#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/31/2203165.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203165_Fobs loop_ _publ_author_name 'Amini, Mostafa M.' 'Mirzaee, Mehdi' 'Yeganeh, Farnaz' 'Ng, Seik Weng' _publ_section_title ; Tris(8-hydroxyquinolinato-\k^2^O,N)oxoniobium(V) dichloromethane disolvate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m147 _journal_page_last m148 _journal_volume 60 _journal_year 2004 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.5985 _cell_length_b 17.6585 _cell_length_c 13.0243 _exptl_crystal_F_000 1432.00 _reflns_d_resolution_high 0.7974 _[local]_cod_data_source_file ci6322Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'Oxotris(8-hydroxyquinolinato)niobium chloroform solvate in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 421.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6418.67 6141.35 129.90 o 4 0 0 67272.33 67077.63 1363.80 o 6 0 0 821.94 598.17 35.69 o 8 0 0 15842.96 15650.89 332.96 o 10 0 0 2038.02 2580.14 115.74 o 12 0 0 3443.09 3675.09 133.57 o 14 0 0 41.29 -4.39 73.07 o 2 1 0 19645.74 19031.02 303.86 o 4 1 0 8394.23 8655.14 129.33 o 6 1 0 22059.79 21180.18 310.53 o 8 1 0 2703.09 2836.51 61.41 o 10 1 0 6377.11 6971.91 145.94 o 12 1 0 35.25 30.49 42.84 o 14 1 0 982.28 959.24 69.27 o 0 2 0 17209.38 22716.16 1097.94 o 2 2 0 2904.87 2834.89 51.10 o 4 2 0 401.56 690.58 27.21 o 6 2 0 10130.93 10849.78 163.89 o 8 2 0 7502.26 7329.80 129.16 o 10 2 0 1850.56 1938.21 87.17 o 12 2 0 5325.25 5467.83 132.51 o 14 2 0 262.42 227.09 59.77 o 2 3 0 326.86 306.67 15.67 o 4 3 0 1850.08 1701.68 36.05 o 6 3 0 3632.81 3079.62 72.02 o 8 3 0 732.37 659.83 32.37 o 10 3 0 1642.56 1400.70 62.43 o 12 3 0 230.21 413.18 63.17 o 14 3 0 2003.88 2219.42 96.31 o 2 4 0 60835.36 63933.93 991.78 o 4 4 0 14117.28 12964.14 222.84 o 6 4 0 1760.85 1819.69 42.68 o 8 4 0 6954.14 7062.54 126.64 o 10 4 0 710.02 592.96 44.53 o 12 4 0 3910.28 3656.39 106.83 o 14 4 0 142.82 129.68 59.78 o 2 5 0 2237.88 2006.37 35.45 o 4 5 0 3471.07 3413.63 61.54 o 6 5 0 74.45 47.10 21.17 o 8 5 0 1701.87 1671.31 47.27 o 10 5 0 3238.79 3006.43 76.25 o 12 5 0 27.36 24.18 48.13 o 14 5 0 1110.41 1208.95 73.74 o 0 6 0 169881.86 196445.56 9441.72 o 2 6 0 170.17 133.77 11.33 o 4 6 0 289.22 252.80 17.24 o 6 6 0 504.75 669.93 27.37 o 8 6 0 9075.67 8952.91 171.67 o 10 6 0 114.26 96.54 36.39 o 12 6 0 2369.49 2424.07 85.93 o 14 6 0 28.39 -4.70 59.03 o 2 7 0 13359.50 14372.53 205.88 o 4 7 0 2050.30 2161.03 42.51 o 6 7 0 6796.86 6445.15 124.06 o 8 7 0 1896.27 2290.17 60.41 