#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/32/2203213.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203213_Fobs loop_ _publ_author_name 'Baby Mariyatra, Mahimaidoss' 'Spencer, Elinor C.' 'Panchanatheswaran, Krishanaswamy' 'Howard, Judith A. K.' _publ_section_title ; Benzoylmethyltriphenylphosphonium hydrogen maleate: supramolecular layer formation due to C---H···O interactions ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o162 _journal_page_last o164 _journal_volume 60 _journal_year 2004 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.5582 _cell_length_b 19.5961 _cell_length_c 24.0030 _exptl_crystal_F_000 2080.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file ob6335Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 03ecs014 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 371.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 306.52 260.27 17.77 o 4 0 0 6849.95 7468.29 425.00 o 6 0 0 2378.03 2188.04 130.14 o 8 0 0 294.04 272.56 26.95 o 10 0 0 3618.67 3255.54 195.15 o 12 0 0 286.92 339.36 58.96 o 2 1 0 2222.30 2128.43 77.29 o 4 1 0 14371.28 14464.44 579.81 o 6 1 0 2428.54 2534.29 105.69 o 8 1 0 1206.05 1176.76 53.50 o 10 1 0 0.66 -5.83 13.28 o 12 1 0 0.89 -35.55 48.89 o 0 2 0 4003.09 3800.65 135.35 o 2 2 0 9838.45 10158.98 362.63 o 4 2 0 113.45 102.04 11.95 o 6 2 0 8800.17 9277.08 374.21 o 8 2 0 1776.61 1762.96 76.88 o 10 2 0 273.12 225.02 24.92 o 12 2 0 317.01 328.41 45.30 o 2 3 0 58708.78 60329.48 2145.42 o 4 3 0 1799.39 1664.87 69.91 o 6 3 0 4565.03 4722.21 192.68 o 8 3 0 4329.48 4244.85 175.24 o 10 3 0 1548.20 1479.26 79.85 o 12 3 0 1977.77 2168.81 141.84 o 0 4 0 19844.48 20233.22 797.53 o 2 4 0 86.33 103.88 9.86 o 4 4 0 1363.16 1545.31 65.06 o 6 4 0 5.91 11.88 9.86 o 8 4 0 70.61 38.01 12.66 o 10 4 0 1244.36 1231.50 74.37 o 12 4 0 1289.81 1542.32 106.75 o 2 5 0 947.64 777.15 30.20 o 4 5 0 488.78 652.52 30.87 o 6 5 0 1746.81 1832.77 91.04 o 8 5 0 459.54 395.54 24.25 o 10 5 0 93.06 111.62 21.79 o 12 5 0 158.93 212.61 36.67 o 0 6 0 102.24 127.34 10.43 o 2 6 0 360.49 340.13 16.76 o 4 6 0 996.71 1213.60 53.01 o 6 6 0 435.94 378.83 22.44 o 8 6 0 3056.83 2968.29 124.70 o 10 6 0 139.46 136.19 22.29 o 12 6 0 30.55 -18.36 22.04 o 2 7 0 6727.25 7025.36 252.16 o 4 7 0 28.13 62.35 10.69 o 6 7 0 289.61 463.12 33.59 o 8 7 0 2036.64 1929.30 84.03 o 10 7 0 15.91 -11.26 27.51 o 12 7 0 430.35 454.98 85.27 o 0 8 0 9938.24 10328.48 475.87 o 2 8 0 2.58 3.09 6.90 o 4 8 0 