#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203371.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203371_Fobs loop_ _publ_author_name 'Lee, Uk' 'Joo, Hea-Chung' 'Park, Ki-Min' _publ_section_title ; A diprotonated hexatungstoplatinate(IV), Na~6~[H~2~PtW~6~O~24~]·22H~2~O ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i55 _journal_page_last i57 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 113.130 _cell_angle_beta 107.170 _cell_angle_gamma 99.480 _cell_length_a 10.0280 _cell_length_b 10.5910 _cell_length_c 12.1090 _exptl_crystal_F_000 1002.00 _reflns_d_resolution_high 0.7699 _[local]_cod_data_source_file br6139Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NAPTW6 POM' _shelx_refln_list_code 4 _shelx_f_calc_maximum 504.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 37391.29 34378.34 187.94 o 2 0 0 14364.97 13796.16 146.98 o 3 0 0 4702.00 4632.77 106.68 o 4 0 0 8678.83 9016.25 158.92 o 5 0 0 287.78 363.75 58.39 o 6 0 0 81415.51 77937.42 617.58 o 7 0 0 26309.16 27134.62 372.18 o 8 0 0 1361.28 1342.80 110.14 o 9 0 0 120.62 192.72 69.85 o 10 0 0 788.21 762.54 99.66 o 11 0 0 4242.51 4508.76 204.42 o -12 1 0 3087.18 2906.35 180.87 o -11 1 0 4373.97 3833.30 191.01 o -10 1 0 27.09 153.05 61.94 o -9 1 0 409.97 376.92 76.93 o -8 1 0 12524.78 12824.04 274.62 o -7 1 0 75248.84 71618.55 625.29 o -6 1 0 1047.52 1085.32 86.74 o -5 1 0 18730.80 17879.70 248.79 o -4 1 0 994.25 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