#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203173.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203173_Fobs loop_ _publ_author_name 'Ilyukhin, Andrey B.' 'Petrosyants, Svetlana P.' _publ_section_title ; The rhombohedral polymorph of scandium formate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m151 _journal_page_last m152 _journal_volume 60 _journal_year 2004 _space_group_IT_number 167 _symmetry_space_group_name_Hall '-R 3 2"c' _symmetry_space_group_name_H-M 'R -3 c :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 10.7252 _cell_length_b 10.7252 _cell_length_c 8.9854 _exptl_crystal_F_000 540.00 _reflns_d_resolution_high 0.6205 _[local]_cod_data_source_file cv6256Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Sc(HCOO)3 in R -3 c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 154.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' 'y, x, -z+1/2' '-x+y, -x, z' '-x, -x+y, -z+1/2' 'x-y, -y, -z+1/2' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' 'y+2/3, x+1/3, -z+5/6' '-x+y+2/3, -x+1/3, z+1/3' '-x+2/3, -x+y+1/3, -z+5/6' 'x-y+2/3, -y+1/3, -z+5/6' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' 'y+1/3, x+2/3, -z+7/6' '-x+y+1/3, -x+2/3, z+2/3' '-x+1/3, -x+y+2/3, -z+7/6' 'x-y+1/3, -y+2/3, -z+7/6' '-x, -y, -z' 'y, -x+y, -z' '-y, -x, z-1/2' 'x-y, x, -z' 'x, x-y, z-1/2' '-x+y, y, z-1/2' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' '-y+2/3, -x+1/3, z-1/6' 'x-y+2/3, x+1/3, -z+1/3' 'x+2/3, x-y+1/3, z-1/6' '-x+y+2/3, y+1/3, z-1/6' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' '-y+1/3, -x+2/3, z+1/6' 'x-y+1/3, x+2/3, -z+2/3' 'x+1/3, x-y+2/3, z+1/6' '-x+y+1/3, y+2/3, z+1/6' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 2 0 20014.10 17809.63 433.19 o 0 3 0 654.40 596.68 12.65 o -2 4 0 1024.42 1443.23 14.50 o -1 5 0 12326.75 12759.37 148.93 o -3 6 0 469.08 404.57 7.29 o 0 6 0 24021.39 27021.34 470.79 o -2 7 0 4244.32 4502.64 43.52 o -4 8 0 738.42 762.74 14.06 o -1 8 0 2533.85 2537.06 21.62 o -3 9 0 689.30 668.04 9.53 o 0 9 0 1177.91 1162.05 19.40 o -5 10 0 2213.51 2375.39 27.73 o -2 10 0 201.69 211.54 3.78 o -4 11 0 779.01 813.34 12.87 o -1 11 0 610.65 624.72 8.35 o -6 12 0 1553.42 1552.95 21.85 o -3 12 0 395.65 419.08 9.37 o 0 12 0 707.72 708.14 14.74 o -5 13 0 992.98 990.22 16.23 o -2 13 0 373.10 395.66 5.37 o -7 14 0 390.31 366.42 7.41 o -4 14 0 487.19 523.10 7.68 o -1 14 0 437.14 