o 10 7 0 5018.56 5438.83 116.67 o 12 7 0 61.55 28.99 50.09 o 14 7 0 1277.28 1399.96 79.90 o 0 8 0 122461.95 142220.97 6843.16 o 2 8 0 2735.84 3094.38 46.37 o 4 8 0 2434.49 2355.08 43.40 o 6 8 0 8785.87 8629.71 162.31 o 8 8 0 5943.51 5797.60 117.96 o 10 8 0 110.37 118.69 38.77 o 12 8 0 4035.00 3671.70 108.49 o 14 8 0 7.89 -39.05 61.91 o 2 9 0 2738.43 3501.04 52.38 o 4 9 0 799.44 689.45 22.69 o 6 9 0 9016.19 8728.69 163.92 o 8 9 0 1347.09 1409.14 48.41 o 10 9 0 1323.56 1314.59 52.62 o 12 9 0 39.64 46.96 47.31 o 14 9 0 912.29 937.27 74.09 o 0 10 0 24350.64 27723.77 1361.91 o 2 10 0 5673.43 6273.60 133.55 o 4 10 0 2590.07 2365.13 68.38 o 6 10 0 1388.18 1401.23 46.86 o 8 10 0 1786.45 1663.08 56.79 o 10 10 0 1121.95 1049.65 55.44 o 12 10 0 4169.42 4070.59 125.53 o 14 10 0 5.54 -171.33 213.66 o 2 11 0 5457.92 6077.62 130.52 o 4 11 0 1776.31 2119.44 64.04 o 6 11 0 2862.20 3049.29 91.45 o 8 11 0 1736.19 1577.72 69.19 o 10 11 0 2406.26 2325.51 117.55 o 12 11 0 99.95 47.66 65.87 o 0 12 0 37538.11 42138.98 2058.43 o 2 12 0 519.13 557.44 42.99 o 4 12 0 2880.50 3142.33 85.40 o 6 12 0 124.84 199.45 42.79 o 8 12 0 6886.80 6347.68 167.15 o 10 12 0 675.91 685.01 66.07 o 12 12 0 2085.02 2155.40 106.45 o 2 13 0 7040.40 7373.71 285.37 o 4 13 0 951.92 990.57 59.99 o 6 13 0 995.00 957.32 74.90 o 8 13 0 1906.86 2182.74 88.22 o 10 13 0 2466.38 2647.70 99.68 o 12 13 0 45.31 80.42 68.29 o 0 14 0 35700.08 38805.81 1905.53 o 2 14 0 438.36 605.25 88.22 o 4 14 0 4682.15 5315.29 132.69 o 6 14 0 338.83 394.31 46.71 o 8 14 0 5456.36 5430.30 150.11 o 10 14 0 88.95 28.61 59.74 o 12 14 0 1486.67 1441.72 86.01 o 2 15 0 4229.23 4033.19 185.63 o 4 15 0 2093.64 2303.40 91.13 o 6 15 0 4729.78 4681.12 127.03 o 8 15 0 1048.48 1065.86 71.23 o 10 15 0 1744.10 1704.12 81.72 o 2 16 0 1580.60 1414.70 167.59 o 4 16 0 5815.16 5452.50 173.69 o 6 16 0 31.92 -40.53 49.00 o 8 16 0 2934.15 2956.66 99.50 o 10 16 0 1294.48 1108.21 73.00 o 2 17 0 2485.19 2439.93 208.18 o 4 17 0 340.06 235.69 65.36 o 6 17 0 5890.29 5845.99 195.10 o 8 17 0 1.77 -36.56 63.20 o 10 17 0 1676.46 1613.60 126.53 o 2 18 0 83.66 96.87 152.65 o 4 18 0 627.35 643.60 73.87 o 6 18 0 1140.57 987.64 91.86 o 8 18 0 2708.35 2432.78 119.25 o 2 19 0 289.30 203.95 153.90 o 4 19 0 74.30 -58.05 58.05 o 6 19 0 281.21 145.68 70.03 o 2 20 0 111.96 47.07 156.39 o 4 20 0 659.56 808.48 68.21 o 6 20 0 55.05 -26.93 68.02 o 2 21 0 820.34 707.48 203.70 o 4 21 0 4.83 -12.56 58.03 o 1 0 1 36086.49 33561.98 605.40 o 2 0 1 604.50 832.02 17.62 o 3 0 1 177613.81 175098.75 2503.00 o 4 0 1 60843.80 