#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:04:12 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180953 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/33/2203369.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203369_Fobs loop_ _publ_author_name 'Musie, Ghezai T.' 'Li, Xiaobao' 'Powell, Douglas R.' _publ_section_title ; Dichlorobis(1-methylimidazole)zinc(II) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m471 _journal_page_last m472 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.789 _cell_angle_gamma 90.000 _cell_length_a 7.9460 _cell_length_b 12.3850 _cell_length_c 12.7410 _exptl_crystal_F_000 608.00 _reflns_d_resolution_high 0.8109 _cod_data_source_file ac6087Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 03111 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 200.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 39161.77 37114.88 967.82 o 4 0 0 3134.52 3011.31 79.13 o 6 0 0 44.37 40.11 3.33 o 8 0 0 3567.39 3449.87 116.58 o 1 1 0 61.35 70.15 1.66 o 2 1 0 2314.62 2224.59 44.42 o 3 1 0 1548.43 1624.04 30.28 o 4 1 0 209.36 269.79 6.22 o 5 1 0 2.30 0.73 1.09 o 6 1 0 1318.68 1215.32 39.66 o 7 1 0 1053.54 972.90 29.02 o 8 1 0 60.09 72.10 5.51 o 9 1 0 190.30 181.64 8.83 o 0 2 0 9108.36 10111.15 306.31 o 1 2 0 4846.86 4775.02 145.15 o 2 2 0 171.10 163.51 4.13 o 3 2 0 1473.20 1423.28 28.97 o 4 2 0 9222.54 9077.11 178.11 o 5 2 0 353.73 307.06 8.74 o 6 2 0 390.85 393.86 16.23 o 7 2 0 29.87 26.29 3.58 o 8 2 0 2254.39 2045.74 66.10 o 9 2 0 72.48 75.69 6.06 o 1 3 0 2613.16 2667.97 48.96 o 2 3 0 892.91 832.20 17.29 o 3 3 0 5431.30 5701.49 112.52 o 4 3 0 309.85 258.66 6.93 o 5 3 0 254.78 220.93 6.12 o 6 3 0 1587.00 1558.21 36.43 o 7 3 0 2637.28 2542.41 69.24 o 8 3 0 46.03 41.94 4.64 o 9 3 0 58.10 61.97 6.05 o 0 4 0 210.79 188.82 14.20 o 1 4 0 1140.60 1189.65 23.37 o 2 4 0 3690.72 3886.14 77.12 o 3 4 0 2430.43 2554.90 51.38 o 4 4 0 14056.89 14622.03 229.03 o 5 4 0 88.49 74.14 3.64 o 6 4 0 2297.05 2258.62 48.81 o 7 4 0 1588.20 1544.55 37.42 o 8 4 0 168.73 167.12 7.96 o 9 4 0 158.78 153.93 8.26 o 1 5 0 2423.96 2512.44 51.41 o 2 5 0 602.30 529.03 11.85 o 3 5 0 6114.45 6034.02 119.56 o 4 5 0 537.89 582.76 14.65 o 5 5 0 307.87 276.57 8.77 o 6 5 0 998.15 996.88 25.15 o 7 5 0 2639.11 2577.49 60.88 o 8 5 0 8.02 7.40 3.56 o 9 5 0 