 9 3 4.72 6.05 0.47 o 7 9 3 5.85 7.53 0.59 o 0 10 3 29.58 25.61 1.18 o 1 10 3 2.06 2.08 0.28 o 2 10 3 7.33 5.93 0.38 o 3 10 3 8.47 8.28 0.56 o 4 10 3 13.43 15.23 0.66 o 5 10 3 5.55 5.00 0.46 o 6 10 3 8.89 9.75 0.67 o 0 11 3 2.02 1.79 0.54 o 1 11 3 1.16 1.30 0.32 o 2 11 3 4.45 4.56 0.42 o 3 11 3 16.15 19.89 0.83 o 4 11 3 0.17 0.86 0.36 o 5 11 3 5.80 7.12 0.63 o 0 12 3 0.13 0.02 0.51 o 1 12 3 6.97 8.20 0.61 o 2 12 3 9.78 12.04 0.70 o 3 12 3 0.79 0.45 0.38 o 0 0 4 45.75 45.80 1.53 o 1 0 4 18.28 33.59 1.33 o 2 0 4 865.76 864.07 11.23 o 3 0 4 619.77 686.77 7.90 o 4 0 4 14.06 13.03 0.64 o 5 0 4 6.13 7.63 0.44 o 6 0 4 67.75 62.05 1.35 o 7 0 4 0.52 0.50 0.26 o 8 0 4 0.01 0.10 0.31 o 9 0 4 0.09 0.07 0.40 o 10 0 4 0.94 0.53 0.49 o 0 1 4 20.75 18.29 0.50 o 1 1 4 403.27 402.34 4.16 o 2 1 4 452.14 467.22 4.41 o 3 1 4 1773.02 1906.87 17.45 o 4 1 4 554.84 595.39 4.95 o 5 1 4 117.32 131.74 2.11 o 6 1 4 2.58 2.92 0.23 o 7 1 4 71.12 69.64 0.95 o 8 1 4 35.92 32.92 0.74 o 9 1 4 22.22 19.59 0.74 o 10 1 4 0.79 0.21 0.34 o 0 2 4 259.96 256.57 4.00 o 1 2 4 390.06 399.63 3.97 o 2 2 4 19.59 29.98 0.64 o 3 2 4 26.48 22.61 0.39 o 4 2 4 15.18 17.79 0.38 o 5 2 4 103.97 100.87 1.42 o 6 2 4 18.05 19.14 0.43 o 7 2 4 52.07 50.84 0.83 o 8 2 4 7.67 7.23 0.39 o 9 2 4 3.22 3.91 0.44 o 10 2 4 0.12 -0.34 0.34 o 0 3 4 603.27 608.13 15.13 o 1 3 4 280.73 293.80 2.89 o 2 3 4 255.17 271.22 2.71 o 3 3 4 174.42 176.98 1.61 o 4 3 4 210.49 214.68 2.13 o 5 3 4 9.80 9.93 0.31 o 6 3 4 66.09 63.33 1.01 o 7 3 4 8.35 7.80 0.36 o 8 3 4 4.25 3.95 0.39 o 9 3 4 1.76 1.44 0.50 o 10 3 4 0.81 0.91 0.76 o 0 4 4 582.12 622.78 10.01 o 1 4 4 39.03 39.79 0.62 o 2 4 4 249.17 260.13 2.44 o 3 4 4 5.74 4.75 0.25 o 4 4 4 204.34 190.39 2.73 o 5 4 4 82.00 75.72 1.01 o 6 4 4 76.86 75.04 1.16 o 7 4 4 1.76 1.81 0.25 o 8 4 4 29.68 32.09 0.77 o 9 4 4 8.58 10.02 0.63 o 0 5 4 11.56 10.59 0.65 o 1 5 4 22.61 20.75 0.49 o 2 5 4 6.18 8.48 0.36 o 3 5 4 31.22 29.56 0.59 o 4 5 4 34.50 31.87 0.65 o 5 5 4 83.20 75.53 1.04 o 6 5 4 108.80 109.77 1.53 o 7 5 4 7.96 4.99 0.49 