59081.82 883.52 o 5 0 1 41454.72 39631.22 572.84 o 6 0 1 4622.19 4694.94 77.35 o 7 0 1 17367.44 17535.15 272.13 o 8 0 1 1836.29 1817.40 42.99 o 9 0 1 1597.53 1793.34 56.45 o 10 0 1 683.57 661.96 44.25 o 11 0 1 5559.38 5075.24 115.00 o 12 0 1 777.65 610.37 50.54 o 13 0 1 694.70 674.71 52.84 o 14 0 1 1.91 -25.83 53.93 o 15 0 1 1296.00 1202.55 94.78 o 0 1 1 1012.28 976.26 19.63 o 1 1 1 15219.47 15391.56 181.39 o 2 1 1 17.83 11.98 7.47 o 3 1 1 30852.85 29953.02 345.55 o 4 1 1 2354.65 2282.40 29.51 o 5 1 1 12490.42 11665.90 125.12 o 6 1 1 1112.32 1216.95 27.40 o 7 1 1 4770.94 4592.25 54.64 o 8 1 1 39.94 48.05 18.19 o 9 1 1 5781.86 5396.93 81.65 o 10 1 1 378.94 317.63 27.65 o 11 1 1 264.22 263.31 32.73 o 12 1 1 35.73 72.89 31.40 o 13 1 1 922.11 1077.06 44.56 o 14 1 1 74.32 59.07 41.47 o 15 1 1 283.74 308.59 59.49 o 1 2 1 13421.23 13996.88 169.13 o 2 2 1 36.35 34.63 7.98 o 3 2 1 2126.33 2522.27 33.39 o 4 2 1 6349.58 6346.78 75.70 o 5 2 1 3011.53 2894.24 36.32 o 6 2 1 5320.67 5657.90 65.38 o 7 2 1 1913.61 1711.15 27.18 o 8 2 1 750.66 765.86 24.10 o 9 2 1 1212.01 1276.50 31.15 o 10 2 1 960.30 977.65 33.58 o 11 2 1 2677.37 2624.50 52.44 o 12 2 1 77.89 -17.06 32.43 o 13 2 1 855.58 922.47 45.25 o 14 2 1 4.76 29.22 41.32 o 15 2 1 731.32 796.28 50.79 o 0 3 1 400.74 524.64 14.45 o 1 3 1 1118.46 1312.80 16.58 o 2 3 1 1086.22 1318.44 20.62 o 3 3 1 409.12 708.89 18.00 o 4 3 1 8.63 -5.54 11.73 o 5 3 1 5925.31 5600.18 68.65 o 6 3 1 3.50 -15.82 15.82 o 7 3 1 148.24 265.63 21.51 o 8 3 1 91.99 68.33 19.11 o 9 3 1 8424.87 8612.67 107.67 o 10 3 1 1388.75 1329.09 36.89 o 11 3 1 803.15 968.23 42.07 o 12 3 1 92.68 81.79 34.32 o 13 3 1 441.93 435.07 40.55 o 14 3 1 3.51 -21.75 40.69 o 15 3 1 567.55 438.50 50.33 o 1 4 1 99843.66 109966.79 1148.05 o 2 4 1 1706.82 1595.46 34.67 o 3 4 1 64.08 122.86 10.28 o 4 4 1 1383.62 1290.46 22.13 o 5 4 1 2495.00 2399.90 37.36 o 6 4 1 1093.22 1037.99 22.89 o 7 4 1 3812.78 3443.83 47.89 o 8 4 1 210.30 127.49 19.92 o 9 4 1 353.61 281.84 22.90 o 10 4 1 36.40 11.11 26.55 o 11 4 1 3793.39 3893.29 76.90 o 12 4 1 19.31 -29.07 34.52 o 13 4 1 667.30 669.71 42.94 o 14 4 1 4.81 -40.70 40.70 o 15 4 1 1134.30 1168.90 53.24 o 0 5 1 15550.41 18218.66 380.10 o 1 5 1 2296.46 2834.18 34.48 o 2 5 1 1940.44 2022.54 24.51 o 3 5 1 85.59 133.12 10.68 o 4 5 1 1143.61 1134.75 20.20 o 5 5 1 7903.18 7366.95 88.09 o 6 5 1 0.01 -3.75 14.80 o 7 5 1 3908.43 3745.23 51.35 o 8 5 1 181.03 209.21 21.24 o 9 5 1 2942.50 2819.93 50.00 o 10 5 1 466.12 503.14 29.06 o 11 5 1 361.43 378.18 34.37 o 12 5 1 7.95 -24.55 34.05 o 