54.58 59.47 7.61 o 0 6 0 85.47 126.09 6.86 o 1 6 0 1502.73 1506.24 31.24 o 2 6 0 33.75 34.52 1.90 o 3 6 0 376.44 370.92 9.49 o 4 6 0 71.66 63.61 4.18 o 5 6 0 33.84 32.06 2.96 o 6 6 0 169.94 157.26 6.68 o 7 6 0 2495.61 2546.12 71.69 o 8 6 0 45.82 49.87 5.28 o 1 7 0 6370.36 6704.76 132.89 o 2 7 0 1712.36 1892.30 39.13 o 3 7 0 8766.97 8988.26 164.21 o 4 7 0 114.70 121.36 4.23 o 5 7 0 112.01 107.87 8.89 o 6 7 0 13.26 13.50 2.74 o 7 7 0 448.95 469.10 14.55 o 8 7 0 0.54 1.13 3.17 o 0 8 0 726.26 776.30 27.72 o 1 8 0 1944.94 2085.55 43.22 o 2 8 0 927.08 915.78 20.42 o 3 8 0 316.00 281.94 8.01 o 4 8 0 779.97 764.80 18.23 o 5 8 0 170.85 179.44 8.32 o 6 8 0 249.82 262.14 9.44 o 7 8 0 1093.65 1146.56 32.18 o 8 8 0 50.25 55.33 6.49 o 1 9 0 2731.79 2754.90 62.28 o 2 9 0 0.77 9.16 6.44 o 3 9 0 2450.11 2479.01 51.43 o 4 9 0 1.45 3.02 2.01 o 5 9 0 1502.27 1493.32 52.76 o 6 9 0 34.07 34.85 4.48 o 7 9 0 3090.14 3104.21 82.61 o 0 10 0 3439.86 3516.45 111.67 o 1 10 0 49.43 41.59 3.88 o 2 10 0 179.49 185.98 7.71 o 3 10 0 1351.90 1340.96 32.55 o 4 10 0 1653.49 1558.91 64.03 o 5 10 0 1125.10 1123.43 33.21 o 6 10 0 349.31 343.69 13.86 o 7 10 0 78.76 76.39 7.08 o 1 11 0 1236.42 1231.73 30.65 o 2 11 0 31.71 31.51 3.78 o 3 11 0 893.37 890.75 23.47 o 4 11 0 256.70 236.79 10.91 o 5 11 0 1113.36 1102.89 33.18 o 6 11 0 119.66 117.12 8.11 o 0 12 0 4802.93 4992.38 157.59 o 1 12 0 22.43 19.76 3.53 o 2 12 0 1005.42 958.74 25.21 o 3 12 0 1669.22 1638.99 39.95 o 4 12 0 310.59 322.36 13.54 o 5 12 0 1124.81 1103.62 33.70 o 1 13 0 181.87 159.83 7.85 o 2 13 0 585.06 584.70 17.54 o 3 13 0 484.97 434.15 21.20 o 4 13 0 5.99 7.90 3.94 o 5 13 0 1.16 -3.16 3.47 o 0 14 0 4100.29 3878.99 125.45 o 1 14 0 831.11 814.66 24.86 o 2 14 0 126.17 120.59 7.29 o 3 14 0 32.09 35.92 5.69 o 1 15 0 1.48 -1.03 2.98 o -9 0 1 294.15 287.68 35.58 o -7 0 1 2849.11 2911.63 163.76 o -5 0 1 210.74 244.17 8.68 o -3 0 1 605.61 530.39 20.20 o -1 0 1 6202.47 6557.54 170.02 o 1 0 1 18149.94 16052.95 417.08 o 3 0 1 31.98 41.15 10.56 o 5 0 1 388.58 376.90 11.86 o 7 0 1 2954.26 2818.87 95.82 o 9 0 1 1369.84 1402.81 79.70 o -9 1 1 389.56 394.58 13.83 o -8 1 1 277.04 273.69 14.68 o -7 1 1 2990.03 2894.44 69.19 o -6 1 1 1391.31 1391.85 31.75 o -5 1 1 1163.84 1144.44 24.76 o -4 1 1 395.98 339.31 7.57 o -3 1 1 19416.63 19799.44 359.36 o -2 1 1 