418.01 6.73 o -6 15 0 189.23 187.08 3.62 o -3 15 0 79.78 93.58 3.07 o -8 16 0 26.88 31.33 5.79 o -5 16 0 65.22 75.19 5.32 o -7 17 0 71.81 72.58 3.38 o -2 3 1 18805.91 16243.53 405.66 o -1 4 1 9044.80 10346.83 206.21 o -3 5 1 1964.31 2364.13 23.61 o -5 6 1 56.03 54.09 2.78 o -2 6 1 60.39 80.66 1.73 o -4 7 1 3075.87 3289.55 21.95 o -1 7 1 582.12 587.99 11.57 o -6 8 1 0.63 -1.16 2.11 o -3 8 1 246.86 276.47 4.78 o -8 9 1 187.22 224.86 27.81 o -5 9 1 445.00 438.44 4.87 o -2 9 1 415.67 462.06 5.99 o -7 10 1 57.03 67.49 1.62 o -4 10 1 56.09 59.99 4.92 o -1 10 1 92.09 88.23 1.88 o -9 11 1 38.75 20.92 2.51 o -6 11 1 81.06 97.61 1.69 o -3 11 1 23.49 31.05 1.78 o -11 12 1 19.13 6.68 3.62 o -8 12 1 29.86 25.21 2.12 o -5 12 1 1.15 7.19 3.93 o -2 12 1 138.52 123.18 2.42 o -10 13 1 5.66 4.35 3.39 o -7 13 1 89.16 94.91 2.77 o -4 13 1 34.22 31.55 2.68 o -1 13 1 37.43 34.72 4.26 o -12 14 1 43.06 46.77 3.36 o -9 14 1 12.02 10.51 4.46 o -6 14 1 26.77 27.13 3.29 o -3 14 1 2.50 7.27 4.52 o -14 15 1 0.03 -5.35 5.90 o -11 15 1 51.78 44.59 4.67 o -8 15 1 29.67 39.94 2.85 o -5 15 1 13.83 10.86 3.70 o -2 15 1 11.30 7.83 5.67 o -13 16 1 4.50 2.01 4.37 o -10 16 1 5.27 10.35 5.44 o -7 16 1 0.00 -2.17 6.08 o -4 16 1 15.37 13.88 3.51 o -9 17 1 2.89 -4.52 5.54 o -6 17 1 45.22 54.25 5.31 o 0 1 2 2883.17 2806.04 77.43 o -2 2 2 18167.12 17983.42 616.19 o -1 3 2 11197.39 11246.29 220.05 o -3 4 2 10148.32 10374.33 128.04 o 0 4 2 174.97 201.60 6.40 o -5 5 2 1729.51 1704.85 28.44 o -2 5 2 6345.02 6603.40 93.39 o -4 6 2 4580.98 4637.96 55.31 o -1 6 2 2665.09 2515.77 37.87 o -6 7 2 2644.24 2637.76 33.26 o -3 7 2 4934.49 4915.26 80.70 o 0 7 2 2556.28 2524.22 55.57 o -8 8 2 2196.49 2311.74 29.79 o -5 8 2 1161.10 1163.66 12.90 o -2 8 2 4625.14 4908.09 42.18 o -7 9 2 1493.73 1516.72 19.26 o -4 9 2 1037.30 1044.48 14.38 o -1 9 2 408.41 415.29 8.52 o -9 10 2 1006.57 969.83 12.40 o -6 10 2 319.20 306.46 3.88 o -3 10 2 2373.84 2387.84 21.22 o 0 10 2 20.26 21.97 3.12 o -11 11 2 841.50 825.75 21.62 o -8 11 2 1017.08 1008.86 14.59 o -5 11 2 1214.04 1195.42 15.41 o -2 11 2 821.34 812.33 17.52 o -10 12 2 700.71 691.04 10.65 o -7 12 2 807.21 837.47 8.47 o -4 12 2 1005.33 1000.46 11.25 o -1 12 2 774.53 795.10 14.22 o -12 13 2 253.05 258.79 4.29 o -9 13 2 197.34 205.43 3.37 o -6 13 2 567.28 585.93 8.46 o -3 13 2 429.85 445.36 6.28 o 0 13 2 176.88 179.98 4.93 o -14 14 2 44.97 48.48 4.90 o -11 14 