#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203265.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203265_Fobs loop_ _publ_author_name 'Strunk, Richard J.' 'Brewer, A. David' 'Ferguson, George' 'Lough, Alan J.' _publ_section_title ; 2,3-Dihydro-5,6-dimethyl-1,4-dithiine 1,1,4-trioxide ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o392 _journal_page_last o394 _journal_volume 60 _journal_year 2004 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.5919 _cell_length_b 9.2507 _cell_length_c 7.9146 _exptl_crystal_F_000 203.99 _reflns_d_resolution_high 0.8271 _[local]_cod_data_source_file bt6407Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' brew1 P21212' _shelx_refln_list_code 4 _shelx_f_calc_maximum 71.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 610.77 511.78 14.77 o 4 0 0 22.71 10.00 3.51 o 6 0 0 4.17 1.62 4.06 o 1 1 0 1163.24 1090.27 35.92 o 2 1 0 1441.95 1452.26 26.54 o 3 1 0 789.66 811.70 15.49 o 4 1 0 139.04 167.01 6.79 o 5 1 0 21.36 22.53 3.47 o 6 1 0 26.45 30.43 4.43 o 0 2 0 39.13 58.61 2.86 o 1 2 0 5049.57 6160.14 137.92 o 2 2 0 24.80 40.14 3.37 o 3 2 0 185.12 164.54 4.13 o 4 2 0 16.97 22.08 1.38 o 5 2 0 33.28 26.51 3.93 o 6 2 0 0.51 7.59 4.20 o 1 3 0 286.30 308.93 9.28 o 2 3 0 147.31 129.13 5.43 o 3 3 0 235.22 254.28 9.07 o 4 3 0 139.37 146.53 4.53 o 5 3 0 176.93 191.35 9.56 o 6 3 0 10.81 10.45 3.39 o 0 4 0 549.57 554.19 27.99 o 1 4 0 29.94 33.25 1.86 o 2 4 0 807.85 846.77 24.43 o 3 4 0 158.32 169.08 13.00 o 4 4 0 237.46 238.44 8.19 o 5 4 0 0.21 4.13 1.80 o 6 4 0 2.15 -0.97 1.45 o 1 5 0 38.09 34.59 2.25 o 2 5 0 22.38 27.32 3.33 o 3 5 0 42.94 38.96 2.68 o 4 5 0 371.05 395.44 13.29 o 5 5 0 14.72 13.01 1.90 o 6 5 0 30.56 24.71 2.25 o 0 6 0 6.61 8.78 4.32 o 1 6 0 507.58 566.31 14.53 o 2 6 0 63.00 51.82 3.38 o 3 6 0 172.50 199.31 7.58 o 4 6 0 0.29 2.62 2.24 o 5 6 0 14.41 10.44 2.05 o 1 7 0 69.56 64.56 3.42 o 2 7 0 0.61 3.76 2.08 o 3 7 0 151.27 167.11 7.42 o 4 7 0 14.97 13.36 2.73 o 5 7 0 45.35 47.89 3.48 o 0 8 0 358.45 417.31 19.51 o 1 8 0 150.77 144.19 8.19 o 2 8 0 129.66 156.71 7.84 o 3 8 0 10.92 13.75 3.04 o 4 8 0 22.59 27.47 3.91 o 1 9 0 24.53 39.40 7.59 o 2 9 0 87.28 75.72 6.65 o 3 9 0 5.51 10.03 3.34 o 4 9 0 32.55 28.70 4.88 o 0 10 0 67.14 64.92 9.82 o 1 10 0 69.69 82.96 17.28 o 2 10 0 3.70 9.76 3.67 o 3 10 0 33.81 43.19 5.00 o 1 11 0 0.66 4.46 4.54 o 0 0 1 221.59 52.10 98.09 o 1 0 1 848.71 752.26 13.88 o 2 0 1 16.03 19.88 1.18 o 3 0 1 595.27 559.04 19.29 o 4 0 1 0.01 5.56 1.31 o 5 0 1 41.22 48.20 4.86 o 6 0 1 1.88 0.64 3.62 o -6 1 1 4.23 3.03 4.06 o -5 