#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:04:12 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180953 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/33/2203376.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203376_Fobs loop_ _publ_author_name 'Fang, Rui-Qin' 'Zhang, Xian-Ming' 'Wu, Hai-Shun' 'Ng, Seik Weng' _publ_section_title ; Bis(1,4-Diazoniabicyclo[2.2.2]octane) octamolybdate(VI) tetrahydrate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m359 _journal_page_last m361 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.704 _cell_angle_gamma 90.000 _cell_length_a 7.8880 _cell_length_b 22.9733 _cell_length_c 10.3234 _exptl_crystal_F_000 1424.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file bt6417Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 407.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 23756.54 24045.64 473.05 o 4 0 0 1735.34 1576.00 55.15 o 6 0 0 6997.89 7057.07 181.37 o 8 0 0 396.78 431.19 31.86 o 1 1 0 15255.50 14815.14 296.57 o 2 1 0 5187.29 5431.25 78.32 o 3 1 0 2490.62 2514.20 41.44 o 4 1 0 3238.24 3278.97 54.47 o 5 1 0 63489.82 64866.82 750.60 o 6 1 0 1440.49 1466.28 38.50 o 7 1 0 15323.68 15995.42 182.67 o 8 1 0 8.68 26.23 9.27 o 0 2 0 92447.68 67123.79 1023.34 o 1 2 0 935.05 1055.80 22.53 o 2 2 0 69506.55 64566.91 921.72 o 3 2 0 1550.49 1249.44 35.23 o 4 2 0 5568.89 5255.90 77.79 o 5 2 0 2335.59 2239.33 45.21 o 6 2 0 1836.55 1758.76 117.04 o 7 2 0 1695.34 1703.87 49.91 o 8 2 0 8171.47 8517.33 133.92 o 1 3 0 864.60 913.82 17.18 o 2 3 0 28032.40 28290.75 465.07 o 3 3 0 67190.41 64335.37 774.39 o 4 3 0 6110.59 6328.42 89.86 o 5 3 0 7716.55 7787.19 110.98 o 6 3 0 428.04 380.70 24.51 o 7 3 0 20612.23 21043.39 231.07 o 8 3 0 29.46 83.27 14.26 o 0 4 0 8535.90 8809.92 132.71 o 1 4 0 234.62 279.92 10.71 o 2 4 0 98757.54 90724.94 1375.34 o 3 4 0 13422.80 15196.62 185.69 o 4 4 0 8405.11 8794.35 117.92 o 5 4 0 13.06 57.49 12.39 o 6 4 0 7167.59 6977.14 129.31 o 7 4 0 1034.77 1162.98 36.25 o 8 4 0 26923.90 28733.60 443.67 o 1 5 0 15865.91 16038.75 166.48 o 2 5 0 777.88 810.12 17.69 o 3 5 0 115722.98 110450.94 1329.25 o 4 5 0 409.02 361.69 14.73 o 5 5 0 5189.68 5433.14 83.95 o 6 5 0 14499.65 14322.43 219.97 o 7 5 0 4109.62 4130.46 76.15 o 8 5 0 215.80 276.91 26.21 o 0 6 0 100244.34 92169.80 2336.73 o 1 6 0 46314.05 43792.11 613.09 o 2 6 0 2407.87 2448.18 43.76 o 3 6 0 5846.13 6445.07 88.55 o 4 6 0 12556.53 