13 5 1 771.14 705.04 43.47 o 14 5 1 1.78 -25.68 41.38 o 15 5 1 192.41 133.54 45.57 o 1 6 1 5479.81 6509.17 80.87 o 2 6 1 87.81 144.25 8.72 o 3 6 1 11723.18 11540.63 126.57 o 4 6 1 66.72 57.44 11.93 o 5 6 1 11615.58 11217.01 127.90 o 6 6 1 738.38 691.02 19.62 o 7 6 1 1081.48 1010.12 26.88 o 8 6 1 75.23 -21.95 21.95 o 9 6 1 289.18 282.82 25.46 o 10 6 1 11.29 25.13 26.29 o 11 6 1 3294.57 3165.45 67.68 o 12 6 1 123.20 126.58 37.63 o 13 6 1 919.06 789.94 44.33 o 14 6 1 0.39 12.96 40.74 o 15 6 1 861.56 948.93 50.82 o 0 7 1 1984.68 2315.72 69.81 o 1 7 1 8392.34 9374.88 113.28 o 2 7 1 615.47 693.00 12.68 o 3 7 1 11281.97 11797.42 129.33 o 4 7 1 26.21 27.32 14.64 o 5 7 1 9991.66 10344.69 123.74 o 6 7 1 82.73 42.01 17.15 o 7 7 1 4877.40 4907.32 69.17 o 8 7 1 777.36 761.51 27.39 o 9 7 1 2428.54 2237.52 44.40 o 10 7 1 15.06 -26.61 26.61 o 11 7 1 374.35 319.28 30.24 o 12 7 1 29.85 14.15 35.28 o 13 7 1 438.50 446.95 40.05 o 14 7 1 1.61 -42.64 42.64 o 1 8 1 7075.62 8444.26 109.98 o 2 8 1 6099.48 7136.24 75.63 o 3 8 1 6086.50 6323.69 69.68 o 4 8 1 525.75 487.02 14.85 o 5 8 1 9691.05 9948.71 121.70 o 6 8 1 943.39 925.50 24.49 o 7 8 1 2842.15 2692.12 44.47 o 8 8 1 327.37 238.77 24.04 o 9 8 1 2826.13 2649.03 47.81 o 10 8 1 50.47 65.22 26.25 o 11 8 1 2126.26 2139.85 46.32 o 12 8 1 95.38 -30.68 35.11 o 13 8 1 1023.26 1062.27 46.70 o 14 8 1 7.30 -35.91 41.31 o 0 9 1 121.84 359.84 87.40 o 1 9 1 82.28 45.16 24.26 o 2 9 1 5813.01 6399.18 62.41 o 3 9 1 5514.71 5230.06 57.02 o 4 9 1 1493.95 1659.46 25.17 o 5 9 1 103.47 133.37 17.17 o 6 9 1 151.66 77.89 26.71 o 7 9 1 74.14 88.26 20.86 o 8 9 1 8.99 -22.65 22.65 o 9 9 1 3355.96 3424.27 54.70 o 10 9 1 115.31 49.97 26.24 o 11 9 1 1184.23 1060.69 35.45 o 12 9 1 59.15 66.99 34.58 o 13 9 1 106.28 140.60 38.10 o 14 9 1 0.50 -44.98 44.98 o 1 10 1 13762.31 15285.28 297.50 o 2 10 1 124.84 127.29 11.86 o 3 10 1 255.15 251.98 15.20 o 4 10 1 1.59 -21.65 22.01 o 5 10 1 1051.25 1095.08 32.83 o 6 10 1 204.98 232.10 23.04 o 7 10 1 2819.32 2727.39 52.07 o 8 10 1 208.76 185.43 28.28 o 9 10 1 1340.18 1367.03 40.84 o 10 10 1 1.81 -31.86 31.86 o 11 10 1 1255.64 1348.73 46.00 o 12 10 1 121.74 71.40 39.65 o 13 10 1 974.09 1116.19 73.79 o 14 10 1 49.78 -196.73 196.73 o 0 11 1 270.46 280.28 64.23 o 1 11 1 1187.62 1344.47 77.59 o 2 11 1 89.08 160.94 17.61 o 3 11 1 797.68 947.28 22.12 o 4 11 1 491.94 551.69 25.40 o 5 11 1 6700.98 6508.92 113.43 o 6 11 1 23.56 -11.93 29.66 o 7 11 1 511.92 423.57 34.26 o 8 11 1 118.52 132.32 35.23 o 9 11 1 5732.02 6159.76 122.91 o 10 11 1 561.06 562.31 45.23 o 