1 1 46.67 39.11 4.52 o -4 1 1 51.59 47.29 2.66 o -3 1 1 52.72 44.15 3.12 o -2 1 1 148.93 115.10 5.59 o -1 1 1 2195.62 2205.21 69.07 o 1 1 1 2193.79 2257.95 43.89 o 2 1 1 148.46 116.31 5.10 o 3 1 1 53.95 51.32 1.97 o 4 1 1 51.79 53.16 2.18 o 5 1 1 46.55 41.33 3.20 o 6 1 1 4.27 4.10 3.20 o -6 2 1 35.12 54.22 9.02 o -5 2 1 4.80 2.37 2.98 o -4 2 1 280.38 290.43 7.70 o -3 2 1 35.54 45.11 2.40 o -2 2 1 177.63 163.68 4.76 o -1 2 1 102.16 119.53 3.01 o 0 2 1 54.71 57.75 1.90 o 1 2 1 103.48 117.74 10.46 o 2 2 1 176.13 170.63 4.00 o 3 2 1 35.49 42.78 1.77 o 4 2 1 280.69 288.80 8.03 o 5 2 1 4.82 2.59 1.19 o 6 2 1 35.37 37.85 4.28 o -6 3 1 1.44 4.88 3.70 o -5 3 1 22.03 18.38 1.36 o -4 3 1 130.74 141.53 7.26 o -3 3 1 121.95 118.17 7.71 o -2 3 1 518.71 481.75 17.61 o -1 3 1 209.13 198.20 5.50 o 0 3 1 601.73 556.24 12.54 o 1 3 1 211.03 194.67 9.55 o 2 3 1 515.89 450.60 11.10 o 3 3 1 122.80 117.35 3.45 o 4 3 1 130.78 149.17 5.42 o 5 3 1 22.12 28.06 2.11 o 6 3 1 1.46 -0.63 2.44 o -6 4 1 2.75 1.80 3.50 o -5 4 1 101.69 118.51 4.70 o -4 4 1 108.80 91.77 5.83 o -3 4 1 221.14 247.08 10.96 o -2 4 1 54.16 74.31 3.60 o -1 4 1 214.11 227.41 6.43 o 0 4 1 134.94 143.36 4.57 o 1 4 1 215.03 216.65 6.69 o 2 4 1 53.42 69.78 3.29 o 3 4 1 220.99 232.18 7.17 o 4 4 1 108.78 106.02 3.38 o 5 4 1 101.92 101.44 6.02 o 6 4 1 2.72 -1.27 1.85 o -6 5 1 5.35 5.90 2.93 o -5 5 1 4.83 10.44 2.05 o -4 5 1 33.87 40.01 4.79 o -3 5 1 319.64 345.56 18.26 o -2 5 1 16.20 26.15 2.59 o -1 5 1 290.91 276.50 8.24 o 0 5 1 376.16 359.21 9.55 o 1 5 1 289.96 257.53 9.54 o 2 5 1 16.35 20.68 4.51 o 3 5 1 318.55 333.58 19.68 o 4 5 1 34.05 36.81 1.97 o 5 5 1 4.81 5.12 1.39 o 6 5 1 5.35 6.08 2.69 o -5 6 1 32.17 28.45 3.27 o -4 6 1 97.86 89.60 4.79 o -3 6 1 42.61 30.65 3.11 o -2 6 1 69.42 68.27 5.16 o -1 6 1 29.24 36.28 2.40 o 0 6 1 68.81 73.40 3.41 o 1 6 1 28.79 31.79 2.37 o 2 6 1 69.63 63.65 3.47 o 3 6 1 42.92 32.33 3.16 o 4 6 1 97.58 102.08 4.14 o 5 6 1 32.06 31.57 3.80 o -5 7 1 5.35 4.15 4.00 o -4 7 1 29.72 27.15 3.84 o -3 7 1 37.52 41.25 6.98 o -2 7 1 118.49 125.26 7.78 o -1 7 1 80.12 86.67 4.28 o 0 7 1 589.84 644.83 18.02 o 1 7 1 79.64 82.07 4.18 o 2 7 1 118.27 115.95 5.51 o 3 7 1 37.46 35.83 3.28 o 4 7 1 29.46 31.51 4.35 o 5 7 1 5.42 4.76 4.42 o -4 8 1 10.18 12.86 3.88 o -3 8 1 46.82 38.92 4.19 o -2 8 1 75.84 83.81 7.02 o -1 8 1 47.12 44.24 3.88 o 0 8 1 61.81 62.45 5.96 o 1 8 1 47.32 41.10 3.40 o 2 8 1 76.21 68.15 4.55 o 3 8 1 46.73 46.28 3.86 o 4 8 1 10.30 18.33 5.79 o -3 9 1 19.01 21.31 5.55 o -2 9 1 34.39 37.10 5.60 o -1 9 1 167.59 195.05 8.48 o 0 9 1 12.39 