12578.30 202.56 o 5 6 0 4818.18 4690.35 81.97 o 6 6 0 3717.90 3577.82 77.73 o 7 6 0 845.31 842.84 38.56 o 8 6 0 1202.66 1171.78 50.01 o 1 7 0 13355.08 13548.69 143.66 o 2 7 0 2439.83 2451.24 26.92 o 3 7 0 1758.01 1550.54 26.29 o 4 7 0 5351.43 5523.37 82.17 o 5 7 0 46043.82 45625.34 1066.19 o 7 7 0 4006.44 3967.35 95.74 o 8 7 0 1339.32 1389.54 55.46 o 0 8 0 68121.71 63748.25 761.81 o 1 8 0 22240.50 22559.63 233.31 o 2 8 0 554.62 535.20 16.09 o 3 8 0 1561.22 1600.67 23.01 o 4 8 0 101.23 96.40 7.96 o 5 8 0 2194.70 2261.33 44.40 o 7 8 0 67.40 81.47 28.19 o 8 8 0 1923.39 2027.88 52.93 o 1 9 0 15.81 19.85 4.32 o 2 9 0 7024.88 6937.00 82.58 o 3 9 0 486.12 575.13 15.39 o 4 9 0 11838.15 11878.02 116.39 o 5 9 0 8164.54 8546.23 118.97 o 6 9 0 171.77 168.63 13.84 o 7 9 0 12881.50 12924.04 177.46 o 8 9 0 863.05 891.75 34.30 o 0 10 0 5526.69 5705.23 105.55 o 1 10 0 2281.39 2219.24 34.10 o 2 10 0 28870.53 29379.93 304.73 o 3 10 0 10140.43 9870.37 97.25 o 4 10 0 2428.57 2296.44 38.37 o 5 10 0 5476.40 5345.61 83.84 o 6 10 0 1633.48 1631.76 68.63 o 7 10 0 1210.95 1176.42 48.94 o 8 10 0 1202.95 1143.73 39.23 o 1 11 0 2356.22 2228.37 35.30 o 2 11 0 22201.15 22743.91 241.18 o 3 11 0 26927.07 27462.11 329.66 o 4 11 0 2436.30 2370.44 40.11 o 5 11 0 3567.49 3692.75 69.40 o 6 11 0 796.62 717.81 47.74 o 7 11 0 5294.42 5389.85 94.06 o 0 12 0 5473.25 5437.58 74.53 o 1 12 0 2209.13 2278.59 37.09 o 2 12 0 6549.25 6353.97 80.31 o 3 12 0 0.35 27.48 6.48 o 4 12 0 9799.64 9575.34 133.23 o 5 12 0 318.92 411.18 20.37 o 6 12 0 3155.74 3128.94 62.87 o 7 12 0 3470.01 3395.14 70.07 o 1 13 0 11898.63 11733.10 117.50 o 2 13 0 1352.10 1404.14 28.74 o 3 13 0 263.46 257.24 13.86 o 4 13 0 119.44 117.50 16.00 o 5 13 0 203.52 221.26 14.62 o 6 13 0 3989.54 3920.18 64.14 o 7 13 0 2258.60 2139.52 54.08 o 0 14 0 2307.66 2433.47 40.98 o 1 14 0 3792.53 4028.74 52.75 o 2 14 0 4864.94 4829.26 67.46 o 3 14 0 5111.36 5230.13 73.37 o 4 14 0 13121.70 13387.52 218.37 o 5 14 0 6208.16 6149.28 99.03 o 6 14 0 63.76 77.95 11.20 o 7 14 0 113.20 148.24 23.82 o 1 15 0 2067.59 2066.58 31.75 o 2 15 0 21060.23 21606.14 208.27 o 3 15 0 7220.56 6933.21 108.72 o 4 15 0 295.60 348.19 31.81 o 5 15 0 2827.69 2717.45 71.18 o 6 15 0 1785.83 1693.13 45.97 o 7 15 0 664.11 655.81 36.39 o 0 16 0 5825.88 5818.84 111.78 o 1 16 0 1422.06 1472.16 26.13 o 2 16 0 263.57 272.39 11.47 o 3 16 0 1527.43 1507.33 38.95 o 4 16 0 3311.26 3169.54 61.57 o 5 16 