6426.69 6952.67 250.89 o 6 8 0 6077.00 5999.88 243.88 o 8 8 0 1916.62 1973.41 101.26 o 10 8 0 950.65 933.05 56.06 o 12 8 0 375.95 425.81 50.54 o 2 9 0 9425.53 9837.89 352.72 o 4 9 0 387.97 263.79 15.43 o 6 9 0 170.44 211.14 18.00 o 8 9 0 2579.52 2523.12 126.17 o 10 9 0 1782.18 1856.60 98.75 o 12 9 0 0.74 30.69 23.46 o 0 10 0 279.21 334.82 20.88 o 2 10 0 5.02 11.70 7.85 o 4 10 0 1609.89 2048.80 77.27 o 6 10 0 292.29 279.80 20.65 o 8 10 0 2776.09 2693.97 134.46 o 10 10 0 520.92 488.73 55.29 o 12 10 0 55.04 33.55 25.49 o 2 11 0 4235.71 4460.45 162.52 o 4 11 0 462.86 408.35 20.52 o 6 11 0 786.04 760.76 38.93 o 8 11 0 3.90 -10.68 17.43 o 10 11 0 512.40 522.43 40.36 o 12 11 0 333.56 316.68 73.63 o 0 12 0 1394.70 1479.73 73.53 o 2 12 0 6147.00 6092.84 220.39 o 4 12 0 2747.37 3024.46 112.51 o 6 12 0 4714.84 4638.42 191.38 o 8 12 0 1087.12 1260.19 60.70 o 10 12 0 1.80 6.04 21.48 o 12 12 0 35.64 45.52 30.62 o 2 13 0 6088.00 6468.68 212.06 o 4 13 0 537.97 553.49 28.05 o 6 13 0 1226.19 1233.68 57.99 o 8 13 0 604.39 540.26 33.92 o 10 13 0 12.38 12.90 20.29 o 0 14 0 1450.58 1530.48 76.79 o 2 14 0 2788.19 3003.15 101.06 o 4 14 0 3132.06 3226.29 120.21 o 6 14 0 16.96 18.22 18.26 o 8 14 0 184.85 140.53 20.32 o 10 14 0 181.61 150.42 34.70 o 2 15 0 664.13 576.93 24.53 o 4 15 0 1150.50 1116.21 46.31 o 6 15 0 1587.78 1703.97 68.46 o 8 15 0 14.80 22.44 18.18 o 10 15 0 2313.52 2414.46 156.59 o 0 16 0 282.06 282.23 23.43 o 2 16 0 3244.67 3477.52 129.30 o 4 16 0 179.34 211.53 23.20 o 6 16 0 882.17 844.48 44.86 o 8 16 0 811.69 922.00 59.05 o 10 16 0 122.30 144.91 34.57 o 2 17 0 2333.72 2491.05 95.51 o 4 17 0 1319.18 1250.71 52.46 o 6 17 0 586.44 599.57 45.45 o 8 17 0 223.70 225.70 28.96 o 10 17 0 18.99 49.09 37.10 o 0 18 0 153.77 138.95 46.01 o 2 18 0 22.26 14.21 13.88 o 4 18 0 91.38 47.80 14.74 o 6 18 0 1350.39 1363.99 65.86 o 8 18 0 455.99 524.90 46.08 o 2 19 0 992.12 1053.82 53.28 o 4 19 0 259.12 204.79 19.63 o 6 19 0 0.06 2.04 19.07 o 8 19 0 202.09 201.51 31.26 o 0 20 0 1168.78 1106.25 78.68 o 2 20 0 618.83 615.20 37.27 o 4 20 0 444.17 384.77 24.77 o 6 20 0 545.11 525.11 35.24 o 8 20 0 45.30 13.80 27.89 o 2 21 0 1466.39 1579.56 92.15 o 4 21 0 572.59 578.28 37.77 o 6 21 0 96.37 111.44 25.25 o 0 22 0 816.50 662.23 56.91 o 2 22 0 909.70 907.30 58.32 o 4 22 0 884.32 865.44 48.01 o 6 22 0 18.28 55.43 31.47 o 2 23 0 3009.31 3195.55 139.43 o 4 23 0 8.47 -21.62 24.08 o 0 24 0 71.52 135.27 32.11 o 2 24 0 185.68 140.09 29.06 o 4 24 0 6.03 -13.20 25.69 o 2 25 0 7.15 -1.92 29.71 o 1 1 1 8886.91 8852.97 188.23 o 2 1 1 37358.32 36393.06 967.32 o 3 1 1 209.66 189.33 8.04 o 4 1 1 6.85 -0.99 4.80 o 5 1 1 18.04 17.67 5.77 o 6 1 1 2282.92 2297.74 68.12 o 7 1 1 529.26 490.53 18.38 o 8 1 1 120.80 98.04 9.20 o 9 1 1 183.70 177.22 12.10 o 10 1 1 14.77 0.88 9.77 o 11 1 1 42.64 18.89 24.86 o 12 1 1 0.22 9.35 20.94 o 13 1 1 439.87 473.25 37.70 o 0 2 1 4275.01 3845.88 108.48 o 1 2 1 746.45 750.95 14.67 o 2 2 1 526.99 545.77 16.07 o 3 2 1 4172.98 4178.30 127.40 o 4 2 1 55.46 51.68 7.41 o 5 2 1 436.19 454.04 16.02 o 6 2 1 13959.22 14676.31 416.67 o 7 2 1 292.09 294.83 13.08 o 8 2 1 611.74 532.31 20.38 o 9 2 1 5033.70 5171.37 150.73 o 10 2 1 334.71 294.52 17.37 o 11 2 1 50.36 32.78 16.66 o 12 2 1 795.04 959.29 53.31 o 13 2 1 32.98 32.53 29.47 o 1 3 1 14487.88 14368.90 305.68 o 2 3 1 6355.96 6714.11 162.05 o 3 3 1 8247.10 8461.22 225.51 o 4 3 1 287.60 312.24 11.86 o 5 3 1 349.17 374.50 14.27 o 6 3 1 2653.59 2855.26 83.75 o 7 3 1 7.09 5.10 6.78 o 8 3 1 366.38 280.60 19.50 o 9 3 1 1662.37 1476.43 47.12 o 10 3 1 23.35 15.19 13.24 o 11 3 1 8.26 28.83 13.99 o 12 3 1 2829.48 3071.93 135.69 o 13 3 1 12.27 -4.94 22.45 o 0 4 1 4711.04 4759.29 142.94 o 1 4 1 15356.83 15118.44 333.89 o 2 4 1 38.45 8.51 3.97 o 3 4 1 1805.87 1971.67 54.16 o 4 4 1 934.53 847.21 25.33 o 5 4 1 353.01 460.40 16.69 o 6 4 1 9613.99 9713.66 296.11 o 7 4 1 66.76 57.58 7.87 o 8 4 1 1604.53 1542.93 48.23 o 9 4 1 45.33 20.60 8.55 o 10 4 1 11.58 -2.53 13.67 o 11 4 1 230.31 211.34 24.43 o 12 4 1 1720.75 1862.63 87.69 o 13 4 1 129.54 161.85 27.44 o 1 5 1 27.11 17.60 5.44 o 2 5 1 2975.87 2902.23 70.89 o 3 5 1 4027.07 4349.46 111.03 o 4 5 1 38.99 6.02 5.60 o 5 5 1 102.91 86.01 7.36 o 6 5 1 119.19 129.05 10.18 o 7 5 1 1619.97 1491.87 49.56 o 8 5 1 4712.67 4701.34 137.06 o 9 5 1 4.77 10.91 10.18 o 10 5 1 36.01 41.63 13.72 o 11 5 1 70.51 29.84 14.72 o 12 5 1 148.66 138.11 21.73 o 13 5 1 94.99 104.21 25.65 o 0 6 1 20151.21 21022.29 628.51 o 1 6 1 18.12 11.56 3.52 o 2 6 1 412.43 386.42 11.30 o 3 6 1 100.73 114.39 7.14 o 4 6 1 8207.62 9043.87 256.26 o 5 6 1 803.00 765.65 25.65 o 6 6 1 400.77 458.81 19.89 o 7 6 1 1161.59 1204.37 46.40 o 8 6 1 248.07 232.07 16.37 o 9 6 1 67.95 49.64 10.98 o 10 6 1 226.03 206.32 17.99 o 11 6 1 84.03 84.49 16.62 o 12 6 1 116.29 120.50 22.25 o 13 6 1 1.05 25.69 24.05 o 1 7 1 3228.12 3240.99 75.50 o 2 7 1 33.44 30.40 5.30 o 3 7 1 223.86 260.68 9.80 o 5 7 1 96.96 85.87 10.63 o 6 7 1 