10.01 2.31 o 1 9 1 167.76 172.81 11.71 o 2 9 1 34.38 33.34 3.92 o 3 9 1 19.00 29.17 3.62 o -2 10 1 7.12 -3.53 3.53 o -1 10 1 18.11 16.89 3.73 o 0 10 1 1.32 6.38 2.78 o 1 10 1 18.17 6.96 2.97 o 2 10 1 7.21 7.91 3.52 o -1 11 1 3.53 13.62 3.73 o 0 11 1 42.36 36.97 6.75 o 1 11 1 3.56 3.99 5.06 o 0 0 2 698.97 672.65 22.37 o 1 0 2 266.10 226.18 9.37 o 2 0 2 15.26 10.70 1.18 o 3 0 2 218.03 224.72 5.48 o 4 0 2 163.96 160.26 6.57 o 5 0 2 97.10 124.23 10.69 o 6 0 2 1.75 -1.10 3.89 o -6 1 2 18.17 26.17 5.00 o -5 1 2 35.89 34.72 2.96 o -4 1 2 86.20 67.86 3.79 o -3 1 2 16.86 24.05 1.37 o -2 1 2 547.99 498.48 11.15 o -1 1 2 1218.07 1161.46 30.10 o 0 1 2 305.40 255.62 7.06 o 1 1 2 1223.05 1203.65 29.83 o 2 1 2 546.99 524.02 12.15 o 3 1 2 16.74 18.84 1.31 o 4 1 2 85.97 83.53 3.00 o 5 1 2 35.97 42.99 3.45 o 6 1 2 18.38 15.63 2.99 o -6 2 2 18.97 13.95 4.82 o -5 2 2 45.89 48.41 6.46 o -4 2 2 225.14 216.81 11.92 o -3 2 2 157.91 143.90 4.07 o -2 2 2 32.55 34.04 2.12 o -1 2 2 751.49 659.27 20.27 o 0 2 2 1316.89 1300.27 30.91 o 1 2 2 745.35 672.33 14.76 o 2 2 2 32.68 32.98 2.69 o 3 2 2 158.34 147.08 4.84 o 4 2 2 225.89 281.56 10.01 o 5 2 2 46.13 42.51 2.55 o 6 2 2 18.92 19.92 4.24 o -6 3 2 7.54 7.48 5.34 o -5 3 2 30.83 28.46 5.87 o -4 3 2 58.94 58.56 2.46 o -3 3 2 448.77 426.14 14.41 o -2 3 2 185.45 162.94 8.04 o -1 3 2 24.66 33.32 1.94 o 0 3 2 463.03 452.38 10.94 o 1 3 2 24.67 34.67 2.43 o 2 3 2 187.50 170.13 5.31 o 3 3 2 447.71 455.65 12.21 o 4 3 2 58.91 61.86 4.80 o 5 3 2 31.10 31.33 2.89 o 6 3 2 7.60 12.77 3.25 o -6 4 2 0.91 -4.15 4.16 o -5 4 2 44.51 40.21 2.24 o -4 4 2 54.39 64.32 8.36 o -3 4 2 92.11 89.48 11.47 o -2 4 2 183.47 174.67 7.12 o -1 4 2 57.25 64.07 2.59 o 0 4 2 611.70 539.87 15.79 o 1 4 2 56.77 67.79 3.56 o 2 4 2 182.94 174.87 13.23 o 3 4 2 92.27 97.53 5.83 o 4 4 2 54.60 62.25 6.59 o 5 4 2 44.54 55.16 8.32 o 6 4 2 0.90 2.43 2.76 o -5 5 2 2.27 -1.80 2.10 o -4 5 2 99.84 101.76 7.24 o -3 5 2 50.36 53.32 3.97 o -2 5 2 37.85 32.91 2.79 o -1 5 2 238.86 256.39 11.33 o 0 5 2 128.92 125.20 6.19 o 1 5 2 238.29 263.17 8.09 o 2 5 2 37.80 41.89 3.66 o 3 5 2 50.12 49.16 4.00 o 4 5 2 99.86 88.37 7.42 o 5 5 2 2.34 5.33 2.71 o -5 6 2 15.23 16.63 2.68 o -4 6 2 15.14 14.33 2.64 o -3 6 2 36.35 38.35 3.15 o -2 6 2 192.99 186.75 9.67 o -1 6 2 339.27 325.09 10.22 o 0 6 2 1.55 9.73 1.79 o 1 6 2 339.91 319.74 12.12 o 2 6 2 193.32 197.93 7.27 o 3 6 2 35.91 43.59 7.14 o 4 6 2 14.89 18.29 3.03 o 5 6 2 15.29 17.36 3.28 o -5 7 2 24.03 13.14 3.20 o -4 7 2 0.41 7.87 2.75 o -3 7 2 41.76 33.30 4.63 o -2 7 2 37.04 43.09 4.94 o -1 7 2 45.65 