11 11 1 355.52 417.91 45.70 o 12 11 1 37.42 -47.26 47.26 o 13 11 1 1534.67 1490.46 84.69 o 1 12 1 7627.03 8691.13 230.89 o 2 12 1 273.91 296.77 23.52 o 3 12 1 3966.94 4254.47 62.84 o 4 12 1 20.50 36.42 36.91 o 5 12 1 4878.57 5025.34 91.30 o 6 12 1 412.71 426.94 30.83 o 7 12 1 1772.55 1919.09 71.52 o 8 12 1 48.87 -22.72 33.65 o 9 12 1 108.18 116.48 36.77 o 10 12 1 256.95 235.03 42.68 o 11 12 1 3370.27 3021.51 76.56 o 12 12 1 184.49 188.20 48.50 o 13 12 1 103.77 -6.88 104.48 o 0 13 1 3961.92 3931.55 178.79 o 1 13 1 942.03 1036.03 64.57 o 2 13 1 1247.91 1325.13 31.07 o 3 13 1 728.44 842.94 27.43 o 4 13 1 1174.10 1222.68 34.44 o 5 13 1 6994.07 7243.97 125.78 o 6 13 1 87.37 100.38 27.90 o 7 13 1 2441.17 2759.84 63.02 o 8 13 1 296.69 317.77 34.84 o 9 13 1 738.91 700.20 42.70 o 10 13 1 88.70 18.54 39.17 o 11 13 1 2.50 -15.75 46.07 o 12 13 1 25.82 23.31 47.69 o 1 14 1 7070.65 7565.87 209.26 o 2 14 1 357.12 398.84 23.49 o 3 14 1 3633.46 3710.99 80.97 o 4 14 1 13.10 14.79 23.44 o 5 14 1 3362.29 3429.73 67.90 o 6 14 1 170.50 165.32 32.94 o 7 14 1 1574.68 1529.22 46.99 o 8 14 1 141.76 -13.54 39.53 o 9 14 1 302.68 287.77 41.12 o 10 14 1 12.23 40.68 41.68 o 11 14 1 1947.03 1971.83 64.76 o 12 14 1 238.76 261.73 51.85 o 0 15 1 1090.38 1101.98 101.41 o 1 15 1 2109.10 2408.81 111.07 o 2 15 1 1.23 29.57 31.01 o 3 15 1 2696.92 2877.24 72.67 o 4 15 1 381.78 358.65 34.83 o 5 15 1 3468.62 3464.92 69.32 o 6 15 1 286.55 205.05 34.53 o 7 15 1 530.82 494.25 36.66 o 8 15 1 0.90 69.99 36.45 o 9 15 1 3581.32 3525.19 80.84 o 10 15 1 73.29 51.22 42.72 o 11 15 1 389.49 374.29 48.77 o 1 16 1 8690.00 8732.73 241.42 o 2 16 1 741.04 677.89 40.58 o 3 16 1 2883.42 2822.94 72.93 o 4 16 1 148.16 97.66 33.77 o 5 16 1 1674.72 1639.28 57.07 o 6 16 1 570.85 558.82 45.34 o 7 16 1 3775.08 3616.69 77.19 o 8 16 1 17.82 12.41 37.75 o 9 16 1 608.27 472.56 43.09 o 10 16 1 4.75 -28.75 43.72 o 0 17 1 4.93 165.83 127.87 o 1 17 1 1392.48 1438.11 102.82 o 2 17 1 289.30 297.35 53.94 o 3 17 1 2589.60 2407.84 65.06 o 4 17 1 32.06 45.73 34.49 o 5 17 1 1883.13 1893.76 69.59 o 6 17 1 36.11 -22.11 42.61 o 7 17 1 467.88 467.89 64.64 o 8 17 1 0.01 -44.11 44.11 o 9 17 1 2729.79 2894.88 72.48 o 10 17 1 0.02 55.91 69.37 o 1 18 1 1997.59 1985.44 116.14 o 2 18 1 353.84 247.89 57.51 o 3 18 1 1316.98 1366.94 61.83 o 4 18 1 1.39 23.18 35.20 o 5 18 1 3097.42 3005.92 83.13 o 6 18 1 131.32 185.40 46.11 o 7 18 1 573.06 619.51 55.31 o 8 18 1 135.57 100.36 53.81 o 0 19 1 124.55 0.75 158.38 o 1 19 1 104.25 186.41 112.49 o 2 19 1 22.09 -60.93 60.93 o 3 19 1 202.24 