o 8 5 4 2.49 2.92 0.39 o 9 5 4 4.94 4.92 0.53 o 0 6 4 2.67 3.87 0.34 o 1 6 4 33.59 36.16 0.59 o 2 6 4 55.57 51.08 0.88 o 3 6 4 169.18 165.03 1.93 o 4 6 4 5.00 5.89 0.31 o 5 6 4 43.86 34.48 0.74 o 6 6 4 12.60 12.51 0.50 o 7 6 4 10.70 11.32 0.55 o 8 6 4 1.36 1.16 0.34 o 9 6 4 2.93 3.34 0.44 o 0 7 4 13.90 12.71 0.59 o 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1.69 1.68 0.38 o 1 3 9 30.05 28.51 0.67 o 2 3 9 3.36 2.42 0.44 o 3 3 9 123.85 120.90 2.88 o 4 3 9 14.79 14.02 0.70 o 5 3 9 2.75 2.95 0.44 o 6 3 9 6.93 6.95 0.59 o 7 3 9 12.99 13.00 0.93 o 0 4 9 2.08 2.60 0.42 o 1 4 9 74.26 74.64 1.47 o 2 4 9 5.87 4.09 0.46 o 3 4 9 8.24 9.32 1.10 o 4 4 9 2.24 2.03 0.40 o 5 4 9 4.52 3.95 0.48 o 6 4 9 1.48 2.95 0.57 o 7 4 9 0.58 0.65 0.51 o 0 5 9 41.87 43.75 1.24 o 1 5 9 43.14 42.10 2.05 o 2 5 9 51.65 52.29 1.25 o 3 5 9 31.77 30.25 1.14 o 4 5 9 12.40 9.99 0.62 o 5 5 9 9.05 10.05 0.68 o 6 5 9 0.52 0.61 0.46 o 7 5 9 2.71 2.04 0.49 o 0 6 9 5.52 5.34 0.55 o 1 6 9 7.62 7.20 0.57 o 2 6 9 47.88 48.10 1.23 o 3 6 9 3.80 4.33 0.49 o 4 6 9 3.33 3.15 0.58 o 5 6 9 6.14 6.48 0.71 o 6 6 9 5.11 5.79 0.60 o 0 7 9 62.63 61.74 2.97 o 1 7 9 23.32 23.82 0.88 o 2 7 9 11.17 10.38 0.71 o 3 7 9 1.62 1.75 0.44 o 4 7 9 6.47 7.42 1.48 o 5 7 9 7.24 8.84 0.81 o 6 7 9 3.65 3.40 1.19 o 0 8 9 0.00 -0.69 0.69 o 1 8 9 0.03 0.45 0.49 o 2 8 9 1.12 1.65 0.43 o 3 8 9 9.64 8.09 0.65 o 4 8 9 5.42 6.43 0.74 o 5 8 9 5.51 6.42 0.78 o 0 9 9 0.09 0.59 0.93 o 1 9 9 3.66 4.30 0.66 o 2 9 9 8.00 9.43 0.70 o 3 9 9 1.81 3.53 0.55 o 0 10 9 7.43 7.65 1.46 o 1 10 9 4.12 4.21 1.29 o 0 0 10 8.72 8.36 0.80 o 1 0 10 1.09 2.12 0.42 o 2 0 10 5.37 4.67 0.67 o 3 0 10 52.14 52.44 2.52 o 4 0 10 1.95 2.45 0.63 o 5 0 10 1.18 0.91 0.54 o 6 0 10 1.66 1.29 1.04 o 7 0 10 1.35 1.89 0.67 o 0 1 10 16.04 16.89 0.77 o 1 1 10 6.05 7.75 0.54 o 2 1 10 76.23 72.65 1.50 o 3 1 10 16.60 17.50 0.88 o 4 1 10 41.32 39.20 1.13 o 5 1 10 22.28 21.50 1.24 o 6 1 10 17.01 16.35 0.82 o 7 1 10 1.85 4.13 0.55 o 0 2 10 1.75 1.74 0.41 o 1 2 10 45.92 49.00 1.04 o 2 2 10 27.31 26.41 