45.16 3.53 o 0 7 2 421.59 446.32 11.98 o 1 7 2 45.42 42.11 3.27 o 2 7 2 36.64 38.99 3.05 o 3 7 2 42.13 38.09 3.85 o 4 7 2 0.43 6.52 3.60 o 5 7 2 23.94 15.10 4.23 o -4 8 2 32.77 32.76 4.80 o -3 8 2 24.53 27.21 3.82 o -2 8 2 50.80 55.24 5.00 o -1 8 2 89.16 96.39 7.19 o 0 8 2 105.05 111.11 4.89 o 1 8 2 89.60 94.85 5.28 o 2 8 2 50.64 53.20 3.91 o 3 8 2 24.56 26.18 3.02 o 4 8 2 32.83 25.46 4.74 o -3 9 2 10.10 9.44 5.46 o -2 9 2 6.45 6.89 3.41 o -1 9 2 65.92 73.21 5.10 o 0 9 2 2.81 4.53 2.44 o 1 9 2 66.29 67.92 4.79 o 2 9 2 6.37 7.76 3.62 o 3 9 2 10.19 5.89 3.40 o -2 10 2 13.49 15.40 3.89 o -1 10 2 9.83 6.30 3.01 o 0 10 2 39.70 42.07 4.78 o 1 10 2 10.00 14.18 4.36 o 2 10 2 13.45 9.79 3.60 o 0 0 3 1800.55 1710.76 79.31 o 1 0 3 82.54 100.15 4.36 o 2 0 3 401.87 404.36 9.93 o 3 0 3 189.88 207.68 5.34 o 4 0 3 78.16 74.86 3.15 o 5 0 3 56.44 56.28 4.91 o 6 0 3 0.90 -0.62 2.44 o -6 1 3 23.97 16.88 3.30 o -5 1 3 103.68 100.25 5.60 o -4 1 3 171.28 171.87 5.96 o -3 1 3 100.57 105.58 2.64 o -2 1 3 484.21 451.96 10.42 o -1 1 3 622.31 615.28 17.58 o 0 1 3 175.86 178.12 5.52 o 1 1 3 619.58 627.62 19.28 o 2 1 3 483.46 446.31 11.48 o 3 1 3 100.56 97.54 3.29 o 4 1 3 171.98 170.15 5.19 o 5 1 3 103.78 107.76 6.12 o 6 1 3 23.79 22.90 4.40 o -6 2 3 11.48 5.99 10.81 o -5 2 3 6.53 2.96 2.42 o -4 2 3 182.09 184.43 4.97 o -3 2 3 324.34 344.52 16.84 o -2 2 3 37.99 33.02 4.04 o -1 2 3 963.79 908.25 24.61 o 0 2 3 1479.46 1549.51 39.35 o 1 2 3 966.88 953.84 21.48 o 2 2 3 37.50 41.21 2.31 o 3 2 3 324.78 338.80 16.85 o 4 2 3 181.56 198.68 7.02 o 5 2 3 6.45 5.32 2.27 o 6 2 3 11.59 9.44 2.59 o -6 3 3 13.32 7.67 4.97 o -5 3 3 48.39 46.36 5.49 o -4 3 3 144.98 140.29 4.87 o -3 3 3 378.17 384.48 10.35 o -2 3 3 69.34 78.95 3.32 o -1 3 3 210.62 207.00 9.95 o 0 3 3 951.60 1040.38 21.89 o 1 3 3 210.50 218.35 6.32 o 2 3 3 68.24 78.01 3.42 o 3 3 3 378.52 406.60 15.10 o 4 3 3 145.50 155.58 8.86 o 5 3 3 48.42 54.95 4.22 o 6 3 3 13.31 10.04 3.38 o -5 4 3 16.83 18.04 1.93 o -4 4 3 15.17 21.02 2.53 o -3 4 3 136.01 124.17 4.70 o -2 4 3 455.78 461.07 12.32 o -1 4 3 76.42 87.22 2.87 o 0 4 3 552.24 573.03 15.47 o 1 4 3 76.35 82.74 6.07 o 2 4 3 456.09 474.49 24.04 o 3 4 3 135.57 125.47 5.78 o 4 4 3 15.01 17.95 3.54 o 5 4 3 16.84 19.27 3.40 o -5 5 3 16.61 13.09 2.27 o -4 5 3 99.80 90.12 5.25 o -3 5 3 37.24 27.84 3.23 o -2 5 3 122.66 127.13 5.13 o -1 5 3 302.83 298.11 9.12 o 0 5 3 335.25 333.96 10.27 o 1 5 3 304.08 309.28 13.95 o 2 5 3 122.62 125.70 5.63 o 3 5 3 37.76 40.10 3.35 o 4 5 3 99.57 117.72 6.50 o 5 5 3 16.53 8.94 3.32 o -5 6 3 4.69 6.82 2.73 o -4 6 3 