1842.39 1891.72 34.88 o -1 1 1 11803.56 11963.30 218.41 o 0 1 1 154.86 115.03 5.03 o 1 1 1 6768.59 7306.35 133.97 o 2 1 1 1261.17 1280.23 30.91 o 3 1 1 13737.86 14167.31 311.10 o 4 1 1 659.77 692.83 28.74 o 5 1 1 3.80 7.19 1.73 o 6 1 1 69.89 64.90 4.17 o 7 1 1 3546.74 3681.56 87.32 o 8 1 1 90.12 80.72 5.64 o 9 1 1 25.74 22.31 4.46 o -9 2 1 15.57 16.79 4.00 o -8 2 1 259.20 271.00 21.13 o -7 2 1 2083.19 2059.35 50.20 o -6 2 1 57.92 46.83 3.55 o -5 2 1 42.58 57.20 3.36 o -4 2 1 1966.83 1864.82 35.23 o -3 2 1 2991.06 3015.69 55.31 o -2 2 1 386.93 419.68 9.17 o -1 2 1 1116.77 1130.71 21.12 o 0 2 1 4632.97 5070.96 104.90 o 1 2 1 9920.46 9995.10 181.39 o 2 2 1 345.73 308.34 10.38 o 3 2 1 1315.40 1333.21 30.71 o 4 2 1 9177.96 9429.22 189.60 o 5 2 1 635.23 624.70 15.93 o 6 2 1 2561.54 2543.63 53.54 o 7 2 1 2228.37 2149.74 52.71 o 8 2 1 2.49 4.59 3.01 o 9 2 1 546.27 536.16 26.51 o -9 3 1 128.62 140.46 7.77 o -8 3 1 22.99 18.66 3.83 o -7 3 1 2403.45 2397.69 51.23 o -6 3 1 1726.26 1645.75 35.42 o -5 3 1 2978.36 2864.72 53.60 o -4 3 1 650.94 603.11 15.21 o -3 3 1 2722.99 2812.72 51.79 o -2 3 1 2836.53 3250.17 59.88 o -1 3 1 6506.20 6655.94 121.33 o 0 3 1 15162.99 15788.50 287.84 o 1 3 1 3359.29 3570.36 72.30 o 2 3 1 1053.52 1095.92 30.02 o 3 3 1 9694.15 9748.13 191.59 o 4 3 1 267.59 279.93 7.48 o 5 3 1 164.23 170.26 6.48 o 6 3 1 7.42 13.18 2.30 o 7 3 1 2962.85 2944.53 70.67 o 8 3 1 6.68 8.44 3.33 o 9 3 1 81.10 98.48 10.18 o -9 4 1 222.31 222.58 11.04 o -8 4 1 621.25 615.50 19.17 o -7 4 1 1401.61 1352.74 33.30 o -6 4 1 98.01 104.31 4.67 o -5 4 1 381.66 368.90 9.79 o -4 4 1 5422.65 5532.55 87.64 o -3 4 1 3267.50 3290.95 65.81 o -2 4 1 201.88 190.90 4.55 o -1 4 1 656.40 729.51 15.50 o 0 4 1 24664.08 24683.12 485.82 o 1 4 1 556.80 633.34 13.60 o 2 4 1 4127.60 4344.07 85.74 o 3 4 1 2581.23 2634.24 57.81 o 4 4 1 5197.44 5331.27 108.51 o 5 4 1 2900.38 2753.40 63.13 o 6 4 1 461.72 492.28 23.94 o 7 4 1 208.04 199.37 8.41 o 8 4 1 1490.71 1425.13 41.72 o 9 4 1 23.53 34.38 4.92 o -9 5 1 12.16 12.88 4.21 o -8 5 1 1112.32 1109.68 29.95 o -7 5 1 1144.15 1137.32 26.27 o -6 5 1 522.17 541.59 19.18 o -5 5 1 2771.42 2783.64 44.79 o -4 5 1 83.94 71.91 2.98 o -3 5 1 66.83 76.42 3.89 o -2 5 1 3715.27 3623.16 73.72 o -1 5 1 917.77 934.49 18.21 o 0 5 1 1526.93 1575.73 36.27 o 1 5 1 1094.07 1140.51 