2 179.32 166.69 3.63 o -8 14 2 355.46 374.75 4.79 o -5 14 2 19.46 13.36 3.05 o -2 14 2 394.79 422.82 6.14 o -13 15 2 141.16 128.76 3.57 o -10 15 2 187.86 196.63 4.64 o -7 15 2 237.38 218.37 4.82 o -4 15 2 200.97 205.12 4.02 o -1 15 2 36.34 32.54 5.68 o -12 16 2 195.07 197.16 4.28 o -9 16 2 382.87 375.14 8.72 o -6 16 2 120.23 130.71 3.43 o -3 16 2 236.68 235.69 4.73 o -8 17 2 121.29 131.83 4.90 o -1 2 3 23.28 34.29 4.42 o -2 4 3 3763.06 4115.94 53.93 o -4 5 3 1170.99 1209.25 12.81 o -1 5 3 164.83 185.40 5.39 o -3 6 3 1186.44 1247.55 22.51 o -5 7 3 39.17 49.24 5.04 o -2 7 3 1499.48 1439.66 13.50 o -7 8 3 20.81 21.72 1.62 o -4 8 3 907.45 830.62 10.94 o -1 8 3 281.86 281.87 8.22 o -6 9 3 23.59 28.60 1.36 o -3 9 3 121.59 131.94 2.01 o -8 10 3 535.69 511.40 7.42 o -5 10 3 14.23 17.27 1.66 o -2 10 3 626.44 594.81 7.48 o -10 11 3 5.39 9.31 3.54 o -7 11 3 84.63 92.05 2.20 o -4 11 3 545.49 583.51 7.91 o -1 11 3 3.17 12.19 3.79 o -9 12 3 13.08 8.89 2.71 o -6 12 3 85.59 73.03 1.95 o -3 12 3 50.66 49.76 2.53 o -11 13 3 51.05 59.76 4.32 o -8 13 3 104.63 104.47 2.19 o -5 13 3 0.03 0.36 4.09 o -2 13 3 279.09 293.52 6.31 o -13 14 3 4.45 8.92 6.33 o -10 14 3 32.66 38.49 2.83 o -7 14 3 4.08 0.06 4.53 o -4 14 3 49.12 55.98 3.75 o -1 14 3 3.03 3.54 3.47 o -12 15 3 35.27 32.93 5.25 o -9 15 3 0.16 -0.34 4.94 o -6 15 3 3.97 0.58 4.37 o -3 15 3 6.49 13.96 3.66 o -11 16 3 0.85 -6.59 6.59 o -8 16 3 74.42 72.32 3.06 o -5 16 3 1.11 -0.39 6.66 o -1 1 4 30.80 195.45 14.57 o 0 2 4 3726.84 3383.18 79.59 o -2 3 4 9658.63 9637.57 144.19 o -4 4 4 10771.61 11198.50 180.52 o -1 4 4 13923.55 14315.07 233.73 o -3 5 4 7646.96 7486.92 177.05 o 0 5 4 1593.56 1562.74 52.11 o -5 6 4 174.64 182.64 2.61 o -2 6 4 2324.36 2342.42 45.38 o -7 7 4 9.47 31.75 8.83 o -4 7 4 3097.58 3052.58 49.29 o -1 7 4 26.10 26.01 1.38 o -6 8 4 719.02 698.33 9.41 o -3 8 4 3038.56 2875.03 37.09 o 0 8 4 1318.25 1411.09 35.14 o -8 9 4 2412.55 2411.72 27.23 o -5 9 4 5136.52 4979.13 64.84 o -2 9 4 1476.74 1418.11 29.13 o -10 10 4 1879.01 1848.50 30.76 o -7 10 4 1439.90 1348.93 21.95 o -4 10 4 1935.01 1978.54 32.73 o -1 10 4 2596.79 2552.37 32.59 o -9 11 4 839.14 811.81 11.79 o -6 11 4 313.94 324.81 4.69 o -3 11 4 566.46 555.44 9.10 o 0 11 4 274.81 261.21 8.77 o -11 12 4 43.48 40.20 3.40 o -8 12 4 271.22 261.46 3.77 o -5 12 4 27.77 29.74 2.07 o -2 12 4 251.68 246.26 3.57 o -13 13 4 154.80 169.88 5.12 o -10 13 4 405.40 