25.02 15.61 4.55 o -3 6 3 5.55 11.77 2.34 o -2 6 3 125.61 119.79 4.69 o -1 6 3 468.95 505.07 13.35 o 0 6 3 0.70 10.81 3.33 o 1 6 3 468.40 524.56 16.31 o 2 6 3 125.14 115.20 6.23 o 3 6 3 5.36 1.23 2.17 o 4 6 3 25.17 24.93 3.47 o 5 6 3 4.67 5.47 3.31 o -4 7 3 9.36 7.09 3.10 o -3 7 3 45.56 45.07 4.25 o -2 7 3 80.26 72.89 3.50 o -1 7 3 139.49 142.06 5.43 o 0 7 3 127.56 153.83 11.68 o 1 7 3 139.54 135.63 6.36 o 2 7 3 81.02 71.09 4.19 o 3 7 3 45.26 48.87 5.25 o 4 7 3 9.29 7.82 3.18 o -4 8 3 11.13 13.38 3.72 o -3 8 3 16.85 14.29 3.45 o -2 8 3 38.23 42.21 3.92 o -1 8 3 32.86 35.26 3.14 o 0 8 3 181.16 200.23 8.51 o 1 8 3 32.76 26.99 4.13 o 2 8 3 37.92 44.63 4.75 o 3 8 3 16.79 14.28 4.12 o 4 8 3 11.15 8.98 5.93 o -3 9 3 15.97 11.08 4.02 o -2 9 3 14.18 8.94 3.28 o -1 9 3 20.11 22.09 3.13 o 0 9 3 20.33 14.13 3.27 o 1 9 3 20.01 22.18 3.46 o 2 9 3 14.15 5.54 3.21 o 3 9 3 15.98 16.10 5.00 o -2 10 3 12.08 12.48 4.43 o -1 10 3 11.96 4.96 3.49 o 0 10 3 24.26 17.95 4.16 o 1 10 3 11.82 6.78 5.65 o 2 10 3 12.17 11.72 4.38 o 0 0 4 167.30 168.68 13.57 o 1 0 4 122.78 112.93 10.94 o 2 0 4 153.61 152.12 7.51 o 3 0 4 72.28 70.79 4.67 o 4 0 4 31.32 33.60 3.11 o 5 0 4 56.34 56.97 3.33 o 6 0 4 0.84 3.70 3.34 o -6 1 4 1.57 -2.90 4.26 o -5 1 4 18.36 19.93 4.85 o -4 1 4 75.08 93.79 2.92 o -3 1 4 54.59 56.80 2.32 o -2 1 4 80.50 74.48 3.13 o -1 1 4 552.62 511.68 23.17 o 0 1 4 40.36 46.06 2.49 o 1 1 4 554.01 539.20 12.55 o 2 1 4 80.06 77.91 2.72 o 3 1 4 53.75 59.54 2.90 o 4 1 4 75.31 90.30 5.88 o 5 1 4 18.38 22.87 4.16 o 6 1 4 1.54 5.09 3.31 o -6 2 4 32.41 22.40 7.19 o -5 2 4 11.22 3.36 2.72 o -4 2 4 127.46 128.96 4.76 o -3 2 4 89.54 92.20 3.74 o -2 2 4 27.30 27.23 1.61 o -1 2 4 246.73 251.43 7.61 o 0 2 4 2.19 23.80 2.23 o 1 2 4 245.74 246.64 6.42 o 2 2 4 27.26 25.39 2.76 o 3 2 4 89.29 87.60 3.59 o 4 2 4 127.48 139.51 6.30 o 5 2 4 11.28 10.66 2.72 o 6 2 4 32.25 34.77 4.36 o -5 3 4 5.20 8.56 1.74 o -4 3 4 37.03 32.78 2.95 o -3 3 4 110.81 119.53 9.84 o -2 3 4 235.33 220.57 8.87 o -1 3 4 17.43 18.60 3.32 o 0 3 4 422.08 424.91 11.38 o 1 3 4 17.17 20.47 3.07 o 2 3 4 235.70 227.72 9.47 o 3 3 4 110.74 118.20 5.91 o 4 3 4 36.81 30.81 3.29 o 5 3 4 5.17 6.99 2.76 o -5 4 4 67.05 63.83 6.65 o -4 4 4 81.80 78.47 4.17 o -3 4 4 119.65 115.36 5.12 o -2 4 4 9.96 12.05 2.11 o -1 4 4 7.38 10.46 1.48 o 0 4 4 177.98 186.00 6.53 o 1 4 4 7.23 11.25 1.80 o 2 4 4 9.99 17.56 2.66 o 3 4 4 120.20 131.07 6.05 o 4 4 4 81.81 78.69 4.79 o 5 4 4 66.80 75.96 5.17 o -5 5 4 3.28 0.93 2.86 o -4 5 4 0.83 1.42 2.30 o -3 5 4 114.35 106.15 5.99 o -2 5 4 28.54 25.27 2.10 o -1 5 4 