23.81 o 2 5 1 765.70 806.52 21.12 o 3 5 1 4180.67 4342.67 86.61 o 4 5 1 27.82 42.20 2.87 o 5 5 1 51.94 57.51 4.51 o 6 5 1 765.96 776.96 20.40 o 7 5 1 549.99 537.21 14.31 o 8 5 1 9.21 12.14 3.53 o -8 6 1 2698.81 2608.53 63.79 o -7 6 1 74.28 73.59 5.03 o -6 6 1 123.22 126.31 6.22 o -5 6 1 845.13 901.19 19.76 o -4 6 1 3478.47 3530.31 71.14 o -3 6 1 1660.17 1673.15 34.64 o -2 6 1 234.28 236.30 6.32 o -1 6 1 0.88 2.77 1.99 o 0 6 1 20966.85 21200.65 415.12 o 1 6 1 33.62 32.17 2.53 o 2 6 1 3764.22 3788.73 84.96 o 3 6 1 23.05 15.81 1.96 o 4 6 1 3478.25 3524.55 79.44 o 5 6 1 165.45 152.21 5.65 o 6 6 1 582.05 562.44 25.51 o 7 6 1 2.95 1.48 2.39 o 8 6 1 1998.54 2071.71 53.39 o -8 7 1 1086.94 1075.80 28.47 o -7 7 1 116.07 112.01 5.85 o -6 7 1 107.20 109.78 5.26 o -5 7 1 12.25 10.96 2.28 o -4 7 1 2.40 7.41 1.65 o -3 7 1 257.82 253.42 6.63 o -2 7 1 2009.65 1934.53 36.82 o -1 7 1 2185.61 2357.79 44.38 o 0 7 1 1641.78 1604.98 33.42 o 1 7 1 279.84 320.22 9.23 o 2 7 1 56.77 57.70 5.16 o 3 7 1 1.31 2.67 1.37 o 4 7 1 239.67 258.26 13.37 o 5 7 1 202.24 207.94 9.04 o 6 7 1 1479.55 1518.67 40.66 o 7 7 1 26.58 33.45 3.82 o 8 7 1 20.45 19.85 4.22 o -8 8 1 1902.92 1923.06 61.51 o -7 8 1 56.71 59.22 4.70 o -6 8 1 127.90 112.72 8.13 o -5 8 1 159.43 151.97 6.05 o -3 8 1 280.79 275.46 7.09 o -2 8 1 100.49 115.02 3.84 o -1 8 1 722.30 719.09 16.37 o 0 8 1 10935.66 11621.75 229.38 o 1 8 1 275.16 258.08 8.14 o 2 8 1 2697.69 2784.46 69.07 o 3 8 1 495.61 450.39 13.14 o 4 8 1 2241.97 2366.07 116.78 o 5 8 1 48.53 55.67 4.11 o 6 8 1 1234.87 1226.33 38.36 o 7 8 1 8.55 11.99 3.53 o 8 8 1 475.58 497.52 18.89 o -7 9 1 1049.89 1016.87 27.35 o -6 9 1 1948.54 1907.98 46.59 o -5 9 1 821.46 843.34 45.45 o -4 9 1 1298.93 1293.78 28.44 o -3 9 1 2.37 2.94 2.10 o -2 9 1 1753.21 1774.06 41.50 o -1 9 1 34.90 44.37 3.69 o 0 9 1 734.85 691.30 19.95 o 1 9 1 767.22 741.89 19.26 o 2 9 1 2739.12 2756.85 62.32 o 3 9 1 2054.80 2008.80 42.22 o 4 9 1 343.84 354.75 19.77 o 5 9 1 300.45 303.42 16.47 o 6 9 1 742.39 720.70 20.36 o 7 9 1 124.38 130.98 7.31 o -7 10 1 663.91 639.54 22.08 o -6 10 1 189.28 189.51 9.91 o -5 10 1 17.64 22.07 4.30 o -4 10 1 3735.58 3476.97 109.81 o -3 10 1 229.79 218.89 8.28 o -2 10 1 295.51 281.89 9.73 o -1 10 1 1.40 5.93 2.29 o 0 10 1 1693.96 1524.47 46.32 o 1 10 1 21.65 23.49 3.18 o 2 10 1 57.82 