371.29 5.56 o -7 13 4 41.36 49.36 3.84 o -4 13 4 611.90 583.36 9.00 o -1 13 4 50.12 53.36 3.81 o -12 14 4 137.70 138.79 3.60 o -9 14 4 805.55 777.83 13.29 o -6 14 4 359.08 375.39 5.69 o -3 14 4 276.50 263.73 4.47 o 0 14 4 338.60 383.55 7.57 o -11 15 4 313.16 296.39 5.79 o -8 15 4 277.38 317.38 5.34 o -5 15 4 565.06 516.08 11.46 o -2 15 4 153.82 167.53 3.72 o -10 16 4 189.74 192.60 3.73 o -7 16 4 197.41 200.55 4.98 o -1 3 5 334.77 350.30 6.73 o -3 4 5 859.11 941.12 10.91 o -2 5 5 3155.31 3222.06 59.98 o -4 6 5 75.71 86.54 2.31 o -1 6 5 33.05 34.93 2.76 o -6 7 5 632.61 633.39 7.86 o -3 7 5 3.04 3.25 2.08 o -5 8 5 1040.33 1014.62 16.40 o -2 8 5 274.31 268.54 6.06 o -7 9 5 0.05 -2.82 2.93 o -4 9 5 369.51 362.82 5.17 o -1 9 5 43.86 46.95 3.50 o -9 10 5 113.74 100.02 2.53 o -6 10 5 32.57 34.99 3.71 o -3 10 5 199.57 191.74 4.38 o -8 11 5 761.22 719.49 10.76 o -5 11 5 3.17 2.86 3.40 o -2 11 5 238.05 221.64 3.24 o -10 12 5 46.45 57.66 2.22 o -7 12 5 16.24 16.82 2.94 o -4 12 5 24.29 23.34 2.33 o -1 12 5 19.43 18.60 3.53 o -12 13 5 74.92 76.42 2.85 o -9 13 5 0.84 -0.41 3.92 o -6 13 5 108.59 99.30 2.76 o -3 13 5 21.55 29.41 4.46 o -11 14 5 70.27 66.28 3.18 o -8 14 5 1.72 -1.56 5.35 o -5 14 5 30.84 32.13 3.20 o -2 14 5 0.64 -4.00 5.02 o -10 15 5 12.19 13.00 3.85 o -7 15 5 19.92 12.70 4.68 o -4 15 5 0.67 7.35 4.88 o -9 16 5 10.56 5.97 5.67 o -6 16 5 1.85 0.28 4.44 o 0 0 6 1386.77 1436.68 31.11 o -1 2 6 5327.17 5328.03 65.26 o -3 3 6 1635.65 1511.64 30.09 o 0 3 6 4938.52 4377.53 114.22 o -2 4 6 4046.47 3951.08 46.56 o -4 5 6 628.71 641.27 7.78 o -1 5 6 1551.56 1516.01 34.65 o -6 6 6 1751.94 1705.38 33.04 o -3 6 6 3003.18 2865.26 69.76 o 0 6 6 1542.39 1592.68 41.16 o -5 7 6 3189.59 3065.81 49.92 o -2 7 6 1829.69 1789.48 28.49 o -7 8 6 1907.07 1837.94 20.42 o -4 8 6 927.36 918.72 12.16 o -1 8 6 2032.69 1971.69 29.39 o -9 9 6 4.99 6.86 3.93 o -6 9 6 1606.07 1588.71 27.14 o -3 9 6 429.38 425.91 9.74 o 0 9 6 656.62 662.13 22.25 o -8 10 6 706.53 724.35 8.93 o -5 10 6 178.49 171.05 4.22 o -2 10 6 804.22 830.20 13.21 o -10 11 6 200.29 206.21 4.79 o -7 11 6 1142.88 1089.18 14.66 o -4 11 6 475.28 487.80 7.12 o -1 11 6 491.85 486.99 9.99 o -12 12 6 481.69 448.36 14.53 o -9 12 6 588.78 571.13 9.16 o -6 12 6 767.06 745.07 10.55 o -3 12 6 437.82 409.57 11.37 o 0 12 6 328.88 345.53 6.99 o -11 13 6 518.48 494.92 15.04 o -8 13 6 284.95 257.35 4.91 o -5 13 6 350.86 356.48 