185.22 37.00 o 4 19 1 149.05 129.48 38.71 o 5 19 1 1387.07 1465.96 59.75 o 6 19 1 28.99 24.90 47.84 o 7 19 1 186.37 240.05 52.66 o 1 20 1 1488.84 1617.66 214.66 o 2 20 1 44.54 -94.52 109.70 o 3 20 1 1217.00 1172.80 54.46 o 4 20 1 1.87 -6.37 40.86 o 5 20 1 670.10 537.19 49.27 o 6 20 1 99.76 99.17 51.44 o 1 21 1 224.73 684.07 199.72 o 2 21 1 21.69 104.18 129.95 o 3 21 1 759.00 862.86 53.21 o 4 21 1 1.00 3.47 54.35 o 0 0 2 108149.76 95823.90 2147.96 o 1 0 2 15125.52 14500.58 210.70 o 2 0 2 6234.43 6197.37 92.21 o 3 0 2 653.42 553.26 44.28 o 4 0 2 22814.23 21775.34 303.39 o 5 0 2 2780.78 3442.55 73.77 o 6 0 2 284.69 361.37 23.11 o 7 0 2 17246.47 16721.54 248.58 o 8 0 2 22444.23 22095.46 410.66 o 9 0 2 4372.18 4195.60 139.09 o 10 0 2 986.03 1041.12 48.44 o 11 0 2 488.43 455.22 43.88 o 12 0 2 4594.99 4747.10 137.30 o 13 0 2 294.68 298.70 46.27 o 14 0 2 432.56 327.57 58.39 o 15 0 2 139.08 93.96 71.03 o 1 1 2 474.55 508.42 12.48 o 2 1 2 17042.66 16168.82 182.62 o 3 1 2 8396.89 8546.77 85.75 o 4 1 2 147.44 221.35 11.32 o 5 1 2 572.08 674.83 15.37 o 6 1 2 9137.75 8779.22 98.46 o 7 1 2 5159.79 5197.75 60.54 o 8 1 2 257.85 292.67 20.48 o 9 1 2 464.10 551.80 37.54 o 10 1 2 7253.27 7223.78 113.84 o 11 1 2 44.90 61.02 27.96 o 12 1 2 11.87 40.10 30.05 o 13 1 2 76.94 44.77 33.82 o 14 1 2 1773.41 1832.36 55.42 o 15 1 2 231.12 161.91 48.03 o 0 2 2 17246.15 17596.38 295.30 o 1 2 2 36.59 37.49 8.12 o 2 2 2 3503.56 3587.73 44.05 o 3 2 2 5402.20 5657.63 64.37 o 4 2 2 3149.82 2571.32 35.03 o 5 2 2 1576.57 1545.46 22.72 o 6 2 2 170.70 203.45 15.85 o 7 2 2 5634.56 5682.51 72.33 o 8 2 2 1511.22 1423.07 29.88 o 9 2 2 9.58 17.48 22.98 o 10 2 2 16.49 19.24 25.21 o 11 2 2 193.65 155.68 28.86 o 12 2 2 1086.31 1087.47 39.07 o 13 2 2 225.60 188.88 36.19 o 14 2 2 65.49 50.65 38.44 o 15 2 2 1.28 -0.59 43.87 o 1 3 2 6.36 25.91 11.43 o 2 3 2 20619.36 19909.41 215.28 o 3 3 2 4718.68 4677.71 55.22 o 4 3 2 2283.56 2154.52 29.98 o 5 3 2 3503.07 3396.85 42.08 o 6 3 2 10547.03 9776.50 108.19 o 7 3 2 2746.17 2646.88 38.70 o 8 3 2 143.33 151.75 19.82 o 9 3 2 7.26 -7.73 20.96 o 10 3 2 837.66 856.77 31.46 o 11 3 2 345.74 353.53 33.80 o 12 3 2 130.01 140.75 34.64 o 13 3 2 104.07 8.19 35.15 o 14 3 2 691.88 818.79 45.70 o 15 3 2 16.32 7.70 47.17 o 0 4 2 3531.65 3592.67 60.03 o 1 4 2 2083.74 2130.44 26.48 o 2 4 2 3648.23 4015.35 47.18 o 3 4 2 6375.52 6133.30 72.54 o 4 4 2 7073.63 6645.85 77.49 o 5 4 2 9701.24 9222.32 106.15 o 6 4 2 197.56 184.95 15.35 o 7 4 2 3588.76 3644.18 48.00 o 8 4 2 7264.86 7218.71 88.53 o 9 4 2 1529.53 1423.57 31.29 