52.81 4.24 o 3 10 1 5.16 5.33 2.35 o 4 10 1 4287.06 4264.89 110.26 o 5 10 1 44.97 47.13 5.38 o 6 10 1 1639.27 1574.95 44.58 o 7 10 1 22.26 18.45 4.56 o -6 11 1 1187.67 1195.66 36.02 o -5 11 1 5.51 2.14 4.07 o -4 11 1 551.91 539.15 27.62 o -3 11 1 2693.56 2734.11 63.04 o -2 11 1 27.45 40.92 5.86 o -1 11 1 4266.44 4237.99 107.71 o 0 11 1 375.43 367.70 11.93 o 1 11 1 2.64 5.00 2.52 o 2 11 1 1819.84 1762.78 42.00 o 3 11 1 1219.33 1129.89 60.05 o 4 11 1 36.52 37.84 4.94 o 5 11 1 6.65 6.28 3.57 o 6 11 1 697.03 614.82 54.57 o -6 12 1 171.15 165.54 10.05 o -5 12 1 43.08 38.86 5.52 o -4 12 1 1169.95 1144.96 34.49 o -3 12 1 187.17 184.41 12.01 o -2 12 1 177.03 188.56 8.22 o -1 12 1 404.52 387.34 12.78 o 0 12 1 360.19 371.71 12.37 o 1 12 1 870.25 862.93 26.65 o 2 12 1 5.50 3.79 2.76 o 3 12 1 11.82 21.65 3.80 o 4 12 1 1184.49 1136.59 34.07 o 5 12 1 83.71 69.98 6.79 o -5 13 1 264.82 270.28 12.91 o -4 13 1 1.26 2.25 3.67 o -3 13 1 1148.28 1199.91 31.05 o -2 13 1 1159.27 1106.49 28.89 o -1 13 1 1410.72 1401.14 35.16 o 0 13 1 97.55 90.26 6.11 o 1 13 1 955.55 920.69 24.80 o 2 13 1 510.84 497.91 15.65 o 3 13 1 2255.54 2217.67 61.34 o 4 13 1 7.79 11.05 4.19 o -3 14 1 297.99 308.29 11.91 o -2 14 1 14.52 16.86 3.88 o -1 14 1 69.77 79.76 6.20 o 0 14 1 93.81 84.78 6.29 o 1 14 1 206.49 198.82 9.04 o 2 14 1 81.45 79.83 6.19 o 3 14 1 144.19 164.67 10.02 o -1 15 1 956.47 934.61 26.08 o 0 15 1 336.13 337.40 14.86 o 1 15 1 498.80 507.16 16.65 o -8 0 2 877.86 846.42 33.03 o -6 0 2 406.58 403.31 23.74 o -4 0 2 24400.95 24035.66 617.02 o -2 0 2 40155.30 35604.89 919.81 o 0 0 2 2575.79 2698.30 54.36 o 2 0 2 9540.83 9819.55 251.68 o 4 0 2 7995.39 8768.94 266.29 o 6 0 2 2563.06 2674.32 90.68 o 8 0 2 2946.76 2800.98 149.06 o -9 1 2 0.23 0.02 3.18 o -8 1 2 2401.44 2520.50 90.92 o -7 1 2 570.13 556.88 16.26 o -6 1 2 483.01 475.11 10.77 o -5 1 2 1003.03 958.88 20.36 o -4 1 2 157.74 144.05 4.04 o -3 1 2 101.57 104.83 2.92 o -2 1 2 7395.37 7508.87 186.46 o -1 1 2 17.98 11.73 1.02 o 0 1 2 1486.22 1569.99 32.33 o 1 1 2 1079.66 1127.03 30.44 o 2 1 2 29.21 23.59 1.85 o 3 1 2 1091.94 1012.60 32.70 o 4 1 2 43.25 44.25 3.90 o 5 1 2 945.04 907.21 27.14 o 6 1 2 1000.91 915.80 47.07 o 7 1 2 216.40 200.23 8.36 o 8 1 2 15.82 21.29 3.91 o 9 1 2 16.58 12.26 3.97 o -9 2 2 60.03 62.12 5.63 o -8 2 2 2024.15 1909.13 66.71 