0 2148.97 2222.99 52.55 o 6 16 0 0.88 22.29 7.88 o 7 16 0 317.70 333.21 27.08 o 1 17 0 13608.00 13476.62 157.95 o 2 17 0 733.94 718.15 18.74 o 3 17 0 167.63 166.18 16.06 o 4 17 0 15.72 39.30 12.59 o 5 17 0 453.42 430.86 21.67 o 6 17 0 3732.85 3708.09 92.88 o 0 18 0 3162.27 3008.32 73.76 o 1 18 0 9932.47 9860.95 123.69 o 2 18 0 5163.91 5378.60 78.96 o 3 18 0 143.28 193.40 21.79 o 4 18 0 9304.29 9249.62 135.51 o 5 18 0 1050.94 1045.80 34.94 o 6 18 0 1696.79 1671.27 58.45 o 1 19 0 109.65 138.78 11.76 o 2 19 0 4413.95 4391.66 69.79 o 3 19 0 854.78 815.49 22.29 o 4 19 0 2805.05 2810.63 59.71 o 5 19 0 1401.74 1401.23 41.94 o 6 19 0 7609.31 7625.32 154.84 o 0 20 0 435.72 444.91 26.82 o 1 20 0 7331.66 7359.78 101.84 o 2 20 0 683.45 713.33 24.51 o 3 20 0 862.86 930.46 28.82 o 4 20 0 5265.15 5282.85 122.98 o 5 20 0 2396.96 2465.66 59.12 o 1 21 0 20289.59 20024.55 230.78 o 2 21 0 2285.99 2310.71 48.48 o 3 21 0 35.58 50.08 10.83 o 4 21 0 8657.31 8785.40 170.71 o 5 21 0 488.13 505.53 34.52 o 0 22 0 3837.42 3731.02 151.35 o 1 22 0 1732.09 1780.98 41.92 o 2 22 0 1983.98 1929.66 44.59 o 3 22 0 4421.07 4326.70 86.67 o 4 22 0 12213.73 12458.69 248.47 o 5 22 0 358.54 379.89 29.45 o 1 23 0 177.68 219.84 15.29 o 2 23 0 11462.05 11648.11 152.44 o 3 23 0 341.99 361.93 32.48 o 4 23 0 9404.55 9602.89 187.17 o 0 24 0 1887.44 1855.45 63.97 o 1 24 0 2525.26 2554.66 54.53 o 2 24 0 12594.73 12606.88 164.24 o 3 24 0 5304.37 5383.02 124.35 o 4 24 0 799.09 829.82 44.19 o 1 25 0 6211.37 6102.66 97.36 o 2 25 0 1007.41 1152.99 36.66 o 3 25 0 1285.90 1206.50 52.41 o 0 26 0 5301.92 5018.51 123.26 o 1 26 0 9140.63 9115.85 131.34 o 2 26 0 10409.15 10329.20 144.99 o 1 27 0 511.02 719.28 30.15 o -7 0 1 16475.27 16240.40 361.52 o -5 0 1 65675.34 63339.15 1817.42 o -3 0 1 21840.47 22359.35 442.41 o -1 0 1 14979.15 14077.38 308.21 o 1 0 1 2537.08 3003.76 55.76 o 3 0 1 4655.31 4215.01 74.63 o 5 0 1 31268.03 31585.67 676.33 o 7 0 1 5435.72 5541.70 116.26 o -7 1 1 279.61 308.83 31.86 o -6 1 1 540.23 548.36 30.05 o -5 1 1 5639.91 5469.76 103.62 o -4 1 1 4270.65 4204.13 79.59 o -3 1 1 8126.83 7833.90 322.54 o -2 1 1 3561.28 3585.66 48.17 o -1 1 1 2580.34 2485.26 41.43 o 1 1 1 39268.27 38960.66 514.22 o 2 1 1 650.81 557.35 11.93 o 3 1 1 13057.53 13436.95 141.20 o 4 1 1 179.24 238.66 9.53 o 5 1 1 59.52 85.15 8.26 o 6 1 1 2901.16 2869.47 58.02 o 7 1 1 217.54 270.83 15.57 o 8 1 1 826.08 818.84 28.60 o -7 2 1 12129.32 