510.18 516.89 19.86 o 7 7 1 547.48 506.72 21.93 o 8 7 1 1834.15 1846.78 66.81 o 9 7 1 6.54 -1.26 11.82 o 10 7 1 74.51 64.19 14.05 o 11 7 1 755.66 808.97 47.05 o 12 7 1 10.99 5.17 16.44 o 13 7 1 109.13 122.22 30.51 o 0 8 1 220.62 287.32 12.53 o 1 8 1 1019.53 1069.68 26.09 o 2 8 1 2780.10 2811.11 69.27 o 3 8 1 1278.15 1542.38 41.45 o 4 8 1 1897.17 1818.89 48.64 o 5 8 1 151.61 219.55 11.64 o 6 8 1 349.40 322.36 15.22 o 7 8 1 33.17 40.19 10.94 o 8 8 1 2814.99 2686.02 94.11 o 9 8 1 132.29 125.78 14.87 o 10 8 1 22.98 14.45 12.81 o 11 8 1 61.86 43.88 14.91 o 12 8 1 36.04 31.38 16.71 o 13 8 1 0.62 7.35 23.84 o 1 9 1 207.16 235.78 8.41 o 2 9 1 17.89 22.75 4.91 o 3 9 1 5408.16 5847.17 149.44 o 4 9 1 59.08 59.55 6.54 o 5 9 1 8.39 -7.46 7.46 o 6 9 1 744.99 749.07 26.57 o 7 9 1 916.65 877.66 30.98 o 8 9 1 1112.98 1014.93 37.80 o 9 9 1 409.64 399.32 25.36 o 10 9 1 10.66 -12.39 12.39 o 11 9 1 86.59 44.88 17.15 o 12 9 1 63.26 33.24 18.25 o 0 10 1 3510.01 3339.33 111.00 o 1 10 1 528.11 503.62 13.35 o 2 10 1 2736.03 2969.10 73.44 o 3 10 1 5615.74 5630.54 144.21 o 4 10 1 1058.26 1003.76 28.61 o 5 10 1 718.22 758.71 24.67 o 6 10 1 67.04 109.32 10.88 o 7 10 1 774.87 829.78 30.08 o 8 10 1 387.39 323.96 19.60 o 9 10 1 34.01 18.18 13.24 o 10 10 1 475.55 472.15 26.26 o 11 10 1 52.91 87.54 28.48 o 12 10 1 170.28 119.24 19.52 o 1 11 1 177.28 164.56 6.88 o 2 11 1 410.01 349.26 11.72 o 3 11 1 613.86 576.77 18.10 o 4 11 1 727.74 701.94 21.70 o 5 11 1 695.94 707.60 22.28 o 6 11 1 119.84 100.41 10.54 o 7 11 1 2328.60 2422.78 73.94 o 8 11 1 46.77 35.30 11.92 o 9 11 1 267.74 249.06 22.34 o 10 11 1 1094.39 1026.16 43.57 o 11 11 1 53.86 30.26 18.43 o 12 11 1 127.46 145.99 21.39 o 0 12 1 1165.51 1198.00 42.78 o 1 12 1 946.23 985.10 25.30 o 2 12 1 1834.91 1885.05 47.98 o 3 12 1 14.14 4.43 6.28 o 4 12 1 22.18 8.53 6.95 o 5 12 1 855.78 913.41 27.53 o 6 12 1 187.98 175.75 12.31 o 7 12 1 1.55 -10.06 10.54 o 8 12 1 117.33 101.43 13.45 o 9 12 1 0.00 -12.96 12.96 o 10 12 1 30.62 48.74 15.97 o 11 12 1 34.65 43.87 17.09 o 12 12 1 200.76 207.61 23.23 o 1 13 1 4.43 4.20 5.80 o 2 13 1 2650.62 2723.93 68.16 o 3 13 1 501.56 476.70 16.50 o 4 13 1 5846.59 6158.90 166.87 o 5 13 1 121.52 85.10 9.25 o 6 13 1 107.33 76.01 10.89 o 7 13 1 69.59 59.05 11.50 o 8 13 1 564.58 564.34 38.24 o 9 13 1 28.63 20.75 14.56 o 10 13 1 810.15 908.10 40.58 o 11 13 1 88.48 92.82 24.55 o 0 14 1 6752.47 7046.83 232.01 o 1 14 1 284.12 251.59 10.54 o 2 14 1 151.26 145.28 7.99 o 3 14 