201.95 200.62 10.40 o 0 5 4 118.27 120.64 10.21 o 1 5 4 202.90 210.56 8.28 o 2 5 4 28.82 25.91 2.85 o 3 5 4 114.25 108.00 7.17 o 4 5 4 0.80 6.30 3.00 o 5 5 4 3.26 -1.38 3.68 o -4 6 4 33.68 31.52 4.20 o -3 6 4 23.43 22.79 2.90 o -2 6 4 69.30 69.98 3.94 o -1 6 4 75.08 81.21 4.57 o 0 6 4 26.54 34.77 4.85 o 1 6 4 75.56 73.04 9.27 o 2 6 4 69.50 68.23 5.01 o 3 6 4 23.32 16.05 2.91 o 4 6 4 33.85 47.32 4.58 o -4 7 4 15.62 16.02 4.45 o -3 7 4 14.67 14.62 2.90 o -2 7 4 63.25 70.75 8.47 o -1 7 4 15.45 13.37 2.68 o 0 7 4 267.31 287.15 16.12 o 1 7 4 15.55 12.02 3.02 o 2 7 4 63.11 65.43 6.91 o 3 7 4 14.80 9.97 3.50 o 4 7 4 15.65 16.20 5.00 o -3 8 4 10.15 8.98 4.08 o -2 8 4 40.48 40.32 3.25 o -1 8 4 4.23 8.77 2.90 o 0 8 4 87.82 78.06 5.20 o 1 8 4 4.22 9.04 2.78 o 2 8 4 40.33 45.18 4.46 o 3 8 4 10.13 6.68 3.81 o -2 9 4 4.58 -0.74 2.59 o -1 9 4 93.71 84.49 5.79 o 0 9 4 25.68 15.99 3.46 o 1 9 4 93.21 81.89 5.91 o 2 9 4 4.59 9.25 6.01 o -1 10 4 28.10 17.12 4.02 o 0 10 4 9.68 10.50 3.99 o 1 10 4 28.08 28.18 4.90 o 0 0 5 1774.52 1789.75 136.00 o 1 0 5 132.82 147.19 7.05 o 2 0 5 119.80 122.79 3.93 o 3 0 5 1.15 3.97 1.54 o 4 0 5 1.68 4.79 1.70 o 5 0 5 2.86 2.95 2.47 o -5 1 5 9.69 5.78 4.51 o -4 1 5 40.06 42.76 3.14 o -3 1 5 73.58 75.12 4.65 o -2 1 5 164.07 162.88 7.93 o -1 1 5 136.59 145.87 11.60 o 0 1 5 2.64 26.09 3.24 o 1 1 5 136.80 147.77 8.45 o 2 1 5 163.77 168.71 5.25 o 3 1 5 73.44 76.48 5.50 o 4 1 5 40.07 45.73 5.28 o 5 1 5 9.62 12.48 2.73 o -5 2 5 10.81 10.94 5.83 o -4 2 5 6.64 4.31 2.22 o -3 2 5 61.59 67.95 4.20 o -2 2 5 41.19 44.59 2.49 o -1 2 5 478.64 451.15 23.89 o 0 2 5 1.39 12.04 2.71 o 1 2 5 477.11 456.03 14.72 o 2 2 5 41.32 42.52 3.24 o 3 2 5 61.36 68.49 3.46 o 4 2 5 6.61 6.03 2.62 o 5 2 5 10.83 5.79 3.19 o -5 3 5 75.09 72.30 3.80 o -4 3 5 28.75 26.98 3.20 o -3 3 5 56.37 54.45 6.26 o -2 3 5 48.53 56.43 3.88 o -1 3 5 16.09 22.74 2.98 o 0 3 5 12.13 21.25 2.57 o 1 3 5 16.08 15.82 2.13 o 2 3 5 48.84 49.14 5.32 o 3 3 5 56.06 62.32 4.04 o 4 3 5 28.51 35.79 4.03 o 5 3 5 75.14 83.95 7.93 o -5 4 5 3.35 6.62 2.72 o -4 4 5 66.15 68.61 4.22 o -3 4 5 68.17 60.29 4.57 o -2 4 5 200.96 208.03 10.85 o -1 4 5 11.91 16.15 4.18 o 0 4 5 89.76 79.66 3.70 o 1 4 5 12.14 12.35 2.06 o 2 4 5 201.51 215.41 9.29 o 3 4 5 68.20 65.13 4.99 o 4 4 5 66.10 64.25 5.92 o 5 4 5 3.35 3.44 5.24 o -4 5 5 115.74 95.03 6.50 o -3 5 5 11.28 10.29 3.69 o -2 5 5 0.84 2.27 1.84 o -1 5 5 6.92 6.99 2.26 o 0 5 5 35.44 36.03 2.97 o 1 5 5 6.88 8.19 1.97 o 2 5 5 0.87 -0.75 2.69 o 3 5 5 11.43 5.59 2.44 o 4 5 5 115.97 122.78 9.58 o -4 6 5 3.20 10.47 3.62 o -3 6 5 