5.15 o -2 13 6 295.31 276.23 6.69 o -13 14 6 123.84 123.55 3.58 o -10 14 6 81.91 90.37 3.85 o -7 14 6 401.72 377.06 7.53 o -4 14 6 101.53 105.47 3.38 o -1 14 6 97.61 105.00 3.40 o -9 15 6 52.87 51.30 3.05 o -6 15 6 246.24 266.40 5.43 o -2 3 7 2147.80 2045.60 18.03 o -1 4 7 844.04 775.08 10.06 o -3 5 7 343.10 302.73 3.82 o -5 6 7 85.80 89.78 1.54 o -2 6 7 290.62 259.25 5.88 o -4 7 7 442.99 431.74 9.27 o -1 7 7 4.28 8.02 3.38 o -6 8 7 323.43 304.33 4.57 o -3 8 7 254.57 240.64 4.18 o -8 9 7 116.46 115.49 2.09 o -5 9 7 46.86 48.18 1.87 o -2 9 7 102.15 94.61 2.08 o -7 10 7 0.02 3.71 3.80 o -4 10 7 1.13 4.78 3.82 o -1 10 7 19.64 22.07 2.30 o -9 11 7 2.08 -0.35 3.46 o -6 11 7 2.84 3.09 4.41 o -3 11 7 1.25 4.22 3.91 o -11 12 7 58.32 52.00 5.14 o -8 12 7 67.30 66.34 4.63 o -5 12 7 67.77 73.50 3.44 o -2 12 7 3.95 -1.44 3.74 o -10 13 7 0.77 -3.56 4.51 o -7 13 7 6.16 -0.40 4.47 o -4 13 7 3.35 -5.22 5.22 o -1 13 7 0.15 -1.14 4.31 o -9 14 7 30.94 25.97 4.02 o -6 14 7 0.30 -3.25 4.49 o -3 14 7 35.67 29.12 4.74 o -8 15 7 14.84 4.38 9.35 o 0 1 8 11268.08 10448.70 235.29 o -2 2 8 1854.95 1813.39 29.13 o -1 3 8 273.38 282.44 4.29 o -3 4 8 691.64 699.96 16.22 o 0 4 8 2544.90 2461.58 54.00 o -5 5 8 6553.00 6180.16 227.99 o -2 5 8 397.03 389.23 4.80 o -4 6 8 1329.20 1318.49 13.81 o -1 6 8 4294.60 4058.21 77.63 o -6 7 8 2484.27 2414.61 29.30 o -3 7 8 423.79 432.65 7.16 o 0 7 8 2329.04 2198.26 50.98 o -8 8 8 843.89 818.18 19.72 o -5 8 8 503.60 495.41 12.70 o -2 8 8 710.88 713.78 11.42 o -7 9 8 236.93 226.62 4.11 o -4 9 8 801.79 809.45 13.42 o -1 9 8 460.54 464.60 8.61 o -9 10 8 458.76 420.99 8.57 o -6 10 8 610.77 627.55 10.05 o -3 10 8 234.36 223.56 3.73 o 0 10 8 457.59 454.54 20.67 o -11 11 8 458.96 433.64 9.20 o -8 11 8 145.10 148.87 4.48 o -5 11 8 891.51 828.56 14.47 o -2 11 8 166.75 174.41 4.84 o -10 12 8 248.82 269.27 5.14 o -7 12 8 543.67 515.83 9.22 o -4 12 8 421.60 429.46 7.64 o -1 12 8 281.73 269.93 5.79 o -9 13 8 400.82 393.77 11.83 o -6 13 8 508.15 504.10 8.93 o -3 13 8 262.89 270.73 5.94 o -8 14 8 265.93 259.60 4.77 o -5 14 8 365.14 377.98 6.09 o -1 2 9 441.95 451.93 6.93 o -2 4 9 1635.41 1499.45 19.45 o -4 5 9 39.39 40.34 1.77 o -1 5 9 172.94 170.31 3.79 o -3 6 9 58.64 59.26 1.50 o -5 7 9 66.46 63.45 2.13 o -2 7 9 4.25 8.41 3.09 o -7 8 9 55.37 53.33 3.09 o -4 8 9 378.36 357.38 5.22 o -1 8 9 119.38 110.72 2.48 o -6 9 9 1.03 1.91 3.84 o -3 9 9 2.54 6.02 