1 577.08 562.76 18.80 o 4 14 1 14.90 6.43 7.67 o 5 14 1 0.22 7.12 8.64 o 6 14 1 1154.05 1020.14 33.03 o 7 14 1 78.92 90.60 13.93 o 8 14 1 36.21 62.90 13.18 o 9 14 1 565.35 506.24 29.20 o 10 14 1 87.96 59.91 18.16 o 11 14 1 23.80 10.57 19.39 o 1 15 1 31.59 36.51 6.75 o 2 15 1 3247.35 3290.74 78.19 o 3 15 1 338.80 298.95 12.37 o 4 15 1 535.95 521.02 18.54 o 5 15 1 992.09 937.90 29.12 o 6 15 1 213.18 179.30 13.25 o 7 15 1 9.39 -11.04 11.04 o 8 15 1 7.74 -5.29 12.62 o 9 15 1 41.23 59.49 16.89 o 10 15 1 5.23 10.43 19.31 o 11 15 1 50.68 56.35 22.34 o 0 16 1 6233.95 6338.69 229.13 o 1 16 1 77.77 67.98 7.55 o 2 16 1 383.87 350.34 14.02 o 3 16 1 329.38 278.51 12.45 o 4 16 1 1.04 -9.22 9.22 o 5 16 1 941.47 946.79 31.61 o 6 16 1 626.26 587.65 23.07 o 7 16 1 67.10 55.25 19.83 o 8 16 1 726.94 783.28 37.62 o 9 16 1 364.61 341.27 28.21 o 10 16 1 180.31 209.65 27.86 o 1 17 1 155.16 155.71 11.32 o 2 17 1 617.47 583.99 20.39 o 3 17 1 181.23 128.43 11.02 o 4 17 1 1435.24 1432.71 44.11 o 5 17 1 805.52 822.35 30.65 o 6 17 1 36.13 25.35 12.38 o 7 17 1 1.31 23.65 14.66 o 8 17 1 650.39 751.42 47.27 o 9 17 1 28.94 26.03 20.48 o 10 17 1 361.86 425.76 34.69 o 0 18 1 513.81 461.07 25.49 o 1 18 1 539.00 459.63 23.65 o 2 18 1 33.20 16.76 9.49 o 3 18 1 292.96 295.00 14.81 o 4 18 1 125.15 103.71 11.06 o 5 18 1 63.17 22.30 10.90 o 6 18 1 139.48 152.28 15.64 o 7 18 1 461.07 438.22 27.35 o 8 18 1 3.56 16.40 19.03 o 9 18 1 0.12 -18.93 18.93 o 1 19 1 330.45 351.97 18.57 o 2 19 1 13.21 -7.93 10.68 o 3 19 1 139.71 115.80 11.80 o 4 19 1 49.42 35.73 10.57 o 5 19 1 4.31 -0.30 10.93 o 6 19 1 2.53 13.48 14.12 o 7 19 1 331.30 371.04 25.83 o 8 19 1 750.58 851.20 41.42 o 9 19 1 0.77 -11.30 18.77 o 0 20 1 5.05 -0.19 17.02 o 1 20 1 320.64 262.87 17.32 o 2 20 1 118.06 137.03 14.46 o 3 20 1 40.01 35.09 12.75 o 4 20 1 72.89 61.37 12.88 o 5 20 1 16.49 10.71 11.82 o 6 20 1 365.51 395.62 21.66 o 7 20 1 193.41 255.58 24.01 o 8 20 1 38.54 58.34 22.08 o 1 21 1 7.94 3.63 12.29 o 2 21 1 2.20 -5.46 14.50 o 3 21 1 235.13 163.52 15.70 o 4 21 1 36.68 25.95 14.47 o 5 21 1 153.70 173.92 21.23 o 6 21 1 79.88 38.94 18.12 o 7 21 1 21.23 12.58 18.27 o 0 22 1 1399.29 1572.54 74.87 o 1 22 1 2.69 -13.84 13.84 o 2 22 1 6.13 -2.94 14.09 o 3 22 1 0.09 -3.39 13.09 o 4 22 1 31.50 2.19 14.40 o 5 22 1 99.64 60.21 18.38 o 6 22 1 139.84 151.27 28.43 o 1 23 1 1160.75 1123.66 44.69 o 2 23 1 174.37 186.00 18.26 o 3 23 1 5.29 -13.50 15.49 o 4 23 1 0.07 6.14 16.21 o 5 23 1 20.73 17.72 19.12 