71.86 73.12 8.82 o -2 6 5 28.16 30.47 3.81 o -1 6 5 130.55 118.27 7.37 o 0 6 5 25.15 37.70 4.98 o 1 6 5 131.56 126.47 7.03 o 2 6 5 28.35 31.60 3.51 o 3 6 5 72.15 68.18 6.65 o 4 6 5 3.21 3.71 3.59 o -3 7 5 48.83 41.80 5.09 o -2 7 5 0.72 5.00 3.16 o -1 7 5 13.15 18.93 3.02 o 0 7 5 2.22 0.79 2.53 o 1 7 5 12.97 16.84 2.97 o 2 7 5 0.73 3.96 3.06 o 3 7 5 48.83 48.45 6.01 o -3 8 5 2.40 0.58 4.50 o -2 8 5 49.14 44.06 3.83 o -1 8 5 60.43 63.95 5.08 o 0 8 5 64.00 55.08 4.99 o 1 8 5 60.41 58.17 10.64 o 2 8 5 49.27 49.17 5.22 o 3 8 5 2.36 5.34 4.17 o -1 9 5 5.98 16.10 5.61 o 0 9 5 24.90 24.20 4.40 o 1 9 5 6.00 10.18 4.15 o 0 0 6 99.21 120.90 21.15 o 1 0 6 189.86 216.92 18.15 o 2 0 6 10.78 12.69 1.97 o 3 0 6 224.29 220.82 11.85 o 4 0 6 3.33 6.66 2.42 o 5 0 6 18.34 18.61 3.64 o -5 1 6 8.42 5.39 1.78 o -4 1 6 1.47 5.47 1.76 o -3 1 6 22.93 29.12 3.62 o -2 1 6 139.10 129.65 5.14 o -1 1 6 328.17 351.60 12.12 o 0 1 6 660.59 653.33 23.55 o 1 1 6 328.15 347.91 11.91 o 2 1 6 138.72 136.00 7.47 o 3 1 6 22.98 29.17 2.77 o 4 1 6 1.42 5.42 2.35 o 5 1 6 8.42 0.83 2.86 o -5 2 6 7.54 7.10 4.96 o -4 2 6 69.08 56.06 4.69 o -3 2 6 11.90 9.83 1.89 o -2 2 6 109.41 104.85 6.12 o -1 2 6 49.11 48.35 3.71 o 0 2 6 62.10 93.85 4.83 o 1 2 6 48.66 45.54 2.74 o 2 2 6 109.17 108.49 5.54 o 3 2 6 11.82 10.60 2.28 o 4 2 6 69.09 71.38 6.58 o 5 2 6 7.52 5.85 5.25 o -4 3 6 57.34 54.98 6.96 o -3 3 6 23.55 27.74 2.18 o -2 3 6 113.94 130.81 9.86 o -1 3 6 164.94 144.00 7.26 o 0 3 6 65.46 68.07 3.74 o 1 3 6 165.14 146.95 9.74 o 2 3 6 113.52 139.43 5.99 o 3 3 6 23.49 26.96 3.67 o 4 3 6 57.32 55.14 6.72 o -4 4 6 13.66 12.13 3.10 o -3 4 6 34.19 20.38 3.39 o -2 4 6 61.47 57.78 5.19 o -1 4 6 10.73 21.98 2.69 o 0 4 6 1.19 2.03 2.74 o 1 4 6 10.90 24.88 2.88 o 2 4 6 61.11 54.21 5.68 o 3 4 6 34.31 39.96 5.64 o 4 4 6 13.63 17.93 3.71 o -4 5 6 23.59 17.18 4.08 o -3 5 6 93.79 98.66 7.48 o -2 5 6 46.67 45.80 3.45 o -1 5 6 68.10 78.39 5.35 o 0 5 6 48.89 35.97 3.19 o 1 5 6 68.43 69.68 4.46 o 2 5 6 46.81 40.46 3.99 o 3 5 6 93.61 98.08 6.99 o 4 5 6 23.60 25.49 6.69 o -3 6 6 8.14 6.42 3.74 o -2 6 6 20.07 21.03 3.70 o -1 6 6 12.61 13.25 2.48 o 0 6 6 9.05 18.98 3.39 o 1 6 6 12.55 12.88 3.19 o 2 6 6 20.23 19.73 3.48 o 3 6 6 8.16 9.50 3.36 o -3 7 6 33.49 25.40 5.30 o -2 7 6 55.15 57.86 4.10 o -1 7 6 32.62 27.93 4.24 o 0 7 6 120.90 117.41 12.50 o 1 7 6 32.43 26.85 4.58 o 2 7 6 55.26 59.82 12.69 o 3 7 6 33.62 38.59 4.93 o -2 8 6 17.05 19.52 3.35 o -1 8 6 20.53 27.94 5.07 o 0 8 6 8.57 9.85 4.88 o 1 8 6 20.58 18.22 4.78 o 2 8 6 17.08 10.95 4.51 o 0 0 7 151.11 197.41 16.88 o 1 0 7 