0.77 o 3 2 10 97.89 92.90 1.80 o 4 2 10 3.48 3.74 0.49 o 5 2 10 7.14 7.08 0.79 o 6 2 10 16.34 15.35 0.79 o 7 2 10 0.07 0.33 0.40 o 0 3 10 8.37 8.51 0.63 o 1 3 10 14.91 17.06 0.64 o 2 3 10 4.15 4.48 0.55 o 3 3 10 7.82 7.92 0.59 o 4 3 10 2.75 2.04 0.43 o 5 3 10 9.99 8.70 0.64 o 6 3 10 0.16 0.42 0.37 o 7 3 10 3.43 4.14 0.68 o 0 4 10 10.28 12.19 1.32 o 1 4 10 5.24 6.45 0.46 o 2 4 10 1.48 1.88 0.40 o 3 4 10 17.89 19.47 0.80 o 4 4 10 5.21 5.18 0.52 o 5 4 10 3.12 4.09 0.52 o 6 4 10 5.02 5.41 0.59 o 0 5 10 0.09 -0.45 0.45 o 1 5 10 3.51 3.96 0.50 o 2 5 10 6.66 6.92 0.57 o 3 5 10 10.01 10.42 0.78 o 4 5 10 1.50 1.32 0.39 o 5 5 10 7.92 7.43 0.62 o 6 5 10 0.30 0.27 0.48 o 0 6 10 45.17 48.07 1.74 o 1 6 10 50.04 51.36 1.29 o 2 6 10 1.30 0.99 0.40 o 3 6 10 0.13 -0.41 0.41 o 4 6 10 3.41 3.04 0.48 o 5 6 10 20.14 20.91 1.12 o 0 7 10 43.41 42.80 2.48 o 1 7 10 19.97 20.91 0.88 o 2 7 10 13.48 12.73 0.74 o 3 7 10 4.28 3.82 0.63 o 4 7 10 8.66 9.30 0.84 o 5 7 10 0.13 0.12 0.68 o 0 8 10 8.25 8.61 1.46 o 1 8 10 2.71 3.08 0.63 o 2 8 10 5.32 6.11 0.61 o 3 8 10 0.52 1.40 0.57 o 0 9 10 2.11 1.72 1.12 o 1 9 10 0.80 0.53 0.74 o 1 0 11 0.00 -0.44 0.55 o 2 0 11 1.17 1.44 0.55 o 3 0 11 20.41 20.57 1.26 o 4 0 11 6.44 7.28 0.85 o 5 0 11 10.90 9.43 0.97 o 6 0 11 7.43 10.79 1.35 o 0 1 11 71.53 68.12 1.72 o 1 1 11 2.47 2.49 0.37 o 2 1 11 5.92 4.40 0.43 o 3 1 11 16.84 16.49 0.77 o 4 1 11 3.03 3.52 0.50 o 5 1 11 6.86 6.61 0.61 o 6 1 11 0.54 1.77 0.47 o 0 2 11 28.07 25.49 1.02 o 1 2 11 21.70 23.49 1.05 o 2 2 11 38.11 38.22 1.22 o 3 2 11 14.73 14.09 0.74 o 4 2 11 5.60 6.84 0.60 o 5 2 11 7.23 5.54 0.58 o 6 2 11 2.84 3.05 0.53 o 0 3 11 0.04 0.93 0.54 o 1 3 11 7.18 9.15 0.54 o 2 3 11 10.69 9.15 0.54 o 3 3 11 1.40 1.46 0.43 o 4 3 11 26.82 25.66 0.97 o 5 3 11 0.12 -0.05 0.36 o 6 3 11 0.35 0.25 0.42 o 0 4 11 1.37 1.51 0.59 o 1 4 11 13.95 14.41 0.64 o 2 4 11 0.97 1.24 0.50 o 3 4 11 6.19 4.53 0.52 o 4 4 11 3.51 4.27 0.54 o 5 4 11 1.14 2.11 0.49 o 0 5 11 0.38 0.64 0.55 o 1 5 11 1.27 1.07 0.43 o 2 5 11 18.35 18.38 1.15 o 3 5 11 6.30 5.46 