o 0 24 1 513.77 471.77 35.30 o 1 24 1 331.71 260.26 20.56 o 2 24 1 369.67 388.76 24.85 o 3 24 1 1.36 8.10 16.38 o 4 24 1 0.52 19.68 18.93 o 1 25 1 51.90 63.19 18.88 o 2 25 1 256.34 273.87 23.06 o 0 0 2 17151.05 16266.14 1291.28 o 2 0 2 820.23 693.76 29.46 o 3 0 2 3.85 10.79 5.51 o 4 0 2 1300.49 1188.81 50.68 o 5 0 2 73.51 108.32 10.60 o 6 0 2 10.93 15.53 8.47 o 7 0 2 384.03 369.85 21.39 o 8 0 2 67.37 67.90 12.53 o 9 0 2 4371.67 4328.29 179.74 o 10 0 2 81.94 33.24 15.39 o 11 0 2 59.51 49.74 20.30 o 12 0 2 128.50 98.71 46.01 o 13 0 2 33.97 53.92 31.52 o 1 1 2 1555.43 1513.12 33.80 o 2 1 2 17901.38 16842.71 548.66 o 3 1 2 0.00 6.56 4.07 o 4 1 2 3538.80 3633.55 111.65 o 5 1 2 493.55 432.13 15.42 o 6 1 2 231.41 214.08 10.34 o 7 1 2 4664.57 4825.29 139.68 o 8 1 2 259.87 244.73 12.82 o 9 1 2 1.82 -2.18 9.06 o 10 1 2 158.94 163.55 17.17 o 11 1 2 13.90 18.84 15.55 o 12 1 2 99.32 79.95 21.95 o 13 1 2 326.28 380.42 32.86 o 0 2 2 13089.99 13365.79 337.04 o 1 2 2 1302.13 1210.42 24.76 o 2 2 2 3520.51 3329.96 101.31 o 3 2 2 7014.38 6890.24 208.68 o 4 2 2 1049.05 1035.76 31.63 o 5 2 2 2007.28 2129.32 67.23 o 6 2 2 573.94 570.79 19.99 o 7 2 2 1179.61 1134.96 36.05 o 8 2 2 603.53 590.27 28.40 o 9 2 2 380.86 369.30 17.35 o 10 2 2 1646.03 1699.63 86.97 o 11 2 2 0.05 -2.32 15.25 o 12 2 2 68.68 111.21 36.74 o 13 2 2 22.59 -11.79 24.98 o 1 3 2 34941.33 33490.16 687.23 o 2 3 2 3.59 -1.10 4.39 o 3 3 2 2700.91 2950.33 90.83 o 4 3 2 14440.80 15225.05 405.99 o 5 3 2 1502.99 1436.97 43.45 o 6 3 2 320.15 274.87 13.20 o 7 3 2 5988.21 6126.72 176.35 o 8 3 2 172.39 164.42 11.15 o 9 3 2 15.99 -7.17 8.65 o 10 3 2 2706.05 2849.66 92.60 o 11 3 2 4.12 0.78 13.90 o 12 3 2 0.51 36.66 20.62 o 13 3 2 303.95 399.65 35.03 o 0 4 2 3223.15 2896.62 87.61 o 1 4 2 458.36 433.48 11.24 o 2 4 2 64134.09 63976.12 1469.45 o 3 4 2 0.52 17.13 6.62 o 4 4 2 99.46 94.51 6.93 o 5 4 2 1066.19 1102.92 34.34 o 6 4 2 841.58 844.20 25.78 o 7 4 2 0.09 -4.44 7.00 o 8 4 2 41.37 14.14 7.63 o 9 4 2 201.49 196.84 14.03 o 10 4 2 1799.35 1825.14 80.71 o 11 4 2 1.76 -0.13 13.24 o 12 4 2 68.14 47.62 18.64 o 13 4 2 8.07 58.02 37.36 o 1 5 2 1767.75 1750.44 47.92 o 2 5 2 7515.86 7380.72 170.68 o 3 5 2 317.16 311.64 10.41 o 4 5 2 501.91 505.94 16.71 o 5 5 2 1233.22 1359.08 41.60 o 6 5 2 0.08 -4.26 5.09 o 7 5 2 1485.95 1389.84 46.60 o 8 5 2 1687.73 1686.41 56.50 o 9 5 2 292.73 297.43 29.42 o 10 5 2 705.53 727.12 38.37 o 11 5 2 83.26 43.35 15.15 o 12 5 2 139.91 151.94 31.01 o 13 5 2 