13157.67 454.36 o -6 2 1 17.24 41.32 9.41 o -3 2 1 13344.68 13346.77 202.46 o -2 2 1 41719.45 41666.73 608.47 o -1 2 1 219.65 177.67 6.46 o 0 2 1 24758.53 24872.82 407.81 o 1 2 1 3827.24 3665.63 41.17 o 2 2 1 8492.36 8244.91 96.72 o 3 2 1 9745.67 9741.34 95.82 o 4 2 1 24595.98 25195.60 232.58 o 5 2 1 1098.63 1160.52 26.23 o 6 2 1 5527.17 5844.41 80.88 o 7 2 1 740.98 708.81 24.44 o 8 2 1 0.75 26.15 12.65 o -7 3 1 6.48 19.62 11.55 o -6 3 1 5188.31 5414.52 107.13 o -5 3 1 24793.30 25483.97 382.41 o -4 3 1 3211.86 3491.51 68.64 o -3 3 1 6191.00 6109.90 101.20 o -2 3 1 65253.46 62198.67 644.73 o -1 3 1 73.72 100.49 7.35 o 0 3 1 658.79 538.48 8.89 o 1 3 1 29226.98 28439.08 295.09 o 2 3 1 19081.77 19262.33 175.27 o 3 3 1 2257.02 2039.43 30.71 o 4 3 1 36.25 81.25 7.52 o 5 3 1 21.19 34.38 5.88 o 6 3 1 5544.47 5472.78 77.03 o 7 3 1 871.12 861.75 27.07 o 8 3 1 5640.65 5595.70 88.32 o -7 4 1 6284.37 5965.15 167.28 o -6 4 1 78.14 85.50 13.07 o -5 4 1 189.74 238.62 13.21 o -4 4 1 384.64 414.36 22.35 o -3 4 1 36364.92 34991.57 973.97 o -2 4 1 8633.58 8988.84 93.99 o -1 4 1 28.53 32.95 3.33 o 0 4 1 7666.03 8005.08 74.87 o 1 4 1 191.91 259.81 15.32 o 2 4 1 26352.25 26568.01 238.37 o 3 4 1 80047.60 78245.35 721.48 o 4 4 1 490.75 464.55 12.70 o 5 4 1 1399.64 1446.61 30.00 o 6 4 1 245.06 250.81 13.72 o 7 4 1 1.49 29.51 7.59 o 8 4 1 2718.09 2759.27 66.84 o -7 5 1 3709.52 3628.11 120.10 o -6 5 1 318.59 307.30 24.48 o -5 5 1 9.83 46.67 8.69 o -4 5 1 13041.61 13311.12 167.90 o -3 5 1 650.34 1106.04 22.46 o -2 5 1 7707.35 7328.85 93.12 o -1 5 1 16511.63 17208.08 251.28 o 0 5 1 1038.83 946.71 19.42 o 1 5 1 34787.27 34587.77 322.83 o 2 5 1 23847.15 24143.72 275.54 o 3 5 1 59078.02 59668.39 539.07 o 4 5 1 12551.88 12542.18 123.55 o 5 5 1 3592.49 3673.32 54.88 o 6 5 1 3190.63 3212.51 54.48 o 7 5 1 6786.06 6999.27 115.08 o 8 5 1 2741.15 2804.22 67.44 o -7 6 1 83.80 102.94 21.45 o -6 6 1 11632.52 12201.26 198.42 o -5 6 1 14961.33 15601.08 319.55 o -4 6 1 545.28 594.71 15.36 o -2 6 1 48002.10 47239.15 743.75 o -1 6 1 37437.75 37049.98 442.10 o 0 6 1 7739.15 7516.50 72.74 o 1 6 1 4161.19 4041.29 35.70 o 2 6 1 7898.53 7490.67 68.75 o 3 6 1 8835.07 9218.25 91.69 o 4 6 1 1025.87 965.35 21.74 o 5 6 1 2849.00 2776.30 58.81 o 6 6 1 11085.98 11016.07 132.42 o 7 6 1 704.85 709.67 29.68 o 8 6 1 1432.22 1353.22 55.87 o -7 7 1 2819.15 2953.35 70.09 o -6 7 1 23390.73 24587.88 314.12 o -5 7 1 146.70 214.41 40.14 