o 10 4 2 2800.34 2685.72 56.66 o 11 4 2 3.32 -30.21 30.21 o 12 4 2 2775.63 2650.37 58.27 o 13 4 2 38.78 62.21 36.25 o 14 4 2 585.68 584.11 45.02 o 15 4 2 25.85 51.20 46.07 o 1 5 2 5445.81 5477.12 61.00 o 2 5 2 9256.62 9027.81 95.15 o 3 5 2 2583.33 2630.37 29.70 o 4 5 2 236.41 229.04 15.86 o 5 5 2 166.74 196.64 14.83 o 6 5 2 5929.84 5680.78 67.49 o 7 5 2 85.69 50.41 17.48 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9 766.26 701.18 49.87 o 7 12 9 770.34 804.96 54.59 o 8 12 9 571.10 587.41 57.80 o 9 12 9 332.35 233.91 77.03 o 0 13 9 806.90 719.95 63.72 o 1 13 9 512.57 516.16 42.74 o 2 13 9 45.26 59.00 40.96 o 3 13 9 1325.76 1402.19 56.42 o 4 13 9 972.74 1016.72 50.44 o 5 13 9 924.10 815.65 48.97 o 6 13 9 1056.15 998.72 54.34 o 7 13 9 125.42 81.13 51.29 o 8 13 9 792.23 884.95 61.56 o 9 13 9 719.49 697.46 71.96 o 1 14 9 1099.83 839.75 49.71 o 2 14 9 1834.91 1871.45 63.57 o 3 14 9 462.66 550.09 47.59 o 4 14 9 0.65 78.29 41.83 o 5 14 9 492.82 491.44 47.64 o 6 14 9 781.25 850.10 54.54 o 7 14 9 853.04 717.52 73.61 o 8 14 9 199.95 279.46 57.45 o 0 15 9 644.68 666.32 64.20 o 1 15 9 628.81 687.61 47.58 o 2 15 9 4.46 3.98 43.71 o 3 15 9 1003.60 1024.05 54.27 o 4 15 9 2620.03 2550.47 103.52 o 5 15 9 917.04 974.96 55.79 o 6 15 9 43.07 41.08 48.74 o 7 15 9 62.90 -15.59 53.62 o 1 16 9 461.88 430.92 47.33 o 2 16 9 875.16 989.42 54.45 o 3 16 9 1190.82 1189.67 56.78 o 4 16 9 149.98 204.29 49.10 o 5 16 9 141.58 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653.87 58.76 o 4 9 14 85.80 80.97 65.08 o 5 9 14 304.31 442.05 125.59 o 0 10 14 6.87 66.80 110.67 o 1 10 14 409.66 510.78 62.18 o 2 10 14 36.52 41.07 58.86 o 3 10 14 302.21 406.24 124.98 o 1 0 15 21.50 -39.28 62.00 o 2 0 15 2119.90 2224.64 133.10 o 3 0 15 472.00 457.30 72.48 o 4 0 15 35.90 100.85 74.98 o 5 0 15 51.98 61.57 79.95 o 0 1 15 1554.17 1619.35 82.00 o 1 1 15 281.40 276.01 54.34 o 2 1 15 59.05 49.32 44.94 o 3 1 15 188.88 217.17 53.27 o 4 1 15 1424.94 1516.96 103.76 o 5 1 15 337.31 344.37 58.45 o 6 1 15 2.49 39.28 148.31 o 1 2 15 448.63 412.68 47.10 o 2 2 15 2067.11 2029.24 72.20 o 3 2 15 128.94 102.24 47.28 o 4 2 15 16.12 -31.93 48.17 o 5 2 15 156.31 134.44 50.03 o 6 2 15 767.96 721.92 209.68 o 0 3 15 1829.82 2264.15 157.38 o 1 3 15 110.70 135.46 45.83 o 2 3 15 151.80 173.29 46.65 o 3 3 15 87.07 -3.22 46.96 o 4 3 15 284.42 223.57 49.63 o 5 3 15 449.99 505.41 52.02 o 1 4 15 627.59 670.21 52.41 o 2 4 15 882.01 905.74 52.58 o 3 4 15 0.94 43.38 47.87 o 4 4 15 107.15 133.60 50.23 o 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