0.56 o 4 5 11 1.78 1.71 0.45 o 5 5 11 1.47 1.69 0.48 o 0 6 11 25.86 31.32 2.29 o 1 6 11 29.47 32.69 1.08 o 2 6 11 2.96 2.91 0.58 o 3 6 11 1.49 2.88 0.59 o 4 6 11 2.48 3.54 0.53 o 0 7 11 0.96 1.30 1.00 o 1 7 11 8.64 6.90 0.97 o 2 7 11 8.13 8.55 0.70 o 3 7 11 4.86 6.08 0.75 o 0 8 11 0.22 0.67 1.06 o 1 8 11 0.12 -0.63 0.63 o 0 0 12 61.07 62.48 2.04 o 1 0 12 0.57 0.08 0.42 o 2 0 12 26.52 25.90 1.37 o 3 0 12 2.87 2.54 0.90 o 4 0 12 1.38 0.38 0.58 o 5 0 12 3.17 3.29 0.80 o 0 1 12 2.64 2.48 0.53 o 1 1 12 25.84 27.89 0.86 o 2 1 12 5.30 4.98 0.49 o 3 1 12 7.61 7.13 0.55 o 4 1 12 1.49 1.36 0.44 o 5 1 12 4.02 5.70 0.62 o 0 2 12 3.16 3.07 0.68 o 1 2 12 1.96 3.49 0.44 o 2 2 12 6.71 6.11 0.51 o 3 2 12 10.87 11.03 0.99 o 4 2 12 1.38 1.66 0.46 o 5 2 12 0.23 0.50 0.43 o 0 3 12 1.46 2.53 0.70 o 1 3 12 11.54 12.27 0.72 o 2 3 12 38.54 39.13 1.19 o 3 3 12 2.57 3.57 0.53 o 4 3 12 3.12 1.91 0.47 o 5 3 12 2.02 2.17 0.49 o 0 4 12 25.71 27.36 1.39 o 1 4 12 0.72 0.60 0.41 o 2 4 12 2.20 1.57 0.79 o 3 4 12 2.17 1.90 0.64 o 4 4 12 0.21 0.47 0.41 o 0 5 12 6.04 4.70 0.81 o 1 5 12 22.03 23.72 1.11 o 2 5 12 10.79 13.03 1.22 o 3 5 12 2.26 2.53 0.50 o 4 5 12 3.85 4.82 0.71 o 0 6 12 0.82 -0.46 0.89 o 1 6 12 11.37 12.65 0.91 o 2 6 12 1.04 1.43 0.54 o 3 6 12 1.16 1.26 0.56 o 0 7 12 10.46 10.79 1.68 o 1 0 13 9.89 10.27 0.83 o 2 0 13 1.87 1.62 0.55 o 3 0 13 0.58 0.74 0.62 o 4 0 13 0.01 -0.12 0.59 o 0 1 13 1.24 0.75 0.64 o 1 1 13 33.84 34.66 0.97 o 2 1 13 4.29 5.38 0.53 o 3 1 13 3.13 3.22 0.56 o 4 1 13 1.66 1.95 0.52 o 0 2 13 16.18 19.03 1.25 o 1 2 13 2.26 2.07 0.44 o 2 2 13 7.04 8.30 0.61 o 3 2 13 3.43 4.07 0.58 o 4 2 13 6.65 5.47 0.72 o 0 3 13 4.73 4.57 0.85 o 1 3 13 2.52 2.02 0.72 o 2 3 13 1.02 1.49 0.49 o 3 3 13 0.01 0.29 0.43 o 0 4 13 10.99 13.16 1.12 o 1 4 13 0.30 0.95 0.66 o 2 4 13 8.80 10.19 0.73 o 0 5 13 1.74 2.14 1.15 o 1 5 13 1.20 2.10 0.75 o 0 0 14 0.00 0.27 0.93 o 1 0 14 17.03 15.41 1.22 o 2 0 14 0.01 -0.78 0.78 o 0 1 14 0.02 0.01 0.63 o 1 1 14 2.78 2.85 0.49 o 0 2 14 33.91 37.74 1.77 o 1 2 14 0.17 0.46 0.55 o