3.77 o -8 10 9 25.18 24.21 4.67 o -5 10 9 19.00 15.17 4.05 o -2 10 9 14.16 15.53 4.80 o -10 11 9 16.66 14.81 3.70 o -7 11 9 15.76 12.97 4.15 o -4 11 9 12.10 14.04 3.92 o -1 11 9 53.03 53.83 2.78 o -9 12 9 3.70 1.54 4.54 o -6 12 9 66.29 75.55 2.84 o -3 12 9 3.15 1.33 6.39 o -8 13 9 6.30 11.23 6.33 o -5 13 9 1.27 -0.19 7.04 o -1 1 10 610.21 578.63 17.94 o 0 2 10 1355.24 1402.87 34.05 o -2 3 10 2279.75 2219.69 23.53 o -4 4 10 978.93 944.01 20.04 o -1 4 10 977.78 968.96 10.26 o -3 5 10 1621.03 1620.10 31.83 o 0 5 10 252.48 264.76 5.63 o -5 6 10 569.02 577.77 13.85 o -2 6 10 1177.09 1189.96 20.20 o -7 7 10 675.15 700.30 15.15 o -4 7 10 954.76 947.59 12.41 o -1 7 10 863.14 866.64 22.40 o -6 8 10 564.55 580.45 7.94 o -3 8 10 923.73 881.38 17.68 o 0 8 10 183.02 179.08 4.74 o -8 9 10 470.15 449.73 6.08 o -5 9 10 189.30 177.15 3.39 o -2 9 10 716.08 699.79 11.21 o -10 10 10 375.01 384.63 7.63 o -7 10 10 423.35 406.52 11.94 o -4 10 10 581.74 599.58 8.94 o -1 10 10 106.53 102.80 2.87 o -9 11 10 449.57 434.75 8.99 o -6 11 10 367.30 393.72 7.38 o -3 11 10 653.99 648.01 9.71 o -8 12 10 271.51 277.73 8.23 o -5 12 10 401.93 410.12 9.74 o -1 3 11 0.02 -4.16 4.16 o -3 4 11 44.86 49.99 6.02 o -2 5 11 111.70 122.02 2.78 o -4 6 11 76.20 73.75 2.68 o -1 6 11 44.41 48.74 2.66 o -6 7 11 16.66 18.28 3.52 o -3 7 11 23.97 26.67 2.42 o -5 8 11 33.28 40.43 2.60 o -2 8 11 181.69 193.77 4.91 o -7 9 11 13.97 22.06 4.05 o -4 9 11 26.47 31.17 5.40 o -1 9 11 4.99 1.72 7.72 o -9 10 11 24.59 30.15 4.30 o -6 10 11 6.54 -2.64 6.37 o -3 10 11 119.36 142.46 3.50 o -5 11 11 3.89 10.45 6.38 o 0 0 12 238.35 266.45 8.89 o -1 2 12 523.16 507.13 7.20 o -3 3 12 1303.07 1293.98 39.47 o 0 3 12 1471.83 1455.31 27.94 o -2 4 12 1292.32 1336.06 19.97 o -4 5 12 898.21 919.93 11.69 o -1 5 12 1025.14 1036.69 18.37 o -6 6 12 56.41 60.12 5.24 o -3 6 12 632.42 633.83 11.41 o 0 6 12 63.07 58.62 3.10 o -5 7 12 247.11 241.09 4.24 o -2 7 12 229.75 227.57 3.40 o -7 8 12 207.50 222.01 5.12 o -4 8 12 1010.40 1059.24 18.81 o -1 8 12 177.12 181.82 5.20 o -6 9 12 646.85 689.97 11.79 o -3 9 12 556.51 589.14 11.87 o -2 3 13 2.13 9.60 3.81 o -1 4 13 51.63 59.86 4.34 o -3 5 13 172.24 186.84 3.57 o -5 6 13 6.04 9.79 3.56 o -2 6 13 75.95 81.35 3.74 o -4 7 13 2.83 -7.23 7.23 o -1 7 13 27.60 36.27 3.81 o 0 1 14 565.39 570.18 12.68 o -2 2 14 702.06 766.00 16.38 o -1 3 14 821.10 864.76 12.20 o -3 4 14 312.70 333.07 5.01 o