o -4 7 1 3155.29 3384.37 46.79 o -3 7 1 5656.57 5912.59 142.79 o -2 7 1 686.73 779.62 39.67 o -1 7 1 13778.12 13394.51 273.10 o 0 7 1 102451.48 92465.67 1273.17 o 1 7 1 10963.30 11672.69 100.41 o 2 7 1 1373.44 1501.49 18.09 o 3 7 1 28038.40 28624.75 259.54 o 4 7 1 5443.71 5456.31 69.99 o 5 7 1 20850.54 21288.75 237.38 o 6 7 1 759.79 753.92 29.81 o 7 7 1 3015.01 3069.00 90.19 o 8 7 1 4552.93 4729.91 116.76 o -8 8 1 4020.22 4044.78 133.58 o -7 8 1 1475.11 1525.49 47.57 o -6 8 1 15292.76 15799.99 370.64 o -5 8 1 26841.01 27863.65 393.64 o -4 8 1 3550.36 3806.21 51.81 o -3 8 1 7778.26 7955.33 106.17 o -2 8 1 5795.47 5739.43 97.69 o -1 8 1 3812.93 3363.07 43.74 o 0 8 1 4950.50 4555.20 48.55 o 1 8 1 647.64 643.22 16.56 o 2 8 1 924.13 1051.25 19.20 o 3 8 1 23978.51 23701.84 243.02 o 4 8 1 8750.32 8503.79 99.85 o 5 8 1 4937.87 5183.22 85.66 o 6 8 1 984.35 979.96 32.74 o 7 8 1 4466.00 4365.99 105.84 o 8 8 1 0.80 51.99 16.24 o -8 9 1 158.29 200.91 19.87 o -7 9 1 22.11 42.51 10.81 o -6 9 1 6272.24 6272.46 106.81 o -5 9 1 18019.61 18039.71 351.21 o -4 9 1 13793.32 14038.91 151.61 o -3 9 1 9385.96 9684.37 126.69 o -2 9 1 81.57 43.51 12.26 o -1 9 1 8763.11 8450.02 95.80 o 0 9 1 4436.29 3879.14 43.38 o 1 9 1 24873.25 26282.03 321.40 o 2 9 1 16335.01 16139.65 127.53 o 3 9 1 2.36 17.03 3.00 o 4 9 1 240.79 219.36 14.15 o 5 9 1 17792.80 18273.50 233.33 o 6 9 1 837.55 882.25 31.61 o 7 9 1 2606.36 2685.69 76.68 o -8 10 1 1102.64 1079.08 77.82 o -7 10 1 8948.47 8835.86 155.76 o -6 10 1 12.59 26.01 7.43 o -5 10 1 5.19 35.31 6.79 o -4 10 1 112.07 181.54 34.85 o -3 10 1 11633.92 11307.53 181.39 o -2 10 1 3006.66 2771.64 121.94 o -1 10 1 23.92 60.00 5.63 o 0 10 1 5341.25 4564.22 50.32 o 1 10 1 60373.18 59218.88 965.58 o 2 10 1 38777.95 38858.21 293.81 o 3 10 1 57.65 65.86 7.03 o 4 10 1 9549.61 9681.07 113.70 o 5 10 1 82.57 92.64 9.03 o 6 10 1 17353.57 17445.80 196.30 o 7 10 1 5430.62 5562.33 85.67 o -8 11 1 17829.66 18126.85 287.58 o -7 11 1 392.73 400.86 34.31 o -6 11 1 108.67 128.55 11.79 o -5 11 1 9099.98 9321.95 131.03 o -4 11 1 8770.68 8745.31 121.48 o -2 11 1 588.36 562.19 15.69 o -1 11 1 2929.53 2891.65 35.31 o 0 11 1 17727.22 18506.82 173.71 o 1 11 1 21073.66 21418.05 200.15 o 2 11 1 25412.81 26093.96 243.48 o 3 11 1 2154.41 2121.70 29.66 o 4 11 1 8186.22 8328.87 116.15 o 5 11 1 9.00 26.36 5.98 o 6 11 1 11193.16 11322.18 138.91 o 7 11 1 9873.14 10180.26 132.76 o -8 12 1 968.62 958.56 