4.44 68.49 25.13 o 0 6 2 4889.29 5179.77 169.62 o 1 6 2 156.68 153.33 6.80 o 2 6 2 1150.27 1241.64 31.51 o 3 6 2 2938.93 2860.57 74.06 o 4 6 2 4553.10 4791.31 136.94 o 5 6 2 2755.06 2868.66 79.18 o 6 6 2 2654.33 2459.62 73.06 o 7 6 2 1848.89 1848.70 60.70 o 8 6 2 442.59 479.50 23.68 o 9 6 2 298.10 247.65 20.70 o 10 6 2 740.17 752.47 34.77 o 11 6 2 823.22 879.46 67.39 o 12 6 2 0.41 -13.00 17.85 o 13 6 2 99.77 94.53 23.88 o 1 7 2 31.46 35.14 4.91 o 2 7 2 172.06 156.77 6.67 o 3 7 2 7.86 13.90 5.46 o 4 7 2 268.47 316.54 12.22 o 5 7 2 265.50 207.92 10.31 o 6 7 2 3480.94 3633.14 113.50 o 7 7 2 2388.50 2314.49 75.00 o 8 7 2 504.99 526.94 25.12 o 9 7 2 440.97 414.56 24.71 o 10 7 2 189.37 122.98 16.58 o 11 7 2 204.65 217.49 19.67 o 12 7 2 83.40 83.79 20.31 o 13 7 2 3.20 -26.01 26.01 o 0 8 2 2902.85 3044.50 110.69 o 1 8 2 2102.54 2041.29 48.42 o 2 8 2 8.60 6.46 4.46 o 3 8 2 79.70 109.10 6.98 o 4 8 2 1895.38 2105.42 55.78 o 5 8 2 1.90 19.00 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4.36 4.10 24.34 o 5 4 28 124.27 97.39 27.07 o 1 5 28 147.03 95.42 26.96 o 2 5 28 202.83 228.36 23.87 o 3 5 28 0.15 12.95 17.13 o 4 5 28 135.08 117.26 20.04 o 5 5 28 340.96 369.77 30.14 o 0 6 28 154.05 110.09 26.28 o 1 6 28 79.68 83.39 18.38 o 2 6 28 42.27 34.68 15.58 o 3 6 28 15.16 24.91 16.83 o 4 6 28 8.41 24.02 18.13 o 5 6 28 59.92 37.21 19.01 o 1 7 28 72.39 68.68 18.35 o 2 7 28 131.25 143.35 20.18 o 3 7 28 449.36 363.88 24.41 o 4 7 28 0.01 -7.44 27.92 o 0 8 28 246.52 234.90 41.13 o 1 8 28 5.06 -7.48 17.04 o 2 8 28 88.34 91.95 21.59 o 3 8 28 84.16 69.47 27.60 o 4 8 28 4.71 16.92 21.17 o 1 9 28 858.25 1043.82 52.09 o 2 9 28 515.07 503.45 35.80 o 3 9 28 134.73 133.09 22.98 o 0 10 28 225.00 240.90 75.49 o 1 10 28 54.55 45.50 21.25 o 2 10 28 16.78 11.60 21.23 o 1 11 28 7.73 -33.14 33.14 o 1 1 29 19.60 34.54 20.92 o 2 1 29 114.41 81.36 41.70 o 3 1 29 5.94 -8.67 19.56 o 4 1 29 233.23 202.72 27.80 o 5 1 29 274.73 258.20 58.24 o 0 2 29 0.20 2.83 50.33 o 1 2 29 48.11 52.93 35.49 o 2 2 29 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25.16 o 3 2 30 175.65 144.34 28.91 o 1 3 30 104.77 50.18 23.02 o 2 3 30 381.67 361.43 32.29 o 3 3 30 15.09 -11.62 21.71 o 0 4 30 363.37 393.28 115.76 o 1 4 30 305.54 223.33 32.74 o 2 4 30 27.22 37.71 25.34 o 3 4 30 5.68 20.50 24.70 o 1 5 30 40.19 30.68 21.16 o 2 5 30 180.59 174.48 21.88 o 0 6 30 252.78 275.09 43.15 o 1 6 30 10.27 -6.04 18.33 o 1 1 31 22.69 -7.94 20.91 o 0 2 31 140.84 197.11 37.58 o