o -7 2 2 382.71 382.40 10.66 o -6 2 2 96.63 87.07 3.63 o -5 2 2 148.17 146.68 4.66 o -4 2 2 2865.64 2530.36 50.90 o -3 2 2 1006.71 1041.17 17.33 o -2 2 2 1503.95 1627.80 30.31 o -1 2 2 4627.54 4954.02 90.44 o 0 2 2 29169.46 26013.65 578.38 o 1 2 2 278.29 277.74 5.97 o 2 2 2 5702.24 6089.87 132.59 o 3 2 2 379.50 356.41 11.38 o 4 2 2 6730.93 7185.02 162.11 o 5 2 2 805.03 842.81 20.73 o 6 2 2 4176.00 3920.70 103.72 o 7 2 2 64.21 64.80 4.87 o 8 2 2 485.60 466.23 15.15 o 9 2 2 5.76 3.93 3.41 o -9 3 2 7.90 8.91 3.78 o -8 3 2 88.62 102.76 6.23 o -7 3 2 1576.77 1535.01 33.86 o -6 3 2 3279.91 3490.88 65.53 o -5 3 2 4417.79 4522.16 83.75 o -4 3 2 5880.05 5815.74 106.78 o -3 3 2 114.53 119.08 3.61 o -2 3 2 501.24 551.47 11.07 o -1 3 2 348.95 303.92 6.44 o 0 3 2 1388.58 1595.83 36.23 o 1 3 2 10806.78 11791.80 214.19 o 2 3 2 6179.38 6525.99 140.46 o 3 3 2 9362.70 9623.03 212.90 o 4 3 2 1425.01 1475.48 31.63 o 5 3 2 510.11 484.59 13.96 o 6 3 2 489.77 508.68 13.33 o 7 3 2 132.05 139.88 6.85 o 8 3 2 115.96 112.15 8.09 o 9 3 2 68.33 74.25 6.28 o -9 4 2 1.18 2.72 3.41 o -8 4 2 2668.49 2764.97 67.11 o -7 4 2 1693.48 1701.20 37.32 o -6 4 2 1366.89 1376.91 51.67 o -5 4 2 1012.36 1031.03 22.55 o -4 4 2 2175.87 2156.48 37.03 o -3 4 2 199.90 174.01 4.55 o -2 4 2 903.66 920.55 17.93 o -1 4 2 66.81 68.86 2.27 o 0 4 2 17910.81 19089.83 382.23 o 1 4 2 2128.26 2237.78 41.58 o 2 4 2 5883.33 6160.02 123.85 o 3 4 2 306.20 290.52 7.75 o 4 4 2 2346.98 2214.85 46.47 o 5 4 2 1800.45 1860.49 43.62 o 6 4 2 2136.88 2073.03 44.23 o 7 4 2 121.29 122.08 6.56 o 8 4 2 77.88 81.63 5.92 o -9 5 2 755.83 799.33 23.45 o -8 5 2 19.84 20.04 3.47 o -7 5 2 1170.37 1121.12 26.42 o -6 5 2 1338.30 1281.70 31.47 o -5 5 2 1696.91 1704.11 36.93 o -4 5 2 1213.80 1196.62 23.61 o -3 5 2 5185.27 5204.83 103.47 o -2 5 2 4.77 6.03 1.03 o -1 5 2 6954.77 6975.81 127.54 o 0 5 2 164.26 140.87 3.77 o 1 5 2 2380.96 2659.68 49.54 o 2 5 2 3208.21 3325.50 96.91 o 3 5 2 8230.16 8242.07 162.53 o 4 5 2 2265.28 2438.04 58.10 o 5 5 2 141.22 148.47 8.13 o 6 5 2 79.75 68.82 4.08 o 7 5 2 2776.13 2637.04 71.45 o 8 5 2 22.79 18.39 4.03 o -9 6 2 20.88 26.78 4.88 o -8 6 2 83.40 83.48 5.31 o -7 6 2 1961.44 1912.12 45.97 o -6 6 2 152.55 167.04 6.32 o -5 6 2 249.56 267.86 6.01 o -4 6 2 2315.51 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