42.66 o -7 12 1 1846.45 1764.65 54.94 o -6 12 1 40.75 47.18 14.71 o -5 12 1 0.94 35.34 7.32 o -4 12 1 173.89 168.53 14.30 o -3 12 1 57391.69 58468.74 839.02 o -2 12 1 4857.41 4910.18 65.39 o -1 12 1 25775.65 26384.45 243.95 o 0 12 1 2726.31 2898.64 43.54 o 1 12 1 14647.47 15435.01 153.27 o 2 12 1 25628.56 26146.53 245.03 o 3 12 1 1974.93 1957.48 34.70 o 4 12 1 2.22 28.02 6.22 o 5 12 1 1083.95 1126.25 29.13 o 6 12 1 215.59 242.82 16.06 o 7 12 1 65.27 97.44 20.43 o -7 13 1 2914.49 2869.52 108.46 o -6 13 1 8168.31 8348.76 216.30 o -5 13 1 183.61 188.32 16.45 o -4 13 1 1737.41 1764.76 66.18 o -3 13 1 6978.35 6579.21 236.84 o -2 13 1 11771.98 11647.67 134.28 o -1 13 1 225.99 308.76 13.30 o 0 13 1 1910.31 1951.82 42.38 o 1 13 1 1889.88 1724.41 27.26 o 2 13 1 600.71 587.55 20.45 o 3 13 1 12448.09 13055.95 134.12 o 4 13 1 27453.11 28096.54 290.03 o 5 13 1 1113.65 1089.19 29.02 o 6 13 1 8824.59 8875.21 117.02 o 7 13 1 6657.94 6789.29 100.24 o -7 14 1 13159.94 13543.67 328.44 o -6 14 1 3014.72 3012.29 108.46 o -5 14 1 7094.52 7087.91 174.02 o -3 14 1 3124.17 2982.23 55.16 o -2 14 1 20602.39 20682.43 224.60 o -1 14 1 62524.59 63611.59 644.60 o 0 14 1 2353.53 2368.67 33.30 o 1 14 1 0.71 22.99 5.30 o 2 14 1 20.57 45.49 6.44 o 3 14 1 12808.80 13070.61 135.57 o 4 14 1 655.91 670.20 25.22 o 5 14 1 42.77 83.20 9.76 o 6 14 1 1501.82 1471.50 37.59 o 7 14 1 18.85 40.74 10.73 o -7 15 1 563.10 584.57 47.18 o -6 15 1 17248.68 17565.17 400.13 o -5 15 1 175.44 200.75 17.54 o -4 15 1 4784.31 4793.27 100.06 o -3 15 1 2294.45 2192.49 46.25 o -2 15 1 35779.32 34413.23 859.58 o -1 15 1 9720.41 9725.47 117.26 o 0 15 1 6812.60 6783.39 92.30 o 1 15 1 0.77 28.48 6.09 o 2 15 1 3935.84 3743.94 83.58 o 3 15 1 2073.67 2019.19 50.77 o 4 15 1 5830.55 6287.19 100.34 o 5 15 1 19413.37 19424.56 252.19 o 6 15 1 3619.03 3598.92 64.37 o -7 16 1 180.26 193.63 30.02 o -6 16 1 589.82 628.07 47.18 o -5 16 1 1814.62 1765.34 77.21 o -4 16 1 3949.64 3457.76 115.81 o -2 16 1 7938.68 7813.70 100.42 o -1 16 1 4329.72 4365.19 64.23 o 0 16 1 5947.98 5609.94 112.71 o 1 16 1 29267.60 30330.96 283.90 o 2 16 1 4714.97 4626.20 59.52 o 3 16 1 16653.03 16607.41 188.32 o 4 16 1 2121.78 2170.13 50.02 o 5 16 1 403.84 443.73 22.75 o 6 16 1 1452.22 1436.45 70.37 o -7 17 1 11.23 29.33 11.86 o -6 17 1 2925.24 2944.89 112.13 o -4 17 1 31482.13 32992.97 404.30 o -3 17 1 12.84 57.69 9.37 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