37.36 39.35 3.44 o 2 0 7 90.47 87.51 4.58 o 3 0 7 30.34 23.86 3.60 o 4 0 7 18.05 21.60 3.76 o -4 1 7 16.36 17.18 2.96 o -3 1 7 7.16 6.21 2.21 o -2 1 7 35.70 32.97 3.58 o -1 1 7 35.99 35.31 3.66 o 0 1 7 7.49 13.33 2.55 o 1 1 7 35.99 37.56 4.11 o 2 1 7 35.62 33.26 3.15 o 3 1 7 7.10 6.90 2.63 o 4 1 7 16.45 16.67 3.88 o -4 2 7 20.67 21.77 4.75 o -3 2 7 33.56 33.92 3.03 o -2 2 7 5.59 2.99 2.02 o -1 2 7 118.67 111.29 6.36 o 0 2 7 1.49 0.64 2.50 o 1 2 7 118.25 119.64 5.51 o 2 2 7 5.51 8.18 2.29 o 3 2 7 33.76 34.27 3.45 o 4 2 7 20.73 17.35 4.77 o -4 3 7 4.74 3.74 3.48 o -3 3 7 28.49 30.65 3.47 o -2 3 7 18.34 14.70 2.57 o -1 3 7 2.35 7.36 2.46 o 0 3 7 4.08 9.49 2.45 o 1 3 7 2.42 11.54 2.32 o 2 3 7 18.33 14.89 3.53 o 3 3 7 28.33 24.69 4.29 o 4 3 7 4.80 -0.26 3.57 o -3 4 7 1.81 4.61 4.23 o -2 4 7 41.81 41.58 3.59 o -1 4 7 3.36 0.27 2.15 o 0 4 7 105.76 91.77 6.27 o 1 4 7 3.28 1.80 2.34 o 2 4 7 41.72 48.55 5.36 o 3 4 7 1.72 5.54 3.08 o -3 5 7 8.75 8.62 5.42 o -2 5 7 3.77 7.24 2.59 o -1 5 7 22.74 18.62 3.03 o 0 5 7 5.74 10.35 2.75 o 1 5 7 22.65 23.32 3.63 o 2 5 7 3.83 10.22 3.20 o 3 5 7 8.77 6.99 5.47 o -2 6 7 14.16 12.48 2.74 o -1 6 7 57.34 55.51 4.39 o 0 6 7 6.23 3.48 2.93 o 1 6 7 57.23 47.44 6.00 o 2 6 7 14.17 16.95 4.09 o -1 7 7 1.61 4.04 3.39 o 0 7 7 79.87 72.70 8.02 o 1 7 7 1.63 -3.18 4.02 o 0 0 8 80.76 77.50 10.06 o 1 0 8 27.71 25.50 3.96 o 2 0 8 78.55 77.79 5.10 o 3 0 8 0.26 3.13 2.52 o -3 1 8 29.05 23.37 3.36 o -2 1 8 32.17 31.65 3.71 o -1 1 8 5.08 10.69 3.08 o 0 1 8 4.91 5.07 2.90 o 1 1 8 5.01 8.48 2.65 o 2 1 8 32.02 35.52 3.66 o 3 1 8 29.08 26.31 3.72 o -3 2 8 40.27 34.76 3.75 o -2 2 8 3.03 4.58 2.61 o -1 2 8 56.77 45.14 5.44 o 0 2 8 28.70 36.38 4.43 o 1 2 8 57.03 49.09 4.39 o 2 2 8 3.02 2.38 2.97 o 3 2 8 40.46 44.92 4.46 o -3 3 8 19.10 18.25 4.23 o -2 3 8 3.17 6.67 2.43 o -1 3 8 13.78 13.26 3.00 o 0 3 8 59.92 41.40 3.79 o 1 3 8 13.62 17.74 3.16 o 2 3 8 3.09 4.63 2.78 o 3 3 8 19.13 15.21 3.91 o -2 4 8 32.43 30.04 4.07 o -1 4 8 17.46 21.84 3.28 o 0 4 8 36.14 34.16 4.27 o 1 4 8 17.35 18.15 3.59 o 2 4 8 32.60 33.05 4.07 o -2 5 8 25.56 34.01 3.63 o -1 5 8 24.25 26.77 3.69 o 0 5 8 17.31 11.28 3.20 o 1 5 8 24.33 28.37 4.36 o 2 5 8 25.48 33.82 5.17 o 0 6 8 7.27 11.87 4.85 o 0 0 9 0.63 -0.33 5.83 o 1 0 9 0.52 7.87 3.24 o 2 0 9 14.57 13.49 3.39 o -2 1 9 23.29 20.49 3.95 o -1 1 9 43.68 53.30 5.85 o 0 1 9 2.52 4.85 3.59 o 1 1 9 43.83 51.84 4.55 o 2 1 9 23.25 22.07 3.78 o -1 2 9 16.75 14.37 4.11 o 0 2 9 0.36 6.59 2.95 o 1 2 9 16.65 18.20 3.50 o -1 3 9 7.56 9.33 5.41 o 0 3 9 79.55 86.37 6.11 o 1 3 9 7.65 8.83 3.85 o